AMINE OM Part-1 Rev.3

8/10/2019 AMINE OM Part-1 Rev.3

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OPERATING MANUAL

FOR

Unit : 810

AMINE TREATING PROCESS UNIT

PAK-ARAB REFINERY LIMITED

MID-COUNTRY REFINERY PROJECT

MAHMOOD KOT, PAKISTAN

JOB No.DOC. No.REV.0-0800S-810-1230-0013DATE 29-OCT- 1998 SHEET 1 OF

125 PREP’DT.TakedaCHK’DN.A.APP’DT. Ki!"a#NDE$REV.DATEPA%EDESCR#PT#ONPREP’DCHK’DAPP’D029-OCT-98A&&FOR

REV#E'T. TakedaN.A.T. Ki!"a31(-APR-99A) a"ked#SS*ED FOR CONSTR*CT#ON+REV#E'ED '#TH $-,P-/29 AND *PDATEDT. TakedaN.A.T. Ki!"a

Project Specification

0

DISTRIBUTIONPARCOKPOIPMTBKWPARCOSITEPMTP-CONTCONSTENGPROCES

S1PIPING1CIVILINSTELECROTARYFIREACOUSTICEQUIPPAINT/INSUPKG(PK)PKG(SH)COMBBLDG/HVACOPERATLABOLEGALPPMPURCH1-1PURCH1-2PURCH1-3PURCH-



Since the Aine T!e"tin# P!oce$$ Unit con$i$t$ o% Aine T!e"tin# Section "n& So'!("te! St!i))in# Section (hich "!e *'ite &i%%e!ent )!oce$$e$ %!o e"ch othe!, thi$o)e!"tin# "n'"+ i$ &ii&e& into t(o PART$ "$ e+o( PART AMINE TREATING SECTIONⅠ from page

PART SOUR !ATER STRIPPER SECTIONⅡ from page 8"

2

-2-EPURCH2-2-IEPED႒GSHIPPINGQAQC!PCMARUBENISITETIC!US!EU



JOB CODE /-/0//OPERATIN1 MANUAL OF AMINE TREATIN1 UNIT J1C DOC. NO. S-02/-234/-//2

SHEET 4 OF 235

PART Ⅰ

AMINE TREATING SECTIONCONTENTS

PA1E

2. 1ENERAL DESCRIPTION.......................................................................................................

2.2. PLANT DUTY....................................................................................................................2.3. DISCUSSION OF PROCESS..................................................................................................2.4. DESI1N BASIS FOR FEED AND PRODUCTS...........................................................................

2.4.2. Fee&$.............................................................................................................................2.4.3. P!o&'ct$........................................................................................................................2.4.4. De$i#n Con$i&e!"tion$...................................................................................................

2.6. MATERIAL BALANCE 7 B.L. CONDITIONS...........................................................................2.6.2. M"te!i"+ "+"nce............................................................................................................2.6.3. B.L. con&ition$..............................................................................................................

2.8. UTILITY AND CHEMICALS RE9UIREMENTS.........................................................................2.8.2. Uti+it: !e*'i!eent$.......................................................................................................2.8.3. Cheic"+ !e*'i!eent$..................................................................................................

3. OPERATIN1 CONDITIONS AND CONTROLS.....................................................................

3.2. DISCUSSION OF PROCESS ;ARIABLES.................................................................................3.2.2. A$o!)tion.....................................................................................................................3.2.3. Re#ene!"tion.................................................................................................................

3.3. PROCESS FLO< AND CONTROL.........................................................................................

3.3.2. De$c!i)tion o% )!oce$$ %+o(...........................................................................................3.3.3. Cont!o+ F+o( P+"n.........................................................................................................

4. EMER1ENCY E9UIPMENT...................................................................................................

4.2. SAFETY ;AL;ES................................................................................................................4.2.2. S'"!: o% S"%et: ;"+e$.............................................................................................4.2.3. S'"!: o% F+"!e Lo"&$...............................................................................................

4.3. CAR SEALED ;AL;ES........................................................................................................4.4. R EMOTE OPERATIN1 ;AL;ES.............................................................................................4.6. I NSTRUMENT ALARMS......................................................................................................4.8. I NSTRUMENT TRIP SETTIN1S.............................................................................................4.5. PROCEDURES FOR SETTIN1 PROTECTI;E RELAYS..............................................................

6. PREPARIN1 UNIT FOR PRE-COMMISSIONIN1.................................................................

6.2. PRE-COMMISSIONIN1........................................................................................................6.3. COMMISSIONIN1 OF UTILITIES..........................................................................................6.4. PRESSURE TESTIN1..........................................................................................................6.6. FLUSHIN1 OUT.................................................................................................................6.8. ACID CLEANIN1 OF R ECIPROCATIN1 COMPRESSOR LINES..................................................6.5. I NSPECTION AND R UN-IN OF PUMPS AND FANS.................................................................6.=. LEAK TEST.......................................................................................................................6.0. I NSPECTION AND R UN-IN OF R ECIPROCATIN1 COMPRESSOR ..............................................6.>. I NSPECTION AND R UN-IN OF CENTRIFU1AL COMPRESSOR .................................................6.2/. LOADIN1 INTERNAL MATERIAL RE9UIRED FOR ABSORBERS, ;ESSELS, PACKED COLUMNS.

6.22. DRYIN1 OUT FIRED HEATER ...........................................................................................



6.23. DRYIN1 OUT R EACTOR SECTION.....................................................................................6.24. PREPARIN1 R EACTORS....................................................................................................6.26. LOADIN1 CATALYST.......................................................................................................6.28. DE1REASIN1 FOR AMINE CIRCULATIN1 SYSTEM.............................................................6.25. PUR1IN1 AND 1AS BLANKETIN1.....................................................................................6.2=. PRE-COMMISSIONIN1 CHECK LIST...................................................................................

8. COMMISSIONIN1...................................................................................................................

8.2. 1ENERAL O;ERALL COMMISSIONIN1 PLAN.......................................................................8.3. DETAILED STEP-BY-STEP START-UP PROCEDURE................................................................8.4. SPECIAL PRECAUTIONS.....................................................................................................

8.4.2. P!ec"'tion %o! ente!in# " cont"in"te& o! ine!t "to$)he!e...........................................8.4.3. D!"inin# Aine So+'tion...............................................................................................

5. NORMAL START-UP ? SHUTDO<N....................................................................................

5.2. NORMAL START-UP AFTER PROLON1ED SHUTDO<N..........................................................5.3. NORMAL OPERATION PROCEDURE AFTER SHORT SHUTDO<N.............................................5.4. NORMAL OPERATION........................................................................................................

5.4.2. P!o&'ct *'"+it: onito!in#............................................................................................5.4.3. O)e!"tion Con&ition$ Monito!in#..................................................................................

5.6. R OUTINE OPERATION........................................................................................................5.6.2. T!o'+e $hootin#............................................................................................................5.6.3. Mi$ce++"neo'$ )!oce&'!e$..............................................................................................5.6.4. Ro'tine cont!o+ te$t$ to e )e!%o!e& : o)e!"to!$........................................................

5.8. 1ENERAL O;ERALL SHUTDO<N PLAN..............................................................................5.5. DETAILED STEP-BY-STEP SHUTDO<N PROCEDURE............................................................5.=. BLANKIN1 OFF.................................................................................................................5.0. OPENIN1 E9UIPMENT.......................................................................................................

5.>. SPECIAL PRECAUTIONS.....................................................................................................

=. EMER1ENCY SHUTDO<N....................................................................................................

=.2. 1ENERAL INSTRUCTIONS..................................................................................................=.3. FIRE.................................................................................................................................=.4. PO<ER FAILURE...............................................................................................................=.6. I NSTRUMENT AIR FAILURE................................................................................................=.8. LP STEAM FAILURE..........................................................................................................=.5. <ATER FAILURE...............................................................................................................

=.5.2. Co+& Con&en$"te %"i+'!e................................................................................................=.5.3. Coo+in# <"te! %"i+'!e....................................................................................................

=.=. FEEDSTOCK FAILURE........................................................................................................

=.0. E9UIPMENT FAILURE........................................................................................................

0. MAJOR E9UIPMENT ? ITS SER;ICE..................................................................................

0.2. SUMMARY TABLES............................................................................................................0.3. TO<ER SUMMARY............................................................................................................

0.3.2. F'e+ 1"$ Aine A$o!e! @ 02/-;3 ............................................................................0.3.3. Aine Re#ene!"to! @ 02/-;8 .......................................................................................

0.4. DRUM SUMMARY.............................................................................................................0.4.2. F'e+ 1"$ Aine A$o!e! Knoco't D!' @ 02/-;2 ..................................................0.4.3. Rich Aine F+"$h D!' @ 02/-;6 ..............................................................................0.4.4. Aine Re#ene!"to! Receie! @ 02/-;5 ........................................................................0.4.6. Le"n Aine C"!on Fi+te! @ 02/-;= ............................................................................

0.4.8. Aine S') T"n @ 02/-;0 ........................................................................................

4




SHEET 8 OF 235

0.4.5. F'e+ 1"$ Aine A$o!e! Inte!%"ce Pot @ 02/-;> .......................................................0.6. R EACTOR SUMMARY.........................................................................................................0.8. FIRED HEATER SUMMARY.................................................................................................0.5. ECHAN1ER SUMMARY....................................................................................................

0.5.2. Aine Re#ene!"to! Reoi+e!$ @ 02/-E3A7B .................................................................0.5.3. Rich7Le"n Aine Ech"n#e! @ 02/-E4 ........................................................................0.5.4. Le"n Aine T!i Coo+e! @ 02/-E> ..............................................................................0.5.6. Aine Re#ene!"to! Con&en$e! @ 02/-EA2 ...................................................................0.5.8. Le"n Aine Coo+e! @ 02/-EA3 ....................................................................................

0.=. PUMP SUMMARY..............................................................................................................0.=.2. Rich Aine F+"$h D!' S+o) Oi+ P')$ @ 02/-P2A7B ...............................................0.=.3. Rich Aine P')$ @ 02/-P3A7B .................................................................................0.=.4. Le"n Aine P')$ @ 02/-P4A7B ................................................................................0.=.6. Aine S') P')$ @ 02/-P8A7B ...............................................................................0.=.8. Aine T!"n$%e! P')$ @ 02/-P5A7B ...........................................................................

0.0. COMPRESSOR SUMMARY..................................................................................................0.>. SPECIAL E9UIPMENT SUMMARY........................................................................................0.2/. LIST OF I NSRUMENTS.....................................................................................................0.22. SUMMARY OF ALL E9UIPMENTS DRI;ERS.......................................................................0.23. CONTROL ;AL;ES...........................................................................................................0.24. FIRED HEATERS..............................................................................................................0.26. MISCELLANEOUS............................................................................................................

>. FLO< PLANS AND PLOT PLAN............................................................................................

>.2. PFD, MSD AND P?IDS...................................................................................................>.3. DESI1N E N1INEERIN1, UTILITY AND SAFETY FLO< PLANS................................................>.4. PLOT PLAN......................................................................................................................>.6. SAFETY SHUTDO<N FUNCTION CHARTS............................................................................

2/. SAFETY...................................................................................................................................

2/.2. EMER1ENCY FIRE PLAN..................................................................................................2/.3. FIRE FI1HTIN1 AND PROTECTI;E E9UIPMENT..................................................................2/.4. FIRE PROTECTION..........................................................................................................2/.6. MAINTENANCE OF E9UIPMENT AND HOUSEKEEPIN1.......................................................2/.8. R EPAIR <ORK .................................................................................................................2/.5. THERMAL EPANSION IN ECHAN1ERS...........................................................................2/.=. <ITHDRA<AL OF SAMPLES..............................................................................................2/.0. SAFE HANDLIN1 OF ;OLATILE AND TOIC MATERIALS INCLUDIN1 CATALYST....................

2/.0.2. Re$)i!"to!: P!otection.................................................................................................2/.0.3. B!e"thin# A))"!"t'$ @ B. A. ......................................................................................

2/.0.4. Poi$ono'$ M"te!i"+......................................................................................................2/.>. PREPARIN1 FOR ENTERIN1 PROCESS E9UIPMENT.............................................................2/.2/. OPENIN1 E9UIPMENT...................................................................................................2/.22. <ORKIN1 IN COLUMNS OR ;ESSELS..............................................................................2/.23. E NTERIN1 TANKS, DRUMS OR OTHER ;ESSELS..............................................................2/.24. PROCEDURE FOR REMO;IN1 SAFETY ;AL;ES................................................................2/.26. <ORK PERMIT PROCEDURE AND <ORK PERMIT FORMATS.............................................2/.28. OPERATION NOTES RELATIN1 TO HAOP RE;IE<.........................................................2/.25. MATERIAL SAFETY DATA SHEET@MSDS OF ALL THE CHEMICALS, CATALYSTS................

22. MISCELLANEOUS.................................................................................................................

22.2. CON;ERSION TABLES......................................................................................................

22.3. 1ENERAL PRE-START UP PROCEDURES............................................................................



22.4. O;ERALL START-UP AND SHUTDO<N OUTLINES..............................................................22.6. OFFSITE SYSTEMS...........................................................................................................22.8. CATALYST AND CHEMICAL LOADIN1 7 UNLOADIN1...........................................................22.5. CATALYST AND CHEMICALS RE9UIREMENTS....................................................................22.=. A NALYTICAL PLAN..........................................................................................................

6




SHEET = OF 235

Genera# $e%&ription

Thi$ "n'"+ coe!$ the o)e!"tion o% the Aine T!e"tin# P!oce$$ Unit o% PARCO MID-COUNTRY REFINERY PROJECT %o! PAK-ARAB REFINERY LIMITED @PARCOin P"i$t"n.

P#ant '(t)

The Aine T!e"tin# P!oce$$ Unit $h"++ con$i$t o% "n Aine A$o!e! Section to t!e"t%'e+ #"$, "n Aine Re#ene!"tion Section, "n& " So'! <"te! St!i))e! Section @ See P"!tII - So'! <"te! St!i))e! Section ..The Aine T!e"tin# P!oce$$ Unit (i++ e &e$i#ne& to !eoe H3S %!o o%% #"$e$ &e!ie&%!o "!io'$ )!oce$$ 'nit$ in the Re%ine!:. T!e"te& #"$ %!o the F'e+ 1"$ AineA$o!e! $h"++ not ecee& 2// o+ )) H3S.The Aine T!e"tin# P!oce$$ Unit (i++ e &e$i#ne& to !e#ene!"te !ich "ine %!o"!io'$ )!oce$$ 'nit$, "n& to )!oi&e +e"n "ine "c to tho$e 'nit$. Aci& #"$ %!o the!e#ene!"tion $ection (i++ e !o'te& to the S'+%'! Recoe!: P!oce$$ Unit @he!ein"%te!c"++e& SRU.

$i%&(%%ion of pro&e%%

Aine $o+'tion o% 3/ (t G DEA @&i-eth"no+ "ine e)+o:e& %o! "ci& #"$ !eo"+.Fo! $i)+icit:, on+: the chei$t!: ino+e& in H3S !eo"+ (i++ e &i$c'$$e&. It $ho'+&

e !e"+ie&, ho(ee!, th"t othe! "ci& #"$e$ @ $'ch "$ CO3 (i++ "+$o 'n&e!#o $ii+"!!e"ction$.H:&!o#en $'+%i&e, H3S o! HSH, i$ " (e" "ci& "n& ionie$ in ("te! to %o! h:&!o#enion$ "n& $'+%i&e ion$

H3S H HS-

Since it i$ " %"i!+: (e" "ci&, on+: " %!"ction o% the H 3S (i++ ionie. Sii+"! ioni"tion(i++ occ'! %o! the othe! "ci&ic co)o'n&$ )!e$ent, %o! e")+e CO3

CO3 H3O H HCO4-

Eth"no+ "ine$ "!e (e" "$e$ "n& ionie in ("te! to %o! "ine ion$ "n& h:&!o:+ion$

@HOCH3CH33 NH H3O @HOCH3CH33 NH3 OH-

<hen H3S &i$$o+e$ into the $o+'tion cont"inin# the "ine ion$, it (i++ !e"ct to %o! "(e"+: on&e& $"+t o% the "ci& "n& the "$e.

@HOCH3CH33 NH3 HS- @HOCH3CH33 NH3SH

The &i$'+%i&e ion i$ th'$ "$o!e& : the "ine $o+'tion.Thi$ $"+t %o!"tion !e"ction &oe$ not #o to co)+etion. A$ the "!!o($ in&ic"te, "n

e*'i+i!i' +ee+ o% h:&!o#en $'+%i&e !e"in$ in the h:&!oc"!on $t!e". The oe!"++!e"ction c"n e $'"!ie& : the %o++o(in# e*'"tion$

@HOCH3CH33 NH H3S @HOCH3CH33 NH3SH

O)e!"tin# "!i"+e$ "!e "&'$t"+e to %"o! the %o!("!& !e"ction o% the e*'"tion "oein the "$o!)tion $te) o% the )!oce$$ "n&, cone!$e+:, "&'$te& to %"o! the !ee!$e!e"ction in the "ine !e#ene!"tion $te) o% the )!oce$$. It i$ the !ee!$ii+it: o% thi$!e"ction th"t )e!it$ $o+ent !e#ene!"tion "n& contin'o'$ !eo"+ o% H3S : "inet!e"tin#.

$e%ign *a%i% for fee' an' pro'(&t%

Fee'%

!ee!$i+e

!ee!$i+e



The F'e+ 1"$ Aine A$o!e! @ 02/-;3 in the Aine T!e"tin# P!oce$$ Unit $h"++ e&e$i#ne& to )!oce$$ o%% #"$e$ %!o the %o++o(in#A$o!e! "t the 1"$ Concent!"tion P!oce$$ UnitA&&ition"+ #"$ $t!e"$, i% "n:, to e &ete!ine& &'!in# the )!oce$$ &e$i#nSt!i))e! O%% 1"$ %!o " %'t'!e Di$ti++"te H:&!ot!e"tin# P!oce$$ Unit.The Aine T!e"tin# P!oce$$ Unit $h"++ e &e$i#ne& to )!oi&e +e"n "ine to, "n& to!e#ene!"te !ich "ine %!o, the %o++o(in#Aine A$o!e! "t the LP1 Me!o P!oce$$ UnitRec:c+e 1"$ Sc!'e! "t the Die$e+M" P!oce$$ UnitF'e+ 1"$ Aine A$o!e! "t the Aine T!e"tin# P!oce$$ Unit

Pro'(&t%

O%% #"$ %!o the F'e+ 1"$ Aine A$o!e! @ 02/-;3 $h"++ e $ent to the !e%ine!: %'e+#"$ $:$te. The &e$i#n H3S +ee+ in the t!e"te& %'e+ #"$ $h"++ not ecee& 2// o+ )).Aci& #"$e$ %!o the Aine !e#ene!"to! $h"++ e !o'te& to the S'+%'! Recoe!: P!oce$$Unit @ SRU .

$e%ign Con%i'eration%

2. Rich "ine (i++ e +o"&e& to no o!e th"n /.44 o+ H3S7o+ DEA. Le"n "ine(i++ e !e#ene!"te& to /./4 o+ H3S7o+ DEA.

3. The F'e+ 1"$ Aine A$o!e! @ 02/-;3 (i++ e &e$i#ne& to )!o&'ce " t!e"te& #"$h"in# no o!e th"n 2// o+ )) H3S.

4. (tG DEA (i++ e '$e& in the Aine T!e"tin# P!oce$$ Unit.6. An "ci& #"$ %+"!e (i++ e )!oi&e& "$ " e"n$ to &i$)o$e o% H3S !ich #"$ (hen the

S'+%'! Recoe!: P!oce$$ Unit i$ $h't &o(n.8. Mech"nic"+ "n& c"!on %i+t!"tion (i++ e inc+'&e& on the +e"n "ine $t!e" +e"in#

the Aine T!e"tin# P!oce$$ Unit.5. An "++o("nce %o! %'t'!e Di$ti++"te h:&!ot!e"tin# P!oce$$ Unit (i++ e )!oi&e& in

the &e$i#n o% the F'e+ 1"$ Aine A$o!e!. Thi$ "++o("nce (i++ e /.08 MMSCFD"n& e o% the $"e co)o$ition "$ the #"$ %!o the 1"$ Concent!"tion P!oce$$Unit.

Materia# *a#an&e + ,-L- &on'ition%

Materia# *a#an&e

St!e" N'e! 2 3 40 63

St!e" N"e@ FEED O%% #"$ %!o1ASCON F't'!e U$e Rich Aine%!oL-MR

Rich Aine%!o Die$e+M"

DEA - - 2.842 3=5.=52

NH4 - - - /./68

H3S 36.>0 5.4 /.8/8 >2.4=3

H3 0/.>0 3/.82 - 8.68/

H3O 2.=6 /.66 48.546 5688.8>

CH6 260.=5 4=.50 - /.6//

C3H5 >>.6> 38.3 /.////6 /.644

C4H0 8.=5 2.65 /.//6 /./==

C6H2/ /.=5 /.2> /.//4 /./44

C8H23 /.3/ /./8 /.////3 /.//0

8




SHEET > OF 235

C5 /./2 /.// - /.//6

C3H6 /.06 /.32 - -

C4H5 /.48 /./> /.///3 -

C6H0 /./2 /./3 /.////8 -C3H5S - - /.///4 -

Mo+e F+o(, Ko+7h! 454.0/ >3.25 4=.50 504/.2=

<ei#ht F+o(, #7h! 5,==4 2,=28 032 260,85>

Mo+e (ei#ht, #7#o+e

20.53 20.52 32.=0 32.=8

Li* ;o+ F+o(, St&47h!

- - /.02 266

Li* Den$it:, #74 - - 2,/42 2,/43

;") ;o+ F+o(, 47h!@ No!

0,520 3,204 - 24=

;") Den$it:, #74@ No!

/.=05 /.=05 - /.30

St!e" N'e! 23 >> >= 222

St!e" N"e @ PRODUCT T!e"te& 1"$ toF'e+ 1"$S:$te

Le"n Aineto L-MR

Le"n Aineto Die$e+M"

1"$ toSRU

DEA /.///4 2.866 3=5.=8 /.//4

NH4 - /.//3 /./4 /.///=

H3S /./23 /./44 8.=4 22=./=

H3 2/2.624 /./// - /./>H3O 0.528 45./4= 5680.8= 2/.55

CH6 205.3=8 - - /./2

C3H5 236.8=3 - - /./2

C4H0 =.328 - - /.//3

C6H2/ /.>60 - - /.//4

C8H23 /.38/ - - /.///5

C5 /./23 - - /.///4

C3H6 2./6= - - /.///4

C4H5 /.64> - - /.///2

C6H0 /./23 - - /.////3

C3H5S - - - /.///4

Mo+e F+o(, Ko+7h! 64/.02 4=.52 5,=62./0 23=.08

<ei#ht F+o(, #7h! =,848 024 268,558 6,204

Mo+e (ei#ht, #7# o+e 2=.6> 32.5 32.5 43.=

Li* ;o+ F+o(, St& 47h! - /.02 263.4 -

Li* Den$it:, #74 - 2,/36 2,/36 -

;") ;o+ F+o(, 47h! @ No! 2/,3/5 - - 4,/3>

;") Den$it:, #74 @ No! /.=40 - - 2.402

Re%e! to the P!oce$$ F+o( Di"#!"@ Att"chent >.2 %o! &et"i+$.



,-L- &on'ition%

F+'i& O!i#in 7 De$tin"tion A"i+"+e P!e$$'!e

@ #7c

3

1

Te)e!"t'!e

@

o

C 2 Incoin#$

O%% 1"$ 1"$ Concent!"tion Unit >.82 63

Rich Aine LP1 Me!o Unit >.25 40

Die$e+M" Unit >.05 86

So'! <"te! SRU - 5/

3 O'tcoin#$

Le"n Aine LP1 Me!o Unit - 52

Die$e+M" Unit 24.=4 52

So'! 1"$ SRU 2./8 52

Uti#it) an' &.emi&a#% re/(irement%

Uti#it) re/(irement%

Re%e! to Att"chent 2.2 @ Uti+it: S'"!:, Doc. No. S-02/-2334-8/2

C.emi&a# re/(irement%

Re%e! to Att"chent 2.3 @ C"t"+:$t "n& Cheic"+ S'"!:, Doc. No. S-02/-2334-8/3%o! &et"i+$.

10




SHEET 22 OF 235

Operating Con'ition% an' Contro#%

$i%&(%%ion of pro&e%% aria*#e%

A*%orption

The "$o!)tion o% H3S into the "ine $o+'tion i$ %"o!e& :2. Lo( te)e!"t'!e3. Lo( "ci& #"$ +o"&in#4. Hi#h "ine concent!"tion6. Hi#h H3S )"!ti"+ )!e$$'!e in the %ee& $t!e"8. Inti"te cont"ctIn #ene!"+ )!"ctice, ite$ 6 "n& 8 "!e not o)e!"tin# "!i"+e$, : it$e+%, h"in# een%ie& : the &e$i#n c!ite!i" %o! the 'nit "n& choice o% e*'i)ent in the "$o!e! &e$i#n.Be "("!e, ho(ee!, th"t +o( %ee& !"te$ c"'$e )oo!e! t!": e%%icienc: "n& th'$ $oe(h"t

)oo!e! H3S !eo"+ th"n (i++ e )o$$i+e "t o! ne"! &e$i#n %+o( !"te$.

Lo( Te)e!"t'!eThe +o(e! the te)e!"t'!e o% the +e"n "ine $o+'tion, the ette! the H3S !eo"+. <hent!e"tin# " h:&!oc"!on #"$, ho(ee!, the +e"n "ine te)e!"t'!e i$ +iite& : thete)e!"t'!e o% the #"$ ein# t!e"te&. The +e"n "ine te)e!"t'!e '$t e "int"ine& 4oC hi#he! th"n the te)e!"t'!e o% the #"$ %ee& $t!e" to "oi& "n: )o$$i+econ&en$"tion o% the$e h:&!oc"!on ")o!$. The +e"n "ine i$ '$'"++: coo+e& to et(een3=-6> oC.

Aci& 1"$ Lo"&in#1oo& "ci& #"$ +o"&in# !eo"+ e%%icienc: &e)en&$ on #oo& "ine $o+'tion !e#ene!"tion,"$ (i++ e &i$c'$$e& +"te!. Ho(ee!, it "+$o &e)en&$ on !e$t!ictin# the H3S +o"&in# in the

!ich "ine to %"o! the %o!("!& &i!ection o% the !e"ction #ien e+o(.


The H3S +o"&in# o% the "ine $o+'tion i$ cont!o++e& : "&'$tent o% the "ineci!c'+"tion !"te. In o$t c"$e$, 'n+e$$ $)eci"+ &e$i#n con$i&e!"tion$ h"e eene)+o:e&, the !ich "ine "ci& #"$ +o"&in# @ H3S )+'$ CO3 $ho'+& not ecee& /.4 to /.6o+$ tot"+ "ci& #"$ )e! o+ o% "ine )!e$ent.Hi#h Aine Concent!"tionThe concent!"tion o% 'ncoine& "ine i$ %"o!e& : hi#h "ine $o+'tion, #oo&!e#ene!"tion, "n& %!ee&o %!o $t!on# "ci&$. P!"ctic"+ "n& econoic"+ con$i&e!"tion$con%i!e& : %ie+& e)e!ience h"e #ene!"++: $ho(n th"t the o)ti' "ine

concent!"tion i$ 3/ (tG %o! DEA. Thi$ i$ "$e& on the +o(e$t he"t !e*'i!eent %o! the&e$i!e& H3S !eo"+, the +o(e$t cheic"+ +o$$e$, "n& the %e(e$t o)e!"tion"+ )!o+e$.The ""i+"+e "ine concent!"tion in the +e"n "ine i$ "in+: "%%ecte& : the e%%icienc:"n& cont!o+ o% "ine !e#ene!"tion. The +o(e! the $'+%i&e content o% the +e"n "ine, the#!e"te! the ""i+"+e "ine concent!"tion %o! !eo"+ o% H3S. In o$t c"$e$, )!o)e!+:!e#ene!"te& +e"n "ine (i++ not cont"in o!e th"n /./4 o+ H3S )e! o+ "ine no!o!e th"n /.2 o+ CO3 )e! o+ "ine.

Regeneration

The !e#ene!"tion o% the "ine $o+'tion, "ct'"++: the !e"&o(n o% the (e"+: on&e&"ine-h:&!o$'+%i&e $"+t, i$ %"o!e& :

2. Hi#h Te)e!"t'!e



3. Lo( )!e$$'!e4. Hi#h $t!i))in# $te" !"te6. Lo( "ine concent!"tion8. Inti"te cont"ctin#The$e con&ition$ "!e cont!o++e& in the "ine $t!i))in# co+'n, $'ect to the %o++o(in#+iit"tion$. Ite 8 i$ not "n o)e!"tin# "!i"+e "n& i$ %ie& &'!in# )+"nt &e$i#n.

Hi#h Te)e!"t'!eThe !e"&o(n o% the "ine-h:&!o$'+%i&e $"+t into H3S "n& "ine, the !ee!$e !e"ctiono% the e*'"tion e+o(, i$ )!oote& : hi#he! te)e!"t'!e$.


Ho(ee!, the eth"no+ "ine$ c"n e the!"++: &eco)o$e& "t te)e!"t'!e$ e#innin# "t"o't 238 oC "n& ecoin# ece$$ie "t 28/ oC. MEA i$ the!"++: o!e $t"+e th"nDEA "n& c"n (ith$t"n& $oe(h"t hi#he! te)e!"t'!e$. The &eco)o$ition te)e!"t'!enee& not e "))!o"che& to )!oi&e "&e*'"te !e#ene!"tion o% eth"no+ "ine $o+'tion$.The $t!i))e! !eoi+e! o't+et te)e!"t'!e i$ #ene!"++: +e$$ th"n 238 oC . Thi$ te)e!"t'!ei$ $'ect to "!i"tion (ith co+'n o)e!"tin# )!e$$'!e, "ine concent!"tion, "n& "ci&#"$ +o"&in#$.It $ho'+& e note& th"t "ine $o+'tion$ "!e o$t+: ("te!. The!e%o!e, te)e!"t'!ech"n#e$ (ith co)o$ition "!e $"++ "n& it i$ the o)e!"tin# )!e$$'!e o% the $t!i))e! th"t&ete!ine$ the te)e!"t'!e o% o)e!"tion.

Lo( P!e$$'!eThe $t!i))in# co+'n i$ o)e!"te& "t the +o(e$t oe!he"& !eceie! )!e$$'!e )o$$i+econ$i$tent (ith &o(n$t!e" "ci& #"$ )!oce$$in# !e*'i!eent$. 1ene!"++:, /.48 to 2./#7c31 "t the "$e o% the $t!i))e! i$ $'%%icient )!e$$'!e to %ee& the "ci& #"$ to theSRU. A$ note& "oe, the +o(e! the )!e$$'!e, the +o(e! the $t!i))e! te)e!"t'!e.

Hi#h St!i))in# Ste" R"teThe +ie!"tion o% the H3S %!o it$ "ine $"+t : te)e!"t'!e i$ "$$i$te& : the#ene!"tion o% $te" in the $t!i))e! !eoi+e!. The $te" &i+'te$ "n& c"!!ie$ "(": H 3S")o! "$ it i$ &i$$oci"te& %!o the "ine. The !e$'+tin# &ec!e"$e in H 3S concent!"tion inthe ")o! "++o($ %o! %'!the! "ine-h:&!o$'+%i&e &i$$oci"tion. No!"+ $t!i))e!o)e!"tion$ !e*'i!e " he"t in)'t "t the $t!i))e! !eoi+e! o% 23/ to 26/ # o% !eoi+e!$te" )!e c'ic ete! o% "ine $o+'tion ci!c'+"te&. Thi$ !eoi+e! $te" !"te (i++ !e$'+tin " !e%+' !"te o% "))!oi"te+: 4 to 8 L;-G o% the ci!c'+"tin# "ine !"te. Lo( Aine Concent!"tion

Hi#he! "ine concent!"tion$ %"o! the !etention o% "ci& #"$ in the $o+'tion. Th'$, the"ine concent!"tion i$ cho$en to e hi#h eno'#h %o! e%%icient "$o!)tion 't +o( eno'#h%o! e%%icient !e#ene!"tion. Un+e$$ $)eci"+ con$i&e!"tion$ "!e )!oi&e& %o! &'!in# &e$i#n,o$t 'nit (i++ o)e!"te o$t e%%icient+: "t et(een 28 to 3/ (t-G "ine concent!"tion.In o$t 'nit$, o!e ("te! i$ +o$t (ith the "ci& #"$ th"n i$ int!o&'ce& (ith the "$o!e!%ee&$toc$. Th'$, " +ie $te" inection )oint i$ '$'"++: )!oi&e& &i!ect+: into the!eoi+e! o't+et +ine to en"+e the "&&ition o% ("te! to "oi& "ine concent!"tioninc!e"$e$.In $oe 'nit$, o!e ("te! i$ !o'#ht into the 'nit th"n i$ +o$t (ith the "ci& #"$. A $+i)$t!e" o% !e%+' +i*'i& c"n e &!"(n o%% the !e%+' )') "n& $ent to the $o'! ("te!$t!i))e! to e+iin"te the ece$$ ("te! 'i+&-') th"t co'+& othe!(i$e c"'$e ece$$ie&i+'tion o% the "ine $o+'tion inento!:.

12




SHEET 24 OF 235

Pro&e%% f#o an' &ontro#

$e%&ription of pro&e%% f#o

So'! %'e+ #"$ i$ %e& to the Aine T!e"tin# Section %!o the 1"$ Concent!"tion Unit. The$:$te i$ &e$i#ne& to h"n&+e "n et!" 38 o+G o% it$ c")"cit: %o! %'t'!e '$e. The $o'! #"$ente!$ the F'e+ 1"$ Aine A$o!e! Knoco't D!' @ 02/-;2 (he!e "n: +i*'i&h:&!oc"!on i$ $e)"!"te& %!o the #"$ $t!e". Li*'i& (hich "cc''+"te$ in the &!' i$ )e!io&ic"++: &!"ine& to the Aci& 1"$ F+"!e He"&e!. The #"$ $t!e" i$ $ent to the F'e+ 1"$Aine A$o!e! @ 02/-;3 (he!e it i$ $c!'e& (ith "ine to !eoe H3S. The t!e"te& #"$%+o($ th!o'#h " "c )!e$$'!e cont!o+ "+e "n& i$ then $ent to the !e%ine!: %'e+ #"$ $:$te.Le"n DEA ente!$ the to) o% the A$o!e! on %+o( cont!o+. Rich "ine $o+'tion +e"e$ the otto o% the A$o!e! on +ee+ cont!o+ "n& %+o($ to the !ich "ine he"&e! $:$te. A+$o "tthe F'e+ 1"$ Aine A$o!e!, "n Inte!%"ce Pot @ 02/-;> i$ )!oi&e& %o! h:&!oc"!on$iin# "n& "ine &!"in"#e to the Aine S') T"n @ 02/-;0 .The !ich "ine he"&e! $:$te co++ect$ !ich "ine %!o the F'e+ 1"$ Aine A$o!e!

+oc"te& in the Aine T!e"tin# Unit, the Aine A$o!e! +oc"te& in the LP1 Me!o Unit "n&the Rec:c+e 1"$ Sc!'e! +oc"te& in the Die$e+M" Unit. The coine& !ich "ine $t!e"%+o($ to the Rich Aine F+"$h D!' @ 02/-;6 (he!e "n: h:&!oc"!on i$ $e)"!"te& %!othe !ich "ine. Li*'i& h:&!oc"!on i$ $e)"!"te& into " !e$e!oi! in the Rich Aine F+"$hD!' "n& c"n e )e!io&ic"++: )')e& to the Li#ht S+o) Oi+ T"n "t the T"n"#e "n&B+en&in# S:$te i" the S+o) Oi+ P') @ 02/-P2A7B . H:&!oc"!on ")o! $e)"!"te& in theRich Aine F+"$h D!', (hich cont"in$ H3S, i$ $c!'e& (ith " $"++ +e"n "ine$+i)$t!e" in the $t"c )o!tion o% the Rich Aine F+"$h D!'. The t!e"te& o%% #"$ i$ $ent tothe Aci& 1"$ Re+ie% He"&e!.Rich "ine %!o the otto o% the Rich Aine F+"$h D!' i$ )')e& i" the Rich AineP')$ @ 02/-P3A7B "n& he"te& in the Rich-Le"n Aine Ech"n#e! @ 02/-E4 . Thehe"te& !ich "ine %+o($ on +ee+ cont!o+ to the Aine Re#ene!"to! @ 02/-;8 . The AineRe#ene!"to! $t!i)$ ne"!+: "++ o% the H3S %!o the !ich "ine, th'$ !e#ene!"tin# it to +e"n

"ine. He"t i$ $'))+ie& to the Aine Re#ene!"to! th!o'#h the $te"-he"te& AineRe#ene!"to! Reoi+e!$ @ 02/-E3A7B : ")o!iin# " )o!tion o% the +e"n "ine in the otto o% the co+'n. A $"++ *'"ntit: o% +ie $t!i))in# $te" i$ inecte& into the !eoi+e!!et'!n +ine$ to "e ("te!-"+"nce the enti!e "ine $:$te.O%%#"$ %!o the to) o% the Aine Re#ene!"to!, cont"inin# H3S, $oe +i#ht h:&!oc"!on$,"n& ("te! ")o! i$ )"!ti"++: con&en$e& : the Aine Re#ene!"to! Con&en$e! @ 02/-EA2 .The t(o-)h"$e $t!e" %!o the Con&en$e! ente!$ the Aine Re#ene!"to! Receie! @ 02/-;5 , (he!e the +i*'i& ("te! i$ $e)"!"te& %!o the !e"inin# "ci& #"$ $t!e". The +i*'i&("te! %!o the Receie! i$ )')e& "$ !e%+' to the to) o% the Aine Re#ene!"to! : theAine Re#ene!"to! Re%+' P')$ @ 02/-P4A7B . The "ci& #"$ %!o the Receie! %+o($ on "c-)!e$$'!e cont!o+ to the SRU.

Le"n "ine %!o the otto o% the Aine Re#ene!"to! %+o($ to the $he++ $i&e o% the Rich-Le"n Aine Ech"n#e!, #iin# ') $oe he"t to the !ich "ine $t!e". The coo+e& +e"n"ine i$ )')e& : the Le"n Aine P')$ @ 02/-P4A7B to the Le"n Aine Coo+e! @ 02/-EA3 .A $+i)$t!e" o% coo+e& +e"n "ine )"$$e$ th!o'#h " $e!ie$ o% th!ee %i+te!$ Mech"nic"+ Fi+te!$@ 02/-ME2A7B to !eoe $o+i&$ &o(n to 3/ ic!on$, C"!on Fi+te! @ 02/-;= to !eoecheic"+ i)'!itie$, "n& the Soc Fi+te!$ @ 02/-ME3A7B to c"tch c"!on %ine$ %!o theC"!on Fi+te!. The $+i)$t!e" o% %i+te!e& +e"n "ine !ecoine$ (ith the +"!#e! $t!e" o%coo+e& +e"n "ine. The coine& "ine $t!e" )!oi&e$ +e"n "ine %o! the %o++o(in#$e!ice$. A $"++ $t!e" o% +e"n "ine i$ $ent on %+o( cont!o+ to the $t"c o% the Rich AineF+"$h D!' to $c!' the o%%#"$ %!o thi$ &!'. Anothe! $t!e" o% +e"n "ine i$ t"en o%% %o! '$e in the LP1 Me!o Unit "n& Die$e+M" Unit. The +"$t $t!e" o% +e"n "ine i$ $ent to theF'e+ 1"$ Aine A$o!e! on %+o( cont!o+.



The Aine T!e"tin# Section "+$o inc+'&e$ "n Aine $to!"#e %"ci+it:. P'!e Aine @ >> (tGDEA (i++ e )e!io&ic"++: &e+ie!e& in '+ "o'nt$ "n& )')e& &i!ect+: to the M"e-')T"n @ 02/-TK2 . The )'!e "ine i$ &i+'te& (ith co+& con&en$"te to the 3/ (tG $o+'tion inthe Aine Sto!"#e T"n @ 02/-TK3 .

Contro# F#o P#an

Le"n Aine $'))+: to A$o!e!$ @Fi#'!e 3.2Re#ene!"te&, o! +e"n, "ine $o+'tion i$ )')e& : the Le"n Aine P')$ th!o'#h theLe"n Aine Coo+e! "n& the %i+t!"tion $:$te to the to) o% the H3S A$o!e! co+'n on%+o( cont!o+. A )"!t o% the tot"+ +e"n "ine $t!e" )!oi&e$ +e"n "ine %o! the %o++o(in#$e!ice$.A $"++ $t!e" o% +e"n "ine i$ $ent on %+o( cont!o+ to the $t"c o% the Rich AineF+"$h D!' to $c!' the o%%-#"$ %!o thi$ &!'. Anothe! $t!e" o% +e"n "ine i$ t"eno%% %o! '$e in the LP1 Me!o Unit "n& Die$e+M" Unit.

Rich Aine Ret'!n to Re#ene!"to! @Fi#'!e 3.3The "ine, !ich in H3S, "n& %o! th"t !e"$on c"++e& !ich "ine, eit$ %!o the "$o!e!

otto, on +ee+ cont!o+ "n& %+o($ to the Rich Aine F+"$h D!' (he!e ent!"ine&h:&!oc"!on$ "!e !eoe&, "n& then $ent to the Aine Re#ene!"to!.

14




SHEET 28 OF 235

Fig(re 2-1 LEAN AMINE SUPPL3 TO A,SOR,ERS

F'e+ 1"$ AineA$o!e! 810451

FRC

Rich AineF+"$h D!'

81045"

2

3

/

Le"n AineMech"nic"+ Fi+te!

8104ME1A+,

FR

Le"nAineT!i

Coo+e! 8104E6

Le"n Aineto

Die$e+M"

Le"n Aineto LP1

Me!o Unit

Le"n Aine

Soc Fi+te! 8104ME2A+,

Le"n AineC"!on Fi+te!

810457

PDIC

Le"n AineCoo+e!

8104EA2

Le"n AineP')

8104PA+,

Rich-Le"n Aine

Ech"n#e! 8104E

RichAine

3

4

4

6

2

Aine Re#ene!"to! 81045

FR

C



Fig(re 2-2 RIC9 AMINE RETURN TO REGENERATOR

16

LIC

LIC

Le"n Aineto Le"n

Aine P')$Rich-Le"n

AineEch"n#e!

8104E

Rich AineP')$

810452A+,

PIC

Rich Aine %!oLP1 Me!o Unit

Rich Aine %!oDie$e+M" Unit

S+o) Oi+ to T"n"#e"n& B+en&in# S:$te

@ Li#ht Oi+ S+o) T"n

S+o) Oi+P')$

8104P1A+,

A'toSto )

M

F'e+ 1"$ AineA$o!e! 810451

3

/

2

LIC

Rich AineF+"$h D!'

81045"

1"$ to Aci& 1"$F+"!e He"&e!

Le"

nAine

AineRe#ene!"to!

81045




SHEET 2= OF 235

Emergen&) E/(ipment

Safet) a#e%

S(mmar) of Safet) 5a#e%

S'"!: o% the $"%et: "+e$ )!oi&e& %o! thi$ 'nit i$ $ho(n e+o(. Re%e! to DATASHEET FOR SAFETY RELIEF ;AL;ES @ S-02/-24=6-4/2 .

T"#. No. Set

#7c3#

Sie "n&

T:)e

Se!ice Loc"tion 1oe!nin# Re+ie%

C"$e

02/-PS;-//2A7B 22.4 4K6 02/-;3 To) o'nte& B+oce& O't+et

02/-PS;-//3A7B 4.8 590 02/-;6 To) o'nte& B+o( :

02/-PS;-//4 >.4 4762 02/-E4 O't+et The!"+

02/-PS;-//6A7B 5./ 4L6 02/-;8 To) o'nte& Fi!e02/-PS;-//8A7B 35.> 4762 02/-ME2 In+et Fi!e

02/-PS;-//5A7B 35.> 4762 02/-ME3 In+et Fi!e

02/-PS;-//= 35.8 2E3 02/-;= To) o'nte& Fi!e

02/-PS;-/24 2/./ 6N5 02/-;6 In+et B+o( :

02/-PS;-/26 20.4 4762 02/-E> In+et The!"+

02/-PS;-/25 5./ 2.273F3 02/-ME6 O't+et B+o( :

S(mmar) of F#are Loa'%

Re%e! to F+"!e Lo"& S'"!:@S-02/-2334-=/2.

Car %ea#e' a#e%

C"! Se"+e& O)en o! C"! Se"+e& C+o$e "+e$ "!e +i$te& e+o(.

Po$ition Line No. 7 Se!ice Sie E*'i)ent 7Line No.

P?ID No.

O)en 02/--FA-/4/2-A2A3P-ST 02/-P=A7B D-02/-2338-2/4

O)en 02/--FA-/4/3-A2A3P-ST 02/-P0A7B D-02/-2338-2/4

O)en 02/--FA-/4/4-A2A3P-ST 02/-P22A7B D-02/-2338-2/4

O)en 02/--FA-/4/6-A2A3P-ST 02/-P2A7B D-02/-2338-2/4

O)en 02/--FA-/4/8-A2A3P-ST 02/-P3A7B D-02/-2338-2/4

O)en 02/--FA-/4/5-A2A3P-ST 02/-P6A7B D-02/-2338-2/4O)en 02/--FA-/4/=-A2A3P-ST 02/-P2/A7B D-02/-2338-2/4

O)en 02/-PS;-2/4 in+et +ine 4 2//-5-SS<-46/4-A2A3

D-02/-2338-222

O)en 02/-PS;-2/4 &i$ch"!#e +ine 3 2//-5-SS<-46/4-A2A3

D-02/-2338-222

O)en 02/-5-SS<-22/2-A2A3 5 2//-5-SS<-46/4-A2A3

D-02/-2338-222

O)en 02/--FA-24/2-A2A3P-ST 02/-;2 D-02/-2338-224

O)en 02/-PS;-//2A in+et +ine 6 02/-;3 D-02/-2338-224

O)en 02/-PS;-//2A &i$ch"!#e +ine 6 02/-;3 D-02/-2338-224

C+o$e 02/-PS;-//2B in+et +ine 6 02/-;3 D-02/-2338-224



O)en 02/-PS;-//2B &i$ch"!#e +ine 6 02/-;3 D-02/-2338-224

O)en 02/-3-FA-24/6-A3A2P-ST 3 02/-;> D-02/-2338-224

O)en 02/-PS;-/24 in+et +ine 5 02/-2/-AM-22/2-

A2A3P

D-02/-2338-226

O)en 02/-PS;-/24 &i$ch"!#e +ine 5 02/-2/-AM-22/2-A2A3P

D-02/-2338-226

O)en 02/--FA-26/6-A2A3P-ST 02/-SN-0 D-02/-2338-226

O)en 02/-PS;-//3A in+et +ine 2/ 02/-;6 D-02/-2338-226

O)en 02/-PS;-//3A &i$ch"!#e +ine 0 02/-;6 D-02/-2338-226

C+o$e 02/-PS;-//3B in+et +ine 2/ 02/-;6 D-02/-2338-226

O)en 02/-PS;-//3B &i$ch"!#e +ine 0 02/-;6 D-02/-2338-226

O)en 02/-3-FA-26/3-A2A3P-ST 3 02/-;6 $t"c D-02/-2338-226

O)en 02/-PS;-//5A &i$ch"!#e +ine 2 02/-ME3A D-02/-2338-228

O)en 02/-PS;-//5B &i$ch"!#e +ine 2 02/-ME3B D-02/-2338-228

O)en 02/-PS;-//= &i$ch"!#e +ine 3 02/-;= D-02/-2338-228O)en 02/-PS;-//8A &i$ch"!#e +ine 2 02/-ME2A D-02/-2338-225

O)en 02/-PS;-//8B &i$ch"!#e +ine 2 02/-ME2B D-02/-2338-225

O)en 02/-3-N3-2=/2-A2A2 3 02/-TK2 D-02/-2338-22=

O)en 02/-2-N3-2=/2-A2A2 2 02/-TK2 D-02/-2338-22=

O)en 02/-3-N3-2=/3-A2A2 3 02/-TK3 D-02/-2338-22=

O)en 02/-2-N3-2=/3-A2A2 2 02/-TK3 D-02/-2338-22=

O)en 02/-6-FA-2=/3-A2A3P-ST 6 02/-;0 D-02/-2338-22=

C+o$e 02/-4-AM-2=/=-A2A2P 4 02/-;0 D-02/-2338-22=

O)en 02/-PS;-//4 in+et +ine 2 02/-0-AM-20/4-A2A3P-IH

D-02/-2338-22>

O)en 02/-PS;-//4 &i$ch"!#e +ine 2 02/-0-AM-20/4-A2A3P-IH

D-02/-2338-22>

O)en 02/-PS;-//6A in+et +ine 5 02/-;8 D-02/-2338-22>

O)en 02/-PS;-//6A &i$ch"!#e +ine 6 02/-;8 D-02/-2338-22>

C+o$e 02/-PS;-//6B in+et +ine 5 02/-;8 D-02/-2338-22>

O)en 02/-PS;-//6B &i$ch"!#e +ine 6 02/-;8 D-02/-2338-22>

C+o$e 02/-2-SS<-3//2-A2A3 2 02/-P6A7B D-02/-2338-23/

O)en 02/--FA-3//3-A2A3P-ST 02/-SN-2/ D-02/-2338-23/

Remote operating a#e%

No !eote o)e!"tin# "+e$ "!e )!oi&e& in thi$ 'nit.

.In%tr(ment a#arm%

In$t!'ent "+"! t:)e "!e +i$te& e+o(. Set "+'e$ o% e"ch "+"! "!e "$ $ho(n e+o(

@2 Lee+ "+"!Unit G

T"# No. Se!ice ALL AL AH AHH P?ID No.

LI-/2> A$o!e! Knoco't D!' Lee+ 50.0 D-02/-2338-224

LIC-//= F'e+ 1"$ Aine A$o!e! Lee+ = 55.= D-02/-2338-224

LIC-/2/ Rich Aine F+"$h D!' Lee+ 2>.= 0/.2 D-02/-2338-226

LI-/3/ R. Aine F+"$h D!' Inte!%"ce >.0 0>.> D-02/-2338-226

18




SHEET 2> OF 235

LI-/=8 Aine M"e-') T"n Lee+ 20.0 >3.8 D-02/-2338-22=

LI-/34 Aine Sto!"#e T"n Lee+ >.4 >8 D-02/-2338-22=

LI-/38 Aine S') T"n Lee+ 26.> 08.2 D-02/-2338-22=

LI-/44 Aine Re#ene!"to! Lee+ 3/ 0/ D-02/-2338-22>LIC-/62 A. Re#ene!"to! Receie! Lee+ 33.8 06.4 D-02/-2338-23/

@3 Te)e!"t'!e A+"!Unit℃

T"# No. Se!ice ALL AL AH AHH P?ID No.

TI-/24 Le"n Aine Coo+e! O't+et 85 55 D-02/-2338-225

TI-/22 A. Re#ene!"to! Botto$ O't+et 24= D-02/-2338-22>

TI-/30 De$')e!he"te! O't+et 26/ 28/ D-02/-2338-22>

@4 F+o( A+"! Unit N47h o! 47h

T"# No Se!ice ALL AL AH AHH P?ID No.

FI-//6 A. A$o!e! Oh& @ T!e"te& #"$ 6038 D-02/-2338-224

FI-/28 Mech"nic"+ Fi+te!$ In+et +ine 28 33 D-02/-2338-225

FIC-/42 Re#ene!"to! Reoi+e!-A O't+et 3.0 D-02/-2338-22>

FIC-/43 Re#ene!"to! Reoi+e!-B O't+et 3.0 D-02/-2338-22>

@6P!e$$'!e A+"!Unit #7c3#


PIC-//3 T!e"te& 1"$ to SRU7 F1 S:$te 0.5 D-02/-2338-224

@8 Di%%e!enti"+ P!e$$'!e A+"!Unit #7c3


PDI-/=> Le"n Aine Soc Fi+te!$ DP 2./ D-02/-2338-228

PDI-/0/ Le"n Aine C"!on Fi+te! DP 2./ D-02/-2338-228

PDIC-/26 PD;-/26 DP 2.4 2.= D-02/-2338-225

PDI-/02 Le"n Aine Mech. Fi+te!$ DP 2./ D-02/-2338-225

@5 Othe! A+"!


;SH-2/0 02/-EA3 ;i!"tion D-02/-2338-225

;SH-238 02/-EA2 ;i!"tion D-02/-2338-23/

T"# No. Se!ice P?ID No.

A->20A7B7E7F 02/-P2A7B Se"+ S:$te T!o'+e D-02/-2338-226

A->2>A7B7E7F 02/-P3A7B Se"+ S:$te T!o'+e D-02/-2338-226

A->3/A7B7E7F 02/-P6A7B Se"+ S:$te T!o'+e D-02/-2338-23/






SHEET 32 OF 235

Preparing Unit for Pre4&ommi%%ioning

The %o++o(in# $ection (i++ &i$c'$$ the "!io'$ "$)ect$ "$$oci"te& (ith thecoi$$ionin# o% the Aine T!e"tin# P!oce$$ Unit. Thi$ $ection cont"in$ in%o!"tion"o't the )!e-coi$$ionin# "n& initi"+ $t"!t-') o% the 'nit. The )!e-coi$$ionin#

)!oce&'!e$ en$'!e th"t the 'nit i$ $"%e, o)e!"+e, "n& con$t!'cte& "$ $)eci%ie& :tho!o'#h in$)ection "n& te$tin#.

Pre4&ommi%%ioning

A$ the con$t!'ction o% the 'nit ne"!$ co)+etion, " +"!#e "o'nt o% (o! '$t e#in ino!&e! to )!e)"!e it %o! $t"!t-'). The$e )!e-coi$$ionin# "ctiitie$ h"e th!ee "in

)'!)o$e$

• To en$'!e, : tho!o'#h in$)ection "n& te$tin#, th"t the 'nit i$ $"%e, o)e!"+e, "n&

con$t!'cte& "$ $)eci%ie&Q

• To o)e!"te e*'i)ent %o! : %+'$hin#, !'nnin# in, etc. "n&• To "c*'"int the o)e!"to!$ (ith the 'nit.

The i)o!t"nce o% the$e "ctiitie$ c"nnot e oe!e)h"$ie&. No "tte! ho( (e++ " 'niti$ &e$i#ne&, i% the e*'i)ent i$ not "$ $)eci%ie&, not )!o)e!+: !o'#ht on $t!e", o! not'n&e!$too& : o)e!"to!$, it (i++ not )e!%o! "$ e)ecte&.A++ o% the %o++o(in# "ctiitie$ "!e !e*'i!e& to )!o)e!+: )!e-coi$$ion thi$ 'nit.Ho(ee!, "n e"ct o!&e! o% )!e$ent"tion nee& not e $t!ict+: oe:e&. De)en&in# on the

)!o#!e$$ o% con$t!'ction, ce!t"in )!oce&'!e$ ": e !e*'i!e& e"!+ie! o! +"te! th"t$'##e$te& he!e. A th!o'#h no(+e&#e o% the enti!e )!e-coi$$ionin# o)e!"tion (i++"++o( the )+"nt )e!$onne+ to $che&'+e "ctiitie$ in the o$t tie-$"in# "n& +"o!e%%icient (":. The$e "!e the nece$$"!: )!e-coi$$ionin# "ctiitie$2. ;e$$e+ In$)ection

3. In$)ection o% othe! M"o! E*'i)ent4. Pi)in# "n& In$t!'ent Chec 6. H:&!o$t"tic Te$tin#8. Line F+'$hin#5. R'n-in o% P')$ "n& D!ie!$=. Se!icin# "n& C"+i!"tion o% In$t!'ent$0. Coi$$ionin# o% Uti+itie$>. A"i+"i+it: Chec o% Cheic"+$, C"t"+:$t$, "n& Othe! M"te!i"+$2/. P+"nt P!e$$'!e Te$t22. Ai! F!eein#23. Coi$$ionin# o% A&&ition"+ P+"nt Se!ice$

Commi%%ioning of Uti#itie%

Uti+itie$ "!e )+"ce& in $e!ice &'!in# coi$$ionin# @ )!e)"!"tion %o! $t"!t-') .Ho(ee!, it $ho'+& e e!i%ie& th"t "++ 'ti+itie$ "!e in $e!ice o! in !e"&ine$$ )!io! to$t"!t-'). Line$ $ho'+& e %+'$he& "n& +e" te$te&. Ste" +ine$ $ho'+& e ("!e& ')$+o(+: to )!eent &""#e %!o ("te! h"e!. A++ $te" t!")$ "n& cont!o+ "+e$ "!e to

e )+"ce& into $e!ice "n& te$te&. The %o++o(in# +i$t o% $:$te$ $ho'+& e coi$$ione&2. P+"nt ("te! "n& t!e"te& ("te! $:$te$. The$e $:$te$ $ho'+& "+!e"&: h"e een

coi$$ione& )!io! to the +ine %+'$hin# )!oce&'!e.3. A++ e+ect!ic"+ "n& +i#ht $:$te$, inc+'&in# ee!#enc: )o(e! "c')$.4. A++ )+"nt "n& in$t!'ent "i! $:$te$.6. Nit!o#en $:$te.8. Ste" "n& con&en$"te $:$te$, ec+'&in# $te" t!"cin# %o! the oent.



5. Con&en$"te $:$te$, !eceiin# con&en$"te %!o $te" t!")$ o% $ee!"+ $te"$:$te$ note& "oe, "!e !e"&: %o! $e!ice. A++ $te" t!")$ $ho'+& e chece&%o! o)e!"i+it:.

=. A++ &!"in$ "n& e%%+'ent $:$te$.0. A++ %i!e %i#htin# "n& othe! ee!#enc: e*'i)ent.>. A++ $to!"#e t"n$ '$t e tho!o'#h+: %+'$he&, +e" te$te&, &!ie&, "n& )e!h")$ "i!-

%!ee& i% the t"n i$ in h:&!oc"!on $e!ice. Tho$e t"n$ th"t h"e een "i!-%!ee&$ho'+& e +e%t 'n&e! $+i#ht )o$itie nit!o#en )!e$$'!e. A++ +ine$ to "n& %!o t"n"#e'$t e %+'$he&, +o(n &!: (ith nit!o#en, "n& )!e$$'!e te$te&.

The $te" t!"cin#, )+"nt coo+in# ("te!, "n& %+"!e $:$te$ (i++ e coi$$ione& "%te!the )+"nt )!e$$'!e te$t h"$ een co)+ete&.

Pre%%(re Te%ting

No %ie+& h:&!o$t"tic )!e$$'!e te$t o% e*'i)ent i$ )+"nne& %o! the 'nit. ;e$$e+$ "!e"$$'e& to h"e et h:&!ote$tin# !e*'i!eent$ in the %"!ic"to! $ho)$. H:&!o$t"ticte$t$ "!e "&e on ne( o! !e)"i!e& e*'i)ent to )!oe the $t!en#th o% "te!i"+$ "n&(e+&$. Thi$ te$t i$ no!"++: )e!%o!e& : con$t!'ction )e!$onne+ "n& it $ho'+& not econ%'$e& (ith othe! +e$$ $ee!e te$t$ #ene!"++: c"!!ie& o't e%o!e " $t"!t-') to chec theti#htne$$ o% connection$.

F#(%.ing o(t

A++ )i)in# '$t e tho!o'#h+: c+e"n o% &e!i$ "n& $c"+e. Thi$ ": e &one "%te!h:&!o$t"tic te$tin#, e%o!e the te$t ("te! i$ &!"ine&. C"!e '$t e t"en not to %+'$h&e!i$ into e*'i)ent.1ene!"++:, +i*'i& +ine$ "!e %+'$he& (ith ("te! "n& tho!o'#h+: &!"ine&. <"te! %+'$he&+ine$ (hich &o not &!"in %!ee+: $ho'+& e +o(n c+e"! (ith "i!. 1"$ +ine$ ": e eithe!("te! %+'$he& o! "i! +o(n, 't ("te! $ho'+& e +o(n %!o #"$ +ine$ i% ("te! %+'$he&.

1"$ +ine$ to co)!e$$o!$ '$t e %!ee o% ("te!.The %o++o(in# ite$ "!e $'##e$te& "$ #'i&e %o! +ine %+'$hin#2. <he!e )!"ctic"+, c+e"n ("te! $ho'+& e $'))+ie& to the e$$e+$, "n& conti#'o'$

+ine$ $ho'+& e %+'$he& "(": %!o the e$$e+. Nee! %+'$h into e*'i)ent.3. No "tte! (h"t the %+'$hin# e&i' - $te", "i!, o! ("te! - "i' o+'e "n&

e+ocit: $ho'+& e '$e& %o! tho!o'#h c+e"nin#.4. Reoe o!i%ice )+"te$ e%o!e %+'$hin#.6. Cont!o+ "+e$ "n& in-+ine in$t!'ent$ $ho'+& e !eoe&.8. In$t!'ent +ine$ $ho'+& e c+o$e& o%% o! &i$connecte&. The in$t!'ent "i! he"&e!

$ho'+& e tho!o'#h+: +o(n (ith c+e"n, &!: "i!.5. Re+ie% "+e$ $ho'+& e +in&e& i% the: h"e een !et'!ne& to $e!ice %o++o(in#

h:&!o$t"tic te$t.

=. Re#'+"te the %+'$hin# e&i' "t it$ $o'!ce. A$ e")+e$, ("te! %!o " e$$e+$ho'+& e !e#'+"te& "t the e$$e+Q "n& $te", "t the "+e in the $'))+: to the+ine ein# +o(n.

0. <he!e )o$$i+e, %+'$h &o(n("!& o! ho!iont"++:.>. A+(":$ %+'$h th!o'#h " )iece o% e*'i)ent$ :)"$$ to "n o)en en& e%o!e %+'$hin#

th!o'#h the e*'i)ent.2/. Di$connect +ine$ "n& ech"n#e!$ "n& %+'$h to the o)enin#$.22. F+'$h th!o'#h "++ ent$ "n& &!"in$.23. At )')$

• Di$connect $'ction "n& &i$ch"!#e )i)in# "n& %+'$h +ine$. Do not int!o&'ce "n:

%+'i& into )') c"$in# e%o!e c+e"nin# the )') $'ction.

• In$t"++ te)o!"!: $c!een$ in )') $'ction $t!"ine!$.

• Reconnect +ine$ %o! ci!c'+"tin# ("te!.

22




SHEET 34 OF 235

• See %'!the! &i$c'$$ion 'n&e! R'n-in o% P')$ "n& D!ie!$.

2. F+'$h o! +o(

• The "in he"&e!, %!o $o'!ce to en&, then

• E"ch +"te!"+ he"&e!, %!o the "in to en&, "n&• E"ch !"nch +ine, %!o the +"te!"+ he"&e! to en&.

2. Fo! $te" $:$te$, %+'$h (e++ th!o'#h &i!t +e# &!"in$ "n& $te" t!") :)"$$e$ e%o!e )+"cin# the t!")$ in $e!ice.

3. S'))+: $te" +ine$ to eecto!$ $ho'+& e &i$connecte& (hi+e ein# c+e"ne&.4. F+'$h th!o'#h o)en en& +ine$. Do not !e$t!ict %+o( in )!inci)+e.6. A%te! )+"cin# the $te" t!")$ in $e!ice, chec (hethe! the t!")$ o)e!"te )!o)e!+:.8. A%te! %+'$hin# o)e!"tion, chec th"t "++ o!i%ice )+"te$ "!e in$t"++e& "n& )o$itione&

co!!ect+: "$ )e! +i$t.5. <hen nece$$"!: e$$e+$ o! &!'$ "!e '$e& "$ ("te! !e$e!oi!$ %o! %+'$hin#, chec

e$$e+$ %o! ("te!-%i++e& &e$i#n. Mo!eoe!, " ("te!-%i++e& $:$te '$t not e &!"ine&(itho't "&e*'"te entin# to "oi& " "c'' con&ition "n& )!o"+e co++")$e o%

e*'i)ent not &e$i#ne& %o! "c''.U)on co)+etion o% +ine %+'$hin# o% "n: $:$te, c"!e%'++: chec th"t "++ te)o!"!:

!e"$ "!e !econnecte&, cont!o+ "+e$ "!e !e)+"ce&, "n& )')$ "+i#nent$ "!e no!"+.A+$o, e!i%: th"t "++ %!ee ("te! h"$ een &!"ine&.

A&i' C#eaning of Re&ipro&ating Compre%%or #ine%

Not "))+ic"+e to thi$ 'nit.

In%pe&tion an' R(n4in of P(mp% an' Fan%

P!o)e! in$t"++"tion "n& o)e!"tion o% )')$ "n& &!ie!$ i$ e$$enti"+ %o! t!o'+e-%!ee

)e!%o!"nce. The )')$ "n& &!ie!$ $ho'+& !eceie c"!e%'+ h"n&+in# &'!in# initi"+ !'n-in. The initi"+ !'n-in o% )')$ i$ #ene!"++: &one : ci!c'+"tin# ("te! th!o'#h the ne(e*'i)ent.Te)o!"!: $t!"ine!$ "!e in$t"++e& in the $'ction +ine o% the )')$, conenient+: +oc"te&%o! !eo"+ "n& c+e"nin#. The $c!een$ $ho'+& e )o$itione& $o th"t &i!t )"!tic+e$ (i++ not#!"it"te to in"cce$$i+e )+"ce$ (hen %+o( i$ $to))e&. D'!in# !'n-in o% )')$, the$t!"ine!$ ": c"'$e $oe !e$t!iction o% %+o(. A$ &e!i$ co++ect$ in the $t!"ine!$, %+o( tothe )')$ (i++ %"++ o%%. <hen thi$ h"))en$ to " cent!i%'#"+ )'), it (i++ e nece$$"!: toth!ott+e the )') &i$ch"!#e : )"!ti"++: c+o$in# the &i$ch"!#e "+e. Thi$ (i++ )!eentthe )') %!o c"it"tin#, (hich c"n c"'$e &""#e to the )'). Ho(ee!, "+$o "oi&!e$t!ictin# the )') &i$ch"!#e to the etent th"t it c"'$e$ inte!n"+ $+i))"#e "n&ece$$ie he"t #ene!"tion.

In $t"!tin# " t'!ine &!ien cent!i%'#"+ )'), the !ot"tion $ho'+& e !o'#ht ') to the$)ee& "$ !")i&+: "$ )o$$i+e. No!"+ o)e!"tin# $)ee&$ "!e '$'"++: "tt"ine& !")i&+: "n&"'to"tic"++: (ith oto!-&!ien )')$, "$$'in# )!o)e! oto! $t"!tin#.The &ee+o)ent o% &i$ch"!#e )!e$$'!e i$ e$$enti"+ to %+'$h "n& +'!ic"te the (e"!in#!in#$. A%te! initi"++: $t"!tin# the )'), c+o$e the &i$ch"!#e "+e %o! " $ho!t tie.S'$e*'ent+:, it i$ "+(":$ "&i$"+e, (he!e )!"ctic"+, to c+o$e the )') &i$ch"!#e "+eie&i"te+: )!io! to $h'ttin# &o(n " cent!i%'#"+ )'). Ho(ee!, &i$ch"!#e "+e$ ono)e!"tin# )o$itie &i$)+"ceent )')$ $ho'+& nee! e c+o$e&. The$e )')$ c"n oe!

)!e$$'!e the$e+e$ "n& &o(n$t!e" +ine$ "n& e*'i)ent. The %o++o(in# ite$ "!e$'##e$te& %o! checin# )!io! to !'n-in2. The "n'%"ct'!e!$ o)e!"tin# in$t!'ction$ %o! "n: $)eci%ic )!ec"'tion$ th"t $ho'+&

e o$e!e&.

3. Co)+etion o% oe!"++ in$t"++"tion.



4. A+i#nent o% )') "n& &!ie! %o! co+& o)e!"tion. No 'n&'e $t!"in : the )i)in# onthe )') o! &!ie! i$ "++o("+e.

6. Coo+in# %+'i& )i)in# "n& $e"+ o! #+"n& oi+ )i)in#

• Conention"++: )"ce& )')$ in hot $e!ice "!e #ene!"++: %'!ni$he& (ith#+"n& oi+. ;e!i%: th"t thi$ in$t"++"tion i$ co!!ect "n& co)+ete.

• Fo! )')$ (ith ech"nic"+ $e"+$, e!i%: th"t "++ o% the co)onent$ o% the

%+'$hin# $:$te @ $'ch "$ $t!"ine!$, $e)"!"to!$, !e$t!iction o!i%ice$, "n& coo+e!$ h"e een co!!ect+: in$t"++e& "n& "!e c+e"n. Lo$$ o% %+'$h o! &i!t: %+'$h ":c"'$e the %"i+'!e o% $e"+$.

2. P"cin# o! $e"+$ "!e in$t"++e&.3. Be"!in#$ "n& $h"%t$ h"e een c+e"ne& )!io! to %in"+ +'!ic"tion.4. P') "n& &!ie! "!e +'!ic"te& "cco!&in# to +'!ic"tion in$t!'ction$.6. Rot"tion o% e+ect!ic oto! &!ie!$ 'nco')+e& %!o the )'). R'n-in 'nco')+e& %o!

" ini' o% %o'! ho'!$, e!i%:in# #oo& oto! o)e!"tion.D'!in# !'n-in, "n: )')$ "!e &e+ie!in# " hi#he! &en$it: +i*'i& @ ("te! th"n the

no!"+ )!oce$$ %+'i&. B't the )')$ &!ie!$ "!e $ie& %o! the no!"+ )')in# %+'i&.Con$e*'ent+:, the!e i$ )otenti"+ %o! the oe!+o"& o% "n: e+ect!ic oto!$. To "oi&oe!+o"&in# the oto! o% " cent!i%'#"+ )'), the %+o( '$t e +iite& : th!ott+in# the

)') &i$ch"!#e "+e. <hen &oin# $o, i% )o$$i+e, chec the ")e!"#e '$"#e "#"in$t&e$i#n. The %o++o(in# )!oce&'!e i$ $'##e$te& %o! )') !'n-in2. Rot"te )') "n& &!ie! : h"n&, e!i%:in# th"t the: !o++ %!ee+:.3. Chec th"t !'n-in ("te! ci!c'+"tion i$ +ine& ').4. O)en $'ction "+e$ %'++:, entin# "i! %!o )i)in# "n& )')$, co)+ete+: %i++in#

(ith +i*'i&.6. E$t"+i$h %+o( o% coo+in# %+'i&, (he!e !e*'i!e&.8. Chec th"t +'!ic"tion i$ $"ti$%"cto!:.

5. M"e $'!e th"t e+ect!ic )o(e! i$ ""i+"+e %!o the $(itch #e"! to the $t"!te! o% thee+ect!ic oto! &!ie!.=. B"!e+: o)en the &i$ch"!#e "+e on the cent!i%'#"+ )').0. St"!t the )')Q i% the )!e$$'!e &oe$ not 'i+& ie&i"te+:, $to) "n& !e$o+e the

)!o+e.>. <hen the &i$ch"!#e )!e$$'!e h"$ inc!e"$e& $"ti$%"cto!i+: "%te! $t"!tin#, #!"&'"++:

o)en the &i$ch"!#e "+e to ot"in the &e$i!e& %+o( !"te.2/. In the eent o% 'n'$'"+ noi$e, i!"tion, oe!he"tin#, o! othe! "no!"+ con&ition$,

$h't the )') &o(n ie&i"te+:. Co!!ect the c"'$e e%o!e !e$'in# '$e o%the )'). Contin'e to chec %o! "no!"+ con&ition$ "$ the$e ": occ'! "%te!

)!o+on#e& o)e!"tion.22. Chec $h"%t $e"+in#Q ech"nic"+ $e"+$ $ho'+& $ho( no +e""#e. Conention"++:

)"ce& $t'%%in# oe$ '$t "+(":$ e )e!itte& to +e" $+i#ht+: to )!oi&e$oe +'!ic"tion "n& to )!eent oe!he"tin#. St'%%in# o #+"n& n't$ "!e#ene!"++: on+: %in#e! ti#ht. A +e"in# ech"nic"+ $e"+ (i++ $ho( $oe +e""#eon $t"!t-'). Ho(ee!, "%te! the )') i$ $t"!te& "n& $to))e& " %e( tie$, the+e""#e ": $to).

23. O)e!"te the )'), &i!ectin# %+o($ th!o'#h "++ $'ction "n& &i$ch"!#e )i)in#ci!c'it$.

24. In$)ect "n& c+e"n $c!een$ "$ !e*'i!e&.26. Rechec "n& !e"+i#n i% !e*'i!e&, "%te! "n: &i$t'!"nce o% )i)in#, $'ch "$ !e*'i!e&

%o! $'ction $c!een in$)ection i% )i)e %+"n#e$ h"e to e )"!te& %o! $c!een!eo"+.

28. <hen $h'ttin# &o(n, c+o$e the &i$ch"!#e "+e %i!$t, "int"inin# &i$ch"!#e )!e$$'!e (hi+e the )') !o++$ to " $to). Thi$ (i++ )!otect "#"in$t the )') !o++in#

24




SHEET 38 OF 235

"c("!&$ $ho'+& the &i$ch"!#e chec "+e +e"$, "n& #ie$ the (e"!in# !in#$ "*'ic %+'$h.

A%te! "++ +ine$ ""i+"+e to " )') h"e h"& $'it"+e %+'$hin#, the te)o!"!: $c!een ": e !eoe&, 't on+: "%te! it h"$ $ho(n %!ee o% &e!i$ on t(o $'cce$$ie e"in"tion$.The )e!"nent $t!"ine!$ ": then e in$t"++e& (he!e !e*'i!e&.

Lea Te%t

The )'!)o$e o% the +e" te$t i$ to chec the )i)in# "n& e*'i)ent %o! ti#htne$$ o%%+"n#e$, connection$, "n& %ittin#$. The$e te$t$ $ho'+& not e con%'$e& (ith theh:&!o$t"tic te$t$ "&e &'!in# con$t!'ction. 1ene!"++: )+"nt "i! o! nit!o#en i$ '$e& %o!thi$ te$t.P!io! to te$t, "++ the in$t!'ent$ (hich h"e een 'no'nte& in the )!eio'$ $te)$ '$t

e !eo'nte&.The te)o!"!: i$o+"tin# +in&$ '$t e !eoe& %o! " %in"+ )!e$$'!e te$t, 't the "tte!:+iit +in&$ '$t !e"in in the c+o$e& )o$ition.The ti#htne$$ te$t '$t e con&'cte& (ithin ce!t"in +oc$ &ii&e& "cco!&in# to the&e$i#n )!e$$'!e o% e"ch e$$e+.

• The !ecoen&e& )!e$$'!e %o! the ti#htne$$ te$t i$ "o't =./ #7c31 @ ""i+"+e

)!e$$'!e in "i! $:$te o! the no!"+ o)e!"tin# )!e$$'!e, (hichee! i$$"++e!.

• Le""#e $h"++ e chece& (ith $o") $o+'tion.

• A++ %+"n#e$ $h"++ e chece& %o! +e""#e "n& !e-ti#htene&, i% +e""#e i$ %o'n&.

• D'!in# the ti#htne$$ te$t, the o)e!"tin# )!e$$'!e $h"++ e "int"ine& "$ $ho(n

"oe.

• A %in"+ +e"7)!e$$'!e te$t (ith )!oce$$ %+'i&$ "t (o!in# )!e$$'!e i$ "&e "$ )"!t

o% the )+"nt $t"!t-') &e$c!ie& in the net $ection.

The te$t )!e$$'!e $ho'+& e he+& %o! " ini' o% one ho'!, (hi+e ee!: %+"n#e "n& oint in the $:$te i$ c+o$e+: e"ine& %o! +e"$. St'o!n %+"n#e +e"$ ": o%ten e$to))e& : $i)+: 'no+tin# "n& !eo+tin# the %+"n#e$. Sc!e(e& connection$ ":!e*'i!e Te%+on t")e.

In%pe&tion an' R(n4in of Re&ipro&ating Compre%%or


In%pe&tion an' R(n4in of Centrif(ga# Compre%%or


Loa'ing interna# materia# re/(ire' for a*%or*er%; e%%e#%; pa&e' &o#(mn%


$r)ing o(t Fire' .eater


$r)ing o(t Rea&tor %e&tion




Preparing Rea&tor%


Loa'ing Cata#)%t


$egrea%ing for Amine Cir&(#ating S)%tem

The )!e$ence o% he": h:&!oc"!on, $'ch "$ #!e"$e o! !'$t inhiition co"tin#$ on e$$e+("++$ "n& inte!n"+$, co'+& c"'$e $e!io'$ "ine e'+$i%ic"tion )!o+e$ i% "++o(e& to!e"in. A+$o "n: !'$t )!e$ent (i++ *'ic+: !e"ct (ith H3S on $t"!t-') to %o! )"!tic'+"tei!on $'+%i&e.Acco!&in#+:, "++ )i)in# "n& e*'i)ent th"t (i++ e in cont"ct (ith the "ine $o+'tion'$t e tho!o'#h+: c+e"ne& "n& &e#!e"$e&. The )!e%e!!e& c+e"nin# $o+'tion i$ 3 (tG$o+'tion o% $o&i' c"!on"te @ N"3CO4, "+$o c"++e& $o&" "$h . Thi$ &e#!e"$in# "n&c+e"nin# $o+'tion i$ )!e)"!e& in the Aine Sto!"#e T"n @02/-TK3 "n& ci!c'+"te&th!o'#ho't the "ine t!e"tin# 'nit, e)+o:in# the no!"+ "ine ci!c'+"tion %+o( )"th.<hi+e ci!c'+"tin#, the $o+'tion i$ i+&+: he"te& (ith the $t!i))e! !eoi+e! to 5/ oC to"i& in the #!e"$e !eo"+.Fo++o(in# tho!o'#h c+e"nin#, the $o&" "$h $o+'tion i$ &!"ine& "n& !e)+"ce& :con&en$"te ("te! "n& the ci!c'+"tion $chee !e)e"te& to !in$e the e*'i)ent. A &et"i+e&&e#!e"$in# )!oce&'!e %o++o($.

NoteThi$ )!oce&'!e )!e$'e$ th"t the "ine t!e"tin# 'nit )!e-coi$$ionin# "ctiitie$ "!eco)+ete, "++ 'ti+itie$ "!e ""i+"+e, "n& in$t!'ent"tion h"$ een chece& o't "n& i$!e"&: %o! $e!ice. The #"$ +"netin# $:$te %o! Aine Sto!"#e T"n c"n e

coi$$ione& "t thi$ tie to h"e it !e"&: (hen "ine $o+'tion i$ )!e)"!e&.

P!e)"!"tion o% De#!e"$in# So+'tionP!e)"!e " 3 (tG $o+'tion o% $o&" "$h (ith $te" con&en$"te in the Aine Sto!"#eT"n.The o+'e o% $o&" "$h $o+'tion !e*'i!e& (i++ e "))!oi"te+: e*'"+ to the o+'e o%"ine inento!: in the otto o% the $t!i))e!, )+'$ e"ch "$o!e! to " 8/G #"'#e #+"$$+ee+, )+'$ 3/ )e!cent o% the Aine Sto!"#e T"n o+'e, )+'$ "))!oi"te+: 38G o%thi$ tot"+ o+'e to "++o( %o! +ine o+'e$, e$$e+ t!": inento!ie$ "n& co)+ete co+'n%+oo&in#, one "t " tie. Thi$ *'"ntit: o% $o+'tion i$ e"$i+: )!e)"!e& '$in# the "ine"e-') %"ci+itie$ "n& the "ine $to!"#e t"n. The "ine $to!"#e t"n c"n e '$e& to&i$$o+e the $o&" "$h in ("te! "$ " concent!"te& $o+'tion. The $o&" "$h $ho'+& e

co)+ete+: &i$$o+e& to "oi& +')in# o% the $o+i& (hich (o'+& c"'$e )')in# "n& )') $c!een )+'##in# )!o+e$.The "ine t!"n$%e! )') i$ '$e& to ci!c'+"te the $o&" "$h $o+'tion in the $to!"#e t"n to

)!oi&e " hoo#eneo'$ $o+'tion. S")+e "n& "n"+:e the $o+'tion to &ete!ine the $o&""$h concent!"tion. A&& o!e ("te! o! $o&" "$h "$ in&ic"te& : the $")+e !e$'+t to"&'$t the $o&" "$h concent!"tion to "))!oi"te+: 3 (tG.

Te)o!"!: Mo&i%ic"tion$ to the Unit2. Reoe the %i+te! e+eent$ %!o the "ine %i+te!$. I% "cti"te& ch"!co"+ h"$ "+!e"&:

een +o"&e& into the %i+te!, i$o+"te the %i+te!$ (ith +oc "+e$ "n& +in&$ to"oi& ci!c'+"tion o% $o&" "$h $o+'tion th!o'#h the.

3. Connect )+"nt "i! o! nit!o#en ho$e$ %itte& (ith te)o!"!: )!e$$'!e !e#'+"to!$ to the

oe!he"& +ine o% e"ch "$o!e! co+'n. Thi$ (i++ )!oi&e " )!e$$'!e $o'!ce

26




SHEET 3= OF 235

(ith (hich to "int"in "&e*'"te )!e$$'!e$ in the co+'n to ci!c'+"te&e#!e"$in# $o+'tion "c to the $t!i))e!. Dete!ine the !e*'i!e& "$o!e!o)e!"tin# )!e$$'!e$ to "$$'!e ci!c'+"tion "c to the Rich Aine F+"$hD!'@02/-;6. In c"$e o% hi#h )!e$$'!e "$o!e!$ (ith thei! !e$)ectie hi#h

)!e$$'!e &!o) !ich "ine cont!o+ "+e$, $)eci"+ )!oi$ion$ $ho'+& e "&e to"++o( %o! cont!o+ o% the "$o!e! +ee+ "t the +o(e!-th"n-&e$i#n )!e$$'!e o%&e#!e"$in#.

4. M"e )!oi$ion$ to ent the !e#ene!"to! )!e$$'!e "$ it $+o(+: inc!e"$e$ &'!in#ci!c'+"tion. I% "i! i$ ein# '$e& to )!e$$'!e the "$o!e!$, entin# o% ece$$!e#ene!"to! )!e$$'!e to " coi$$ione& %+"!e he"&e! '$t e "oi&e&.Sii+"!+:, "ine e$$e+ !e+ie% "+e$ '$t e i$o+"te& to )!eent %+"!e #"$+e""#e into the $:$te (hich i#ht %o! " co'$tion it'!e.

6. M"e " te)o!"!: ho$e connection et(een the +e"n "ine ci!c'+"tion )')&i$ch"!#e "n& the $te"-o't o! othe! $'it"+e connection the Aine Re#ene!"to!Receie! @02/-;5 to inc+'&e thi$ e$$e+ in the &e#!e"$in# )!oce&'!e.

Inento!: "n& Ci!c'+"teP!io! to inento!: o% "ine $o+'tion, co+& "n& hot ("te! ci!c'+"tion $h"++ e con&'cte&(ith c+e"n ("te! to "e )!e-c+e"nin# o% the $:$te.2. 1"'#e the Aine Sto!"#e T"n "n& !eco!& the "ct'"+ o+'e o% the $o&" "$h

$o+'tion ""i+"+e. Kee) " !eco!& %o! %'t'!e !e%e!ence o% the tot"+ o+'e o%$o&" "$h $o+'tion '+ti"te+: !e*'i!e& to e$t"+i$h $t"+e ci!c'+"tion in the 'nit.Thi$ e"$'!eent (i++ "+$o e he+)%'+ (hen the initi"+ "ine o+'e i$

+en&e& %o! $t"!t-') o% the 'nit.3. U$in# the Aine T!"n$%e! P'), %i++ the Aine Re#ene!"to! Receie! (ith $o&"

"$h $o+'tion i" the te)o!"!: ho$e connection. E)t: the !eceie! to theAine Re#ene!"to! '$in# the !e%+' )'). Re)e"t thi$ %i++in# "n& e)t:in#th!ee tie$. I% tie )e!it$, (ith the !e#ene!"to! o%% #"$ cont!o+ "+e +oce&in, %i++ the Aine Re#ene!"to! Con&en$e! "n& oe!he"& +ine (ith $o&" "$h

$o+'tion once i" the $"e te)o!"!: ho$e connection "n& e)t: (ith the!e%+' )').CAUTION Do not %i++ the oe!he"& +ine i% the oe!he"& con&en$e! t'e$ "!e"+'in'. 1ene!"++:, the "ine t!"n$%e! )') c")"cit: i$ $"++ "n& thi$initi"+ inento!:in# (i++ e tie con$'in#.

4. Fo++o(in# the c+e"n$in# o% the !e#ene!"to! oe!he"& $:$te, !o'te the incoin#$o&" "$h $o+'tion %!o the t!"n$%e! )') &i$ch"!#e into the $'ction o% the +e"n"ine ci!c'+"tion )')$. Thi$ (i++ "c $o+'tion into the !e#ene!"to! otto$

: (": o% the +e"n7!ich ech"n#e!.6. <hen " 8/G +ee+ "))e"!$ in the "ine !e#ene!"to! otto +ee+ #+"$$, $t"!t the

+e"n "ine ci!c'+"tion )'), "n& e#in to inento!: (o!in# +ee+$ in e"ch"$o!e! i" the no!"+ +e"n "ine t!"n$%e! +ine. Thi$ ": h"e to e &one

"tch(i$e to )!eent " +o$$ o% +ee+ in the !e#ene!"to! otto.8. <hen (o!in# +ee+$ h"e een e$t"+i$he& in the "$o!e!$ "n& the !e#ene!"to!,

)!e$$'!e e"ch "$o!e!$ "n& the !e#ene!"to!, )!e$$'!e e"ch "$o!e! to it$ )!e&ete!ine& ci!c'+"tion )!e$$'!e (ith the te)o!"!: ho$e "n& )!e$$'!e!e#'+"to! connection on the oe!he"& +ine.

5. Be#in ci!c'+"tion to e"ch "$o!e!. Coi$$ion e"ch "$o!e! otto +ee+cont!o++e! (hen +ee+$ "!e e$t"+i$he& "n& !et'!n the $o&" "$h $o+'tion "c tothe !e#ene!"to!.

=. S'))+eent the !e#ene!"to! $o&" "$h $o+'tion +ee+ "$ nece$$"!: (ith "&&ition"+$o+'tion to o! %!o the +e"n "ine $to!"#e t"n to "int"in " 8/G (o!in#+ee+ in the !e#ene!"to!.

0. Line o't the ci!c'+"tion !"te$ "t o! ne"! &e$i#n "ine ci!c'+"tion !"te$.



>. <ith the ci!c'+"tion %+o($ $t"i+ie&, c"!e%'++: coi$$ion the "ine !e#ene!"to!!eoi+e! "n& #!"&'"++: inc!e"$e the ci!c'+"tin# $o&" "$h te)e!"t'!e to 5/ oC.

NOTE The +e"n "ine coo+e! $ho'+& not e in $e!ice.2/. M"int"in $o&" "$h $o+'tion ci!c'+"tion %o! " ini' o% %o'! ho'!$, )!e%e!"+: 36

ho'!$, to "$$'!e th"t "++ $'!%"ce$ "!e cont"cte& : the $o&" "$h $o+'tion.Reee! to !o'te " $+i)$t!e" th!o'#h the e)t: %i+te! ho'$in#$.

22. A%te! the $o&" "$h $o+'tion h"$ ci!c'+"te& %o'! ho'!$, %+oo& e"ch "$o!e! (ith$o&" "$h $o+'tion 'nti+ it i$ co)+ete+: %'++ to "e $'!e th"t "++ inte!n"+$'!%"ce$ h"e een (ette& "n& &e#!e"$e&. M"e $'!e th"t no e*'i)ent i$oe!-)!e$$'!e& &'!in# thi$ $te). A+$o %+oo& the "ine $to!"#e t"n (hen"))!o)!i"te.

23. S")+e "n& "n"+:e the $o&" "$h $o+'tion &'!in# ci!c'+"tion to "$$'!e th"t the $o&""$h i$ not tot"++: con$'e&. I% thi$ i$ the c"$e, "&&ition"+ $o&" "$h $ho'+& e"&&e& to the ci!c'+"tin# $o+'tion.

24. S+o(+: !e&'ce the $te" %+o( to the !e#ene!"to! !eoi+e! 't contin'e the $o&" "$hci!c'+"tion %o! " %e( "&&ition"+ ho'!$ to "++o( it to #!"&'"++: coo+ to"))!oi"te+: 40 oC .

26. Sh't &o(n the +e"n "ine ci!c'+"tion )') "n& &i$contin'e ci!c'+"tion. P!e$$'!ethe $o&" "$h $o+'tion %!o e"ch "$o!e! to the "ine !e#ene!"to!. I% the!e#ene!"to! %o'n&"tion +o"&in# (i++ )e!it, it too c"n e %+oo&e& (ith $o&" "$h$o+'tion %o! the o$t e%%ectie &e#!e"$in#.

28. A$ $o&" "$h $o+'tion i$ &!"ine& %!o )')$, +ine$, "n& e$$e+$, the "ine $')(i++ e %i++e& (ith the '$e& $o&" "$h $o+'tion. The $') i$ )')e& o't i" "te)o!"!: ho$e to the !e%ine!: oi+: ("te! $e(e! $:$te.

25. Fin"++:, &!"in "++ e$$e+$, t"n$, )')$, "n& +ine$ o% the &i!t: $o&" "$h $o+'tion"in# $'!e $oe !e$i&'"+ )!e$$'!e !e"in$ on "++ co+'n$ to "oi& "n: ch"nce o% " "c''.

<"te! Rin$e2. Ree$t"+i$h (o!in# +ee+$ in the !e#ene!"to! "n& "$o!e!@$ "$ e%o!e 't thi$

tie '$e co+& con&en$"te in$te"& o% $o&" "$h $o+'tion. Thi$ ": e &one "$ )!eio'$+: o't+ine& %o! the $o&" "$h $o+'tion o! : '+ti)+e ho$e connection$to the t!e"te& ("te! $'))+: he"&e!, (hichee! i$ o!e conenient. Do not%o!#et to !in$e the !e#ene!"to! oe!he"& $:$te.

3. P!ocee& "$ o't+ine& %o! the $o&" "$h $o+'tion ece)t th"t ci!c'+"tion o% the ("te!%o! %o'! ho'!$ c"n e &one "t "ient te)e!"t'!e 'n+e$$ c+i"tic con&ition$%"o! $+i#ht ("!in#.

4. <hen !in$in# i$ co)+ete, &!"in the ("te! to the $e(e!, "#"in t"in# c"!e to"int"in )o$itie )!e$$'!e on "++ e*'i)ent.

6. Rein$t"++ the "ine %i+te! e+eent$ (hen ("$hin# "n& !in$in# i$ co)+ete.

8. Chec "n& c+e"n ') )') $c!een$ one %in"+ tie.

P(rging an' ga% *#aneting

Be%o!e "&ittin# h:&!oc"!on$ into "n: )!oce$$ +ine$ o! e$$e+$, $"%e !e%ine!: )!"ctice!e*'i!e$ th"t the 'nit e %!ee& o% "i!. The "i! ": e &i$)+"ce& (ith ("te!, $te", o!ine!t #"$, $'ch "$ nit!o#en. The $:$te '$t e )'!#e& to )!eent %o!"tion o%e)+o$ie ie& #"$ )!io! to "&ittin# %+""+e "te!i"+$.I% $te" i$ '$e&, )!ec"'tion$ $ho'+& e t"en to "oi& the %o++o(in# )otenti"+ )!o+e$o! h""!&$2. Co++")$e D'e to ;"c'' Soe o% the e$$e+$ ": not e &e$i#ne& %o! "c''.

Thi$ e*'i)ent '$t not e "++o(e& to $t"n& +oce& in (ith $te" $ince the

con&en$"tion o% the $te" (i++ &ee+o) " "c''. Th'$, the e$$e+ '$t e

28




SHEET 3> OF 235

ente& &'!in# $te"in# "n& then ie&i"te+: %o++o(e& ') (ith %'e+ #"$ o!nit!o#en )'!#e "t the conc+'$ion o% the $te"-o't.

3. F+"n#e "n& 1"$et$ Le"$ The!"+ e)"n$ion "n& $t!e$$ &'!in# ("!-') o%e*'i)ent "+on# (ith &i!t: %+"n#e %"ce$ c"n c"'$e $"++ +e"$ "t %+"n#e$ "n&#"$ete& oint$. The$e '$t e co!!ecte& "t thi$ tie.

4. <"te! H"e!in# C"!e '$t e t"en to )!eent ("te! h"e!in# (hen$te" )'!#in# the 'nit. See!e e*'i)ent &""#e c"n !e$'+t %!o ("te!h"e!in#.The %o++o(in# $te)$ !ie%+: o't+ine "i! %!eein# : $te" )'!#in#

6. Po!tion$ to e $te" )'!#e& inc+'&e "++ the co+'n$, e$$e+$, he"t ech"n#e!$,"n& +ine$.

8. P')$, $i#ht #+"$$e$, +ee+ #"'#e$ "n& in$t!'ent$ "!e not to e $te"e&-o't.Thi$ c"n e &one : c+o$in# thei! in+et "n& o't+et "+e$.

5. <hen the 'nit i$ &ii&e& into " n'e! o% $ection$ %o! $te" )'!#in#, it '$t e $o "!!"n#e& th"t $te" i$ inecte& %!o one en& o% the $ection "n& +o(n o't %!o the othe! en&.

=. O)en hi#h )oint ent$ "n& +o( )oint &!"in$ on the e$$e+$ to e $te" )'!#e&.A%te! o)enin# "++ ent$ "n& &!"in$, $te" )'!#e i$ con&'cte& : o)enin#the "+e "t the $te" o't+et "n& +o(in# in $te" %!o the $te" o'tconnection. C"!e '$t e t"en not to c"'$e h"e!in# (henint!o&'cin# $te". It ": e nece$$"!: to "e ') "&&ition"+ $te"connection$ to )!o)e!+: )'!#e $oe )i)in# (hich ": e &e"&-en&e&.

0. Tho!o'#h+: )'!#e "++ e*'i)ent "n& "$$oci"te& )i)in# o% "i!. The )!o#!e$$ o%the $te" )'!#e c"n e %o++o(e& : "!in# ') the P?I &i"#!" toin&ic"te the +ine$ )'!#e&. ;e!i%: th"t $'%%icient &!"in$ "!e o)en to &!"inthe con&en$"te (hich (i++ co++ect in +o( $)ot$ in the 'nit.

>. <hen the $te" )'!#in# i$ co)+ete&, $t"!t to c+o$e "++ the ent$ "n& &!"in$.To )!eent the c!e"tion o% ne#"tie )!e$$'!e (ithin the $:$te, the

inection o% " +itt+e $te" '$t e contin'e& 'nti+ the $'$e*'ent %i++in# o% %'e+ #"$ o! nit!o#en i$ $t"!te&.

2/. A%te! $te" )'!#in# "++ the $ection$ o% the 'nit, o)en "++ the +oc "+e$ th"th"$ een c+o$e& &'!in# the $te" )'!#in# o)e!"tion to en"+e the$'$e*'ent %'e+ #"$ o! nit!o#en %i++in# th!o'#ho't the $:$te.

22. St"!t to int!o&'ce %'e+ #"$ o! nit!o#en into "++ e$$e+$ "n& then c't "c the$te" %+o( 'nti+ it i$ $to))e&. Re#'+"te the %'e+ #"$ o! nit!o#en %+o( "n&the !e&'ction o% $te" $o th"t "c'' &'e to con&en$in# $te" i$ notc!e"te& in "n: e$$e+ o! th"t the !e%ine!: %'e+ #"$ $:$te )!e$$'!e i$ not"))!eci"+: !e&'ce&. Int!o&'ce %'e+ #"$ o! nit!o#en into the $:$te to

)!eent "c''. M"int"in the )!e$$'!e (ithin the $:$te "t /.8 2./#7c31. <hen the $:$te i$ 'n&e! %'e+ #"$ )!e$$'!e, chec the O3

content. @ O3 content $h"++ e +e$$ th"n 2./ o+G. . At ee!: )'!#in#$te), the )!e$$'!e o% e"ch e*'i)ent '$t e e)t 'n&e! it$ !e$)ectie&e$i#n )!e$$'!e.

23. D!"in "n: !e$i&'"+ con&en$"te %!o the 'nit.

Pre4&ommi%%ioning &.e& #i%t

Thi$ )!oce&'!e &e$c!ie$ in #ene!"+ te!$ the $te)$ to e %o++o(e& %o! )+"cin# the 'niton $t!e". The e"ct $e*'ence o% eent$ &e)en&$ on the %+o( $chee o% the )"!tic'+"!'nit. Ho(ee!, the %o++o(in# $te)$ '$t e co)+ete& e%o!e ch"!#in# %ee& #"$ to theUnit.2. A++ 'nnece$$"!: +in&$ "!e !eoe&,

3. A++ !e+ie% "+e$ "!e te$te& "n& in$t"++e&.



4. The %+"!e he"&e! i$ )'!#e& "n& in $e!ice.6. The $e(e!$ "!e in $e!ice.8. The %'e+ #"$ i$ in $e!ice.5. A++ in$t!'ent$ "n& cont!o+ $:$te$ "!e !e"&: %o! $e!ice.=. A++ 'ti+itie$ "!e in $e!ice.0. Cont!o+ "+e$ "n& :)"$$e$ "!e +oce& in.

30




SHEET 42 OF 235

Commi%%ioning

Genera# oera## &ommi%%ioning p#an

<ith the 'nit &e#!e"$e&, !in$e&, "n& 'n&e! "n o:#en-%!ee #"$ )o$itie )!e$$'!e, the 'niti$ no( !e"&: %o! $t"!t-'). The "ine $o+'tion c"n e )!e)"!e& "n& inento!ie& into the'nit. The "ct'"+ o+'e o% "ine $o+'tion !e*'i!e& c"n e e$t "$ce!t"ine& %!o the&"t" ot"ine& &'!in# the &e#!e"$in# o)e!"tion$.The initi"+ $t"!t-') con$i$t$ o% the %o++o(in# $e*'enti"+ "ctiite$2. P!e)"!"tion o% "ine $o+'tion.3. Inento!:in# "ine to Re#ene!"to! "n& A$o!e!$.4. Int!o&'ction o% %ee& to 'nit.6. E$t"+i$hin# Aine ci!c'+"tion.8. Coi$$ionin# o% Re#ene!"to! Reoi+e!.5. Coi$$ionin# o% Aine %i+te!$.=. Fin"+ A&'$tent$ o% O)e!"tin# )"!"ete!$.

$etai#e' %tep4*)4%tep %tart4(p pro&e'(re

P!e)"!"tion o% Aine So+'tion

Re%e! to the $ection 22.8.

Inento!:in# Aine to Re#ene!"to! "n& A$o!e!$.2. Con%i! th"t the "ci& %+"!e $:$te h"$ een "i! %!ee& "n& i$ in $e!ice. A+$o

con%i! th"t "n: i$o+"tion +in&$ )!eio'$+: in$t"++e& to i$o+"te the 'nit %!othe %+"!e $:$te h"e een !eoe&.

3. T!"n$%e! the "ine $o+'tion %!o the Aine Sto!"#e T"n @ 02/-TK3 to the

Aine Re#ene!"to! @ 02/-;8 (ith the Aine T!"n$%e! P')$ @ 02/-P5A7B . A$ the "ine +ee+ in the Re#ene!"to! inc!e"$e$, )e!io&ic"++: $t"!tthe Le"n Aine P')$ @ 02/-P4A7B "n& t!"n$%e! "ine to the "$o!e!$'nti+ " i$i+e (o!in# +ee+ i$ ot"ine& in e"ch "$o!e! co+'n.

4. <ith " (o!in# +ee+ @ c". 8/G in the "$o!e! +ee+ #+"$$, contin'e to inento!:%!e$h "ine to "n 08G +ee+ in the Re#ene!"to! otto. Thi$ "&&ition"+o+'e o% "ine, "n& )!o"+: o!e, (i++ e !e*'i!e& (hen h:&!oc"!on %+o(to the "$o!e! c"'$e$ "n inc!e"$e in "ine inento!: on the "$o!e! t!":$.

6. ;e!i%: th"t the "ine !e#ene!"to! o%%-#"$ +ine $te" "cetin# i$ coi$$ione& "n&th"t "++ $te" t!")$ "!e )"$$in# con&en$"te. The$e (i++ !e*'i!e checin# e"ch "n&ee!: $hi%t. Initi"++:, e)ect to c+e"n the$e $te" t!")$ %!e*'ent+: 'nti+ "++ o% the &i!th"$ een &i$+o&#e& %!o the )i)e "cet.

Int!o&'ction o% Fee& to Unit2. Int!o&'ce the h:&!oc"!on %ee& to e"ch "$o!e!, $+o(+: )!e$$'!in# e"ch "$o!e!

to the &e$i#n o)e!"tin# )!e$$'!e$.3. Coi$$ion the )!e$$'!e cont!o++e! @ PIC-//3 %o! the F'e+ 1"$ Aine

A$o!e!@02/-;3.4. Re%e! to the O)e!"tin# M"n'"+ o% the LP1 Me!o P!oce$$ Unit %o! the Aine

A$o!e!@0/3-;2 "n& th"t o% the Die$e+" P!oce$$ Unit %o! the Rec:c+e 1"$Sc!'e!@306-;8.

E$t"+i$hin# Aine Ci!c'+"tion



2. St"!t the Le"n Aine P')$ @ 02/-P4A7B "n& $en& +e"n "ine to e"ch "$o!e!.Set the %+o( cont!o++e! @ FIC-/25 "t i& $c"+e "n& e!i%: it$ o)e!"tion %o! theF'e+ 1"$ Aine A$o!e!@02/-;3.

3. ;e!i%: th"t e"ch "$o!e! otto h"$ " (o!in# +ee+, 'n+oc the +ee+ cont!o+"+e @ L;-//= , "n& e!i%: th"t the +ee+ cont!o+ i$ o)e!"tin# co!!ect+: "n&!ich "ine i$ ein# !et'!ne& to the Rich Aine F+"$h D!'@02/-;6.

4. <hen 02/-;6 h"$ " (o!in# +ee+, coi$$ion the Rich Aine P')@02/-P3A7B"n& then )'t LIC-/2/ into "'to.

6. T!"n$%e! "ine $o+'tion %!o the Aine Sto!"#e T"n@02/-TK3 to the AineRe#ene!"to!@02/-;8 "$ !e*'i!e& to "int"in "n "&e*'"te (o!in# +ee+ in theAine Re#ene!"to! otto. Thi$ i$ the $'!#e !e$e!oi! %o! the enti!e "ine $:$te"n& '$t nee! e $o +o( th"t the )') +o$e$ $'ction, o! $o hi#h th"t the !eoi+e!!et'!n +ine i$ %+oo&e&.

Note I% the coi$$ion o% the Die$e+" Unit i$ &e+":e& "n& it i$ &i%%ic'+t to"int"in $'%%icient "ine ci!c'+"tion to o)e!"te the )')$, $oe o% the +e"n "ine $h"++

e B:)"$$e& to the Rich Aine F+"$h D!'@02/-;6 : '$in# " :)"$$ +ine@02/-5-AM-28/4-A3A2P.Coi$$ionin# o% Re#ene!"to! Reoi+e! 2. <ith the "ine ci!c'+"tion e$t"+i$he&, coi$$ion the $te" %+o( to the Aine

Re#ene!"to! Reoi+e! @ 02/-E3A7B . Int!o&'ce the $te" $+o(+: $o "$ to he"t') the !eoi+e! :et "oi& ("te! h"e! c"'$e& : !")i&con&en$"tion7e)"n$ion.

3. Coi$$ion the Le"n Aine Coo+e! @ 02/-EA3 "n& the Aine Re#ene!"to!Con&en$e! @ 02/-EA2 .

4. A$ the Aine Re#ene!"to! )!e$$'!e !i$e$, coi$$ion the "ine !e#ene!"to! "ci&#"$ )!e$$'!e cont!o+ @ PIC-/64 to $en& the "ci& #"$ to the "ci& #"$ %+"!e. TheAine Re#ene!"to! Receie! @ 02/-;5 o)e!"tin# )!e$$'!e (i++ e $et

et(een /.48 "n& /.= #7c31.

6. <hen con&en$e& +i*'i& e#in$ "cc''+"tin# in the Aine Re#ene!"to! Receie!, )!e)"!e the Re#ene!"to! Re%+' P')$ @ 02/-P6A7B %o! o)e!"tion. <hen "(o!in# +ee+ i$ ot"ine&, $t"!t the !e%+' )') "n& e#in !e%+'in# "c tothe Re#ene!"to!. Coi$$ion the Aine Re#ene!"to! Receie! +ee+ cont!o+@ LIC-/62 , e!i%: it$ o)e!"tion, "n& )+"ce it on "'to"tic cont!o+.

8. Contin'e inc!e"$in# the he"t in)'t to the Aine Re#ene!"to! Reoi+e! :inc!e"$in# the $te" !"te 'nti+ the &e$i#n !e%+' !"te i$ "chiee&. At thi$ tie,e!i%: th"t the )!o)e! te)e!"t'!e$ h"e een "chiee&Q t:)ic"+ te)e!"t'!e$ "!eo%ten "$ %o++o($

Re#ene!"to! Fee& 00->4 oCReoi+e! ;")o! 22/-232 oC

Re#ene!"to! To) 2/5-225 oC

Re%+' 52 oCLe"n Aine 52 oC

Coi$$ionin# o% Le"n Aine Fi+te!$

2. ;e!i%: th"t the "ine %i+te! e+eent$ (e!e in$t"++e& in the %i+te!$.3. C!"c o)en the %i+te! in+et "n& $+o(+: %i++ (ith +e"n "ine (hi+e entin# "n: #"$

)!e$ent.4. <ith the %i+te!$ +i*'i& %'++, %'++: o)en the in+et "n& o't+et #"te "+e$. A&'$t the

&i%%e!enti"+ )!e$$'!e o! %+o( cont!o++e! to $en& the &e$i#n "o'nt o% "ine$o+'tion th!o'#h the %i+te!$. Do not ecee& the "n'%"ct'!e!$ !ecoen&e&"i' )!e$$'!e &i%%e!enti"+ "c!o$$ thi$ %i+te!$. T:)ic"++:, thi$ "i'

&i%%e!enti"+ i$ 2.8 #7c3.

32




SHEET 44 OF 235

6. Be )!e)"!e& to c+e"n the %i+te!$ *'ite %!e*'ent+: &'!in# the %i!$t o! t(o o% (eeo)e!"tion.

Fin"+ A&'$tent$ o% O)e!"tin# P"!"ete!$2. <ith the "ine t!e"tin# 'nit in %'++ o)e!"tion, inc!e"$e the "ine %+o( !"te to e"ch

"$o!e! to the &e$i#n !"te. Thi$ %+o( !"te (i++ )!o"+: e hi#he! th"nnece$$"!: 't (i++ $oe(h"t o%%$et the +o(e! t!": e%%iciencie$ e)ecte& (hen"$o!e! h:&!oc"!on %ee& !"te$ "!e e+o( &e$i#n.

3. An:tie the "ine ci!c'+"tion !"te i$ "&'$te&, "n "&'$tent o% the $te" !"te tothe Re#ene!"to! Reoi+e! (i++ e !e*'i!e& to ee) the he"t in)'t "n&!e#ene!"tion in the )!o)e! !"n#e. A '$e%'+ e: i$ to "&'$t the $te" in)'t toee) the Re#ene!"to! !e%+' !"te "t " con$t"nt )e!cent"#e o% the tot"+ "ineci!c'+"tion !"te, con$i$tent (ith #oo& !e#ene!"tion, o% co'!$e. T:)ic"++:, thetot"+ $te" !e*'i!eent @ Re#ene!"to! !eoi+e! )+'$ +ie $te" (i++ e in the!"n#e o% 23/ to 26/ # o% $te" )e! c'ic ete! o% "ine $o+'tionci!c'+"te&. .

4. The !ecoen&e& $")+in# "n& "n"+:tic"+ te$tin# $ho'+& e e#'n ie&i"te+: to&ete!ine i% %'!the! )+"nt "&'$tent$ "!e !e*'i!e&.

Spe&ia# pre&a(tion%

Pre&a(tion for entering a &ontaminate' or inert atmo%p.ere

Nit!o#en i$ non-toic. => o+-G o% the "i! (e !e"the i$ nit!o#en, 32 o+-G i$ o:#en.Ho(ee!, in e$$e+$ o! "!e"$ (he!e the!e i$ " hi#h concent!"tion o% nit!o#en, the!e i$"+$o " &e%icienc: o% o:#en %o! !e"thin#. B!e"thin# "n "to$)he!e &e%icient in o:#[email protected]., "n ine!t "to$)he!e (i++ !")i&+: !e$'+t in &iine$$, 'ncon$cio'$ne$$, o! &e"th&e)en&in# on the +en#th o% e)o$'!e. Do not ente! o! een )+"ce :o'! he"& into " e$$e+

(hich h"$ " hi#h concent!"tion o% nit!o#en. Do not $t"n& c+o$e to " "+e (he!enit!o#en i$ ein# ente& %!o e*'i)ent "t " hi#h !"te (hich i#ht te)o!"!i+: c"'$e "&e%icienc: in o:#en c+o$e to the "+e.Re%ine!: )e!$onne+ (ho &o h"e to ente! " cont"in"te& o! ine!t "to$)he!e $ho'+&%o++o( "++ )!e$c!ie& $t"n&"!& $"%et: )!ec"'tion$ "n& !e#'+"tion$ (hich "))+: %o! the!e%ine!:. OSHA !e#'+"tion$ conce!nin# the '$e o% !e$)i!"to!$ @3> CFR S')"!t 2,Section 2>2/,246 $ho'+& e !e"& "n& tho!o'#h+: 'n&e!$too&.It i$ "+$o i)o!t"nt to e)h"$ie th"t i% " )e!$on h"$ ente!e& " e$$e+ "n& ecoe'ncon$cio'$, no in&ii&'"+ $ho'+& #o in to he+) hi (itho't %i!$t )'ttin# on " %!e$h "i!"$, con%i!in# th"t the "i! $'))+: i$ $"%e, &onnin# " $"%et: h"!ne$$, "n& en+i$tin# the"i& o% " ini' o% t(o othe! )eo)+e to !e"in ie&i"te+: o't$i&e o% the e$$e+ to"$$i$t hi. Thi$ ": $ee to e "n oio'$ ("!nin#, 't )eo)+e &o %o!#et thi$ in the

t!"'" o% "n ee!#enc: $it'"tion. O%ten the %i!$t tho'#ht i$ to $"e the )e!$on in&i$t!e$$ "n& )eo)+e ente! the e$$e+ (itho't )!o)e! )!otection on+: to $'cc' to the$"e h""!& (itho't "n:one e+$e ein# )!e$ent to $"e the.

$raining Amine So#(tion

D'!in# no!"+ o)e!"tion, hot "ine $o+'tion "oe 5/ '$t not e &!"ine& to the℃

c+o$e& "ine !ecoe!:. I% &o $o, the 'n&e!#!o'n& )i)e i#ht e !oen &'e to the!"+e)"n$ion.



Norma# Start4(p < S.(t'on

Norma# %tart4(p after pro#onge' %.(t'on

The )!oce&'!e '$e& %o! $t"!tin# ') the Aine T!e"tin# Section "%te! "n: $h't&o(n i$i&entic"+ to the )!oce&'!e '$e& %o! initi"+ $t"!t-'). Fo++o( Section 8.3 @ Det"i+e& $te)-

:-$te) )!oce&'!e o% thi$ "n'"+ %o! !e$t"!tin# o% the Aine T!e"tin# Section.

Norma# operation pro&e'(re after %.ort %.(t'on

It i$ "$$'e& th"t the %o++o(in# con&ition$ "!e "int"ine&

• No!"+ +ee+ o% "ine $o+'tion i$ e)t %o! e"ch "$o!e! "n& the Aine

Re#ene!"to!

• A )o$itie )!e$$'!e i$ e)t in e"ch "$o!e! : e"n$ o% %ee& %+'i& o! %'e+ #"$ o!

nit!o#en.

• A++ )')$ h"e een $to))e&.The 'nit c"n e coi$$ione&, $t"!tin# %!o Coi$$ionin# o% Re#ene!"to! Reoi+e!o% the $te) : $te) )!oce&'!e$ #ien in $ection 8.3.

Norma# Operation

Pro'(&t /(a#it) monitoring

The "o! conce!n in "ine t!e"te& $t!e"$ i$ the *'"ntit: o% H 3S in the t!e"te& )!o&'ct"n& the e%%ectiene$$ (ith (hich the "$o!e! i$ !eoin# H3S.Fo! thi$ !e"$on, !e#'+"! "n"+:$i$ i$ no!"++: "&e on+: %o! H3S. The !ecoen&e&etho&$ %o! &"i+: "n"+:$i$ o% "))!o)!i"te $t!e"$ "!e +i$te& e+o(.

St!e" L" Metho& An"+:$i$A$o!e! %ee& UOP > H3S

UOP 323 H3S, RSH, COST!e"te& )!o&'ct UOP 323 H3S, RSH, COS

It i$ "+$o '$e%'+ to h"e " %ee& co)o$ition "n"+:$i$ %o! !e%e!ence i% "n ')$et occ'!$.The!e%o!e, " 1LC "n"+:$i$ o% e"ch "$o!e! %ee& i$ "+$o !e*'i!e& on " &"i+: "$i$.

Operation Con'ition% Monitoring

In o!&e! to "int"in #oo& H3S !eo"+, the "ine concent!"tion, H3S content, "n&

i$'"+ "))e"!"nce o% the +e"n "ine '$t e contin'o'$+: onito!e&. It i$ "+$oi)o!t"nt to onito! the o+e !"tio o% "ci& #"$ to "ine, o! "ci& #"$ +o"&in#, o% the !ich"ine $o+'tion %!o e"ch "$o!e!. <hen thi$ o+ !"tio ecee&$ "o't /.8 o! /.5, the"ine $o+'tion ecoe$ inc!e"$in#+: co!!o$ie to("!& c"!on $tee+ )i)in#, )"!tic'+"!+:"t e+e"te& te)e!"t'!e$. It i$ &e$i!"+e to ee) the o+ !"tio o% "ci& #"$ to "ine in the!ich "ine e+o( /.6 : inc!e"$in# the "ine ci!c'+"tion !"te to e"ch "$o!e! 'nti+ thi$!"tio i$ "tt"ine&.The !ecoen&e& "n"+:tic"+ etho&$ %o! $i)+e onito!in# o% the$e $t!e"$ "!e +i$te&

e+o(St!e" L" Metho& An"+:$i$

Le"n Aine UOP 036 o! 038 F!ee AineUOP 03= A))"!ent H3S

Rich Aine UOP 03= A))"!ent H3S

34




SHEET 48 OF 235

The "))"!ent H3S content o% the "ine $o+'tion i$ #ene!"++: !e)o!te& in #!"in$@ "!ei"te& #! o% H3S )e! #"++on o% "ine $o+'tion. Thi$ "+'e i$ cone!te& to theo+e !"tio o% H3S to "ine : the %o++o(in# e)!e$$ion$

@ H3S, #! 7 #"+ @ 8.4 2/-4 7 DEA, (tG o+e !"tio

Ro(tine operation

Tro(*#e %.ooting

The!e h"e een "n: )")e!$ )'+i$he& on the $'ect o% "n"+:tic"+ cont!o+ o% "ine$o+'tion. So)hi$tic"te& )!oce&'!e$ h"e een )'+i$he& to "n"+:e "n& oe!coech!onic )!o+e$. It i$ e:on& the $co)e o% the$e o)e!"tin# in$t!'ction$ to !e)!o&'cetho$e )")e!$, 't thei! ei$tence $ho'+& e entione& %o! tho$e (ho $ee "&&ition"+in%o!"tion. The %o++o(in# ite$ "!e %'!ni$he& "$ " #'i&e %o! "$$i$t"nce (hen !o'tine"n"+:tic"+ te$t$ inten&e& %o! onito!in# )+"nt )e!%o!"nce $ee con%'$in# o!incon$i$tent.

Tot"+ AineThe UOP te$t etho&$ 036 "n& 038, !e%e!!e& to )!eio'$+: in the O)e!"tion$Monito!in# &i$c'$$ion, ention %!ee "ine.The$e etho&$ e!e+: tit!"te "++ "$ic co)o'n&$ )!e$ent in " $")+e (ith $t"n&"!&ie&"ci& to the eth:+ !e& in&ic"to! en&)oint "n& c"++ the %!ee "ine : c"+c'+"tin# the"$ i% the: (e!e "++ "ineQ thi$ i$ *'ite $'it"+e %o! !o'tine cont!o+ )'!)o$e$, %o! e")+ethe nee& %o! ("te! "e-'), 't i$ cheic"++: inco!!ect, ece)t %o! %!e$h $o+'tion$.Pe!io&ic"++:, the!e%o!e, the +e"n "ine $ho'+& e chece& %o! tot"+ "ine : UOPMetho& 030 "n& %!ee "ine : UOP 036 o! 038 i$ "n in&ic"tion o% the )!e$ence o%

"ine &e#!"&"tion )!o&'ct$.A$ "n initi"+ #o"+ "n& 'nti+ )+"nt o)e!"tion &ict"te$ othe!(i$e, &o not +et the tot"+"ine content to ecee& the %!ee "ine content : o!e th"n 3 (tG.. Thi$ i$cont!o++e& : )"!ti"+ )'!#in# "n& )"!ti"+ !e)+"ceent o% the )+"nt inento!: (ith %!e$h3/ (tG DEA $o+'tion.

Thio$'+%"teO:#en ente!in# the "ine $:$te in "n: "nne! *'ic+: !e"ct$ (ith "ine-h:&!o$'+%i&e to %o! "ine-thio$'+%"te. Un+ie "ine-h:&!o$'+%i&e, "ine thio$'+%"te i$he"t-$t"+e 'n&e! Re#ene!"to! con&ition$ "n& (i++ #!"&'"++: inc!e"$e in concent!"tion'n+e$$ !eoe& : )'!#in#.Thio$'+%"te (i++ !e"ct (ith io&ine in the te$t to "))"!ent H3S, UOP 03=, "n& e inc+'&e&

"$ H3S in the c"+c'+"tion. The!e%o!e, thio$'+%"te $ho'+& e &ete!ine& (ee+: : the"n"+:tic"+ te$t etho& UOP 020 to "e ce!t"in th"t "n: hi#h "))"!ent H3Sconcent!"tion in the +e"n "ine i$ not thio$'+%"te.Thio$'+%"te concent!"tion $ho'+& e e)t +o( "n& $ho'+& not ecee& 8/ #!"in$7#"++on(hen c"+c'+"te& "$ "))"!ent H3S.

A))"!ent H3SA$ '$t &i$c'$$e&, UOP Metho& 03= %o! "))"!ent H3S &oe$ not &i$c!iin"te et(eent!'e H3S "n& thio$'+%"teQ oth "!e inc+'&e& in the "n"+:$i$. Hi#h "+'e$ o% "))"!ent H3Sin the +e"n "ine co'+& e (!on#+: inte!)!ete& "$ )oo! Re#ene!"to! )e!%o!"nce (hen,in %"ct, thio$'+%"te o! othe! co)o'n&$ "!e "t %"'+t. Fo! e")+e, $o&i' $'+%i&e,

)!e$ent ec"'$e o% c"'$tic cont"in"tion, i$ "+$o tit!"te& "$ "))"!ent H3S. The!e i$ "



$i)+e te$t th"t c"n *'ic+: &ete!ine i% in"&e*'"te Re#ene!"to! )e!%o!"nce o! othe!co)o'n&$ "!e the c"$e o% the hi#h "))"!ent H3S.Dete!ine the "))"!ent H3S content in " )o!tion o% " +e"n "ine $")+e '$in# UOP03=. A&& 2// + o% the $"e +e"n "ine $")+e to " 8// + %+"$, "&& 2// + o%&i$ti++e& ("te!, &!o) in " %e( oi+in# $tone$, "n& oi+ the $")+e oe! " hot )+"te in "+"o!"to!: %'e hoo& 'nti+ the o+'e o% $")+e i$ !e&'ce to 2// +. Reoe the 8//+ %+"$ %!o the hot )+"te, "&& &i$ti++e& ("te! i% nece$$"!: to !econ$tit'te the o!i#in"+$")+e o+'e, coo+, "n& "#"in &ete!ine the "))"!ent H3S content o% the !e$'+t"nt$")+e : UOP 03=. I% the $")+e "%te! oi+in# no( in&ic"te$ " 'ch +o(e!concent!"tion o% "))"!ent H3S, in"&e*'"te $t!i))in# in the )+"nt Re#ene!"to! ": e "

)!o+eQ inc!e"$e the !eoi+e! $te" !"te. I%, ho(ee!, the "))"!ent H3S concent!"tionh"$ not #!e"t+: &iini$he&, the "ine $o+'tion i$ )!o"+: cont"in"te& (iththio$'+%"te, $o&i' $'+%i&e, o! $oe othe! "te!i"+ (hich tit!"te$ "$ "))"!ent H3S."&&ition"+ +"o!"to!: (o! c"n )in)oint the )!o+e.

Fo"in#Fo"in# in the Re#ene!"to! o! #"$ "$o!e! "n& e'+$i%ic"tion o% "ine "n&h:&!oc"!on in the +i*'i&7+i*'i& "$o!e! "!e $oetie$ )!o+e$. The$e )!o+e$ c"n

e +"!#e+: "oi&e& : #oo& *'"+it: cont!o+ o% the "ine $o+'tion to ee) "ine "n& "ci&#"$ concent!"tion$ in the )!o)e! !"n#e "n& : #oo& %i+t!"tion $:$te "inten"nce $oth"t the "ine $o+'tion i$ "+(":$ c+e"! "n& i$i+: %!ee o% )"!tic'+"te "tte! (hen "#!" $")+e i$ ie(e& in &i!ect +i#ht. 1oo& )+"nt "inten"nce to *'ic+: !eoe "n:+i*'i& h:&!oc"!on "cc''+"tion %!o noco't )ot$ "n& "$o!e! $i +ine$ "!ee$$enti"+. I% %o"in# o! e'+$i%ic"tion occ'!$ &e$)ite the$e )!ec"'tion$, '&icio'$ '$eo% $i+icon "nti%o" "#ent$ (i++ '$'"++: e+iin"te the )!o+e.The $i)+e %o" te$t c"n e o% ene%it (hen '$e& !o'tine+: to onito! )+"nt $o+'tion$%o! %o"in# ten&enc:, )"!tic'+"!+: t"in# note o% "n: ch"n#e$, "n& i% '$e& to

)!e&ete!ine ini' "nti%o" inection !"te$, $ho'+& " )+"nt %o"in# )!o+e

&ee+o).The!e "!e e%%ectie "nti%o" "#ent$ %o! inection into the "ine $o+'tion to $'))!e$$%o"in#. Hi#h oi+in# "+coho+$ $'ch "$ o+e:+ "+coho+ h"e een '$e& "$ "nti%o""#ent$. C'!!ent )!"ctice %"o!$ the '$e o% the hi#h+: e%%ectie "n& e"$i+: h"n&+e&$i+icone "nti%o" "#ent$, $'ch "$ Do( Anti%o" A.Anti%o" "#ent$ $ho'+& not e inecte& 'n+e$$ %o"in# e)e!ience in the )+"nt in&ic"te$thei! nee&. <hen nee&e&, on+: " %e( )"!t$ )e! i++ion, '$'"++: +e$$ th"n 2/ )"!t$ :(ei#ht o% the $i+icone co)o'n& )e! i++ion )"!t$ : (ei#ht o% )+"nt "ine $o+'tion,(i++ e%%ectie+: $'))!e$$ %o"in#.In the c"$e o% #"$ t!e"tent, the $i+icone$ c"nnot e$c")e the 'nitQ th'$, contin'o'$"&&ition i$ not !e*'i!e&. Anti%o" "#ent$ "))+ie& in&i$c!iin"te+: (hen )+"nt o)e!"tion&oe$ not !e*'i!e the c"n "ct'"++: )!oote %o"in# "n& +e"& to o)e!"tin# &i%%ic'+tie$.

Mi%&e##aneo(% pro&e'(re%

Fi+te! o)e!"tionTo "int"in the &i%%e!enti"+ )!e$$'!e "c!o$$ the enti!e %i+te!in# $:$te@ " $e!ie$ o%ech"nic"+ %i+te!, c"!on %i+te! "n& $oc %i+te! %!o ecee&in# o! %"i+in# e+o( 2.8#7c3, PD;-/26 i$ o)ene& o! c+o$e&. The %i+te!$ "!e %o! $+i)-$t!e" %+o( "n& )"$$(h"tee! %+o( i$ )o$$i+e (ith " 2.8 #7c3 &i%%e!enti"+.The &e$i#n %+o( i$ 32 47h, 't (hen the c"!t!i&#e$ "!e c+e"n, o!e %+o( (i++ )"$$th!o'#h the %i+te!$.<hen the %+o( th!o'#h the %i+te!$ &!o)$ to 2> 47h,"t " &i%%e!enti"+ )!e$$'!e o% 2.8#7c3, the %i+te!$ $ho'+& e ch"n#e& oe! "n& c+e"ne&.

36




SHEET 4= OF 235

Anti%o" inectionAnti%o" "#ent $ho'+& e inecte& i% %o"in# e)e!ience in the )+"nt in&ic"te$ it$ nee&.Contin'o'$ "&&ition i$ not !e*'i!e&.Inection Point$

• Rich "ine +ine ')$t!e" o% Rich-Le"n Aine Ech"n#e!@02/-E4 %o! Aine

Re#ene!"to!@02/-;8

• Le"n Aine +ine ')$t!e" o% Le"n Aine T!i Coo+e!@02/-E> %o! F'e+ 1"$

Aine A$o!e!@02/-;3

Siin# o)e!"tionTo "oi& %o"in# t!o'+e$ it i$ i)o!t"nt to !eoe +i*'i& h:&!oc"!on "cc''+"tion inF'e+ 1"$ Aine A$o!e!@02/-;3.Monito! L1-T //4 )e!io&ic"++:. An& &i$ch"!#e +i*'i& h:&!oc"!on$ to F'e+ 1"$A$o!e! Inte!%"ce Pot@02/-;>

Ro(tine &ontro# te%t% to *e performe' *) operator%

Re%e! to $ection 22.=.

Genera# oera## %.(t'on p#an

No!"+ $h't&o(n con$i$t$ o% the %o++o(in# $e*'enti"+ "ctiitie$2. C'ttin# o%% %ee& $t!e"$3. Re#ene!"tion o% "ine $o+'tion4. Recoe!: o% the !e#ene!"te& "ine $o+'tion6. <"te! ci!c'+"tion

$etai#e' %tep4*)4%tep %.(t'on pro&e'(re

2. Th!ott+e the %ee& %+o( !"te$ to e"ch "$o!e! &o(n to 8/ G +o"&. An& "+$o th!ott+e+e"n "ine %+o( !"te$ to e"ch "$o!e! &o(n to 5/G o% &e$i#n.

3. Coi$$ion +e"n "ine :)"$$ +ine to 02/-;6 to "int"in "ine $o+'tionci!c'+"tion "%te! $h'ttin# &o(n e"ch "$o!e!..

4. Die!t the "ci& #"$ &i$ch"!#e to "ci& #"$ %+"!e.6. B+oc in %ee& $t!e" to e"ch "$o!e!. An& "int"in eno'#h )!e$$'!e in e"ch

"$o!e! to %o!ce !ich "ine to the Rich Aine F+"$h D!'@ 02/-;6.8. Sto) the +e"n "ine $'))+: to e"ch "$o!e!.5. M"int"inin# "t +e"$t one ci!c'+"tion.=. Sto) the $te" in)'t to the Aine Re#ene!"to! Reoi+e!$@02/-E3A7B.0. O)en the :)"$$ o% F;-/4> to )') "$ 'ch +i*'i& "$ )o$$i+e to the Aine

Re#ene!"to!@02/-;8 "n& then $h't &o(n the Aine Re#ene!"to! Re%+'P')$@02/-P6A7B . Sh't &o(n the Aine Re#ene!"to! Con&en$e!@ 02/-EA2 "$ (e++.

>. <hen ci!c'+"tin# "ine $o+'tion h"$ coo+e& to 88 to 5/ , t!"n$%e! +e"n "ine to℃

Aine Sto!"#e T"n@02/-TK3 : '$in# "ine )')o't +ine.2/. Sh't-&o(n the "ine ci!c'+"tin# +oo)@ Rich Aine P')$@02/-P3A7B, Le"n

Aine P')$@02/-P4A7B "n& Le"n Aine Coo+e!@02/-EA-3.22. D!"in o't !e"inin# "ine in "++ e*'i)ent "n& )i)in#23. Con&'ct ("te! ci!c'+"tion o% oe!"++ "ine ci!c'+"tin# +oo) to ("$h o't !e"inin#

"ine in$i&e the $:$te.24. Ste" o't "++ e$$e+$ "n& &!'$ %o! in$)ection.



,#aning off

Ee!: +ine connectin# to " no+e on the e$$e+ to e ente!e& '$t e +in&e& o%% "t thee$$e+. Thi$ inc+'&e$ &!"in$ connectin# to " c+o$e& $e(e!, 'ti+it: connection$ "n& "++

)!oce$$ +ine$. In$t"++ "&&ition"+ +in&$ "t the "tte!: +iit$ "$ nece$$"!: %o! $"%et:. The+oc"tion o% e"ch +in& $ho'+& e "!e& on " "$te! )i)in# "n& in$t!'ent"tion&i"#!"$ @P?ID$, e"ch +in& $ho'+& e t"##e& (ith " n'e! "n& " +i$t o% "++ +in&$"n& thei! +oc"tion$ $ho'+& e "int"ine&. One )e!$on $ho'+& e #ien !e$)on$ii+it: %o! the "++ +in&$ in the 'nit to "oi& e!!o!$.

Opening e/(ipment

The "!e" "!o'n& the e$$e+ "n(":$ $ho'+& "+$o e $'!e:e& %o! )o$$i+e $o'!ce$ o%&"n#e!o'$ #"$e$ (hich i#ht ente! the e$$e+ (hi+e the )e!$on i$ in$i&e. E")+e$inc+'&e "cet:+ene c:+in&e!$ %o! (e+&in# "n& )!oce$$ ent o! &!"in connection$ in the$"e o! "&oinin# 'nit$. An: h""!&$ %o'n& in the $'!e: $ho'+& e i$o+"te& o!!eoe&.S"%e "cce$$ '$t e )!oi&e& oth to the ete!io! "n& inte!io! o% the e$$e+ to eente!e&. The ete!io! "cce$$ $ho'+& e " $o+i&, )e!"nent +"&&e! "n& )+"t%o! o!$c"%%o+&in# $t!on# eno'#h to $'))o!t the )eo)+e "n& e*'i)ent (ho (i++ e ino+e& inthe (o! to e )e!%o!e&.Acce$$ to the inte!io! $ho'+& "+$o e $t!on# "n& $o+i&. Sc"%%o+&in# i$ )!e%e!!e& (hen thee$$e+ i$ +"!#e eno'#h to )e!it it to e '$e&. The $c"%%o+&in# "$e $ho'+& !e$t %i!+:on the otto o% the e$$e+ "n& e $o+i&+: "ncho!e&. I% the $c"%%o+&in# i$ t"++, the$c"%%o+&in# $ho'+& e $'))o!te& in $ee!"+ )+"ce$ to )!eent $(":. The )+"t%o! o"!&$$ho'+& e $t'!&: "n& c")"+e o% $'))o!tin# $ee!"+ )eo)+e "n& e*'i)ent "t the $"etie "n& "+$o e %i!+: %"$tene& &o(n. R'n#$ $ho'+& e )!oi&e& on the $c"%%o+&in#$)"ce& "t " co%o!t"+e &i$t"nce %o! c+iin# on the $t!'ct'!e.

I% $c"%%o+&in# (i++ not %it in the e$$e+, " +"&&e! c"n e '$e&. A !i#i& +"&&e! i$ "+(":$ )!e%e!!e& oe! " !o)e +"&&e! "n& i$ e$$enti"+ to "oi& %"ti#'e &'!in# +en#th: )e!io&$ o%(o! in$i&e " e$$e+. The otto "n& to) o% the +"&&e! $ho'+& e $o+i&+: "ncho!e&. I%"&&ition"+ $'))o!t i$ ""i+"+e, then the +"&&e! $ho'+& "+$o e "ncho!e& "t inte!e&i"te+oc"tion$. <hen )o$$i+e, " $o+i& $'))o!t $ho'+& )"$$ th!o'#h the +"&&e! 'n&e! " !'n#,the!e: )!oi&in# $'))o!t %o! the enti!e (ei#ht $ho'+& the otto $'))o!t %"i+. On+:one )e!$on "t " tie $ho'+& e "++o(e& on the +"&&e!.<hen " !o)e +"&&e! i$ '$e&, the !o)e$ $ho'+& e tho!o'#h+: in$)ecte& )!io! to e"ch ne(

o. A++ !'n#$ $ho'+& e te$te& %o! $t!en#th, (hethe! the: e "&e o% et"+ o! (oo&.E"ch !o)e '$t e in&ii&'"++: $ec'!e& to "n io"+e $'))o!t. I% )o$$i+e, " $o+i&$'))o!t $ho'+& )"$$ th!o'#h the +"&&e! $o th"t " !'n# c"n he+) $'))o!t the (ei#ht "n&the otto o% the +"&&e! $ho'+& e %"$tene& to " $'))o!t to )!eent the +"&&e! %!o

$(in#in#. A$ (ith the !i#i& +"&&e!, on+: one )e!$on $ho'+& c+i the +"&&e! "t " tie.A+$o !e%e! to Section 2/.23 Ente!in# t"n$, &!'$ o! othe! e$$e+$.

Spe&ia# pre&a(tion%

<hen &!"inin# o't the "ine $o+'tion %!o the Aine Re#ene!"to!, "e $'!e th"t the"ine $o+'tion in it h"$ "+!e"&: coo+e& &o(n to 5/ . Then o)en the &!"in "+e %o!℃

the c+o$e& "ine !ecoe!:.Othe!(i$e, the 'n&e!#!o'n& )i)e i#ht e !oen &'e to the!"+ e)"n$ion.

38




SHEET 4> OF 235

Emergen&) S.(t'on

Genera# in%tr(&tion%

Ee!#enc: $h't&o(n, c")"cit: !e&'ction, o! o&i%ie& o)e!"tion o% the Aine T!e"tin#Section c"n !e$'+t %!o "n: o% the %o++o(in# c"'$e$

• Lo$$ o% Uti+itie$ - +o$$ o% +o( )!e$$'!e $te", coo+in# ("te!, e+ect!ic"+ )o(e!, o!

in$t!'ent$ "i!.

• E*'i)ent %"i+'!e o% $oe e*'i)ent ite$ the )+"nt !e*'i!e )+"nt $h't&o(n o!

c")"cit: !e&'ction.

• Lo$$ o% Fee&

• Fi!e "n& othe! Ee!#encie$

• Lo$$ o% )') ete!n"+ %+'$hin# %+'i&

The etent to (hich the )+"nt (i++ h"e to e $h't &o(n &e)en&$ on the $)eci%icee!#enc:. In "n: ee!#enc:, &ete!ine the etent o% the ee!#enc: con&ition, "n&

&eci&e ho( to co)e (ith it. Then )!ocee& (ith one o% the %o++o(in# "ction$ "$ ("!!"nte& : the ee!#enc:

H"n&+e the ee!#enc: "$ " +oc"+ie& con&ition (itho't $h'ttin# &o(n the !e$t o%the )+"nt. Fo! e")+e, in the c"$e o% " %"'+t: cont!o+ "+e. B+oc in "n& :)"$$the "+%'nctionin# ite 'nti+ !e)"i!$ c"n e "&e.OR Sh't &o(n the 'nit '$in# the no!"+ $h't&o(n )!oce&'!e &e$c!ie& in Section 5.3.OR Sh't &o(n the 'nit '$in# the ee!#enc: )!oce&'!e$ #ien e+o( %o! " $)eci%icee!#enc:. In eec'tin# ee!#enc: $h't&o(n $te)$, the no!"+ $h't&o(n

)!oce&'!e &et"i+e& in Section 5.3 $ho'+& e %o++o(e& "$ c+o$e+: "$ )o$$i+e.

Fire

Con$e*'enceI% " %i!e occ'!$ in the )+"nt, th"t $ection o% e*'i)ent in (hich the %i!e h"$ occ'!!e&'$t e i$o+"te& to con%ine %i!e "n& &e)!e$$'!e& to e+iin"te the $o'!ce o% co'$ti+e"te!i"+. Un+e$$ the %i!e i$ $"++ "n& c"n e h"n&+e& *'ic+: the )+"nt (i++ $h't&o(n.O)e!"tin# $')e!i$o! on &'t: (i++ "&i$e on $h't&o(n, "$e& on !e%ine!: )!oce&'!e$ in

)+"ce.

Action$Fo++o( o)e!"tion $')e!i$o!$ o!&e!$ on $h't&o(n "n& %i!e%i#htin# )!oce&'!e$.I% )+"nt '$t e $h't&o(n

• Reoe "++ he"t in)'t to the )+"nt.• B+oc in %ee&$ "n& )!o&'ct $t!e"$.

• I$o+"te $ection o! "!e" (he!e %i!e i$ occ'!!in#, to !eoe co'$tion $o'!ce.

• De)!e$$'!e "!io'$ co+'n$ "n& e$$e+$ to %+"!e.

• Sh't&o(n !e"inin# )o!tion$ o% )+"nt "$ tie "n& ci!c'$t"nce$ )e!it o! !e*'i!e.

Poer fai#(re

<hen "n& e+ect!ic"+ )o(e! %"i+'!e occ'!$, the Aine T!e"tin# Section (i++ e $h't&o(n. The )+"nt i$ &e$i#ne& to %"i+ $"%e (hen +o$$ o% )o(e! occ'!$,. A t!'e ee!#enc:ei$t$ (hen "n e+ect!ic"+ )o(e! %"i+'!e occ'!$.

Con$e*'ence



The )+"nt (i++ h"e to e $h't &o(n. Fee& (i++ e +o$t , !e%+' to co+'n$ (i++ e +o$t,"n& te)e!"t'!e$ "n& )!e$$'!e$ in co+'n$ (i++ !i$e.

Action$

λ M"e $'!e "++ )')$ "!e &o(n @"++ e+ect!ic &!ien.

λ B+oc in "n'"++: $te" in+et "+e$ to the !eoi+e! "n& +oc in o't+et "+e$.

λ B+oc in "++ %ee& "n& )!o&'ct $t!e"$ in the )+"nt.

λ B+oc in "++ )')$.

λ Fo++o( the )!ece&in# "ction (ith "n o!&e!+: $h't&o(n '$in# the no!"+ $h't&o(n

)!oce&'!e$ &e$c!ie& in Section 5.3.C"'tionM"int"in " )o$itie )!e$$'!e in the !e#ene!"to! "$ it coo+$ : '$in# nit!o#en.

In%tr(ment Air fai#(re

A t!'e ee!#enc: ei$t$ (hen in$t!'ent "i! i$ +o$t.

Con$e*'ence<hen "n in$t!'ent "i! %"i+'!e occ'!$ the )+"nt (i++ $h't&o(n. The )+"nt i$ &e$i#ne& to%"i+ $"%e (hen in$t!'ent$ "i! i$ +o$t.

Action$

• B+oc %ee& in+et "+e "t "tte!: +iit$.

• Fo++o( the )!ece&in# "ction (ith "n o!&e!+: $h't&o(n '$in# the no!"+ $h't&o(n

)!oce&'!e &e$c!ie& in Section 5.3.

• M"int"in " )o$itie )!e$$'!e on the )+"nt "$ it coo+$ : '$in# nit!o#en. Do not +et

the !e#ene!"to! #o 'n&e! " "c''.

LP Steam fai#(re

A t!'e ee!#enc: ei$t$ (hen $te" i$ +o$t.Con$e*'enceI% +o( )!e$$'!e $te" i$ +o$t, "ine $t!i))in# $te" "n& he"tin# $te" to the !eoi+e!$(i++ e +o$t. The!e%o!e )+"nt (i++ e $h't &o(n.

Action$P!ocee& (ith " no!"+ $h't&o(n (hen the ee!#enc: $te)$ "!e co)+ete.

!ater fai#(re

Co#' Con'en%ate fai#(re

Con&en$"te i$ '$e& inte!ittent+: in thi$ 'nit, the!e%o!e, the!e i$ no $e!io'$ con$e*'ence%o!e$een (hen it %"i+$. Ho(ee!, " con&en$"te %"i+'!e (hen it i$ !e*'i!e& (i++ h"e "ne%%ect on the "ine &i+'tion o)e!"tion o% the 'nit..

Coo#ing !ater fai#(re

<hen " coo+in# ("te! %"i+'!e occ'!$, the )+"nt o)e!"tion con&ition$ '$t e "&'$te&.Con$e*'ence$

40




SHEET 62 OF 235

Coo+in# %o! +e"n "ine coo+e!$ (i++ e +o$t !e$'+tin# in " $+i#ht inc!e"$e in +e"n "inete)e!"t'!e to the "$o!e!.P') coo+in# (i++ e +o$t. Action$

• Monito! the H3S content in the t!e"te& $t!e"$.

• Monito! the !e+e"nt )')$. I% "n: )') h"$ to e $h't &o(n, (ho+e $ection (i++

e $h't &o(n.

Fee'%to& fai#(re

Con$e*'enceI% %ee& i$ +o$t ec"'$e o% " )o(e! %"i+'!e, the )+"nt '$t e $h't &o(n "$ o't+ine& 'n&e!E+ect!ic"+ F"i+'!e. I% +o$t ec"'$e o% %ee&$toc %"i+'!e then " 'nit $h't &o(n co'+&h"))en.

Action<hen +o$$ o% %ee& occ'!$, the %o++o(in# "ction $ho'+& e t"en

• M"int"in )+"nt in hot $t"n&: o&e 'nti+ %ee& i$ ""i+"+e.

• <hen %ee& i$ ""i+"+e, )!ocee& (ith the )+"nt $t"!t-') "$ &i$c'$$e& in Section 5.5.

• I% %ee& i$ +o$t %o! " +on# tie )e!io&, %o++o( ee!#enc: $te)$ (ith "n& o!&e!+:

$h't&o(n '$in# the no!"+ $h't&o(n )!oce&'!e &e$c!ie& in Section 5.3.

E/(ipment fai#(re

Con$e*'enceA "o! e*'i)ent %"i+'!e (i++ $h't &o(n the 'nit %o! !e)"i!$.

ActionUn&e! thi$ ee!#enc: con&ition, ie&i"te+: initi"te the %o++o(in# )!oce&'!e

• P!ocee& (ith " no!"+ $h't&o(n (hen the ee!#enc: $te)$ "!e co)+ete.

• H"e "inten"nce +in& the ino+e& e*'i)ent %o++o(in# the no!"+ +in&in#

)!oce&'!e.

• A("it in$t!'ction$ %!o o)e!"tin# $')e!i$o!.



Ma=or E/(ipment < it% Seri&e

S(mmar) ta*#e%

Re%e! to Att"chent 0.2 @ E*'i)ent Li$t o% Aine T!e"tin# P!oce$$ Unit, Doc. No. S-02/-2336-2/2 .

Toer %(mmar)

F(e# Ga% Amine A*%or*er > 810452 ?

Thi$ "$o!e! i$ '$'"++: " "+e o! $iee t!": co+'n. Le"n "ine $o+'tion ente!$ i" "&i$t!i'to! ne"! the to) o% the co+'n, %+o($ "c!o$$ e"ch t!":, "n& eit$ "$ !ich "ine%!o the otto "ine !e$e!oi! on +ee+ cont!o+. Fee& #"$ %i!$t )"$$e$ th!o'#h "noco't &!' %'!ni$he& (ith " &ei$te! )"& to !eoe ent!"ine& +i*'i& i$t, +i*'i&, o! con&en$"te )!io! to ente!in# the "$o!e!. The %ee& #"$ ente!$ th!o'#h "n in+et&i$t!i'to! +oc"te& ie&i"te+: e+o( the otto t!":. H3S in the #"$ i$ !eoe& "$ the#"$ )"$$e$ ')("!& th!o'#h the t!": o)enin#$ "n& '+e$ th!o'#h the "ine $o+'tion one"ch t!":. The t!e"te& #"$ )"$$e$ th!o'#h " i$t e+iin"to! "n& eit$ %!o the "$o!e!to), on )!e$$'!e cont!o+. A $iin# no+e i$ )!oi&e& in the ("++ o% the otto "ine!e$e!oi! to )e!it !eo"+ o% +i*'i& h:&!oc"!on (hich i#ht co++ect on the "ine$'!%"ce.

Amine Regenerator > 81045 ?

Thi$ co+'n i$ %itte& (ith "+e t!":$. Rich "ine ente!$ ne"! the to) $i&e o% the co+'nth!o'#h "n "ine %ee& &i$t!i'to! +oc"te& e+o( the to) t!":, th!ee t!":$ &o(n %!o theto) t!":. The t!":$ "!e the conention"+ t:)e (ith the t:)ic"+ "!!"n#eent o% (ei!$ "n&

cho!&"+ &o(ncoe!$.The otto t!": i$ " +i*'i&-ti#ht "cc''+"to! t!": (ith " cente! )i)e %o! "$cen&in#")o! "n& " &!"(-o%% (e++ &i!ectin# "++ &e$cen&in# +i*'i& to the $te" he"te& !eoi+e!.He"t in)'t to the !eoi+e! i$ cont!o++e& eithe! : %+o( cont!o+ o% the $te" con&en$"te!eoe& %!o the t'e$i&e o% thi$ ech"n#e!. A 22/-23/ oC !eoi+e! o't+et te)e!"t'!ei$ t:)ic"+ %o! " 3/ (tG "ine $:$te "t /.= #7c31.A ete!e& +ie $te" connection i$ )!oi&e& into the !eoi+e! o't+et +ine. Ste" i$inecte& "t thi$ )oint to co)en$"te ("te! +o$t (ith the "ci& #"$ %!o the oe!he"&$:$te "n& the!e: "&'$t the "ine concent!"tion.

$r(m %(mmar)

F(e# Ga% Amine A*%or*er @no&o(t $r(m > 810451 ? The F'e+ 1"$ Knoco't D!' i$ " e!tic"+ e$$e+ @ "&e o% KCS %'!ni$he& (ith "&ei$te! )"& to $e)"!"te ent!"ine& +i*'i& i$t, +i*'i& h:&!oc"!on, o! con&en$"te %!othe o%%-#"$ $t!e" )!io! to ente!in# the "$o!e!. The %ee& #"$ ente!$ th!o'#h "n in+et&i$t!i'to! +oc"te& +e$$ th"n " ete! e+o( the &ei$te! o% the e$$e+. The %ee& #"$

)"$$e$ th!o'#h the i$t e+iin"to! "n& eit$ %!o the e$$e+ to) to the "$o!e!. The"cc''+"te& h:&!oc"!on +i*'i& i$ &!"ine& inte!ittent+: to the "ci& #"$ %+"!e.

Ri&. Amine F#a%. $r(m > 81045" ?

The Rich Aine F+"$h D!' i$ " ho!iont"+ $ett+e! e$$e+ (ith " $"++ &i$en#"#in#

$t"c on the to). The coine& !ich "ine $t!e" %!o the ')$t!e" 'nit$ %+o($ to the

42




SHEET 64 OF 235

Rich Aine F+"$h D!' (he!e "n: +i*'i& h:&!oc"!on i$ $e)"!"te& %!o the !ich"ine.An in+et &i$t!i'to! i$ )!oi&e& to "oi& ece$$ in+et t'!'+ence "n& )!oote "n een%+o( &i$t!i'tion th!o'#h the e$$e+. It con$i$t$ o% " $in#+e )i)e "!!"n#e& e!tic"++:th!o'#h ne"!+: the %'++ (i&th o% the e$$e+ &i"ete! (ith one %'++ +en#th $+ot %"cin# thene"!e$t e$$e+ )"!tition.Li*'i& h:&!oc"!on i$ $e)"!"te& into " !e$e!oi! in the e$$e+ "n& c"n e )e!io&ic"++:

)')e& to the Li#ht S+o) Oi+ T"n.H:&!oc"!on ")o! $e)"!"te& in the Rich Aine F+"$h D!', (hich cont"in H3S, i$$c!'e& (ith " $"++ +e"n "ine $+i)$t!e" in the $t"c )o!tion. The $t"c i$ )"ce&(ith 38 &i"ete! c"!on R"$chi# !in#$ %o! cont"ct "n& the +e"n "ine ente!$th!o'#h " &i$t!i'to! +oc"te& "t the to) en& o% the $t"c.Rich "ine %!o the otto o% the Rich Aine %+"$h D!' i$ )')e& to the AineRe#ene!"to! %o! !e#ene!"tion.

Amine Regenerator Re&eier > 81045 ?

The Aine Re#ene!"to! Receie! i$ " e!tic"+ e$$e+ th"t i$ "&e ') o% KCS. It i$ )!oi&e& to $e)"!"te the )"!ti"++: con&en$e& @ t(o-)h"$e $t!e" %!o the AineRe#ene!"to! con&en$e!. The $t!e" ente!$ the e$$e+ th!o'#h " &i$t!i'to! +oc"te& +e$$th"n " ete! e+o( the e$h +"net. The e$$e+ i$ )!oi&e& (ith " thic e$h +"netto !eoe "n: ent!"ine& +i*'i& %!o the "ci& #"$ $t!e". The +i*'i& ("te! %!o the!eceie! i$ )')e& "$ !e%+' to the to) t!": o% the Aine Re#ene!"to!. The "ci& #"$%+o($ on "c-)!e$$'!e cont!o+ to the S'+%'! Recoe!: Unit.

Lean Amine Car*on Fi#ter > 810457 ?

The Le"n Aine C"!on Fi+te! i$ " e!tic"+ e$$e+ @ "&e ') o% KCS %i++e& (ith#!"n'+"! c"!on to " hei#ht o% 32// %!o otto t"n#ent +ine. The C"!on Fi+te! i$

)!oi&e& to !eoe cheic"+ i)'!itie$ %!o the $+i)$t!e" o% coo+e& +e"n "ine.The !e#ene!"te& +e"n "ine $o+'tion ente!$ the e$$e+ th!o'#h " 6 &i$t!i'to! "t the to)en& o% the e$$e+ "n& %+o($ &o(n("!&$ th!o'#h the c"!on e&, !eoin# thei)'!itie$. The )!o&'ct $t!e" #oe$ o't %!o the otto o% the e$$e+ "n& $ent to the%in"+ %i+t!"tion $:$te.The e$$e+ i$ &e$i#ne& %o! oth "c'' "n& +i*'i&-%'++ con&ition$.

Amine S(mp Tan > 810458 ?

An 'n&e!#!o'n& $') t"n i$ )!oi&e& to e the en& &e$tin"tion @ %in"+ $to!"#e o%+e"n7!ich "ine $o+'tion$ &i$ch"!#e& %!o the 'nit &'!in# no!"+ o)e!"tion, ee!#enc:$it'"tion$ "n& 'nit $h't&o(n. The e$$e+ (i++ e "&e "in+: %!o KCS "n& to e

)!oi&e& (ith 5 co!!o$ion "++o("nce. The in&ic"te& e$$e+ "n& "$$oci"te& )i)in#(i++ e e+o( #!"&e.The e$$e+ i$ )!oi&e& (ith " &e&ic"te& )') %o! t!"n$%e!!in# "ine $o+'tion to theRich Aine F+"$h D!'.

F(e# Ga% Amine A*%or*er Interfa&e Pot > 810456 ?

The F'e+ 1"$ Aine A$o!e! Inte!%"ce Pot i$ )!oi&e& %o! h:&!oc"!on $iin# "n&"ine &!"in"#e to the Aine S') T"n.The Inte!%"ce Pot i$ " $"++ e!tic"+ e$$e+ "&e %!o KCS. The e$$e+ i$ "tt"che& tothe otto-$i&e o% the F'e+ 1"$ Aine A$o!e! to !eoe +i*'i& h:&!oc"!on"cc''+"tin# %!o the A$o!e!.



The e$$e+ i$ $'))+ie& (ith $t!i))in# $te" to ")o!ie the $ie& h:&!oc"!on$ %!othe Aine A$o!e!. H:&!oc"!on ")o! i$ $ent to the "ci& #"$ %+"!e %!o the to) o% thee$$e+ "n& the !ich "ine $o+'tion &!"ine& to the Aine S') T"n.

Rea&tor %(mmar)


Fire' .eater %(mmar)


EB&.anger %(mmar)

Amine Regenerator Re*oi#er% > 8104E2A+, ?

The Aine Re#ene!"to! Reoi+e!$ "!e t''+"! he"t ech"n#e!$ )!oi&e& to $'))+: he"tto the Aine Re#ene!"to!. LP $te" #oe$ th!o'#h the t'e $i&e (hi+e the +e"n "ine i$")o!ie& on the $he++ $i&e.The t(o ho!iont"+ !eoi+e!$ "!!"n#e& in )"!"++e+ "!e o% BJU t:)e he"t ech"n#e!$ (ithit$ $he++ "n& coe! con$t!'cte& (ith KCS "n& the t'e$ "n& othe! inte!n"+$ (ithSt"in+e$$ Stee+ @ SS . Both the $he++ $i&e "n& t'e $i&e o% the ech"n#e!$ (i++ e

)!oi&e& (ith in$'+"tion.

Ri&.+Lean Amine EB&.anger > 8104E ?

The Rich7Le"n Aine Ech"n#e! i$ " ho!iont"+, AES t:)e t''+"! he"t ech"n#e!(hich i$ )!oi&e& %o! he"t !ecoe!: )'!)o$e$. The !ich DEA $o+'tion %!o the Rich

Aine F+"$h D!', e%o!e ente!in# the Aine Re#ene!"to!, i$ he"te& "$ it )"$$e$th!o'#h the SS t'e $i&e o% the ech"n#e! (hi+e the +e"n DEA $o+'tion %!o theRe#ene!"to! otto i$ coo+e& &o(n on the KCS $he++ $i&e.

Lean Amine Trim Coo#er > 8104E6 ?

The Le"n Aine T!i Coo+e! i$ )!oi&e& to #ie the nece$$"!: coo+in# to the +e"n "ine$o+'tion )!io! to ente!in# the Aine A$o!e!. Thi$ ho!iont"+ ech"n#e! (i++ e o% t:)eAES "n& (i++ e con$t!'cte& (ith KCS. Coo+in# ("te! (i++ e )"$$e& th!o'#h the t'e$i&e "n& the +e"n "ine to the $he++ $i&e.

Amine Regenerator Con'en%er > 8104EA1 ?

The Aine Re#ene!"to! Con&en$e! i$ "n "i! coo+e& ech"n#e! '$e& %o! coo+in# theoe!he"& ")o! o% the Aine Re#ene!"to! %!o 2/= oC to 52 oC. Thi$ con&en$e! (i++ econ$t!'cte& (ith KCS (ith 8./ co!!o$ion "++o("nce on the he"&e!$. Po$t-(e+& he"tt!e"tent i$ !e*'i!e&. F"n$ in the "i! ": $h"++ e the $t"n&"!& t:)e @ SP (he!e +"&e

)itch c"n e "&'$te& "n'"++: (hen %"n i$ $to))e&.

Lean Amine Coo#er > 8104EA2 ?

The Le"n Aine Coo+e! i$ "n "i! coo+e& ech"n#e! )!oi&e& %o! coo+in# the +e"n "ine$o+'tion %!o the Aine Re#ene!"to! %!o 2/2 oC to 52 oC. Thi$ "i! %"n coo+e! (i++ econ$t!'cte& (ith KCS "n& to e )o$t-(e+& he"t t!e"te&. One h"+% o% %"n$ in the "i! ":

$h"++ e "'to-"!i"+e @ A; t:)e (he!e the +"&e )itch i$ "'to"tic"++: "&'$te& to

44




SHEET 68 OF 235

&e$i!e& "n#+e : "n'"+ "&'$tent o% " !eote cont!o+ no into " )ne'"tic"++:"ct'"te& !e+": $:$te. Re"inin# %"n@$ $h"++ e the $t"n&"!& t:)e @ SP (he!e +"&e

)itch c"n e "&'$te& "n'"++: (hen %"n i$ $to))e&.

P(mp %(mmar)

Ri&. Amine F#a%. $r(m S#op Oi# P(mp% > 8104P1A+, ?

The Rich Aine F+"$h D!' S+o) Oi+ P') i$ )!oi&e& to )e!io&ic"++: t!"n$%e! the"cc''+"te& $+o) oi+ %!o the F+"$h D!' to the +i#ht $+o) oi+ t"n "t the T"n"#e "n&B+en&in# S:$te. The S+o) Oi+ P')$ (i++ e cent!i%'#"+ t:)e )')$ "n& (i++ econ$t!'cte& (ith S-8 c+"$$ $tee+.

Ri&. Amine P(mp% > 8104P2A+, ?

The Rich Aine P') i$ )!oi&e& to t!"n$%e! the !ich "ine $o+'tion %!o the RichAine F+"$h D!' to the Aine Re#ene!"to! i" the Rich7Le"n Aine Ech"n#e!.The$e !ich "ine )')$ "!e o% " cent!i%'#"+ t:)e "n& (i++ e con$t!'cte& (ith S-8 c+"$$$tee+. C"$in# to e )o$t-(e+& he"t t!e"te&.

Lean Amine P(mp% > 8104PA+, ?

The Le"n Aine P') i$ )!oi&e& to t!"n$%e! the !e#ene!"te& +e"n "ine $o+'tion %!othe Aine Re#ene!"to! i" the Rich7Le"n Aine Ech"n#e! to the +e"n "ine '$e!$@ "$o!e!$ . The$e +e"n "ine )')$ "!e o% " cent!i%'#"+ t:)e "n& (i++ e con$t!'cte&(ith S-8 c+"$$ $tee+. C"$in# to e )o$t-(e+& he"t t!e"te&.

Amine S(mp P(mp% > 8104PA+, ?

The Aine S') P') i$ )!oi&e& to t!"n$%e! inte!ittent+: the "cc''+"te& "ine$o+'tion %!o the Aine S') T"n to the Rich Aine F+"$h D!'. The$e )')$ "!eo'nte& on the t"n "n& the: "!e o% " cent!i%'#"+ t:)e . The$e )')$ "!e con$t!'cte&(ith $tee+.

Amine Tran%fer P(mp% > 8104PA+, ?

The Aine T!"n$%e! P') i$ )!oi&e& to t!"n$%e! the %!e$h +e"n "ine $o+'tion %!o theAine Sto!"#e T"n to the +e"n "ine '$e!$ @ "$o!e!$ . The$e t!"n$%e! )')$ "!e o%" cent!i%'#"+ t:)e "n& (i++ e con$t!'cte& (ith S-8 c+"$$ $tee+. C"$in# to e )o$t-(e+&he"t t!e"te&.

Compre%%or %(mmar)


Spe&ia# e/(ipment %(mmar)


Li%t of In%r(ment%

In$t!'ent$ )!oi&e& %o! thi$ 'nit "!e +i$te& in In$t!'ent Sche&'+e %o! Aine T!e"tin#

P!oce$$ Unit, Doc'ent No. S-02/-24=/-2/2.



S(mmar) of a## e/(ipment% 'rier%

Re%e! to Att"chent 0.2@ E*'i)ent Li$t

Contro# a#e%

The %o++o(in# t"+e i$ " $'"!: o% %"i+'!e "ction o% C;$ "n& U$.

T"# No. Se!ice F"i+'!e

Action

P?ID No.

02/-F;-/25 Le"n Aine to F.1. Aine A$o!e! F"i+ C+o$e D-02/-2338-224

02/-P;-//3 T!e"te& F'e+ #"$ %!o Aine A$o!e! F"i+ C+o$e D-02/-2338-224

02/-L;-//= Rich Aine %!o F. 1. Aine A$o!e! F"i+ C+o$e D-02/-2338-224

02/-P;-//0 Rich Aine to Rich Aine F+"$h D!' F"i+ O)en D-02/-2338-226

02/-F;-/2= Le"n Aine to Rich Aine F+"$h D!' F"i+ C+o$e D-02/-2338-226

02/-PD;-/26 Le"n Aine B:)"$$in# Fi+te!$ F"i+ O)en D-02/-2338-225

02/-PC;-/35 F.1. P'!#e to Aine S') T"n ;ent +ine NA D-02/-2338-22=

02/-L;-/2/ Rich Aine to Aine Re#ene!"to! F"i+ C+o$e D-02/-2338-22>

02/-F;-/3>74/ Ste" Inection to Aine Re#ene!"to! F"i+ C+o$e D-02/-2338-22>

02/-F;-/42743 Con&en$"te %!o A. Re#ene!"to! Reoi+e!$ F"i+ C+o$e D-02/-2338-22>

02/-T;-/3= Boi+e! Fee& <"te! to De$')e!he"te! F"i+ C+o$e D-02/-2338-22>

02/-F;-/4> Aine Re#ene!"to! Re%+' F"i+ O)en D-02/-2338-23/

02/-P;-/64A A. Re#ene!"to! Receie! #"$ to S'+%'! P+"nt F"i+ C+o$e D-02/-2338-23/

02/-P;-/64B Re#ene!"to! Receie! #"$ to Re+ie% He"&e! F"i+ O)en D-02/-2338-23/

Fire' .eater% Not "))+ic"+e to thi$ 'nit.

Mi%&e##aneo(%

Re%e! to the Att"chent 0.2.

46




SHEET 6= OF 235

F#o P#an% an' P#ot P#an

PF$; MS$ an' P<I$%

Re%e! to the %o++o(in# "tt"chent$Att"chent >.2 P!oce$$ F+o( Di"#!" @ D-02/-2334-2/2 Att"chent >.3 M"te!i"+ Se+ection Di"#!" @ D-02/-2334-8/2Att"chent >.4 Pi)in# "n& In$t!'ent Di"#!" @D-02/-2338-2/2,2/3,2/4,

D-02/-2338-222,224 23/, 24/ 246

$e%ign Engineering; (ti#it) an' %afet) f#o p#an%

Re%e! to the %o++o(in# "tt"chent$Att"chent >.6 Pi)in# "n& In$t!'ent Di"#!" @ UFD @ D-0/2-2338-242 245 Att"chent >.8 A!e" C+"$$i%ic"tion @ D-02/-240/-//2 Att"chent >.5 Fi!e P!otection S:$te L":o't %o! P!oce$$ A!e"

@ D->35-2338-//4 Att"chent >.= Fi!e Etin#'i$he! L":o't %o! P!oce$$ "n& Uti+it: A!e"

@ D->35-2338-/22 Att"chent >.0 A!!"n#eent o% 1"$ Detecto!$ %o! P!oce$$ A!e"

@ D->35-2338-/34 Att"chent >.> A!!"n#eent o% Fi!e A+"! S:$te E*'i)ent %o! <ho+e Re%ine!:A!e" @ D->35-2338-/32 Att"chent >.2/ L":o't %o! <ho+e Fi!e P!otection S:$te

@ D->35-2338-//3

P#ot P#an

Re%e! toAtt"chent >.22 P+ot P+"n o% KM7LM7Aine Unit$ @ D-02/-2338-//2

Safet) S.(t'on f(n&tion &.art%

Re%e! toAtt"chent >.23 C"'$e "n& E%%ect Ch"!t @ S-02/-24=2-6/2



Safet)

To )!eent "cci&ent$ it i$ o% the 'to$t i)o!t"nce th"t "++ )e!$onne+ e in$t!'cte& )!o)e!+: o% the %o++o(in# $'ectQThe +e"$ "n& !e$)on$ii+itie$ o% the o)e!"to!$The etho&$ to "cco)+i$h thi$ in " $"%e "nne!.The %o++o(in# $"%et: !e#'+"tion coe! o)e!"tion$ o% )"!tic'+"! conce!n to the )e!$onne+!e$)on$i+e %o! the Aine T!e"tin# P!oce$$ Unit. The: "!e inten&e& to $'))+eent "n:ei$tin# #ene!"+ !e%ine!: $"%et: !e#'+"tion$ (hich coe! "++ 'nit$Q !e%e!ence $ho'+& e"&e to the +"tte! %o! "++ )oint$ not entione& e+o(Q. Mech"nic"+ c!"%t$en (o!in#on hi$ 'nit (i++ e #oe!ne& : thei! o(n &e)"!tent"+ $"%et: !e#'+"tion$, 't theo)e!"to! $ho'+& $ee th"t none o% the %o++o(in# $"%et: !e#'+"tion$ "!e io+"te& :ech"nic"+ (o!e!$.In "&&ition to $)eci%ic"++: &e%ine& !'+e$ "n& )!"ctice$, the ee!ci$e o% #oo& '&#ent :ee!: )e!$on ino+e& i$ e$$enti"+ to $"%e o)e!"tion : ee!: )e!$on ino+e& i$ e$$enti"+to $"%e o)e!"tion. An o)e!"to! $ho'+& e "+e!t %o! "n: $it'"tion (hich i#ht )!e$ent "

)e!$onne+ h""!&. It $ho'+& "+$o e the !e$)on$ii+it: o% e"ch )e!$on %"i+i"! (ith the )+"nt to ("!n othe! (o!e!$ (ho ente! the )+"nt o% )o$$i+e h""!&$ the: co'+&enco'nte!.A++ )e!$onne+ '$t no( the +oc"tion "n& '$e o% $"%e+: $ho(e!, %i!e etin#'i$he!, )+"nt%i!e "+"!, "n& "in i$o+"tion "+e$, %i!e ho$e$ "n& h:&!"nt$, %i!e +"net$, #"$ "$$"n& !e$)i!"to!$, "n& othe! )!otectie e*'i)ent $'ch "$ h"!& h"t$, !'e! #+oe$, etc.So&" "ci& o! %o" t:)e etin#'i$he! '$t not e '$e& on %i!e "!o'n& e+ect!ic"+e*'i)ent ec"'$e the ("te! $o+'tion (i++ con&'ct e+ect!icit: "n& ": "##!""te the&i%%ic'+t: o! !e$'+t in the e+ect!oc'tion o% )e!$onne+.C"!on &ioi&e o! &!: )o(&e! etin#'i$he! ": e '$e& $"%e+: on e+ect!ic"+ %i!e$. Thec"!on tet!"ch+o!i&e etin#'i$he!$ +ie!"te )oi$ono'$ %'e$ "n& $ho'+& not e '$e& in "con%ine& $)"ce, 'n+e$$ )!ec"'tion$ "!e t"en to "oi& !e"thin# the ")o!$.

1"$ "$$ o! !e"thin# "))"!"t'$ '$t e (o!n (henee! toic %'e$ "!e enco'nte!e&.S"%et: h"t$ '$t e (o!n (hen o't&oo!$.1+oe$ "n& #o##+e$ o! %"ce $hie+&$ $ho'+& e (o!n (he!e toic o! hot ")o! o! +i*'i& i$enco'nte!e&, "n& "!e !ecoen&e& %o! '$e (hi+e $")+e$ "!e ein# (ith&!"(n "n&$o+'tion$ "&e ').Fi!e etin#'i$he!$ '$t e !ech"!#e& ie&i"te+: "%te! '$e. A++ $te" "n& ("te! ho$ee*'i)ent '$t e )'t "c in )+"ce "%te! '$e. Acce$$ to $'ch e*'i)ent '$t not eo$t!'cte&.1"$ "$$ '$t h"e %!e$h c"!t!i&#e$ in$t"++e& "%te! '$e.

Emergen&) fire p#an

The %i!e )!otection $:$te o% the )+"nt i$ &e$i#ne& to )!eent %i!e occ'!!ence, cont!o+%i!e e$c"+"tion, o! etin#'i$h %i!e (ithin $ho!t )e!io& o% tie, "$$'in# the!e (i++ e noo't$i&e %i!e %i#htin# "$$i$t"nce, (ith on+: one "o! %i!e "t " tie.

Fire fig.ting an' prote&tie e/(ipment

The!e "!e %ie ("te! h:&!"nt$ (ith onito!$ "n& +ie ho$e !ee+$ in the )!oce$$ "!e".S'it"+e %i!e etin#'i$he! '$t e !e"&i+: ""i+"+e. The "!e" "!o'n& "n etin#'i$he! o!h:&!"nt '$t e c+e"! $o th"t e*'i)ent i$ !e"&i+: "cce$$i+e in c"$e o% ee!#enc:.Fo! &et"i+$, $ee the !e+e"nt &!"(in# %o! the %i!e %i#htin# $:$te.In c"$e o% %i!e in the )!oce$$ %"ci+it:, the!e i$ " ch"nce th"t e$$e+$ o! &!'$ (i++ %"++&o(n ec"'$e o% oe!he"tin# o% the $'))o!t$. The %i!e %i#htin# $ho'+& e &one %!o the

(in&("!&.

48




SHEET 6> OF 235

In o!&e! to )!eent the $)!e"& o% %i!e, it i$ nece$$"!: to coo+ &o(n ne"! e*'i)ent '$in#the %i!e ("te! $:$te, $)eci"+ e*'i)ent %o! %i!e %i#htin# "n& "+$o %i!e %i#htin# t!'c$.I% the )!oce$$ 'nit i$ in o)e!"tion, it i$ nece$$"!: to $h't &o(n the 'nit.

DO NOT E;ACUATE o! ;ENT "n: h:&!oc"!on to "to$)he!e.Re%e! to FIRE PROTECTION SYSTEM LAYOUT FOR PROCESS AREA, D->35-2338-//4 @ Att"chent >.5 %o! &et"i+$.

Fi!e "+"! $:$teRe%e! to ARRAN1EMENT OF FIRE ALARM SYSTEM E9UIPMENT FOR<HOLE REFINERY AREA , D->35-2338-/32 @ Att"chent >.>.A+$o, Re%e! to FIRE ETIN1UISHER LAYOUT FOR PROCESS ? UTILITYAREA , D->35-2338-/22 @ Att"chent >.= .

Fie& <"te! Monito!$P!oi$ion %o! %ie& ("te! onito!$ $h"++ e )e! LAYOUT FOR <HOLE FIREPROTECTION SYSTEM, D->35-2338-//3 @ Att"chent >.2/ .Fie& ("te! onito!$ h"e "n e%%ectie no+e !"n#e o% "t +e"$t 4/ "n& " &i$ch"!#ec")"cit: o% 2>// +ite! )e! in'te$. Monito!$ "!e "!!"n#e& $o th"t "n: e*'i)ent to e

)!otecte& ": e coe!e& : t(o %ie& onito!$ (ith " !"&i'$ o% "t +e"$t 4/. Monito!$"!e +oc"te& "))!oi"te+: 28 %!o the e*'i)ent ein# )!otecte&.

Fi!e H:&!"nt$The "i' &i$t"nce et(een %i!e h:&!"nt$ $e!in# the )!oce$$ 'nit$ $h"++ e 8/ete!$ o! +e$$ "$ &ete!ine& : the e*'i)ent $e!e&.

Lie Ho$e Ree+ St"tion$He": &'t: ho$e !ee+$ h"in# 6/ ete!$ o% 43 h"!& oo$te! ho$e e*'i))e& (ith 40

co')+in#$ "n& cont"in $t!"i#ht $t!e"7%o# no+e, $h"++ e )!oi&e& "$ e"n$ %o!*'ic ("te! "))+ic"tion : one "n.

Fire Prote&tion

Re%e! to LAYOUT FOR <HOLE FIRE PROTECTION SYSTEM, D->35-2338-//3 @ Att"chent >.2/ %o! &et"i+$.St!'ct'!e $tee+, Pi)e !"c$, E*'i)ent S'))o!t$, "in $'))o!t$ o% he"te! "!e%i!e)!oo%e&. @ Re%e! to S-///-24B/-//2. The %o++o(in# "!e )!ec"'tion$ to "oi& %i!e2. Le"in# %+"n#e$, #+"n&$, o! !oen #"'#e #+"$$e$ c"n !e+e"$e "n: h:&!oc"!on #"$

o! +i*'i& to the "!e", c!e"tin# " %i!e h""!&. A++ e*'i)ent $ho'+& e te$te& %o!

+e"$ e%o!e $t"!t-').3. A++ $:$te$ "!e to e )'!#e& to #ie " non-e)+o$ie "to$)he!e.4. T!"$h "n& !'i$h "!e " %i!e "n& $t'+in# h""!&. Pic it '), "n o)e!"to! $ho'+&

e )!o'& o% " c+e"n 'nit.6. Oe!he"tin# e$$e+$ : $te" ": c"'$e &""#e to the inte!n"+ "$$e+:.8. S)i++e& oi+ o! cheic"+$ "!o'n& 'nit$ o! in t!enche$ $ho'+& e c+e"ne& ') "t once.5. Soin# in the )!oce$$ "!e" c"n c"'$e %i!e$ "n& e)+o$ion$. Soe on+: in

&e$i#n"te& "!e"$.=. <e+&in# o! othe! (o! (hich c"n c"'$e $)"!$ in the )!oce$$ "!e" c"n c"'$e %i!e$

"n& e)+o$ion$. M"e the "!e" $"%e %o! $'ch (o! "n& ot"in the nece$$"!: )e!it%!o the )!o)e! "'tho!itie$ e%o!e coencin# (o!.



Maintenan&e of e/(ipment an' .o(%eeeping

2. O)e!"tin# e*'i)ent $ho'+& e chece& %!e*'ent+: %o! $i#n$ o% +e""#e,oe!he"tin#, o! co!!o$ion, $o th"t 'n$"%e con&ition$ ": e co!!ecte& e%o!ethe: !e$'+t in $e!io'$ con$e*'ence$. Un'$'"+ con&ition$ $ho'+& e !e)o!te& "tonce.

3. 1'"!& "!o'n& oin# $h"%t$, co')+in# e+t$, etc., (hich h"e een !eoe& %o!!e)"i!$ o% the e*'i)ent '$t e !e)+"ce& (hen !e)"i! (o! i$ co)+ete&.

4. Too+$, )iece$ o% )i)e etc., $ho'+& nee! e +e%t +:in# on )+"t%o!$ o! !"i+in#$ o%o)e!"tion e*'i)ent (he!e the: c"n e noce& o%% "n& in'!e $oeone

e+o(.6. Acce$$ to +"&&e!$ "n& %i!e e$c")e$ '$t e e)t c+e"!. <"$te "te!i"+ "n& !e%'$e

'$t e )'t in )!o)e! +oc"tion$ (he!e the: (i++ not o%%e! %i!e o! $t'+in#h""!&$.

8. Li*'i& $)i++$ '$t e c+e"ne& ') ie&i"te+:. B+"net #"$ +e"$ (ith $te" "n&ie&i"te+: !e)o!t +e"$ %o! !e)"i!.

5. In the eent th"t e+ect!ic"+ e*'i)ent &oe$ not %'nction )!o)e!+:, noti%: thee+ect!ic"+ &e)"!tent "n& $t": c+e"! o% the e*'i)ent 'nti+ the e+ect!ici"n"!!ie$.

=. 1"$ c:+in&e!$ $ho'+& e $to!e& $o th"t the: c"nnot %"++ oe!. 1'"!& c")$ '$t!e"in in )+"ce oe! the "+e$ o% c:+in&e!$ (hich "!e not in '$e.

0. C"!e $ho'+& e t"en (hen in$t"++in# $c"%%o+&in# to en$'!e th"t the (oo&en o"!&$&o not cont"ct hot e*'i)ent "n& th"t no )"!t i$ "++o(e& to i)"i! %!ee "cce$$on o)e!"tion"+ e*'i)ent e.#. +"&&e!$, $t"i!(":$, ("+(":$ o! "+e$.Sc"%%o+&in# $ho'+& e !eoe& ie&i"te+: on co)+etion o% the (o! inh"n&.

>. S(itch )')$ !e#'+"!+: (hen $)"!e$ "!e )!oi&e&. Thi$ (i++ "$$'!e $t"!t the $)"!e )') (i++ e !e"&: (hen nee&e&.

Repair or

2. Mech"nic"+ (o! "!o'n& "n& o)e!"tin# 'nit '$t e e)t to " ini', "n& theini' n'e! o% en $ho'+& e '$e&.

3. No ech"nic"+ (o! on the e*'i)ent i$ to e &one (itho't " )!o)e!+: "'tho!ie&(o! )e!it.

4. S"%et: h"t$ '$t e (o!n : "++ )e!$onne+ in "++ "!e"$ "t "++ tie$.6. No '!nin#, (e+&in#, o)en %i!e$, o! othe! hot (o! $h"++ e "++o(e& in the "!e" 'n+e$$

"'tho!ie& : " (o! )e!it. C"tch "$in$, "nho+e$, "n& othe! $e(e!connection$ '$t e )!o)e!+: $e"+e& o%% to )!eent the +e""#e o% #"$e$ (hich": i#nite ')on cont"ct (ith "n o)en %+"e.

8. No )e!$onne+ $h"++ ente! " e$$e+ %o! "n: )'!)o$e (h"t$oee! 'nti+ it h"$ een"&e*'"te+: )'!#e&, +"ne& o%%, then te$te& to en$'!e %!ee&o %!o noio'$ o!in%+""+e #"$e$ "n& "n ent!: )e!it i$$'e&.

5. <hen %+'$hin# e*'i)ent (ith " %i!e ho$e, the %i!e ho$e '$t e e*'i))e& (ith " chec "+e to )!eent "c%+o( into the %i!e "in.

=. Line$ o)e!"tion "t " +o( te)e!"t'!e i#ht %!"ct'!e i% 'n&'+: $t!e$$e&Q the!e%o!e, &onot )h:$ic"++: $t!ie the$e +ine$ "n& "oi& o)e!"tion con&ition$ (hich (o'+&c"'$e " ("te! h"e! to $t"!t.

0. Do not '$e +i#ht &i$ti++"te$ $'ch "$ #"$o+ine o! n")hth" to c+e"n "chine!: o! %o! "n:othe! c+e"nin# )'!)o$e$.

>. E*'i)ent $ho'+& not e +e%t o)en oe!ni#ht. At the en& o% e"ch &":$ (o! +"n$ o!$)"&e$ $ho'+& e in$t"++e& to )!eent ent!: o% %+""+e "te!i"+$ &'e to "+e+et-:.

50




SHEET 82 OF 235

2/. <e+&in# c:+in&e!$ $ho'+& e !eoe& %!o $ite to " &e$i#n"te $"%e "!e" "t the en& o%e"ch (o!in# &":.

T.erma# eBpan%ion in eB&.anger%

Bec"'$e o% $e!io'$ "cci&ent$ c"'$e& : the!"+ e)"n$ion o% +i*'i& t!"))e& inech"n#e!$ the %o++o(in# )!oce&'!e$ i$ o't+ine& in "n e%%o!t to e+iin"te thi$ h""!&.2. <hen the coo+e! $i&e o% "n ech"n#e! i$ to e :)"$$e& (hi+e hot "te!i"+ i$

)"$$in# th!o'#h the othe! $i&e, the &!"in o! ent $ho'+& e chece& e%o!e :)"$$in# to $ee th"t it i$ not )+'##e&.

3. <hen the ech"n#e! i$ :)"$$e&, the +ee&e! o! ent $ho'+& e "!!"n#e& $o th"t the )!e$$'!e c"n e &i$$i)"te& to " $'it"+e )+"ce.

4. <"!nin# $i#n$ "$ %o++o($ $ho'+& e in$t"++e& on "++ ech"n#e!$ (he!e it i$ )o$$i+eto +oc in the co+& $i&e o% "n ech"n#e! (ith hot +i*'i& #oin# th!o'#h the othe!$i&e.

!it.'raa# of %amp#e%

S")+e$ $h"++ e (ith&!"(n %!o the 'nit on+: : "'tho!ie& )e!$onne+.P!otectie e*'i)ent, %"ce "$$ o! #o##+e$, "n& $'it"+e #+oe$ '$t e (o!n %o!$")+in# +i*'i&$ o! $o+i&$. A cont"ine! '$t nee! e %i++e& to the !i, in o!&e! toiniie !i$ o% $'$e*'ent $)i++"#e.<hen $")+in# "n: )!o&'ct +i*'i&$, #+oe$ "n& #o##+e$ (i++ e (o!n.<hen $")+in# "n: "te!i"+, #"$ o! +i*'i&, the $")+in# +ine '$t e %+'$he& +on#eno'#h to !eoe &o!"nt "te!i"+$ to in$'!e th"t the $")+e ot"ine& !e)!e$ent$ thec'!!ent $t!e". P"$$ eno'#h #"$ th!o'#h the $")+e e$$e+ to in$'!e the &i$)+"ceent o% the )'!#e #"$ "n& to "&'$t the te)e!"t'!e o% the $")+e! to th"t the co)o$ition i$ not&i$to!te& : con&en$"tion o! %+"$hin#, etc.

<hen the $")+e co)o$ition i$ !e)!e$ent"tie o% the $o'!ce "te!i"+, 'n&i$to!te& :%+"$h ")o!i"tion. Ce!t"in c+"$$e$ o% $")+e$ ": !e*'i!e ine!t "to$)he!e$ , coo+in#o! $)eci"+ c"!!:in# &eice$. <e"! "))!oe& )e!$on"+ $"%et: e*'i)ent "n& ee!ci$ec"'tion to "oi& in'!ie$.

Safe .an'#ing of o#ati#e an' toBi& materia#% in&#('ing &ata#)%t

The $"%et: !'+e$ #ien e+o( "!e %o! the )!otection o% +i%e "n& +i, "n& the )!eentiono% )!o)e!t: +o$$. It i$ e)ecte& th"t !e%ine!: )eo)+e (i++ ee!ci$e coon $en$e,"+e!tne$$, "n& #oo& '&#ent in c"!!:in# the o't. I% ee! the!e i$ "n: &o't "$ to the$"%et: "$)ect o% " )"!tic'+"! o)e!"tion, con$'+t :o'! $')e!i$o! ie&i"te+:.

Re%pirator) Prote&tion

Re%e! to Att"chent >.0 ARRAN1EMENT OF 1AS DETECTORS FOR PROCESSAREA @ D->35-2338-/34 .Mo$t !e%ine!: #"$e$, othe! th"n "i!, "!e h"!%'+ to h'"n ein#$ i% inh"+e& in $'%%icientconcent!"tion. Toic #"$e$ ": e c+"$$i%ie& "$ eithe! "$)h:i"tin# o! i!!it"tin#.A$)h:i"tin# #"$e$ ": c"'$e &e"th : !e)+"cin# the "i! in the +'n#$ o! : !e"ction(ith the o:#en c"!!ie& in the +oo&Q e")+e$ "!e h:&!o#en $'+%i&e c"!on onoi&e,"n& $oe. I!!it"tin# #"$e$ ": c"'$e in'!: o! &e"th not on+: : "$)h:i"tin# 't "+$o

: '!n$ inte!n"+ "n& ete!n"+7 e")+e$ "!e ch+o!ine "n& $'+%'! &ioi&e.To #'"!& "#"in$t the inh"+"tion o% h"!%'+ #"$e$

• Sec'!e " #"$ te$t ce!ti%ic"te $ho(in# the #"$ con&ition o% the e$$e+ i$ $"%e %o!

ent!:.



• St"n& on the (in&("!& $i&e o% "n o)e!"tin# %!o (hich #"$e$ e$c")e.

• P!oi&e )!o)e! enti+"tion.

• A++ )e!$onne+ $ho'+& ecoe %"i+i"! (ith the "cce)te& etho& o% "!ti%ici"+

!e$)i!"tion in o!&e! to !en&e! "$$i$t"nce to "n: one oe!coe : #"$, e+ect!ic$hoc, o! &!o(nin#.

I% "n:one i$ oe!coe : #"$, hi$ !e$c'e! $ho'+&

• Nee! "tte)t " !e$c'e 'n+e$$ "n "$$i$t"nt i$ $t"n&in# :.

• P!otect hi$e+% e%o!e "tte)tin# " !e$c'e : (e"!in# !e"thin# "))"!"t'$.

• 1et the icti to %!e$h "i! "$ $oon "$ )o$$i+e.

• 1ie "!ti%ici"+ !e$)i!"tion "n& $en& hi$ "$$i$t"nt to c"++ %o! e&ic"+ "i&.

<hen '$in# " !e"thin# "))"!"t'$, e $'!e th"t the "$ %it$ the %"ce )!o)e!+:. Te$t it : the "))!oe& te$t etho&.<e"! the co!!ect t:)e o% !e"thin# "))"!"t'$, $'ite& to the $it'"tion enco'nte!e&.

,reat.ing Apparat(% > ,- A- ?

The!e "!e %o'! t:)e$ o% !e"thin# "))"!"t'$ in #ene!"+ !e%ine!: $e!ice. The: "!e thec"ni$te! t:)e "$, the %!e$h "i! ho$e +ine B. A., the co)!e$$e& "i! $e+%-cont"ine& B. A."n& the co)!e$$e& "i! +ine t!o++e: B. A.2. The c"ni$te! t:)e "$ 'ti+ie$ " %i+te! e+eent to "$o! the )oi$ono'$ #"$ %!o

the "i! "n& i$ '$e& on+: : )e!$onne+ (o!in# "t the TEL7TML 'i+&in# o%%7on+o"&in#.U$e thi$ "$ on+: in the o)en "i! o! (he!e the #"$ concent!"tion i$ +e$$ th"n3G, not in " t"n o! othe! con%ine& $)"ce. A c"ni$te! t:)e "$ &oe$ not

)!otect the '$e! "#"in$t " &e%icienc: o% o:#en. A +i%e+ine $ho'+& e '$e& in*'e$tion"+e +oc"tion$.<hen " $e"+ i$ !eoe& %!o " c"ni$te!, "! the &"te on the c"ni$te!, "n&"%te! one :e"! &i$c"!& it !e#"!&+e$$ o% ho( +itt+e it h"$ een '$e&.A !eco!& o% the "o'nt o% tie th"t the c"ni$te! h"$ een '$e& '$t e e)t on" t"# "tt"che& to the c"ni$te!. Do not ecee& the )e!i$$i+e tie +iit %o! the

)"!tic'+"! c"ni$te! ein# '$e&. In%o! S"%et: De)"!tent (hen tie +iit i$ne"!.

3. The %!e$h "i! ho$e +ine !e"thin# "))"!"t'$ h"$ " +en#th o% "i! ho$e tho'#h (hichthe (e"!e! &!"($ in the "i! !e*'i!e& %o! !e$)i!"tion.<hen " "n '$t ente! " t"n, $e(e!, o! othe! con%ine& "!e" (he!e the"to$)he!e i$ 3/G o! o!e o% the +o(e! e)+o$ie +iit, o! cont"in$ ei&enceo% h:&!o#en $'+%i&e o! othe! toic "te!i"+$, " %!e$h "i! !e"thin# "))"!"t'$'$t e '$e&. It i$ to e '$e& $'ect to the %o++o(in# con&ition$

• The %!ee en& o% the "i! ho$e +ine '$t e )+"ce& (he!e on+: %!e$h "i! c"n ente!

it, 't not o!e th"n 2// ete! o% ho$e $ho'+& e '$e&.

• A +i%e e+t "n& !o)e $ho'+& "+(":$ e '$e& (ith the en& %ie& $o th"t it (i++

not %"++ "c into the t"n o! $e(e!.

• Be $'!e th"t the h"!ne$$ i$ 'c+e& c+o$e to the (e"!e!$ o&: $o th"t it (i++

not $+i) oe! hi$ $ho'+&e!$ i% " !o)e !e$c'e i$ nece$$"!:.2. The co)!e$$e& "i! $e+% cont"ine& !e"thin# "))"!"t'$ h"$ " $e+%-cont"ine& "i!

$'))+: c"!!ie& on the "c o% the '$e!. It i$ one o% t(o o% the %o'! t:)e$ th"t i$co)+ete+: in&e)en&ent o% o't$i&e "i!.It i$ '$e& )!inci)"++: in ee!#encie$.A%te! '$e, "+(":$ noti%: the )!o)e! &e)"!tent $o th"t the: c"n !ech"!#e thec:+in&e!$ "$ $oon "$ )o$$i+e.

52




SHEET 84 OF 235

3. Co)!e$$e& "i! +ine t!o++e: !e"thin# "))"!"t'$. Thi$ !e"thin# "))"!"t'$ i$ "+$oco)+ete+: in&e)en&ent o% o't$i&e "i!. It i$ )!inci)"++: '$e& (he!e the %!e$h "i! +ine !e"thin# "))"!"t'$ (o'+& e 'n$'it"+e.

Poi%ono(% Materia#

A "tte! o% 'to$t conce!n %o! "++ o)e!"tin# )e!$onne+ i$ the )!e$ence o% H3S in$t!e"$.Re%e! to ARRAN1EMENT OF 1AS DETECTORS FOR PROCESS AREA @ D->35-2338-/34.

9)'rogen S(#fi'e >92S?

H3S i$ " co+o!+e$$ #"$ $+i#ht+: he"ie! th"n "i! @it "cc''+"te$ in +o( $)ot$- e "("!e.It i$ hi#h+: %+""+e "n& " &"n#e!o'$ %i!e !i$. H:&!o#en $'+%i&e i$ "n e)+o$ie #"$(hich (i++ e)+o&e in concent!"tion$ o% 6.4G @4.6G "t 26> to 68G : o+'e in℃

"i!. H:&!o#en $'+%i&e e)+o$ion$ "!e o$t +ie+: to occ'! in the ")o! $)"ce oe! +i*'i&$'+%'!, ec"'$e "$ +i*'i& $'+%'! i$ coo+e& o! "#it"te&, it eo+e$ H3S into ")o! $)"ce"oe it. S'ch ")o! ei$t$ "oe the +i*'i& $'+%'! in the $'+%'! )it, (hich '$t e$(e)t (ith "i! to )!eent " 'i+&') o% H3S to e)+o$ie. H3S i$ e"$i+: i&enti%ie& in e!:+o(, non-%"t"+ concent!"tion$ @/.24 )) : the $t!on# )'n#ent o&o! o% !otten e##$.Ho(ee!, $ince H3S &e"&en$ :o'! $en$e o% $e++, &o not !e+: on it$ o&o! to ("!n :o' o% it$ )!e$ence in +eth"+ concent!"tion$. NoteH3S i$ et!ee+: )oi$ono'$, @o!e )oi$ono'$ th"n the h:&!o#en c:"ni&e #"$ '$e& inthe #"$ ch"e!$ "n& !e"thin# "n: concent!"tion '$t e "oi&e&. S:)to$ o%

)oi$onin# "!: (ith the concent!"tion "n& +en#th o% e)o$'!e.

H3S i$ )!e$ent in the %ee& %!o the %!"ction"to! oe!he"& $:$te "n& in "n: +ine$ "n&e$$e+$ in the )+"nt. NoteH3S +e"$ $ho'+& nee! e "))!o"che& (itho't $e+% cont"ine& !e"thin# #e"! "n& "$t"n&-: "n in )o$ition (ith !e"thin# #e"!.H3S onito!$ h"e een )!oi&e& to &etect H3S +e"$ in )"!tic'+"! "!e"$ o% o&e!"te tohi#h concent!"tion$. Becoe %"i+i"! (ith the +oc"tion o% thi$ $"%et: e*'i)ent "n& it$o)e!"tion.

P!ec"'tion$ to Aoi& D"n#e! %!o H:&!o#en S'+%i&e 1"$<o!in# in "n: concent!"tion o% h:&!o#en $'+%i&e i$ not &e$i!"+e. <he!e nece$$"!:,(o! c"n e &one %o! "n ei#ht ho'! )e!io& in " concent!"tion ') to 2/)) @/.//2G :

o+'e in " "i!, )!oi&in# contin'"+ chec$ "!e "&e : " *'"+i%ie& #"$ te$te! '$in# "n"))!oe& H3S 1"$ Detecto!. Un&e! no ci!c'$t"nce$ $ho'+& "n:one (o! inconcent!"tion #!e"te! th"n 2/ )) (itho't )!o)e! !e$)i!"to!: e*'i)ent "n& "))!o"+o% " $')e!i$o!.Bec"'$e o% the &"n#e!o'$ %!o the !e+e"$e o% h:&!o#en $'+%i&e #"$, the %o++o(in#

)!ec"'tion$ '$t e $t!ict+: o$e!e&Do not (o! o! )e!it "n:one to (o! in "n "!e" $'$)ecte& o% cont"inin# "concent!"tion o% h:&!o#en $'+%i&e #"$ (itho't %i!$t h"in# the "!e" te$te& : " *'"+i%ie&#"$ te$te!, '$in# "n "))!oe& H3S &etecto!.Re)o!t "t once "n: +e""#e o% #"$ o! "n: #"$eo'$ "!e"$ "$ $oon "$ &i$coe!e&.Kee) o't o% #"$eo'$ "!e"$ "n& ee) othe!$ o't.St": on the (in&("!& $i&e o% the "!e" "$ +on# "$ the con&ition ei$t$.



<hen nece$$"!: to ent e*'i)ent cont"inin# h:&!o#en $'+%i&e o! h:&!o#en $'+%i&e e"!in# "te!i"+, '$e " ent o! !e+ie% $:$te, i% )!oi&e&. Aoi& entin# thi$ #"$ &i!ect+:to the "to$)he!e.M"int"in "&e*'"te enti+"tion o% "n: enc+o$e& $)"ce (he!e +e""#e o% #"$e$ i#htocc'!.I% it $ho'+& e nece$$"!: in "n ee!#enc: to ente! "n& "!e" (he!e the!e i$ "n:

)o$$ii+it: o% h:&!o#en $'+%i&e #"$ ein# )!e$ent, )"!tic'+"!+: in enc+o$e& +oc"tion$(he!e the #"$ co'+& "cc''+"te, '$e " Scott Ai!-P". H"e " "n $t"n&in# : in " $"%e+oc"tion e*'i))e& (ith " !e"thin# "))"!"t'$ "n&, i% nece$$"!:, '$e " +i%e +ine.

P!inci)+e$ %o! Ee!#enc: ActionI% "n: ee!#enc: $it'"tion &ee+o)$ &'e to e$c")in# h:&!o#en $'+%i&e #"$, o$e!e the%o++o(in# )!inci)+e$ %o! $"%et:Fi!$t #et o't "n& ("!n "++ othe!$ to $t": c+e"! o% the h""!&o'$ "!e"$.Do not "tte)t to !e$c'e "n:one 'n+e$$ :o' "!e (e"!in# !e"thin# #e"!. Yo'! %i!$t &'t:i$ to $'on he+) e%o!e "tte)tin# " !e$c'e.Do not, 'n&e! "n: ci!c'$t"nce$, t!: to &ete!ine the concent!"tion o% h:&!o#en $'+%i&e"$ : it$ o&o!. I% it$ )!e$ence i$ $'$)ecte&, h"e the +oc"tion te$te& (ith "n "))!oe&H:&!o#en S'+%i&e 1"$ Detecto!.In c"$e " "n i$ oe! coe, $'on he+), #et hi into the %!e$h "i! "t once, "n& e#in"!ti%ici"+ !e$)i!"tion, '$in# "n inh"+"to! i% ""i+"+e. S'on " &octo! "$ $oon "$

)o$$i+e. B't &o not $to) "!ti%ici"+ !e$)i!"tion.An: )e!$on oe!coe : #"$ '$t e e)t ("!, een &'!in# "!ti%ici"+ !e$)i!"tion. U$e"n:thin# ""i+"+e (hich ": e $'it"+e %o! thi$ )'!)o$e, $'ch "$ ee!#enc: +"net$,co"t$ etc. <hen the )"tient h"$ !ecoe!e& "n& c"n e $"%e+: oe&, he '$t e $et tothe ho$)it"+ : "'+"nce "n& nee! "++o(e& to $t"n& 'nti+ !e+e"$e& : the &octo!.

Nitrogen

N3 i$ "n ine!t #"$ '$e& %o! )'!#in# e*'i)ent o! "int"inin# " )o$itie )!e$$'!e ine!t#"$ +"net on " e$$e+.

N3 i$ neithe! )oi$ono'$ no! %+""+e, 't c"!e '$t e ee!ci$e& (hen (o!in# in$i&ee*'i)ent th"t h"$ eenN3 )'!#e&. A&e*'"te enti+"tion '$t e )!oi&e& "n&"))!o)!i"te !e"thin# &eice$ (o!n. To !e"the "n "to$)he!e hi#h in N3, co'+& !e$'+tin $'%%oc"tion.Be%o!e ente!in# e$$e+$ th"t h"e een )'!#e& (ith N3, " chec '$t e "&e %o!

)!o)e! o:#en content )!io! to ent!:. R")i& ")o!i"tion o% +i*'i& nit!o#en c"n c"'$e$ee!e '!n$ on cont"ct (ith the $in.

Ammonia

Aoni" i$ " co+o!+e$$ #"$ (ith "n et!ee+: )'n#ent o&o! M": c"'$e "!:in# &e#!ee$o% i!!it"tion to the e:e$, $in, o! 'co'$ e!"ne$.Re%e! to MSDA Sheet$ %o! the "oe "te!i"+$ %o! o!e &et"i+e& in%o!"tion.

So'i(m 9)'roBi'e > NaO9 Ca(%ti& So'a ?

Re%e! to the "))!o)!i"te $"%et: '++etin )'+i$he& : the N"tion"+ S"%et: Co'nci+ o! theM"n'%"ct'!in# Chei$t$ A$$oci"tion.C"'$tic $o+'tion, coon+: c"++e& +:e, "n& technic"++: no(n "$ $o&i' h:&!oi&e, i$'$e& $o (i&e+: in )et!o+e' !e%inin#, th"t it$ )otenti"+ h""!&$ "!e o%ten c"!e+e$$+:oe!+ooe&. Ce!t"in #ene!"+ )!ec"'tion$ $ho'+& e o$e!e&.

54




SHEET 88 OF 235

1o##+e$ o! %"ce $hie+&$ $ho'+& e (o!n "t "++ tie$ in the )!oce$$in# "!e". P"in%'+in'!: "n& )o$$i+e +in&ne$$ c"n !e$'+t i% c"'$tic !e"che$ the e:e$. A '+e! %o'nt"in$ho'+& e )!oi&e& %o! the )'!)o$e o% ("$hin# the e:e$ i% "n "cci&ent $ho'+& occ'!.Bo!ic "ci& $o+'tion $ho'+& e ""i+"+e %o! %i!$t "i& "%te! ("$hin# the in'!e& e:e (ithco)io'$ *'"ntitie$ o% ("te!. A++ e:e in'!: c"$e$, een $+i#ht, $ho'+& e !e%e!!e& to "

)h:$ici"n.<o!en $ho'+& e i)!e$$e& th"t c"'$tic &oe$ not #ie ie&i"te ("!nin# o% it$

)!e$ence on the $in : '!nin# o! i!!it"tion, "$ in the c"$e o% "n: othe! cheic"+$. A$ee!e '!n c"n !e$'+t %!o c"'$tic e%o!e the in&ii&'"+ !e"+ie$ it$ )!e$ence on the$in. Ho(ee!, the )!e$ence o% c"'$tic on the $in e%o!e '!nin# $en$"tion &ee+o)$c"n e !eco#nie& : it$ $+i))e!: "n& $o"): %ee+in#. A )h:$ici"n $ho'+& e con$'+te& inc"$e o% " $ee!e $in '!n. Soe !e%ine!$ ee) " t' o% &i+'te& ine#"! h"n&: tone't!"+ie c"'$tic on too+$, !'e! #+oe$, etc., "%te! ("$hin# in ("te!.In ie( o% the %o!e#oin#, (o!en $ho'+& e in$t!'cte& to (e"!, in "&&ition to %"ce$hie+&$ o! #o##+e$, !'e! #+oe$ "n& !'e! ")!on$ (hen )e!%o!in# "n: (o! (hiche)o$e$ the to c"'$tic. De)en&in# ')on con&ition$, it ": e "&i$"+e to (e"!

)!otectie !'e! %oot(e"!, "$ c"'$tic i$ &e$t!'ctie to +e"the!. Inci&ent"++:, cotton"te!i"+ i$ o!e !e$i$t"nt to c"'$tic th"n (oo+, "n& the!e%o!e i$ )!e%e!"+e %o! c+othin#.A+tho'#h it $ho'+& not e con$i&e!e& "$ " )!otectie "te!i"+.<hen c"'$tic h"$ coe into cont"ct (ith the $in, the "!e" $ho'+& e ie&i"te+:%+'$he& (ith ("te! %o! $ee!"+ in'te$, "n& &e)en&in# ')on the $ee!it: o% thee)o$'!e, thi$ "n e %o++o(e& : " t(o )e!cent "cetic "ci& ("$h to ne't!"+ie "n: +"$tt!"ce$ o% c"'$tic. F"ci+itie$ %o! *'ic "ction in the "tte! o% ("te! ("$hin# $ho'+& e""i+"+e.A t!e"&+e o)e!"te& $"%et: $ho(e! e*'i))e& (ith " *'ic o)enin# "+e $ho'+& ein$t"++e& in the "!e". In co+& $e"$on$ )!oi$ion$ $ho'+& , o% co'!$e, e "&e to $'))+:(ith ("! ("te!.

Preparing for entering pro&e%% e/(ipment

An:one ente!in# " e$$e+ (hich ": cont"in "n ine!t o! cont"in"te& "to$)he!e '$t%o++o( $"%et: )!ec"'tion$ "n& !'+e$ (hich "))+:. The e$$e+$ ": cont"in H3$ o! othe!toic "te!i"+ in "&&ition to h:&!oc"!on$.The!e%o!e, the %o++o(in# )!ec"'tion$ $ho'+& e inc+'&e& in the $t"n&"!& )!oce&'!e.The e$$e+$ $ho'+& e i$o+"te& : )o$itie "ction, $'ch "$ +in&in#, to ec+'&e "++$o'!ce$ o% h:&!oc"!on, %'e+ #"$, $te", "i!, etc.the !e%ine!: $"%et: o%%ice! "n& $')e!i$o!: )e!$onne+ (i++ #ie thei! )e!i$$ion %o!e$$e+ ent!: "%te! the: h"e "&e the "))!o)!i"te te$t$.In$t"++ "n "i! oe! o't$i&e the e$$e+ to $(ee) "(": "n: ")o!$.The "n ente!in# the e$$e+ '$t e e*'i))e& (ith " %!e$h "i! "$ in )!o)e! (o!in#

con&ition, (ith " %!e$h "i! $'))+:.The!e $ho'+& e ""i+"+e "n& !e"&: %o! ie&i"te '$e "n& t!"n$%e! to the "n in thee$$e+, " $e)"!"te "i! $'))+: (hich i$ in&e)en&ent o% e+ect!ic"+ )o(e!.The "n ente!in# the e$$e+ $ho'+& (e"! " $"%et: h"!ne$$ (ith )!o)e!+: "tt"che& $"%et:+ine.I% the (o! ino+e$ " +"!#e &i$t"nce "oe the %+oo! o% the e$$e+, $c"%%o+&in# o!$'))o!t %+oo!in# '$t e 'i+t to )!eent &"n#e!o'$ %"++$.The!e $ho'+& e " $)"!e %!e$h "i! "$ co)+ete (ith it$ o(n $e)"!"te "i! $'))+:, to"++o( " $econ& "n to ente! the e*'i)ent *'ic+: in c"$e o% "n ee!#enc:. Thi$ $)"!ee*'i)ent '$t e co)"ct eno'#h to "++o( the $econ& "n to ente! th!o'#h the"n(": (hi+e ente!in# the e*'i)ent.The API )'+ic"tion 1'i&e %o! In$)ection o% Re%ine!: E*'i)ent o! the NIOSH

)'+ic"tion No. 0=-224Q A 1'i&e to S"%et: in Con%ine& S)"ce$ c"n e !e%e!!e& to %o!



"&&ition"+ in%o!"tion on $"%et: )!oce&'!e$ %o! e$$e+ ent!: "n& "cci&ent )!eentione"$'!e$.

Opening e/(ipment

Ee!: +ine connectin# to " no+e on the e$$e+ to e ente!e& '$t e +in&e& "t thee$$e+. Thi$ inc+'&e$ &!"in$ connectin# to " c+o$e& $e(e!, 'ti+it: connection$ "n& "++

)!oce$$ +ine$. The +oc"tion o% e"ch +in& $ho'+& e "!e& on " "$te! )i)in# "n&in$t!'ent"tion &i"#!" @ P?ID , e"ch +in& $ho'+& e t"##e& (ith " n'e! "n& " +i$to% "++ +in&$ "n& thei! +oc"tion$ $ho'+& e "int"ine&. One )e!$on $ho'+& e #ien!e$)on$ii+it: %o! the "++ +in&$ in the 'nit to "oi& e!!o!$.The "!e" "!o'n& the e$$e+ "n(":$ $ho'+& "+$o e $'!e:e& %o! )o$$i+e $o'!ce$ o%&"n#e!o'$ #"$e$ (hich i#ht ente! the e$$e+ (hi+e the )e!$on i$ in$i&e. E")+e$inc+'&e "cet:+ene c:+in&e!$ %o! (e+&in# "n& )!oce$$ ent o! &!"in connection$ in the$"e o! "&oinin# 'nit$. An: h""!&$ %o'n& in the $'!e: $ho'+& e i$o+"te& o!!eoe&.S"%e "cce$$ '$t e )!oi&e& oth to the ete!io! "n& inte!io! o% the e$$e+ to eente!e&. The ete!io! "cce$$ $ho'+& e " $o+i&, )e!"nent +"&&e! "n& )+"t%o! o!$c"%%o+&in# $t!on# eno'#h to $'))o!t the )eo)+e "n& e*'i)ent (ho (i++ e ino+e& inthe (o! to e )e!%o!e&.Acce$$ to the inte!io! $ho'+& "+$o e $t!on# "n& $o+i&. Sc"%%o+&in# i$ )!e%e!!e& (hen thee$$e+ i$ +"!#e eno'#h to )e!it it to e '$e&. The $c"%%o+&in# "$e $ho'+& !e$t %i!+: onthe otto o% the e$$e+ "n& e $o+i&+: "ncho!e&. I% the $c"%%o+&in# i$ t"++, the$c"%%o+&in# $ho'+& e $'))o!te& in $ee!"+ )+"ce$ to )!eent $(":. The )+"t%o! o"!&$$ho'+& e $t'!&: "n& c")"+e o% $'))o!tin# $ee!"+ )eo)+e "n& e*'i)ent "t the $"etie "n& "+$o e %i!+: %"$tene& &o(n. R'n#$ $ho'+& e )!oi&e& on the $c"%%o+&in#$)"ce& "t " co%o!t"+e &i$t"nce %o! c+iin# on the $t!'ct'!e.I% $c"%%o+&in# (i++ not %it in the e$$e+ " +"&&e! c"n e '$e&. A !i#i& +"&&e! i$ "+(":$

)!e%e!!e& oe! " !o)e +"&&e! "n& i$ e$$enti"+ to "oi& %"ti#'e &'!in# +en#th: )e!io&$ o%(o! in$i&e " e$$e+. The otto "n& to) o% the +"&&e! $ho'+& e $o+i&+: "ncho!e&. I%"&&ition"+ $'))o!t i$ ""i+"+e, then the +"&&e! $ho'+& "+$o e "ncho!e& "t inte!e&i"te+oc"tion$. <hen )o$$i+e, " $o+i& $'))o!t $ho'+& )"$$ th!o'#h the +"&&e! 'n&e! " !'n#,the!e: )!oi&in# $'))o!t %o! the enti!e (ei#ht $ho'+& the otto $'))o!t %"i+. On+:one )e!$on "t " tie $ho'+& e "++o(e& on the +"&&e!.<hen " !o)e +"&&e! i$ '$e&, the !o)e$ $ho'+& e tho!o'#h+: in$)ecte& )!io! to e"ch ne(

o. A++ !'n#$ $ho'+& e te$te& %o! $t!en#th, (hethe! the: e "&e o% et"+ o! (oo&.E"ch !o)e '$t e in&ii&'"++: $ec'!e& to "n io"+e $'))o!t. I% )o$$i+e, " $o+i&$'))o!t $ho'+& )"$$ th!o'#h the +"&&e! $o th"t " !'n# c"n he+) $'))o!t the (ei#ht "n&the otto o% the +"&&e! $ho'+& e %"$tene& to " $'))o!t to )!eent the +"&&e! %!o$(in#in#. A$ (ith the !i#i& +"&&e!, on+: one )e!$on $ho'+& c+i the +"&&e! "t " tie.

!oring in &o#(mn% or e%%e#%

It i$ !ecoen&e& th"t "n: "n (o!in# in " e$$e+ (hich h"$ "n ine!t o! cont"in"te&"to$)he!e not e )e!itte& to oe too %"! "(": o! into "n: ti#ht "!e"$, $'ch "$th!o'#h " %!"ction"to! t!": "n(":. The !e"$on %o! thi$ )!ec"'tion i$ th"t $ho'+& the"n &ee+o) $oe &i%%ic'+t: (hi+e e+o( " t!":, %o! e")+e, to " )oint (he!e he co'+&not %'nction )!o)e!+: o! +o$t con$cio'$ne$$, it (o'+& e et!ee+: &i%%ic'+t %o! the$'!ei++"nce te" o't$i&e the e$$e+ to )'++ the "n ') th!o'#h the $"++ t!": "n(":

: '$e o% the $"%et: +ine.An: one (o!in# in the otto o% the co+'n o! e$$e+ $ho'+& e "("!e o% the h""!&o% %"++in# oect$. H"!& h"t$ $ho'+& e (o!n , 't the$e (i++ not )!oi&e tot"+ )!otection

"#"in$t he": oect$. The (o!en $ho'+& e ("!ne& to )": "ttention, to +oo, "n&

56




SHEET 8= OF 235

+i$ten. The "inten"nce $')e!i$o! $ho'+& e c"!e%'+ (hen $che&'+in# (o!, to "oi&h"in# )eo)+e in the otto o% the e$$e+ (hen the!e i$ he": (o! #oin# on in the to)o% the co+'n o! e$$e+$.A co'nic"tion $:$te $ho'+& e )!oi&e& %o! the "n(": ("tch $o th"t the: c"n*'ic+: c"++ %o! he+) in the eent th"t the )e!$onne+ in$i&e the e$$e+ enco'nte! &i%%ic'+t:.A !"&io, te+e)hone, o! )'+ic "&&!e$$ $:$te i$ nece$$"!: %o! th"t )'!)o$e.

Entering tan%; 'r(m% or ot.er e%%e#%

Be%o!e ente!in# " e$$e+, the !e%ine!:$ $"%et: )!ec"'tion$ $ho'+& e o$e!e&. The$e'$'"++: inc+'&e the %o++o(in# $")+in# the e$$e+ %o! toic ")o!$ "n& o:#enconcent!"tion, (e"!in# " $"%et: h"!ne$$, "n& h"in# "n "tten&"nt o't$i&e the e$$e+.An 'n"tten&e& e$$e+ $ho'+& nee! e ente!e&

Pro&e'(re for remoing %afet) a#e%

Be%o!e !eoin# the $"%et: "+e, it i$ !e*'i!e& to con%i! th"t oth $i&e o% i$o+"tion"+e "!e +oce& "n& &e)!e$$'!e& $"%e+:. It i$ "+$o !e*'i!e& to con%i! th"t the $et

)!e$$'!e o% $)"!e $"%et: "+e i$ )!o)e!+: "&'$te& on the te$tin# %"ci+it: in ("!eho'$e"n& +oc "+e o% oth in+et "n& o't+et +ine in %ie+& "!e c"!-$e"+e&-o)en.

!or permit pro&e'(re an' or permit format%

Be%o!e ente!in# the e$$e+, " e$$e+ ent!: )e!it '$t e ot"ine&. A e$$e+ ent!: )e!itin$'!e$ th"t "++ !e$)on$i+e )"!tie$ no( th"t (o! i$ ein# con&'cte& in$i&e o% " e$$e+"n& e$t"+i$he$ " $"%e )!e)"!"tion )!oce&'!e to %o++o( in o!&e! to )!eent i$t"e$(hich co'+& !e$'+t in "n "cci&ent The )e!it i$ t:)ic"++: i$$'e& : the $"%et: en#inee! o!

: the $hi%t $')e!i$o!.

The )e!it $ho'+& e "$e& on " $"%et: chec+i$t to e co)+ete& e%o!e it i$ i$$'e&.The )e!it $ho'+& "+$o !e*'i!e$ the $i#n"t'!e$ o% the $"%et: en#inee!, the $hi%t$')e!i$o!, "n& the )e!$on th"t )e!%o!e& the o:#en toic "n& e)+o$ie #"$ chec onthe e$$e+ "to$)he!e. Fo'! co)ie$ o% the )e!it $ho'+& e )!oi&e&. One co): #oe$ tothe $"%et: en#inee!, one to the $hi%t $')e!i$o!, one to the cont!o+ !oo, "n& one co):$ho'+& e )o$te& )!oinent+: on the "n(": th!o'#h (hich the )e!$onne+ (i++ ente! thee$$e+.The )e!it $ho'+& e !ene(e& e%o!e e"ch $hi%t "n& "++ co)ie$ o% the )e!it $ho'+& e!et'!ne& to the $"%et: en#inee! (hen the (o! i$ co)+ete. A&&ition"+ !e*'i!eent$ o!

)!oce&'!e$ ": e i)o$e& : the !e%ine!, 't the %o!e#oin# i$ con$i&e!e& the ini'"cce)t"+e %o! #oo& $"%et: )!"ctice.



Operation note% re#ating to 9ADOP reie

Re%e! to HAOP STUDY REPORT, S-02/-233/-2/2 "n& HAOP ACTIONFOLLO<-UP LIST, S-02/-233/-2/3.

Action

No.

Recoen&"tion O)e!. M"n'"+

Section No.

R-33 O)e!"tin# )!oce&'!e (i++ hi#h+i#ht th"t thi$ +ine '$t not e

o)ene& &'!in# no!"+ o)e!"tion "n& '$t e o)ene& on+:

(hen the +i*'i& i$ coo+e& &o(n e+o( 5/ &'!in# $h't &o(n℃

o)e!"tion.

4 "n& 5.>

Materia# %afet) 'ata %.eet>MS$S? of a## t.e &.emi&a#%; &ata#)%t%

Re%e! to the Att"chent 2/.2.@+"te! on

58




SHEET 8> OF 235

Mi%&e##aneo(%

Coner%ion ta*#e%

English - Metric Conversions and Abbreviations

M'+ti)+ie&En#+i$h Unit A!e. B: . Met!ic Unit A!e.

+en#th inch in 38.6 i++iete! %oot %t 4/6.0 i++iete!

"!e" $*'"!e %oot %t3 /./>3>/ $*'"!e ete! 3

o+'e c'ic %oot %t4 /./3043 c'ic ete! 4

$t"n&"!& c'ic SCF /./3035 $t"n&"!& c'ic $t& 4

%eet o% #"$ ete!$ o% #"$#"++on #"+ /.//4=08 c'ic ete! 4

"!!e+ + /.28>/ c'ic ete! 4

te)e!"t'!e&e#!ee$ F"h!enheit OF OC87>@OF-43 &e#!ee$ Ce+ci'$ OC

)!e$$'!e)o'n& )e! $*'"!e inch )$i 5.0>8 i+o)"$c"+ P"inch o% e!c'!: "t 43F in H# /.2444 i+o)"$c"+ P"

inch o% ("te! "t 6C in H3O /.36>2 i+o)"$c"+ P" )o'n& )e! $*'"!e inch )$i /./=/4/ i+o#!"$ )e! #7c3

$*'"!e centiete!

"$$ )o'n& "$$ + o! + /.6845 i+o#!" #

ene!#:B!iti$h The!"+ Unit Bt' 2./88 i+oJo'+e J

)o(e! ho!$e)o(e! h) /.=65 i+o("tt <B!iti$h The!"+ Bt'7h! /.3>42 ("tt <Unit$ )e! ho'!

UOP c"+c'+"te$ $t"n&"!& c'ic %eet o% #"$ "t 5/ F "n& 26.5>5 )$i". UOP )!o)o$e$ toc"+c'+"te $t"n&"!& c'ic ete!$ o% #"$ "t 28 C "n& 2/2.438 P".

Genera# pre4%tart (p pro&e'(re%

Re%e! to S---.@Ho+&

Oera## %tart4(p an' %.(t'on o(t#ine%

Re%e! to S---.@Ho+&

Off%ite %)%tem%

The!e i$ no inte!connection et(een the "ine t!e"tin# $ection "n& the o%%$ite $:$te.



Cata#)%t an' &.emi&a# #oa'ing + (n#oa'ing

P!e)"!"tion o% Aine So+'tionAine (i++ e $'))+ie& to the Aine T!e"tin# Unit in '+ *'"ntit: "$ 08 (t G DEA "tthe Aine M"e-') T"n @ 02/-TK2 . The "ine (i++ e &i+'te& to " 3/ (tG DEA$o+'tion in the Aine Sto!"#e T"n @ 02/-TK3 '$in# Co+& Con&en$"te "$ the ("te!$o'!ce.2. Fo! the initi"+ %i++, "n e$ti"te& *'"ntit: o% 3/8 4 o% 3/ (tG DEA $o+'tion (i++

e !e*'i!e&. Thi$ inc+'&e$ the o+'e !e*'i!eent %o! "++ th!ee "$o!e!$ "tAine T!e"tin# Unit, LP1 Me!o Unit, Die$e+M" Unit, one Rich AineF+"$h D!' @ 02/-;6 , "n& one Aine Re#ene!"to! @ 02/-;8 . The 3/8 4o+'e i$ e*'i"+ent to 4> 4 @ 62,62/ # )'!e DEA )+'$ 255 4 @ 258,56/# Co+& Con&en$"te. It i$ "ntici)"te& th"t the 'nit (i++ $t"!t ') in )h"$e$ "n&th"t the enti!e initi"+ %i++ (i++ not e !e*'i!e& "t one tie.

3. P!io! to the )!e)"!"tion o% the "ine $o+'tion, c+e"n the Aine M"e-') T"n@ 02/-TK2 , Aine Sto!"#e T"n @ 02/-TK3 "n& "$$oci"te& )i)in#. Lo"&the concent!"te& "ine to the Aine M"e-') T"n.

4. Ch"!#e Co+& Con&en$"te into the Aine Sto!"#e T"n ') to the !e*'i!e& +i*'i&+ee+. Line ') the Aine T!"n$%e! P') %!o the Aine M"e-') T"n to theAine Sto!"#e T"n.

6. An& then $t"!t the Aine T!"n$%e! P') @ 02/-P5A %o! the t!"n$%e! o% the!e*'i!e& concent!"te& "ine. Coi$$ion the N3 +"net $:$te o% the AineSto!"#e T"n ec"'$e "i! &e#!"&e$ the "ine $o+'tion.

8. M"e ci!c'+"tion o% the "ine $o+'tion $to!e& in the Aine Sto!"#e T"n : '$in#the ci!c'+"tion +oo) )!oi&e& %o! the t"n i" the Aine T!"n$%e! P') tohoo#enie the $o+'tion.

5. An"+:e the "ine content o% the ci!c'+"tin# $o+'tion "n& "&'$t the concent!"tionto the !e*'i!e& concent!"tion.

Cata#)%t an' &.emi&a#% re/(irement%

Re%e! to the Att"chent 2.3.

Ana#)ti&a# P#an

Re%e! to the o)e!"tin# "n'"+ %o! L"o!"to!: !e#"!&in# )!oce&'!e$ to o)e!"te+"o!"to!: e*'i)ent "n& $)eci"+ )!ec"'tion$ to cheic"+$, S-///-234/- @L"te!.

Recoen&e& $")+in# !e*'i!eent$ "!e )!oi&e& in the t"+e e+o(. Te$t %!e*'enc:$ho(n i$ " !o'#h %i#'!e "n& (i++ e o)tiie& (ith e)e!ience in )+"nt o)e!"tion.

@2 Fee& So'! 1"$ to F'e+ 1"$ Aine A$o!e! @02/-SN2

Ite Te$t Metho& No!"+ St"!t-')

Co)o$ition 1LC A$ !e*.@2 A$ !e*.@2

H3S Detecto! t'e o! UOP 323 A$ !e*.@2 A$ !e*.@2

CO3 De+ete& @3 - -

Note@2 Thi$ $t!e" i$ the $"e "$ $)on#e "$o!e! +e"n o%% #"$ in 'nit 622.A $")+e (i++ e no!"++: t"en %!o 622-SN8.

Note@3 CO3 &oe$ not ei$t.

@3 T!e"te& $(eet #"$ %!o F'e+ 1"$ Aine A$o!e! @02/-SN3

60




SHEET 52 OF 235


H3S Detecto! t'e o! UOP 323 27D 27D

@4 Rich Aine %!o F'e+ 1"$ Aine A$o!e!@02/-SN4


A))"!ent H3S UOP 03= A$ !e*. A$ !e*.

@6 Rich Aine %!o Rich Aine F+"$h D!'@02/-SN6

No!"++: no te$t i$ !e*'i!e&.@8

@5 Le*n Aine to A$o!e!$ @02/-SN8


Dieth"no+"ine UOP 036 27D 27D

A))"!ent H3S UOP 03= 27D 27D

Thio$'+%"te UOP 020 27< 27<

Tot"+ Aine UOP 030 27< 27<

C"!on Dioi&e De+ete& @2 - -

A))e"!ence ;i$'"+ 27D 27D

Fo" Te$t See thi$ "n'"+ A$ !e*. A$ !e*.

Note @2 CO3 &oe$ not ei$t.

@= Le"n Aine %!o Le"n Aine Soc Fi+te!$@02/-SN5@0

No!"++: no te$t i$ !e*'i!e&.

@> Rich Aine %!o F'e+ 1"$ Aine A$o!e! Inte!%"ce Pot@02/-SN=@2/

No!"++: no te$t i$ !e*'i!e&.

@22S+o) Oi+ %!o Rich Aine F+"$h D!' @02/-SN0

No!"++: no te$t i$ !e*'i!e&.

@23Re%+' ("te! %!o Aine Re#ene!"to! Re%+' P')$ @02/-SN>

No!"++: no te$t i$ !e*'i!e&.

@24Aci& 1"$ to SRU @02/-SN2/


H3S De+ete& @2

CO3 De+ete& @2

H:&!oc"!on$ De+ete& @2

Note@2 hi#h+: Toic.



@22M"e-') Aine %!o Aine Sto!"#e T"n @02/-SN20

Ite Te$t Metho& No!"+ St"!t-')Dieth"no+"ine UOP 036 A$ !e*. A$ !e*.

62




SHEET 54 OF 235

AMINE SOLUTION FOAM TEST

Sco)eThi$ te$t i$ inten&e& %o! the &ete!in"tion o% the %o"in# ch"!"cte!i$tic$ o% "*'eo'$"ine $o+'tion$. It i$ )"!tic'+"!+: '$e%'+ in co)"!in# )+"nt $")+e$ (ith c+e"n,+"o!"to!: )!e)"!e& $o+'tion$.

P!inci)+eAi! i$ '+e& th!o'#h the $")+e "t " e"$'!e& !"te %o! %ie in'te$, "n& the %o"hei#ht "n& %o" $t"i+it: "!e e"$'!e&.

A))"!"t'$Sto) ("tch, c"+i!"te& in $econ&$.Fo" te$t "))"!"t'$Q $ee Fi#'!e 22.=.

P!oce&'!ePo'! 3// + o% "n "ine $")+e into the 2,/// + c:+in&e!. Connect the "i! &e+ie!:t'e$ "n& int!o&'ce oi+-%!ee "i! "t %o'! +ite!$ %o! in'te.A++o( the '+in# to contin'e %o! %ie in'te$, $to) the "i! %+o( "n& $t"!t the$to)("tch. Ie&i"te+: !eco!& the hei#ht o% the %o" "n& "+$o !eco!& the tie, in$econ&$, %o! the %o" to !e" co)+ete+: "%te! the "i! $'))+: i$ $h't o%%.

Fo" Hei#htThe &i%%e!ence in + et(een the hei#ht o% the %o" "n& the initi"+ hei#ht o% the +i*'i&@ 3// + .

Fo" B!e" TieThe tie in $econ&$ %o! the %o" to !e" co)+ete+: "%te! the "i! $'))+: i$ $h't o%%.

Coent$Thi$ etho& c"n e '$e& to e"+'"te the e%%ect$ o% "nti%o" "#ent$ on the )+"nt "ine$")+e. C"!e $ho'+& e ee!ci$e& in c+e"nin# the e*'i)ent $ince " e!: $"++ "o'nto% "nti%o" "#ent o! $'!%"ct"nt ": "%%ect the te$t.



FI1URE 22.=

FOAMIN1 APPARATUS

CAPILLARYTUBE

AIR INAIROUT

1AS DISPERSION TUBECYLINDRICAL, FRITTED 1LASSETRA COURSE, 0 88/ -

1RADUATEDCYLINDER 2/// MILLILITER

1ASDISPERSIONTUBE

NO. 23STOPPER

AIR IN

FLO<METER,MONOMETER TYPE

2/// +

=8/ +

38/ +

8//

+

Documents

AMINE OM Part-1 Rev.3