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Alpha Analytical Deliverable PackageAlpha SDG: L1215002Client: Anchor QEA, LLCSite: NEWTOWN CREEK RI
The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in its entirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.
Page 1 of 296
Sample Receipt
Page 2 of 296
Sample Delivery Group Information
Page 3 of 296
Sample Delivery Group Form
L1215002Laboratory Job number:
COURIERSamples Delivered by:
TrackingnumN/ABill Of Laden
PresentCoc Present
IntactContainer Status Samples rec'd in Westborough 08/22/12@17:20-6c (5393)
Sample IDs
YesAll Containers Accounted For?
NoWere Extra Samples Received?
YesDo Sample Labels and COC agree?
YesAre Samples in Appropriate Containers?
YesAre Samples Received within Holding time?
N/ApH of Samples upon Receipt
Initial pH Final pHpreserved in house with
N/AChlorine Check
Other Issues
NoAre VOA/VPH Vials Present?
YesAre samples Properly Preserved?
Reagent H2O Preserved vials Frozen on
N/AFrozen by Client
N/A
N/ASoils: Is MeOHCovering the Soil?
N/AAqueous: Do Vials Contain Head Space?
B
A
Absent
Absent
Yes
Yes
No
No
No
No
No
No
Cooler SealIce Present
Blue IcePresent Temp. (Celsius)
Frozenupon Receipt
Delivered Direct fromSite
3.7 - IR Gun
4.1 - IR Gun
08/21/2012 17:44
Anchor QEA, LLCClient Account:
Received:
Call Tracker #
Project Number:
Project Name:
120782-01.01
NEWTOWN CREEK RI
Received by: DIANNE JANAK
Page 4 of 296
Sample Delivery Group Form
C Absent Yes No No No5.1 - IR Gun
Project Manager: Review Date:Chris Anderson 08/31/2012
Page 5 of 296
LIMS Chain of Custody
Page 6 of 296
ALPHA ANALYTICAL LABORATORIES, INC. LOGIN CHAIN OF CUSTODY REPORT
Sep 07 2012, 10:55 am
Login Number: L1215002Account: ANCHOR Anchor QEA, LLCProject: 120782-01.01 Newtown Creek RI
Received: 21AUG12 Due Date: 18SEP12 Sample # Client ID Mat PR Collected Container ______________________________________________________________________________________________________
L1215002-01 EK002SG-000015-2012 3 S0 21AUG12 09:06 1-Amber-A.1,1-Amber-A.25,1-Amber-A.5,1-Glass-A.06 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sediments A2-DPKG-FULL Package Due Date: 09/04/12
A2-DPKG-FULL,A2-FE-6020T,A2-MN-6020T,A2-TOC-9060-2REPS,A2-TS,ADR-FEE,DISPOSAL,NH3-4500,SULFIDE-9030
L1215002-02 EK002SG-000015-2012 3 S0 21AUG12 09:06 1-Amber-A.5 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
SUB-GEOTESTING
L1215002-03 EK001SG-000015-2012 3 S0 21AUG12 09:31 1-Amber-A.1,1-Amber-A.25,1-Amber-A.5,1-Glass-A.06 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
A2-FE-6020T,A2-MN-6020T,A2-TOC-9060-2REPS,A2-TS,ADR-FEE,DISPOSAL,NH3-4500,SULFIDE-9030
L1215002-04 EK001SG-000015-2012 3 S0 21AUG12 09:31 1-Amber-A.5 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
SUB-GEOTESTING
L1215002-05 EK010SG-000015-2012 3 S0 21AUG12 10:14 1-Amber-A.1,1-Amber-A.25,1-Amber-A.5,1-Glass-A.06 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
A2-FE-6020T,A2-MN-6020T,A2-TOC-9060-2REPS,A2-TS,ADR-FEE,DISPOSAL,NH3-4500,SULFIDE-9030
L1215002-06 EK010SG-000015-2012 3 S0 21AUG12 10:14 1-Amber-A.5 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
SUB-GEOTESTING
______________________________________________________________________________________________________
Page 1
Page 7 of 296
ALPHA ANALYTICAL LABORATORIES, INC. LOGIN CHAIN OF CUSTODY REPORT
Sep 07 2012, 10:55 am
Login Number: L1215002Account: ANCHOR Anchor QEA, LLCProject: 120782-01.01 Newtown Creek RI
Received: 21AUG12 Due Date: 18SEP12 Sample # Client ID Mat PR Collected Container ______________________________________________________________________________________________________
L1215002-07 NC071SG-000015-2012 3 S0 21AUG12 10:49 1-Amber-A.1,1-Amber-A.25,1-Amber-A.5,1-Glass-A.06 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
A2-FE-6020T,A2-MN-6020T,A2-TOC-9060-2REPS,A2-TS,ADR-FEE,DISPOSAL,NH3-4500,SULFIDE-9030
L1215002-08 NC071SG-000015-2012 3 S0 21AUG12 10:49 1-Amber-A.5 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
SUB-GEOTESTING
L1215002-09 NC059SG-000015-2012 3 S0 21AUG12 11:06 1-Amber-A.1,1-Amber-A.25,1-Amber-A.5,1-Glass-A.06 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
A2-FE-6020T,A2-MN-6020T,A2-TOC-9060-2REPS,A2-TS,ADR-FEE,DISPOSAL,NH3-4500,SULFIDE-9030
L1215002-10 NC059SG-000015-2012 3 S0 21AUG12 11:06 1-Amber-A.5 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
SUB-GEOTESTING
L1215002-11 NC1059SG-000015-201 3 S0 21AUG12 11:06 1-Amber-A.1,1-Amber-A.25,1-Glass-A.06 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
A2-FE-6020T,A2-MN-6020T,A2-TOC-9060-2REPS,A2-TS,ADR-FEE,DISPOSAL,NH3-4500,SULFIDE-9030
L1215002-12 NC1059SG-000015-201 3 S0 21AUG12 11:06 1-Amber-A.5 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
SUB-GEOTESTING
______________________________________________________________________________________________________
Page 2
Page 8 of 296
ALPHA ANALYTICAL LABORATORIES, INC. LOGIN CHAIN OF CUSTODY REPORT
Sep 07 2012, 10:55 am
Login Number: L1215002Account: ANCHOR Anchor QEA, LLCProject: 120782-01.01 Newtown Creek RI
Received: 21AUG12 Due Date: 18SEP12 Sample # Client ID Mat PR Collected Container ______________________________________________________________________________________________________
L1215002-13 NC058SG-000015-2012 3 S0 21AUG12 11:33 1-Amber-A.1,1-Amber-A.25,1-Amber-A.5,1-Glass-A.06 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
A2-FE-6020T,A2-MN-6020T,A2-TOC-9060-2REPS,A2-TS,ADR-FEE,DISPOSAL,NH3-4500,SULFIDE-9030
L1215002-14 NC058SG-000015-2012 3 S0 21AUG12 11:33 1-Amber-A.5 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
SUB-GEOTESTING
L1215002-15 NC046SG-000015-2012 3 S0 21AUG12 11:57 1-Amber-A.1,1-Amber-A.25,1-Amber-A.5,2-Glass-A.06 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sediments QC ONTHIS SAMPLE Package Due Date: 09/04/12
A2-DUP,A2-FE-6020T,A2-MN-6020T,A2-MS,A2-TOC-9060-2REPS,A2-TS,ADR-FEE,DISPOSAL,DUP,NH3-4500,SULFIDE-9030
L1215002-16 NC046SG-000015-2012 3 S0 21AUG12 11:57 2-Amber-A.5 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
SUB-GEOTESTING
L1215002-17 MC006SG-000015-2012 3 S0 21AUG12 13:48 1-Amber-A.1,1-Amber-A.25,1-Amber-A.5,1-Glass-A.06 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
A2-FE-6020T,A2-MN-6020T,A2-TOC-9060-2REPS,A2-TS,ADR-FEE,DISPOSAL,NH3-4500,SULFIDE-9030
L1215002-18 MC006SG-000015-2012 3 S0 21AUG12 13:48 1-Amber-A.5 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
SUB-GEOTESTING
______________________________________________________________________________________________________
Page 3
Page 9 of 296
ALPHA ANALYTICAL LABORATORIES, INC. LOGIN CHAIN OF CUSTODY REPORT
Sep 07 2012, 10:55 am
Login Number: L1215002Account: ANCHOR Anchor QEA, LLCProject: 120782-01.01 Newtown Creek RI
Received: 21AUG12 Due Date: 18SEP12 Sample # Client ID Mat PR Collected Container ______________________________________________________________________________________________________
L1215002-19 MC002SG-000012-2012 3 S0 21AUG12 14:26 1-Amber-A.1,1-Amber-A.25,1-Amber-A.5,1-Glass-A.06 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
A2-FE-6020T,A2-MN-6020T,A2-TOC-9060-2REPS,A2-TS,ADR-FEE,DISPOSAL,NH3-4500,SULFIDE-9030
L1215002-20 MC002SG-000012-2012 3 S0 21AUG12 14:26 1-Amber-A.5 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
SUB-GEOTESTING
L1215002-21 EB008SG-000015-2012 3 S0 21AUG12 15:01 1-Amber-A.1,1-Amber-A.25,1-Amber-A.5,1-Glass-A.06 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
A2-FE-6020T,A2-MN-6020T,A2-TOC-9060-2REPS,A2-TS,ADR-FEE,DISPOSAL,NH3-4500,SULFIDE-9030
L1215002-22 EB008SG-000015-2012 3 S0 21AUG12 15:01 1-Amber-A.5 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
SUB-GEOTESTING
L1215002-23 EB006SG-000015-2012 3 S0 21AUG12 15:32 1-Amber-A.1,1-Amber-A.25,1-Amber-A.5,1-Glass-A.06 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
A2-FE-6020T,A2-MN-6020T,A2-TOC-9060-2REPS,A2-TS,ADR-FEE,DISPOSAL,NH3-4500,SULFIDE-9030
L1215002-24 EB006SG-000015-2012 3 S0 21AUG12 15:32 1-Amber-A.5 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
SUB-GEOTESTING
______________________________________________________________________________________________________
Page 4
Page 10 of 296
ALPHA ANALYTICAL LABORATORIES, INC. LOGIN CHAIN OF CUSTODY REPORT
Sep 07 2012, 10:55 am
Login Number: L1215002Account: ANCHOR Anchor QEA, LLCProject: 120782-01.01 Newtown Creek RI
Received: 21AUG12 Due Date: 18SEP12 Sample # Client ID Mat PR Collected Container ______________________________________________________________________________________________________
L1215002-25 EK021SG-000015-2012 3 S0 21AUG12 16:07 1-Amber-A.1,1-Amber-A.25,1-Amber-A.5,1-Glass-A.06 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
A2-FE-6020T,A2-MN-6020T,A2-TOC-9060-2REPS,A2-TS,ADR-FEE,DISPOSAL,NH3-4500,SULFIDE-9030
L1215002-26 EK021SG-000015-2012 3 S0 21AUG12 16:07 1-Amber-A.5 "All data to be "J" qualified to the MDL" Metals Please digest 2 grams of sample for sedimentsPackage Due Date: 09/04/12
SUB-GEOTESTING
L1215002-27 SRM1650B 3 S0 21AUG12 12:00 0- | Package Due Date: 09/04/12
A2-TOC-9060-2REPS
______________________________________________________________________________________________________
Page 5
Logged By: Chris Anderson
Page 11 of 296
Container Tracking
Page 12 of 296
ALPHA ANALYTICAL LABORATORIESContainer Tracking Report
Transaction From ToContainer ID Type Status Date Response Location Operator Response Location Operator
L1215002-01A Amber-A.1 INTACT 27-AUG-12 CUSTODY A2-METALS PREP Bruce Hutchings A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Bruce Hutchings
L1215002-01A Amber-A.1 INTACT 27-AUG-12 A2-CUSTODY A2-CUSTODY-NOAA3 Bruce Hutchings A2-METALS PREP A2-METALS PREP Bruce Hutchings
L1215002-01A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-WET CHEMISTRY Kathy Bates A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Kathy Bates
L1215002-01A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-CUSTODY-NOAA3 Kathy Bates A2-WET CHEMISTRY A2-WET CHEMISTRY Kathy Bates
L1215002-01A Amber-A.1 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Dianne Janak
L1215002-01A Amber-A.1 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-01E Amber-A.25 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-01E Amber-A.25 INTACT 29-AUG-12 WETCHEM WETCHEM John D'Apollo CUSTODY CUSTODY John D'Apollo
L1215002-01E Amber-A.25 INTACT 29-AUG-12 CUSTODY CUSTODY John D'Apollo WETCHEM WETCHEM John D'Apollo
L1215002-01E Amber-A.25 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-01E Amber-A.25 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-01E Amber-A.25 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-01F Glass-A.06 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-01F Glass-A.06 INTACT 25-AUG-12 WETCHEM WETCHEM Marc Pollard CUSTODY CUSTODY Marc Pollard
L1215002-01F Glass-A.06 INTACT 25-AUG-12 CUSTODY CUSTODY Marc Pollard WETCHEM WETCHEM Marc Pollard
L1215002-01F Glass-A.06 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-01F Glass-A.06 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-01F Glass-A.06 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-01X Amber-A.5 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-FREEZ-1 A2-CUSTODY-FREEZ-1 Dianne Janak
L1215002-01X Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-02A Amber-A.5 INTACT 24-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - SUB TRANSFER - SUB Dianne Janak Comments: Sent to GeoTesting Express
L1215002-02A Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-03A Amber-A.1 INTACT 27-AUG-12 CUSTODY A2-METALS PREP Bruce Hutchings A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Bruce Hutchings
L1215002-03A Amber-A.1 INTACT 27-AUG-12 A2-CUSTODY A2-CUSTODY-NOAA3 Bruce Hutchings A2-METALS PREP A2-METALS PREP Bruce Hutchings
Page 13 of 296
Transaction From ToContainer ID Type Status Date Response Location Operator Response Location Operator
L1215002-03A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-WET CHEMISTRY Kathy Bates A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Kathy Bates
L1215002-03A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-CUSTODY-NOAA3 Kathy Bates A2-WET CHEMISTRY A2-WET CHEMISTRY Kathy Bates
L1215002-03A Amber-A.1 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Dianne Janak
L1215002-03A Amber-A.1 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-03E Amber-A.25 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-03E Amber-A.25 INTACT 29-AUG-12 WETCHEM WETCHEM John D'Apollo CUSTODY CUSTODY John D'Apollo
L1215002-03E Amber-A.25 INTACT 29-AUG-12 CUSTODY CUSTODY John D'Apollo WETCHEM WETCHEM John D'Apollo
L1215002-03E Amber-A.25 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-03E Amber-A.25 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-03E Amber-A.25 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-03F Glass-A.06 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-03F Glass-A.06 INTACT 25-AUG-12 WETCHEM WETCHEM Marc Pollard CUSTODY CUSTODY Marc Pollard
L1215002-03F Glass-A.06 INTACT 25-AUG-12 CUSTODY CUSTODY Marc Pollard WETCHEM WETCHEM Marc Pollard
L1215002-03F Glass-A.06 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-03F Glass-A.06 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-03F Glass-A.06 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-03X Amber-A.5 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-FREEZ-1 A2-CUSTODY-FREEZ-1 Dianne Janak
L1215002-03X Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-04A Amber-A.5 INTACT 24-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - SUB TRANSFER - SUB Dianne Janak Comments: Sent to GeoTesting Express
L1215002-04A Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-05A Amber-A.1 INTACT 27-AUG-12 CUSTODY A2-METALS PREP Bruce Hutchings A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Bruce Hutchings
L1215002-05A Amber-A.1 INTACT 27-AUG-12 A2-CUSTODY A2-CUSTODY-NOAA3 Bruce Hutchings A2-METALS PREP A2-METALS PREP Bruce Hutchings
L1215002-05A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-WET CHEMISTRY Kathy Bates A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Kathy Bates
L1215002-05A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-CUSTODY-NOAA3 Kathy Bates A2-WET CHEMISTRY A2-WET CHEMISTRY Kathy Bates
Page 14 of 296
Transaction From ToContainer ID Type Status Date Response Location Operator Response Location Operator
L1215002-05A Amber-A.1 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Dianne Janak
L1215002-05A Amber-A.1 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-05E Amber-A.25 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-05E Amber-A.25 INTACT 29-AUG-12 WETCHEM WETCHEM John D'Apollo CUSTODY CUSTODY John D'Apollo
L1215002-05E Amber-A.25 INTACT 29-AUG-12 CUSTODY CUSTODY John D'Apollo WETCHEM WETCHEM John D'Apollo
L1215002-05E Amber-A.25 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-05E Amber-A.25 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-05E Amber-A.25 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-05F Glass-A.06 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-05F Glass-A.06 INTACT 25-AUG-12 WETCHEM WETCHEM Marc Pollard CUSTODY CUSTODY Marc Pollard
L1215002-05F Glass-A.06 INTACT 25-AUG-12 CUSTODY CUSTODY Marc Pollard WETCHEM WETCHEM Marc Pollard
L1215002-05F Glass-A.06 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-05F Glass-A.06 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-05F Glass-A.06 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-05X Amber-A.5 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-FREEZ-1 A2-CUSTODY-FREEZ-1 Dianne Janak
L1215002-05X Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-06A Amber-A.5 INTACT 24-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - SUB TRANSFER - SUB Dianne Janak Comments: Sent to GeoTesting Express
L1215002-06A Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-07A Amber-A.1 INTACT 27-AUG-12 CUSTODY A2-METALS PREP Bruce Hutchings A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Bruce Hutchings
L1215002-07A Amber-A.1 INTACT 27-AUG-12 A2-CUSTODY A2-CUSTODY-NOAA3 Bruce Hutchings A2-METALS PREP A2-METALS PREP Bruce Hutchings
L1215002-07A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-WET CHEMISTRY Kathy Bates A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Kathy Bates
L1215002-07A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-CUSTODY-NOAA3 Kathy Bates A2-WET CHEMISTRY A2-WET CHEMISTRY Kathy Bates
L1215002-07A Amber-A.1 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Dianne Janak
L1215002-07A Amber-A.1 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
Page 15 of 296
Transaction From ToContainer ID Type Status Date Response Location Operator Response Location Operator
L1215002-07E Amber-A.25 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-07E Amber-A.25 INTACT 29-AUG-12 WETCHEM WETCHEM John D'Apollo CUSTODY CUSTODY John D'Apollo
L1215002-07E Amber-A.25 INTACT 29-AUG-12 CUSTODY CUSTODY John D'Apollo WETCHEM WETCHEM John D'Apollo
L1215002-07E Amber-A.25 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-07E Amber-A.25 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-07E Amber-A.25 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-07F Glass-A.06 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-07F Glass-A.06 INTACT 25-AUG-12 WETCHEM WETCHEM Marc Pollard CUSTODY CUSTODY Marc Pollard
L1215002-07F Glass-A.06 INTACT 25-AUG-12 CUSTODY CUSTODY Marc Pollard WETCHEM WETCHEM Marc Pollard
L1215002-07F Glass-A.06 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-07F Glass-A.06 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-07F Glass-A.06 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-07X Amber-A.5 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-FREEZ-1 A2-CUSTODY-FREEZ-1 Dianne Janak
L1215002-07X Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-08A Amber-A.5 INTACT 24-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - SUB TRANSFER - SUB Dianne Janak Comments: Sent to GeoTesting Express
L1215002-08A Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-09A Amber-A.1 INTACT 27-AUG-12 CUSTODY A2-METALS PREP Bruce Hutchings A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Bruce Hutchings
L1215002-09A Amber-A.1 INTACT 27-AUG-12 A2-CUSTODY A2-CUSTODY-NOAA3 Bruce Hutchings A2-METALS PREP A2-METALS PREP Bruce Hutchings
L1215002-09A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-WET CHEMISTRY Kathy Bates A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Kathy Bates
L1215002-09A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-CUSTODY-NOAA3 Kathy Bates A2-WET CHEMISTRY A2-WET CHEMISTRY Kathy Bates
L1215002-09A Amber-A.1 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Dianne Janak
L1215002-09A Amber-A.1 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-09E Amber-A.25 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-09E Amber-A.25 INTACT 29-AUG-12 WETCHEM WETCHEM John D'Apollo CUSTODY CUSTODY John D'Apollo
Page 16 of 296
Transaction From ToContainer ID Type Status Date Response Location Operator Response Location Operator
L1215002-09E Amber-A.25 INTACT 29-AUG-12 CUSTODY CUSTODY John D'Apollo WETCHEM WETCHEM John D'Apollo
L1215002-09E Amber-A.25 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-09E Amber-A.25 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-09E Amber-A.25 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-09F Glass-A.06 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-09F Glass-A.06 INTACT 25-AUG-12 WETCHEM WETCHEM Marc Pollard CUSTODY CUSTODY Marc Pollard
L1215002-09F Glass-A.06 INTACT 25-AUG-12 CUSTODY CUSTODY Marc Pollard WETCHEM WETCHEM Marc Pollard
L1215002-09F Glass-A.06 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-09F Glass-A.06 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-09F Glass-A.06 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-09X Amber-A.5 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-FREEZ-1 A2-CUSTODY-FREEZ-1 Dianne Janak
L1215002-09X Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-10A Amber-A.5 INTACT 24-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - SUB TRANSFER - SUB Dianne Janak Comments: Sent to GeoTesting Express
L1215002-10A Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-11A Amber-A.1 INTACT 27-AUG-12 CUSTODY A2-METALS PREP Bruce Hutchings A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Bruce Hutchings
L1215002-11A Amber-A.1 INTACT 27-AUG-12 A2-CUSTODY A2-CUSTODY-NOAA3 Bruce Hutchings A2-METALS PREP A2-METALS PREP Bruce Hutchings
L1215002-11A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-WET CHEMISTRY Kathy Bates A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Kathy Bates
L1215002-11A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-CUSTODY-NOAA3 Kathy Bates A2-WET CHEMISTRY A2-WET CHEMISTRY Kathy Bates
L1215002-11A Amber-A.1 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Dianne Janak
L1215002-11A Amber-A.1 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-11E Amber-A.25 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-11E Amber-A.25 INTACT 29-AUG-12 WETCHEM WETCHEM John D'Apollo CUSTODY CUSTODY John D'Apollo
L1215002-11E Amber-A.25 INTACT 29-AUG-12 CUSTODY CUSTODY John D'Apollo WETCHEM WETCHEM John D'Apollo
L1215002-11E Amber-A.25 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
Page 17 of 296
Transaction From ToContainer ID Type Status Date Response Location Operator Response Location Operator
L1215002-11E Amber-A.25 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-11E Amber-A.25 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-11F Glass-A.06 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-11F Glass-A.06 INTACT 25-AUG-12 WETCHEM WETCHEM Marc Pollard CUSTODY CUSTODY Marc Pollard
L1215002-11F Glass-A.06 INTACT 25-AUG-12 CUSTODY CUSTODY Marc Pollard WETCHEM WETCHEM Marc Pollard
L1215002-11F Glass-A.06 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-11F Glass-A.06 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-11F Glass-A.06 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-12A Amber-A.5 INTACT 24-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - SUB TRANSFER - SUB Dianne Janak Comments: Sent to GeoTesting Express
L1215002-12A Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-13A Amber-A.1 INTACT 27-AUG-12 CUSTODY A2-METALS PREP Bruce Hutchings A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Bruce Hutchings
L1215002-13A Amber-A.1 INTACT 27-AUG-12 A2-CUSTODY A2-CUSTODY-NOAA3 Bruce Hutchings A2-METALS PREP A2-METALS PREP Bruce Hutchings
L1215002-13A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-WET CHEMISTRY Kathy Bates A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Kathy Bates
L1215002-13A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-CUSTODY-NOAA3 Kathy Bates A2-WET CHEMISTRY A2-WET CHEMISTRY Kathy Bates
L1215002-13A Amber-A.1 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Dianne Janak
L1215002-13A Amber-A.1 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-13E Amber-A.25 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-13E Amber-A.25 INTACT 29-AUG-12 WETCHEM WETCHEM John D'Apollo CUSTODY CUSTODY John D'Apollo
L1215002-13E Amber-A.25 INTACT 29-AUG-12 CUSTODY CUSTODY John D'Apollo WETCHEM WETCHEM John D'Apollo
L1215002-13E Amber-A.25 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-13E Amber-A.25 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-13E Amber-A.25 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-13F Glass-A.06 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-13F Glass-A.06 INTACT 25-AUG-12 WETCHEM WETCHEM Marc Pollard CUSTODY CUSTODY Marc Pollard
Page 18 of 296
Transaction From ToContainer ID Type Status Date Response Location Operator Response Location Operator
L1215002-13F Glass-A.06 INTACT 25-AUG-12 CUSTODY CUSTODY Marc Pollard WETCHEM WETCHEM Marc Pollard
L1215002-13F Glass-A.06 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-13F Glass-A.06 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-13F Glass-A.06 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-13X Amber-A.5 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-FREEZ-1 A2-CUSTODY-FREEZ-1 Dianne Janak
L1215002-13X Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-14A Amber-A.5 INTACT 24-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - SUB TRANSFER - SUB Dianne Janak Comments: Sent to GeoTesting Express
L1215002-14A Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-15A Amber-A.1 INTACT 27-AUG-12 CUSTODY A2-METALS PREP Bruce Hutchings A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Bruce Hutchings
L1215002-15A Amber-A.1 INTACT 27-AUG-12 A2-CUSTODY A2-CUSTODY-NOAA3 Bruce Hutchings A2-METALS PREP A2-METALS PREP Bruce Hutchings
L1215002-15A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-WET CHEMISTRY Kathy Bates A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Kathy Bates
L1215002-15A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-CUSTODY-NOAA3 Kathy Bates A2-WET CHEMISTRY A2-WET CHEMISTRY Kathy Bates
L1215002-15A Amber-A.1 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Dianne Janak
L1215002-15A Amber-A.1 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-15E Amber-A.25 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-15E Amber-A.25 INTACT 29-AUG-12 WETCHEM WETCHEM John D'Apollo CUSTODY CUSTODY John D'Apollo
L1215002-15E Amber-A.25 INTACT 29-AUG-12 CUSTODY CUSTODY John D'Apollo WETCHEM WETCHEM John D'Apollo
L1215002-15E Amber-A.25 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-15E Amber-A.25 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-15E Amber-A.25 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-15F Glass-A.06 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-15F Glass-A.06 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-15F Glass-A.06 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-15F Glass-A.06 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
Page 19 of 296
Transaction From ToContainer ID Type Status Date Response Location Operator Response Location Operator
L1215002-15F1 Glass-A.06 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-15F1 Glass-A.06 INTACT 25-AUG-12 WETCHEM WETCHEM Marc Pollard CUSTODY CUSTODY Marc Pollard
L1215002-15F1 Glass-A.06 INTACT 25-AUG-12 CUSTODY CUSTODY Marc Pollard WETCHEM WETCHEM Marc Pollard
L1215002-15F1 Glass-A.06 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-15F1 Glass-A.06 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-15F1 Glass-A.06 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-15X Amber-A.5 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-FREEZ-1 A2-CUSTODY-FREEZ-1 Dianne Janak
L1215002-15X Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-16A Amber-A.5 INTACT 24-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - SUB TRANSFER - SUB Dianne Janak Comments: Sent to GeoTesting Express
L1215002-16A Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-16D Amber-A.5 INTACT 24-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - SUB TRANSFER - SUB Dianne Janak Comments: Sent to GeoTesting Express
L1215002-16D Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-17A Amber-A.1 INTACT 27-AUG-12 CUSTODY A2-METALS PREP Bruce Hutchings A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Bruce Hutchings
L1215002-17A Amber-A.1 INTACT 27-AUG-12 A2-CUSTODY A2-CUSTODY-NOAA3 Bruce Hutchings A2-METALS PREP A2-METALS PREP Bruce Hutchings
L1215002-17A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-WET CHEMISTRY Kathy Bates A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Kathy Bates
L1215002-17A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-CUSTODY-NOAA3 Kathy Bates A2-WET CHEMISTRY A2-WET CHEMISTRY Kathy Bates
L1215002-17A Amber-A.1 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Dianne Janak
L1215002-17A Amber-A.1 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-17E Amber-A.25 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-17E Amber-A.25 INTACT 29-AUG-12 WETCHEM WETCHEM John D'Apollo CUSTODY CUSTODY John D'Apollo
L1215002-17E Amber-A.25 INTACT 29-AUG-12 CUSTODY CUSTODY John D'Apollo WETCHEM WETCHEM John D'Apollo
L1215002-17E Amber-A.25 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-17E Amber-A.25 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
Page 20 of 296
Transaction From ToContainer ID Type Status Date Response Location Operator Response Location Operator
L1215002-17E Amber-A.25 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-17F Glass-A.06 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-17F Glass-A.06 INTACT 25-AUG-12 WETCHEM WETCHEM Marc Pollard CUSTODY CUSTODY Marc Pollard
L1215002-17F Glass-A.06 INTACT 25-AUG-12 CUSTODY CUSTODY Marc Pollard WETCHEM WETCHEM Marc Pollard
L1215002-17F Glass-A.06 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-17F Glass-A.06 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-17F Glass-A.06 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-17X Amber-A.5 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-FREEZ-1 A2-CUSTODY-FREEZ-1 Dianne Janak
L1215002-17X Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-18A Amber-A.5 INTACT 24-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - SUB TRANSFER - SUB Dianne Janak Comments: Sent to GeoTesting Express
L1215002-18A Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-19A Amber-A.1 INTACT 27-AUG-12 CUSTODY A2-METALS PREP Bruce Hutchings A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Bruce Hutchings
L1215002-19A Amber-A.1 INTACT 27-AUG-12 A2-CUSTODY A2-CUSTODY-NOAA3 Bruce Hutchings A2-METALS PREP A2-METALS PREP Bruce Hutchings
L1215002-19A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-WET CHEMISTRY Kathy Bates A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Kathy Bates
L1215002-19A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-CUSTODY-NOAA3 Kathy Bates A2-WET CHEMISTRY A2-WET CHEMISTRY Kathy Bates
L1215002-19A Amber-A.1 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Dianne Janak
L1215002-19A Amber-A.1 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-19E Amber-A.25 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-19E Amber-A.25 INTACT 29-AUG-12 WETCHEM WETCHEM John D'Apollo CUSTODY CUSTODY John D'Apollo
L1215002-19E Amber-A.25 INTACT 29-AUG-12 CUSTODY CUSTODY John D'Apollo WETCHEM WETCHEM John D'Apollo
L1215002-19E Amber-A.25 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-19E Amber-A.25 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-19E Amber-A.25 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-19F Glass-A.06 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
Page 21 of 296
Transaction From ToContainer ID Type Status Date Response Location Operator Response Location Operator
L1215002-19F Glass-A.06 INTACT 25-AUG-12 WETCHEM WETCHEM Marc Pollard CUSTODY CUSTODY Marc Pollard
L1215002-19F Glass-A.06 INTACT 25-AUG-12 CUSTODY CUSTODY Marc Pollard WETCHEM WETCHEM Marc Pollard
L1215002-19F Glass-A.06 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-19F Glass-A.06 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-19F Glass-A.06 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-19X Amber-A.5 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-FREEZ-1 A2-CUSTODY-FREEZ-1 Dianne Janak
L1215002-19X Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-20A Amber-A.5 INTACT 24-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - SUB TRANSFER - SUB Dianne Janak Comments: Sent to GeoTesting Express
L1215002-20A Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-21A Amber-A.1 INTACT 27-AUG-12 CUSTODY A2-METALS PREP Bruce Hutchings A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Bruce Hutchings
L1215002-21A Amber-A.1 INTACT 27-AUG-12 A2-CUSTODY A2-CUSTODY-NOAA3 Bruce Hutchings A2-METALS PREP A2-METALS PREP Bruce Hutchings
L1215002-21A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-WET CHEMISTRY Kathy Bates A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Kathy Bates
L1215002-21A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-CUSTODY-NOAA3 Kathy Bates A2-WET CHEMISTRY A2-WET CHEMISTRY Kathy Bates
L1215002-21A Amber-A.1 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Dianne Janak
L1215002-21A Amber-A.1 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-21E Amber-A.25 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-21E Amber-A.25 INTACT 29-AUG-12 WETCHEM WETCHEM John D'Apollo CUSTODY CUSTODY John D'Apollo
L1215002-21E Amber-A.25 INTACT 29-AUG-12 CUSTODY CUSTODY John D'Apollo WETCHEM WETCHEM John D'Apollo
L1215002-21E Amber-A.25 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-21E Amber-A.25 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-21E Amber-A.25 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-21F Glass-A.06 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-21F Glass-A.06 INTACT 25-AUG-12 WETCHEM WETCHEM Marc Pollard CUSTODY CUSTODY Marc Pollard
L1215002-21F Glass-A.06 INTACT 25-AUG-12 CUSTODY CUSTODY Marc Pollard WETCHEM WETCHEM Marc Pollard
Page 22 of 296
Transaction From ToContainer ID Type Status Date Response Location Operator Response Location Operator
L1215002-21F Glass-A.06 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-21F Glass-A.06 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-21F Glass-A.06 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-21X Amber-A.5 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-FREEZ-1 A2-CUSTODY-FREEZ-1 Dianne Janak
L1215002-21X Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-22A Amber-A.5 INTACT 24-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - SUB TRANSFER - SUB Dianne Janak Comments: Sent to GeoTesting Express
L1215002-22A Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-23A Amber-A.1 INTACT 27-AUG-12 CUSTODY A2-METALS PREP Bruce Hutchings A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Bruce Hutchings
L1215002-23A Amber-A.1 INTACT 27-AUG-12 A2-CUSTODY A2-CUSTODY-NOAA3 Bruce Hutchings A2-METALS PREP A2-METALS PREP Bruce Hutchings
L1215002-23A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-WET CHEMISTRY Kathy Bates A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Kathy Bates
L1215002-23A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-CUSTODY-NOAA3 Kathy Bates A2-WET CHEMISTRY A2-WET CHEMISTRY Kathy Bates
L1215002-23A Amber-A.1 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Dianne Janak
L1215002-23A Amber-A.1 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-23E Amber-A.25 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-23E Amber-A.25 INTACT 29-AUG-12 WETCHEM WETCHEM John D'Apollo CUSTODY CUSTODY John D'Apollo
L1215002-23E Amber-A.25 INTACT 29-AUG-12 CUSTODY CUSTODY John D'Apollo WETCHEM WETCHEM John D'Apollo
L1215002-23E Amber-A.25 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-23E Amber-A.25 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-23E Amber-A.25 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-23F Glass-A.06 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-23F Glass-A.06 INTACT 25-AUG-12 WETCHEM WETCHEM Marc Pollard CUSTODY CUSTODY Marc Pollard
L1215002-23F Glass-A.06 INTACT 25-AUG-12 CUSTODY CUSTODY Marc Pollard WETCHEM WETCHEM Marc Pollard
L1215002-23F Glass-A.06 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-23F Glass-A.06 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
Page 23 of 296
Transaction From ToContainer ID Type Status Date Response Location Operator Response Location Operator
L1215002-23F Glass-A.06 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-23X Amber-A.5 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-FREEZ-1 A2-CUSTODY-FREEZ-1 Dianne Janak
L1215002-23X Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-24A Amber-A.5 INTACT 24-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - SUB TRANSFER - SUB Dianne Janak Comments: Sent to GeoTesting Express
L1215002-24A Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-25A Amber-A.1 INTACT 27-AUG-12 CUSTODY A2-METALS PREP Bruce Hutchings A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Bruce Hutchings
L1215002-25A Amber-A.1 INTACT 27-AUG-12 A2-CUSTODY A2-CUSTODY-NOAA3 Bruce Hutchings A2-METALS PREP A2-METALS PREP Bruce Hutchings
L1215002-25A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-WET CHEMISTRY Kathy Bates A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Kathy Bates
L1215002-25A Amber-A.1 INTACT 23-AUG-12 CUSTODY A2-CUSTODY-NOAA3 Kathy Bates A2-WET CHEMISTRY A2-WET CHEMISTRY Kathy Bates
L1215002-25A Amber-A.1 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-NOAA3 A2-CUSTODY-NOAA3 Dianne Janak
L1215002-25A Amber-A.1 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-25E Amber-A.25 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-25E Amber-A.25 INTACT 29-AUG-12 WETCHEM WETCHEM John D'Apollo CUSTODY CUSTODY John D'Apollo
L1215002-25E Amber-A.25 INTACT 29-AUG-12 CUSTODY CUSTODY John D'Apollo WETCHEM WETCHEM John D'Apollo
L1215002-25E Amber-A.25 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-25E Amber-A.25 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-25E Amber-A.25 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-25F Glass-A.06 INTACT 31-AUG-12 CUSTODY CUSTODY Richard Scott R-28 FRIDGE R-28 FRIDGE Richard Scott
L1215002-25F Glass-A.06 INTACT 25-AUG-12 WETCHEM WETCHEM Marc Pollard CUSTODY CUSTODY Marc Pollard
L1215002-25F Glass-A.06 INTACT 25-AUG-12 CUSTODY CUSTODY Marc Pollard WETCHEM WETCHEM Marc Pollard
L1215002-25F Glass-A.06 INTACT 22-AUG-12 TRANSFER - WESTBORO TRANSFER - WESTBORO Richard Scott CUSTODY CUSTODY Richard Scott
L1215002-25F Glass-A.06 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - WESTBORO TRANSFER - WESTBORO Dianne Janak
L1215002-25F Glass-A.06 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-25X Amber-A.5 INTACT 22-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak A2-CUSTODY-FREEZ-1 A2-CUSTODY-FREEZ-1 Dianne Janak
Page 24 of 296
Transaction From ToContainer ID Type Status Date Response Location Operator Response Location Operator
L1215002-25X Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
L1215002-26A Amber-A.5 INTACT 24-AUG-12 CUSTODY A2-CUSTODY-REFRIDGE Dianne Janak TRANSFER - SUB TRANSFER - SUB Dianne Janak Comments: Sent to GeoTesting Express
L1215002-26A Amber-A.5 INTACT 22-AUG-12 A2-LOGIN A2-LOGIN Dianne Janak A2-CUSTODY-REFRIDGE A2-CUSTODY-REFRIDGE Dianne Janak
Page 25 of 296
Chain of Custody
Page 26 of 296
L 12 I~O()2.
305 W Grand Ave Suite 300, Montvale, New Jersey 07645; ph: 201.930.9690
Client: Newtown Creek Group
* "ft. AN. CH OR\I..;, OE A ::::::::::; ENVIRONMENTAL SAMPLE CHAIN OF CUSTODY
Project: Newtown Creek
COCID:
Sample Custodian:
Lab:
AAL-20120821-163510
dp
Alpha Analytical Labs
CDCCollected # LabSample Field Sample ID Matrix Containers Analytical Program ac'Number Date Time
001 EK002SG.000015.20120821 SE 08/21/2012 09:06 5 Newtown Creek Surface Sediment 0002 EK001SG.000015.20120821 SE 08/21/2012 09:31 5 Newtown Creek Surface Sediment 0003 EK010SG.000015.20120821 SE 08/21/2012 10:14 5 Newtown Creek Surface Sediment 0004 NC071SG.000015.20120821 SE 08/21/2012 10:49 5 Newtown Creek Surface Sediment 0
0 005 NC059SG-000015.20120821 SE 08/21/2012 11:06 5 Newtown Creek Surface Sediment 0'l- 006 NC1059SG.000015-20120821 SE 08/21/2012 11:06 4 Newtown Creek Surface Sediment 0y 007 NC058SG-000015-20120821 SE 08/21/2012 11:33 5 Newtown Creek Surface Sediment 0(., 008 NC046SG-000015.20120821 SE 08/21/2012 11:57 7 Newtown Creek Surface Sediment [!]If 009 MC006SG-000015.20120821 SE 08/21/2012 13:48 5 Newtown Creek Surface Sediment 0
010 MC002SG.000012-20120821 SE 08/21/2012 14:26 5 Newtown Creek Surface Sediment 0'L 011 EB008SG-000015-20120821 SE 08/21/2012 15:01 5 Newtown Creek Surface Sediment 0<f 012 EB006SG.000015-20120821 SE 08/21/2012 15:32 5 Newtown Creek Surface Sediment 0
013 EK021SG-000015.20120821 SE 08/21/2012 16:07 5 Newtown Creek Surface Sediment 0
/,2-J.r.f5Ct:J
\
7,3'1, I
II, //3. ,15.1t 7,19,20
21.2
2-~.22..S;u.
Comment:
fLet~; c ~ted:
.•.....,\'-t -.M!C'tplLd-.A'<P~'8 122hz oiJ .~fJ1
ece'ved 8 .
11'L\ 4- OatelTime ti /~
8/21'OJ~9~-~~!o?~
eceived 8 .
sig~ur. ~
't?.(,~
Page 1 of 1
Page 27 of 296
FIELD _SAMPLE_IDEB006SG-0000 15-20 121EB006SG-0000 15-20 121EB006SG-0000 15-20 12(EB006SG-000015-2012(EB006SG-000015-2012(EB006SG-000015-2012(EB008SG-000015-2012(EB008SG-000015-2012(EB008SG-0000 15-20 12(EB008SG-000015-2012(EB008SG-000015-2012(EB008SG-000015-2012(EKOO1SG-OOOO15-20 121EK001 SG-000015-2012(EK001 SG-000015-20121EK001 SG-000015-20121EK001 SG-000015-20121EK001 SG-000015-20121EK002SG-000015-2012(EK002SG-000015-2012(EK002SG-000015-2012(EK002SG-000015-2012(EK002SG-000015-2012(EK002SG-000015-2012(EK010SG-000015-2012(EK010SG-000015-2012(EK010SG-000015-2012(EK010SG-000015-2012(EK010SG-000015-2012(EK010SG-000015-2012(EK021 SG-OOOO15-20 121EK021 SG-000015-20121EK021 SG-OOOO15-20 121EK021 SG-OOOO15-20 121EK021 SG-000015-20121EK021 SG-000015-20121MC002SG-000012-2012MC002SG-000012-2012MC002SG-000012-2012MC002SG-000012-2012MC002SG-000012-2012MC002SG-000012-2012MC006SG-000015-2012
MATRIXSESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESE
SAMPLE SAMPLE_DATE _TIME TEST_REQUEST8/21/2012 15:32 Ammonia8/21/2012 15:32 Archive8/21/2012 15:32 Grainsize8/21/2012 15:32 Iron & manganese8/21/2012 15:32 Sulfide8/21/2012 15:32 TOC8/21/2012 15:01 Ammonia8/21/2012 15:01 Archive8/21/2012 15:01 Grainsize8/21/2012 15:01 Iron & manganese8/21/2012 15:01 Sulfide8/21/2012 15:01 TOC8/21/2012 9:31 Ammonia8/21/2012 9:31 Archive8/21/2012 9:31 Grainsize8/21/2012 9:31 Iron & manganese8/21/2012 9:31 Sulfide8/21/2012 9:31 TOC8/21/2012 9:06 Ammonia8/21/2012 9:06 Archive8/21/2012 9:06 Grainsize8/21/2012 9:06 Iron & manganese8/21/2012 9:06 Sulfide8/21/2012 9:06 TOC8/21/2012 10:14 Ammonia8/21/2012 10:14 Archive8/21/2012 10:14 Grainsize8/21/2012 10:14 Iron & manganese8/21/2012 10:14 Sulfide8/21/2012 10:14 TOC8/21/2012 16:07 Ammonia8/21/2012 16:07 Archive8/21/2012 16:07 Grainsize8/21/2012 16:07 Iron & manganese8/21/2012 16:07 Sulfide8/21/2012 16:07 TOC8/21/2012 14:26 Ammonia8/21/2012 14:26 Archive8/21/2012 14:26 Grainsize8/21/2012 14:26 Iron & manganese8/21/2012 14:26 Sulfide8/21/2012 14:26 TOC8/21/2012 13:48 Ammonia
METHODSM4500NH3HNAASTM 0422EPA 6010B/6020EPA 9030BEPA 9060SM4500NH3HNAASTM 0422EPA 6010B/6020EPA 9030BEPA 9060
, SM4500NH3HNAASTM 0422EPA 601OB/6020EPA 9030BEPA 9060SM4500NH3HNAASTM 0422EPA 601 OB/6020EPA 9030BEPA 9060SM4500NH3HNAASTM 0422EPA 601 OB/6020EPA 9030BEPA 9060SM4500NH3HNAASTM 0422EPA 601 OB/6020EPA 9030BEPA 9060SM4500NH3HNAASTM 0422EPA 601 OB/6020EPA 9030BEPA 9060SM4500NH3H
Page 1 of 2
TURN_A CONTAINROUND_ TAT_UN ER_COUTIME IT NT30 DAYS 0-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0
SAMPLE_CUSTO
LAB_QC COC_ID DIANNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL -20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dp
Page 28 of 296
MATRIXSESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESE
FIELD_SAMPLE_IDMC006SG-000015-2012MC006SG-000015-2012MC006SG-000015-2012MC006SG-000015-2012MC006SG-000015-2012NC046SG-000015-2012'NC046SG-000015-2012'NC046SG-000015-2012'NC046SG-000015-2012'NC046SG-000015-2012'NC046SG-0000 15-20 12'NC058SG-000015-2012'
; NC058SG-000015-2012' ;NC058SG-000015-2012'NC058SG-000015-2012'NC058SG-000015-2012'NC058SG-000015-2012'NC059SG-0000 15-20 12'NC059SG-000015-2012'NC059SG-000015-2012'NC059SG-000015-2012'NC059SG-000015-2012'NC059SG-000015-2012'NC071 SG-000015-2012'NC071 SG-000015-2012'NC071 SG-OOOO15-20 12'NC071 SG-000015-2012'NC071 SG-000015-2012'NC071 SG-000015-2012'NC1 059SG-000015-201;NC1 059SG-000015-201;NC 1059SG-0000 15-201:NC1 059SG-000015-201,NC1 059SG-000015-201,
SAMPLE SAMPLE_DATE _TIME TEST_REQUEST8/21/2012 13:48 Archive8/21/2012 13:48 Grainsize8/21/2012 13:48 Iron & manganese8/21/2012 13:48 Sulfide8/21/2012 13:48 TOC8/21/2012 11 :57 Ammonia8/21/2012 11 :57 Archive8/21/2012 11 :57 Grainsiie8/21/2012 11 :57 Iron & manganese8/21/2012 11 :57 Sulfide8/21/2012 11 :57 TOC8/21/2012 11 :33 Ammonia8/21/2012 11:33 Archive8/21/2012 11 :33 Grainsize8/21/2012 11 :33 Iron & manganese8/21/2012 11 :33 Sulfide8/21/201211:33 TOC8/21/2012 11 :06 Ammonia8/21/2012 11 :06 Archive8/21/2012 11 :06 Grainsize8/21/2012 11 :06 Iron & manganese8/21/2012 11 :06 Sulfide8/21/2012 11:06 TOC8/21/2012 10:49 Ammonia8/21/2012 10:49 Archive8/21/2012 10:49 Grainsize8/21/2012 10:49 Iron & manganese8/21/2012 10:49 Sulfide8/21/2012 10:49 TOC8/21/2012 11 :06 Ammonia8/21/2012 11 :06 Grainsize8/21/2012 11 :06 Iron & manganese8/21/2012 11 :06 Sulfide8/21/2012 11 :06 TOC
METHODNAASTM 0422EPA 60108/6020EPA 90308EPA 9060SM4500NH3HNAASTM 0422EPA 60108/6020EPA 90308EPA 9060SM4500NH3HNAASTM 0422EPA 60108/6020EPA 90308EPA 9060SM4500NH3HNAASTM 0422EPA 60108/6020EPA 90308EPA 9060SM4500NH3HNAASTM 0422EPA 60108/6020EPA 90308EPA 9060SM4500NH3HASTM 0422EPA 60108/6020EPA 90308EPA 9060
Page 2 of 2
TURN_A CONTAINROUND_ TAT_UN ER_COUTIME IT NT-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0-1 DAYS 130 DAYS 230 DAYS 130 DAYS 230 DAYS 130 DAYS 0-1; DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 030 DAYS 130 DAYS 130 DAYS 130 DAYS 1
SAMPLE_CUSTO
LA8_QC COC_ID DIANNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpYES AAL-20120821-163510 dpYES AAL-20120821-163510 dpYES AAL-20120821-163510 dpYES AAL-20120821-163510 dpYES AAL-20120821-163510 dpYES AAL-20120821-163510 dpNO AAL-20120821-163510 dp
; NO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dp
Page 29 of 296
CHAIN OF CUSTODY PAGE1 OF'1 Date Rec'd in Lab:
!-iA.ANALYTICAL
Project Name: Newtown CreekWestborough,MATEL: 508-898-9220
FAX: 508-898-9193
Mansfield,MATEL: 508-822-9300
FAX: 508-822-3288
••..••• ra .1iut:U['
""
.'."IeI.
o FAX
o ADEx
-r:r.mF.ll'i1'i'lll:(:lo
Add'i Deliverables
al.""_.!"I.l.I.
Please provide ANCHOR EQUIS EDD and reference Newtown Creek
Other Project Specific Requirements/CommentslDetection Limits:
IS YOUR PROJECTMA MCP or CT RCP?
Client: Alpha Analytical
Address: 320 Forbes Blvd,Mansfield, MA 02048
Phone: 508-844-4122
Fax: 508-822-3288:,Email: [email protected]
o Thesesampleshavebeenpr~viOUSlyanalyzedbyAlpha
Sample SpecificComments •L1215002-02 1
L1215002-04 1
L1215002-06 1
L1215002-08 1
L1215002-10 1
SAMPLEHANDLINGFiltration
o Doneo Nol Neededo LabIa doPresetVation
o Lablodo(Please specifybelow)
L1215002-12
L1215002-14
L1215002-16
L1215002-18
L1215002-20
'~Il~~~"lurryai1:i(;rii;ltj~9~ willnot ,'.". fll!.r1'~~I,.,~nY.¥!Ji9jgUitieSa~~o;;r"S()!,ve(j,A1I.s~,~ples\> :':~u9!"itt.••d,i:I~,,-S,ub~I~'"-Alpha'sPaymenlTeims:' "
0 0 00 0 00 0 00 0 00 0 00 0 00 0 00 0 00 0 00 0 0. . .
. - .
Datemme
Criteria
Received By:
-"ml~'m.tJ=rn-1.RMiI!"ler.l"I::II.l~"[eI::II~:I.}i'.IiI.Are MCPAnalytical Methods Reguired?Are CT RCP (Reasonable Confidence Protocolsl Reauired?
o No
o No
ANALYSIS
DYes
DYes
MCP PRESUMPTIV
State/Fed Prooram
\
I I I I I I I I,
NN"!'I:)
:2I- W(/) I-« «w <..>N ::::iu; Q.
::>z I:)
~ 0Cl a
I I I I I I I
[gI 0 0 0 0 0 0 0 0[gI 0 0 0 0 0 0 0 0[gI 0 0 0 0 0 0 0 0[gI 0 0 0 0 0 0 0 0[gI 0 0 0 0, 0 0 0 0!Xl 0 0 0 0 D 0 0 0[gI 0 0 0 0 0 0 0 0[gI [gI 0- 0 0 0 0 0 0[gI 0 0 0 0 0 0 0 0[gI 0 0 0 0 0 0 0 0
. . .
- I--, .
ished By:
Time:
Sample I Sampler'sMatrix Initials
8/21112 0906 se'diment
8/21/12 0931 sediment
8/21/12 1014 sediment
8/21/12 1049 sediment
8/21/12 1106 sediment
8/21/12 1106 sediment
8/21/12 1133 sediment
8/21/12 1133 sediment
8/21/12 1348 sediment
8/21112 1426 sedimenti
Container Type
• Preservative
Due Date:
ALPHA Quote #.
Turn-Around Time
~ Standard 0 Rush (ONLYIF PRE-APPROVED)
Project Location:
Project#:
Proiect Manaaer: Chris Anderson
Sample ID-
ALPHA Lab ID.-.(L~b'U~'eon!~)A
FORM NO; 01-01(1)(reY.30-JUl-07)
EK002SG-000015-20120821
EK001 SG-000015-20120821
EK010SG-000015-20120821
NC071 SG-000015-20120821
NC059SG-000015-20120821
NC1059SG-000015-20120821
NC058SG-000015-20120821
NC046SG-000015-20120821
MC006SG-000015-20120821
MC002SG-000012-20120821
PLEASE ANSWER QUESTIONS ABOVE!
Page 30 of 296
Sample SpecificComments
SAMPLE HANDLING
Filtrationo Done
o Nol Neededo Lilblodo
Preservation
o Lablodo(Please specifybelow)
L1215002-22
L1215002-24
L1215002-26
DYesDYes
ANALYSIS
Time:
NNv0:2I-U)«wN
Sampler'sCi5Z
Initials ~C>
sediment ~ 0 0 0 0 0 0 0 0 0 0 0sediment ~ 0 0 0 0 0 0 0 0 0 0 0sediment ~ 0 0 0 0 0 0 0 0 0 0 0
0 0 0 0 0 0 0 0 0 0 0 0.0 0 0 0 0' 0 0 0 0 0 0 00 0 0 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 0 0 0 0
Container Type
Preservative
Receive.d By: DaterTime
o Rush (ONLY IF PRE.APPROVED)
1607
1532
15018/21/12
8/21/12
8/21/12
~ Standard
ALPHAQ t #
Due Date:
Project Location:
Pro'ect#:
• ¥. ~ , .' : ' - ~ '" .'. .."
ifurn-Around Time ,,' ."A,~'''',,',
CHAIN OF CUSTODY
Sample 10
EB008SG-000015-20120821
EB006SG-000015-20120821
EK021 SG-000015-20120821
I-iANAlYT1CAL
Please provide ANCHOR EQUIS EDO and reference Newtown Creek
Fax: 508-824-3288
Email: [email protected]
o These samples have been Previously analyzed by Alpha
Other Project Specific Requirements/Comments/Detection Limits:
Address: 320 Forbes Blvd
Mansfield, MA 02048
Phone: 508-844-4122
ALPHALabID;(Lab Use Oilly)'
FORM NO: 01-01(1)(re ••..30-JUL.Qr)
PLEASE ANSWER QUESTIONS ABOVE!
IS YOUR PROJECTMA MCP or CT RCP?
Page 31 of 296
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Metals
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ICPMS Analysis
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Sequence Logs
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Work Group
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ALPHA ANALYTICAL LABORATORIES, INC. Metals Batch Report - Total Metals (Mass Spec) - A2-6020T Batch WG557278 for dept. 5
Aug 31, 2012 14:08
As Ba Cd Cu Ni Ag Tl Ti Fe Ca Mg Na V Si Ha Zr Sample No. Client No. Sample I.D. Mat Due Sb B Be Cr Pb Se Sr Sn Zn Mn Al K Co Mo W W 60 _______________________________________________________________________________________________________________________________________________________________________________
L1215002-01 EK002SG-000015-20 3 0918 X X
L1215002-03 EK001SG-000015-20 3 0918 X X
L1215002-05 EK010SG-000015-20 3 0918 X X
L1215002-07 NC071SG-000015-20 3 0918 X X
L1215002-09 NC059SG-000015-20 3 0918 X X
L1215002-11 NC1059SG-000015-2 3 0918 X X
L1215002-13 NC058SG-000015-20 3 0918 X X
L1215002-15 NC046SG-000015-20 3 0918 X X
L1215002-17 MC006SG-000015-20 3 0918 X X
L1215002-19 MC002SG-000012-20 3 0918 X X
L1215002-21 EB008SG-000015-20 3 0918 X X
L1215002-23 EB006SG-000015-20 3 0918 X X
L1215002-25 EK021SG-000015-20 3 0918 X X
WG557278-1 Laboratory Method 3 X X
WG557278-2 Laboratory Contro 3 X X
WG557278-3 Duplicate Sample 3 X X
WG557278-4 Matrix Spike 3 X X
WG557278-5 Serial Dilution 3 X X
Comments:
WG557278-3 L1215002-15WG557278-4 L1215002-15WG557278-5 L1215002-15
_______________________________________________________________________________________________________________________________________________________________________________
Page 1
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Tune
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Sample Raw Data
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Digestion Logs ICPMS
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True Values
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Table IV: Initial Calibration Levels and ICV/CCV Concentrations
Analyte STD1 STD2 ICV,CCV (μg/L) (μg/L) (μg/L)
Ag 100 50 Al 10050 5050 As 100 50 B 100 50 Ba 100 50 Be 100 50 Ca 10100 5050 Cd 100 50 Co 100 50 Cr 100 50 Cu 100 50 Fe 10100 5050 K 10000 5500
Mg 10100 5050 Mn 100 50 Mo 100 50 Na 10000 5050 Ni 100 50 Pb 100 50 Sb 100 50 Se 100 50 Si 50 25 Sn 100 50 Sr 100 50 Ti 100 50 Tl 100 50 V 100 50 Zn 100 50
Interferent
ICSA, ICSAB (mg/L)
Cl- 2000 Ca 300
Fe, Na 250 Al, Mg, P, K, S 100
C 200 Mo, Ti 2
All analyte concentrations in ICSAB = 100 ppb except for Ag and Ba = 50 ppb
Page 123 of 296
Analyte LCS,MS
WaterLCS,MS
soilLCS,MS Tissue
(μg/L) (μg/L) (μg/L)
Ag 40 40 40 Al 5000 20000 5000 As 1000 4000 1000 B 1000 4000 1000 Ba 1000 4000 1000 Be 500 2000 500 Ca 5000 4000 5000 Cd 500 2000 500 Co 1000 4000 1000 Cr 1000 4000 1000 Cu 1000 4000 1000 Fe 5000 20000 5000 K 5000 20000 5000
Mg 5000 20000 5000 Mn 1000 4000 1000 Mo 1000 4000 1000 Na 5000 20000 5000 Ni 1000 4000 1000 Pb 1000 4000 1000 Sb 1000 40 1000 Se 1000 4000 1000 Si 1000 4000 1000 Sn 400 400 400 Sr 1000 4000 1000 Ti 1000 4000 1000 Tl 1000 4000 1000 V 1000 4000 1000 Zn 1000 4000 1000
Mercury: ICV, CCV, LCS and MS = 2.5 ppb. Arsenic Hydride, Selenium Hydride: ICV, CCV, LCS and MS = 5 ppb. Mercury by Method 1631: ICV,CCV = 0.005 ppb, LCS, MS = 0.005 ppb.
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Wet Chemistry
Page 125 of 296
Total Solids Analysis
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Sample Raw Data
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ALPHA ANALYTICAL LABS Last Change 04/09/09 GFF
WET CHEMISTRY DEPARTMENT File A2-TS_S.xltPERCENT TOTAL SOLIDS
Sample Number: _________________ Product: A2-TSAnalyte: Solids, Total
Client: _______________ Analysis Date: 8/23/2012 11:45Technician: KB
Analysis: %TOTAL SOLIDS Work group: WG556644in solids MDL: 0.10%
Method: STM 2540-B
105 degrees CTare Gross Net Net Net Net Net
Weight Weight Weight(1) Weight(2) Weight(3) Weight(4) Weight(5) RESULTSample Number (gm) (gm) (gm) (gm) (gm) (gm) (gm) %
1.32 3.5
1.33 3.14
1.34 2.45
1.32 2.65
1.33 3.05
1.32 3.47
1.32 3.37
1.33 3.09
1.33 3.48
1.32 4.26
1.32 6.1
1.32 2.44
1.34 2.34
1.33 4.5
Comments:
Page 128 of 296
Work Group
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ALPHA ANALYTICAL LABORATORIES, INC.
Alpha WORK GROUP REPORT (wk02)
Aug 25 2012, 08:51 am
Work Group: WG556644 for Department: 7 Wet Chemistry
Created: 23-AUG-12 Due: Operator: KB
Sample Client ID C Product Matrix Stat UA HOLD DUE PR Location ____________________________________________________________________________________________________________________________________
L1215002-01 EK002SG-000015-20120 S A2-TS SOIL DONE U 0828 0918 S0 Amber-A.1 L1215002-03 EK001SG-000015-20120 S A2-TS SOIL DONE U 0828 0918 S0 Amber-A.1 L1215002-05 EK010SG-000015-20120 S A2-TS SOIL DONE U 0828 0918 S0 Amber-A.1 L1215002-07 NC071SG-000015-20120 S A2-TS SOIL DONE U 0828 0918 S0 Amber-A.1 L1215002-09 NC059SG-000015-20120 S A2-TS SOIL DONE U 0828 0918 S0 Amber-A.1 L1215002-11 NC1059SG-000015-2012 S A2-TS SOIL DONE U 0828 0918 S0 Amber-A.1 L1215002-13 NC058SG-000015-20120 S A2-TS SOIL DONE U 0828 0918 S0 Amber-A.1 L1215002-15 NC046SG-000015-20120 S A2-TS SOIL DONE U 0828 0918 S0 Amber-A.1 L1215002-17 MC006SG-000015-20120 S A2-TS SOIL DONE U 0828 0918 S0 Amber-A.1 L1215002-19 MC002SG-000012-20120 S A2-TS SOIL DONE U 0828 0918 S0 Amber-A.1 L1215002-21 EB008SG-000015-20120 S A2-TS SOIL DONE U 0828 0918 S0 Amber-A.1 L1215002-23 EB006SG-000015-20120 S A2-TS SOIL DONE U 0828 0918 S0 Amber-A.1 L1215002-25 EK021SG-000015-20120 S A2-TS SOIL DONE U 0828 0918 S0 Amber-A.1 WG556644-1 Duplicate Sample S A2-TS SOIL DONE U
Comments:
WG556644-1 L1215002-15
____________________________________________________________________________________________________________________________________
Page 1
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Supporting Documentation
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Organic Carbon Analysis
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Sequence Logs
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Sample Raw Data
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ALPHA ANALYTICAL LABS Last Change 04/23/12 TJT
Wet Chemistry Department File A2-TOC9060-2REPS.xltTOTAL ORGANIC CARBON
SOP No.: W-028 Product: A2-TOC-9060-2REPSAnalyte: Total Organic Carbon
Analysis: TOC (2 Reps) Analysis Date: 8/28/2012 9:00Technician: SF
Method: EPA 9060 Work group: WG556725RDL: 0.01%
LCS/SRM Conc. (%): 4.4MS Rep 1 Conc. (%): 1.701 MSD Rep 1 Conc. (%): ____MS Rep 2 Conc. (%): 1.543 MSD Rep 2 Conc. (%): ____ REP1 REP2 FINAL RESULT FINAL RESULT
MDL RESULT RESULT REP1 % REP2 %Sample Number Multiplier mg/Kg mg/Kg COMMENTS
BLANK 0.0 0.0 0.0000
75440.0 92840.0 9.2840
66660.0 60520.0 6.0520
88550.0 86610.0 8.6610
62080.0 61990.0 6.1990
50880.0 50000.0 5.0000
54840.0 54840.0 5.4840
39540.0 37870.0 3.7870
37660.0 38640.0 3.8640
62730.0 62610.0 6.2610
35200.0 31200.0 3.1200
119300.0 110030.0 11.0030
89620.0 87520.0 8.7520
38420.0 37800.0 3.7800
17840.0 18190.0 1.8190
DUP 37900.0 39240.0 3.9240
Sample Number Conc %
REP1
mg/Kg
REP2
mg/KgREP1 Result
%REP2
% % RecoveryREP2 %
Recovery
SRM WG556725-2 4.4 43940 4.3940
Sample Number %
REP1
mg/KgREP2
mg/KgREP1 Result
%REP2
% % RecoveryREP2 %
Recovery
MS WG556725-4 1.701 55460 5.5460 115
1.543
Native Sample Result (%)
Notes
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Work Group
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ALPHA ANALYTICAL LABORATORIES, INC.
Alpha WORK GROUP REPORT (wk02)
Aug 29 2012, 06:20 am
Work Group: WG556725 for Department: 7 Wet Chemistry
Created: 23-AUG-12 Due: Operator: ES
Sample Client ID C Product Matrix Stat UA HOLD DUE PR Location ____________________________________________________________________________________________________________________________________
L1215002-01 EK002SG-000015-20120 S A2-TOC-9060-2REPS SOIL DONE U 0918 0918 S0 Amber-A.1 L1215002-03 EK001SG-000015-20120 S A2-TOC-9060-2REPS SOIL DONE U 0918 0918 S0 Amber-A.1 L1215002-05 EK010SG-000015-20120 S A2-TOC-9060-2REPS SOIL DONE U 0918 0918 S0 Amber-A.1 L1215002-07 NC071SG-000015-20120 S A2-TOC-9060-2REPS SOIL DONE U 0918 0918 S0 Amber-A.1 L1215002-09 NC059SG-000015-20120 S A2-TOC-9060-2REPS SOIL DONE U 0918 0918 S0 Amber-A.1 L1215002-11 NC1059SG-000015-2012 S A2-TOC-9060-2REPS SOIL DONE U 0918 0918 S0 Amber-A.1 L1215002-13 NC058SG-000015-20120 S A2-TOC-9060-2REPS SOIL DONE U 0918 0918 S0 Amber-A.1 L1215002-15 NC046SG-000015-20120 S A2-TOC-9060-2REPS SOIL DONE U 0918 0918 S0 Amber-A.1 L1215002-17 MC006SG-000015-20120 S A2-TOC-9060-2REPS SOIL DONE U 0918 0918 S0 Amber-A.1 L1215002-19 MC002SG-000012-20120 S A2-TOC-9060-2REPS SOIL DONE U 0918 0918 S0 Amber-A.1 L1215002-21 EB008SG-000015-20120 S A2-TOC-9060-2REPS SOIL DONE U 0918 0918 S0 Amber-A.1 L1215002-23 EB006SG-000015-20120 S A2-TOC-9060-2REPS SOIL DONE U 0918 0918 S0 Amber-A.1 L1215002-25 EK021SG-000015-20120 S A2-TOC-9060-2REPS SOIL DONE U 0918 0918 S0 Amber-A.1 L1215002-27 SRM1650B S A2-TOC-9060-2REPS SOIL DONE U 0918 0918 S0 Glass-A.1 WG556725-1 Laboratory Method Bl S A2-TOC-9060-2REPS SOIL DONE U WG556725-2 Standard Reference M S A2-TOC-9060-2REPS SOIL DONE U WG556725-3 Duplicate Sample S A2-TOC-9060-2REPS SOIL DONE U WG556725-4 Matrix Spike S A2-TOC-9060-2REPS SOIL DONE U
Comments:
WG556725-3 L1215002-15WG556725-4 L1215002-15
____________________________________________________________________________________________________________________________________
Page 1
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Sample Preparation
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Total Sulfide Analysis
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Sample Raw Data
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ALPHA ANALYTICAL Last Change 10/29/10
WET CHEMISTRY DEPARTMENT File Sulfide-Total-S.xltSULFIDE, TOTAL
SOP No.: 07-30 Product: SULFIDE-9030Curve Calibration Date : 3/6/2012
Curve Identifier: 030612aAnalysis: Method:
Instrument: Wavelength: 664 nm Work group: wg557078
LCS Volume(ml): 1.0 RDL: 0.5 mg/kgLCS/MS Concentration (mg/l): 65.820 Cell: 1 cm
MS/MSD Volume(ml): 2
Standard ID Peak Area Dilution Calibration Curve ug/100ml abs Volume: 50ml
43.88 0.337 1.0 0.007129 0.015454722 r-919
Sulfide 1 Reagent:
ICV/LCS Concentration (mg/kg): 6.58 0.2N NaOH:
Sample FINALWeight Conc. Dilution RDL RESULT
Time Date Sample number (gm) Absorbance (ug S/100ml) Factor Multiplier (mg/kg)1:12pm 8/25/2012 10 0.326 1 Recovery1:13pm 8/25/20121:22pm 8/25/20121:14pm 8/25/20121:14pm 8/25/20121:15pm 8/25/20121:15pm 8/25/20121:22pm 8/25/20121:16pm 8/25/20121:17pm 8/25/20121:16pm 8/25/20123:21pm 8/25/20123:31pm 8/25/20123:22pm 8/25/20123:22pm 8/25/20123:23pm 8/25/20123:23pm 8/25/20123:24pm 8/25/20123:24pm 8/25/2012
1:12pm 8/25/20123:25pm 8/25/2012 10 35.060 200 DUP
Sample Sample Dilution Spike conc. RDL Spike RecoverySample number weight Absorbance Result mg/kg Factor mg/kg Multiplier Result mg/kg %
3:27pm 8/25/2012 10 691.46 13.16 766.15#DIV/0! #VALUE!
1:13pm 8/25/2012 10 6.58 5.26
Reagents/Media Information
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COMMENTS & OBSERVATIONS
BLANKICV/LCSL1215002-01L1215002-03L1215002-05L1215002-07L1215002-09L1215002-11ccbccvL1215002-13L1215002-15L1215002-17L1215002-19L1215002-21L1215002-23L1215002-25ccbccv
000000000
WG557078-1WG557078-3
WG557078-40
WG557078-2
Page 167 of 296
Work Group
Page 168 of 296
ALPHA ANALYTICAL LABORATORIES, INC.
Alpha WORK GROUP REPORT (wk02)
Sep 04 2012, 10:34 am
Work Group: WG557078 for Department: 7 Wet Chemistry
Created: 25-AUG-12 Due: Operator: mp
Sample Client ID C Product Matrix Stat UA HOLD DUE PR Location ____________________________________________________________________________________________________________________________________
L1215002-01 EK002SG-000015-20120 S SULFIDE-9030 SOIL DONE U 0828 0918 S0 Glass-A.06 L1215002-03 EK001SG-000015-20120 S SULFIDE-9030 SOIL DONE U 0828 0918 S0 Glass-A.06 L1215002-05 EK010SG-000015-20120 S SULFIDE-9030 SOIL DONE U 0828 0918 S0 Glass-A.06 L1215002-07 NC071SG-000015-20120 S SULFIDE-9030 SOIL DONE U 0828 0918 S0 Glass-A.06 L1215002-09 NC059SG-000015-20120 S SULFIDE-9030 SOIL DONE U 0828 0918 S0 Glass-A.06 L1215002-11 NC1059SG-000015-2012 S SULFIDE-9030 SOIL DONE U 0828 0918 S0 Glass-A.06 L1215002-13 NC058SG-000015-20120 S SULFIDE-9030 SOIL DONE U 0828 0918 S0 Glass-A.06 L1215002-15 NC046SG-000015-20120 S SULFIDE-9030 SOIL DONE U 0828 0918 S0 Glass-A.06 L1215002-17 MC006SG-000015-20120 S SULFIDE-9030 SOIL DONE U 0828 0918 S0 Glass-A.06 L1215002-19 MC002SG-000012-20120 S SULFIDE-9030 SOIL DONE U 0828 0918 S0 Glass-A.06 L1215002-21 EB008SG-000015-20120 S SULFIDE-9030 SOIL DONE U 0828 0918 S0 Glass-A.06 L1215002-23 EB006SG-000015-20120 S SULFIDE-9030 SOIL DONE U 0828 0918 S0 Glass-A.06 L1215002-25 EK021SG-000015-20120 S SULFIDE-9030 SOIL DONE U 0828 0918 S0 Glass-A.06 WG557078-1 Laboratory Method Bl S SULFIDE-9030 SOIL DONE U WG557078-2 Laboratory Control S S SULFIDE-9030 SOIL DONE U WG557078-3 Duplicate Sample S SULFIDE-9030 SOIL DONE U WG557078-4 Matrix Spike S SULFIDE-9030 SOIL DONE U
Comments:
WG557078-3 L1215002-15WG557078-4 L1215002-15
____________________________________________________________________________________________________________________________________
Page 1
Page 169 of 296
Ammonia Analysis
Page 170 of 296
Sequence Logs
Page 171 of 296
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Sample Raw Data
Page 173 of 296
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Work Group
Page 185 of 296
ALPHA ANALYTICAL LABORATORIES, INC.
Alpha WORK GROUP REPORT (wk02)
Sep 04 2012, 10:34 am
Work Group: WG558038 for Department: 7 Wet Chemistry
Created: 30-AUG-12 Due: Operator: DM
Sample Client ID C Product Matrix Stat UA HOLD DUE PR Location ____________________________________________________________________________________________________________________________________
L1215002-01 EK002SG-000015-20120 S NH3-4500 SOIL DONE U 0918 0918 S0 Amber-A.25 L1215002-03 EK001SG-000015-20120 S NH3-4500 SOIL DONE U 0918 0918 S0 Amber-A.25 L1215002-05 EK010SG-000015-20120 S NH3-4500 SOIL DONE U 0918 0918 S0 Amber-A.25 L1215002-07 NC071SG-000015-20120 S NH3-4500 SOIL DONE U 0918 0918 S0 Amber-A.25 L1215002-09 NC059SG-000015-20120 S NH3-4500 SOIL DONE U 0918 0918 S0 Amber-A.25 L1215002-11 NC1059SG-000015-2012 S NH3-4500 SOIL DONE U 0918 0918 S0 Amber-A.25 L1215002-13 NC058SG-000015-20120 S NH3-4500 SOIL DONE U 0918 0918 S0 Amber-A.25 L1215002-15 NC046SG-000015-20120 S NH3-4500 SOIL DONE U 0918 0918 S0 Amber-A.25 L1215002-17 MC006SG-000015-20120 S NH3-4500 SOIL DONE U 0918 0918 S0 Amber-A.25 L1215002-19 MC002SG-000012-20120 S NH3-4500 SOIL DONE U 0918 0918 S0 Amber-A.25 L1215002-21 EB008SG-000015-20120 S NH3-4500 SOIL DONE U 0918 0918 S0 Amber-A.25 L1215002-23 EB006SG-000015-20120 S NH3-4500 SOIL DONE U 0918 0918 S0 Amber-A.25 L1215002-25 EK021SG-000015-20120 S NH3-4500 SOIL DONE U 0918 0918 S0 Amber-A.25 WG558038-1 Laboratory Method Bl S NH3-4500 SOIL DONE U WG558038-2 Laboratory Control S S NH3-4500 SOIL DONE U WG558038-3 Duplicate Sample S NH3-4500 SOIL DONE U WG558038-4 Matrix Spike S NH3-4500 SOIL DONE U
Comments:
WG558038-3 L1215002-15WG558038-4 L1215002-15
____________________________________________________________________________________________________________________________________
Page 1
Page 186 of 296
Sample Preparation
Page 187 of 296
Page 188 of 296
Alpha Report
Page 189 of 296
L1215002
Anchor QEA, LLC
120782-01.01
NEWTOWN CREEK RI
Client:
Project Name:
Project Number:
09/11/12
320 Forbes Boulevard, Mansfield, MA 02048-1806
Lab Number:
Report Date:
508-822-9300 (Fax) 508-822-3288 800-624-9220 - www.alphalab.com
720 Olive Way
Suite 1900
Delaney PetersonATTN:
ANALYTICAL REPORT
Seattle, WA 98101
Certifications & Approvals: NY (11627), CT (PH-0141), NH (2206), NJ NELAP (MA015), RI (LAO00299), PA (68-02089), LA NELAP (03090),FL (E87814), TX (T104704419), WA (C954), DOD (L2217.01), USDA (Permit #P330-11-00109), US Army Corps of Engineers.
(206) 287-9130Phone:
The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in itsentirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.
Serial_No:09111209:35
Page 1 of 76 Page 190 of 296
L1215002-01
L1215002-02
L1215002-03
L1215002-04
L1215002-05
L1215002-06
L1215002-07
L1215002-08
L1215002-09
L1215002-10
L1215002-11
L1215002-12
L1215002-13
L1215002-14
L1215002-15
L1215002-16
L1215002-17
L1215002-18
L1215002-19
L1215002-20
L1215002-21
L1215002-22
L1215002-23
L1215002-24
L1215002-25
L1215002-26
L1215002-27
Alpha Sample ID
EK002SG-000015-20120821
EK002SG-000015-20120821
EK001SG-000015-20120821
EK001SG-000015-20120821
EK010SG-000015-20120821
EK010SG-000015-20120821
NC071SG-000015-20120821
NC071SG-000015-20120821
NC059SG-000015-20120821
NC059SG-000015-20120821
NC1059SG-000015-20120821
NC1059SG-000015-20120821
NC058SG-000015-20120821
NC058SG-000015-20120821
NC046SG-000015-20120821
NC046SG-000015-20120821
MC006SG-000015-20120821
MC006SG-000015-20120821
MC002SG-000012-20120821
MC002SG-000012-20120821
EB008SG-000015-20120821
EB008SG-000015-20120821
EB006SG-000015-20120821
EB006SG-000015-20120821
EK021SG-000015-20120821
EK021SG-000015-20120821
SRM1650B
Client ID
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Sample Location
NEWTOWN CREEK RI
120782-01.01
Project Name:Project Number:
Lab Number: Report Date:
L121500209/11/12
08/21/12 09:06
08/21/12 09:06
08/21/12 09:31
08/21/12 09:31
08/21/12 10:14
08/21/12 10:14
08/21/12 10:49
08/21/12 10:49
08/21/12 11:06
08/21/12 11:06
08/21/12 11:06
08/21/12 11:06
08/21/12 11:33
08/21/12 11:33
08/21/12 11:57
08/21/12 11:57
08/21/12 13:48
08/21/12 13:48
08/21/12 14:26
08/21/12 14:26
08/21/12 15:01
08/21/12 15:01
08/21/12 15:32
08/21/12 15:32
08/21/12 16:07
08/21/12 16:07
08/21/12 12:00
Collection Date/Time
Serial_No:09111209:35
Page 2 of 76 Page 191 of 296
NEWTOWN CREEK RI
120782-01.01
Project Name:
Project Number:
Lab Number:
Report Date:L1215002
09/11/12
Case Narrative
The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation
or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report.
Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet all of the requirements of
NELAC, for all NELAC accredited parameters. The data presented in this report is organized by parameter (i.e. VOC, SVOC, etc.). Sample
specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list for each individual sample,
followed by the Laboratory Batch Quality Control at the end of each parameter. If a sample was re-analyzed or re-extracted due to a
required quality control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is
designated with an "R" or "RE", respectively. When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the
associated samples for each element are noted in the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific %
recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report. Performance criteria for CAM and RCP methods
allow for some LCS compound failures to occur and still be within method compliance. In these instances, the specific failures are not
narrated but are noted in the associated QC table. This information is also incorporated in the Data Usability format for our Data Merger tool
where it can be reviewed along with any associated usability implications. Soil/sediments, solids and tissues are reported on a dry weight
basis unless otherwise noted. Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the
back of the report.
In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria for CAM and RCP methods allow for some
quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the
associated QC table. The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed
along with any associated usability implications.
Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical
Standards requested on the Chain of Custody.
HOLD POLICY
For samples submitted on hold, Alpha's policy is to hold samples free of charge for 30 days from the date the project is completed. After 30
days, we will dispose of all samples submitted including those put on hold unless you have contacted your Client Service Representative and
made arrangements for Alpha to continue to hold the samples.
Please contact Client Services at 800-624-9220 with any questions.
Serial_No:09111209:35
Page 3 of 76 Page 192 of 296
Case Narrative (continued)
NEWTOWN CREEK RI
120782-01.01
Project Name:
Project Number:
Lab Number:
Report Date:L1215002
09/11/12
Total Metals
All sediment samples have elevated detection limits for all analytes due to the additional dilutions (20x) required
by the elevated concentrations of target analytes in the samples.
The WG557278-4 MS recovery, performed on L1215002-15, is above the acceptance criteria for Total Iron
(193%); however, the spike does not apply because the sample concentration is greater than four times the
spike amount added.
Sulfide
All samples have elevated detection limits due to the dilutions required to quantitate the results within the
calibration range.
The WG557078-4 MS recovery, performed on L1215002-15, is above the acceptance criteria for Sulfide
(430%); however, the spike does not apply because the sample concentration is greater than four times the
spike amount added.
I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report.
Authorized Signature:
Title: Technical Director/Representative Date: 09/11/12
Serial_No:09111209:35
Page 4 of 76 Page 193 of 296
METALS
Serial_No:09111209:35
Page 5 of 76 Page 194 of 296
FF
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
09/11/12
SAMPLE RESULTS
EK002SG-000015-20120821Client ID:08/21/12 09:06Date Collected:08/21/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1215002-01Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Iron, Total
Manganese, Total
34300
219
mg/kg
mg/kg
20
20
367
3.67
08/29/12 09:59
08/29/12 09:59
1,6020A
1,6020A
PD
PD
08/27/12 13:29
08/27/12 13:29
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 26%
D
MDL
37.8
0.816
Serial_No:09111209:35
Page 6 of 76 Page 195 of 296
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
09/11/12
SAMPLE RESULTS
EK001SG-000015-20120821Client ID:08/21/12 09:31Date Collected:08/21/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1215002-03Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Iron, Total
Manganese, Total
33500
219
mg/kg
mg/kg
20
20
437
4.37
08/29/12 10:00
08/29/12 10:00
1,6020A
1,6020A
PD
PD
08/27/12 13:29
08/27/12 13:29
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 22%
D
MDL
45.1
0.973
Serial_No:09111209:35
Page 7 of 76 Page 196 of 296
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
09/11/12
SAMPLE RESULTS
EK010SG-000015-20120821Client ID:08/21/12 10:14Date Collected:08/21/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1215002-05Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Iron, Total
Manganese, Total
32900
200
mg/kg
mg/kg
20
20
456
4.56
08/29/12 10:01
08/29/12 10:01
1,6020A
1,6020A
PD
PD
08/27/12 13:29
08/27/12 13:29
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 22%
D
MDL
47.0
1.01
Serial_No:09111209:35
Page 8 of 76 Page 197 of 296
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
09/11/12
SAMPLE RESULTS
NC071SG-000015-20120821Client ID:08/21/12 10:49Date Collected:08/21/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1215002-07Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Iron, Total
Manganese, Total
37500
304
mg/kg
mg/kg
20
20
398
3.98
08/29/12 10:02
08/29/12 10:02
1,6020A
1,6020A
PD
PD
08/27/12 13:29
08/27/12 13:29
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 25%
D
MDL
41.0
0.886
Serial_No:09111209:35
Page 9 of 76 Page 198 of 296
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
09/11/12
SAMPLE RESULTS
NC059SG-000015-20120821Client ID:08/21/12 11:06Date Collected:08/21/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1215002-09Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Iron, Total
Manganese, Total
33300
306
mg/kg
mg/kg
20
20
331
3.31
08/29/12 10:05
08/29/12 10:05
1,6020A
1,6020A
PD
PD
08/27/12 13:29
08/27/12 13:29
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 29%
D
MDL
34.1
0.736
Serial_No:09111209:35
Page 10 of 76 Page 199 of 296
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
09/11/12
SAMPLE RESULTS
NC1059SG-000015-20120821Client ID:08/21/12 11:06Date Collected:08/21/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1215002-11Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Iron, Total
Manganese, Total
32600
300
mg/kg
mg/kg
20
20
326
3.26
08/29/12 10:06
08/29/12 10:06
1,6020A
1,6020A
PD
PD
08/27/12 13:29
08/27/12 13:29
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 30%
D
MDL
33.6
0.726
Serial_No:09111209:35
Page 11 of 76 Page 200 of 296
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
09/11/12
SAMPLE RESULTS
NC058SG-000015-20120821Client ID:08/21/12 11:33Date Collected:08/21/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1215002-13Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Iron, Total
Manganese, Total
37100
433
mg/kg
mg/kg
20
20
371
3.71
08/29/12 10:07
08/29/12 10:07
1,6020A
1,6020A
PD
PD
08/27/12 13:29
08/27/12 13:29
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 25%
D
MDL
38.3
0.826
Serial_No:09111209:35
Page 12 of 76 Page 201 of 296
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
09/11/12
SAMPLE RESULTS
NC046SG-000015-20120821Client ID:08/21/12 11:57Date Collected:08/21/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1215002-15Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Iron, Total
Manganese, Total
38700
468
mg/kg
mg/kg
20
20
334
3.34
08/29/12 10:08
08/29/12 10:08
1,6020A
1,6020A
PD
PD
08/27/12 13:29
08/27/12 13:29
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 28%
D
MDL
34.4
0.743
Serial_No:09111209:35
Page 13 of 76 Page 202 of 296
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
09/11/12
SAMPLE RESULTS
MC006SG-000015-20120821Client ID:08/21/12 13:48Date Collected:08/21/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1215002-17Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Iron, Total
Manganese, Total
22500
109
mg/kg
mg/kg
20
20
258
2.58
08/29/12 10:11
08/29/12 10:11
1,6020A
1,6020A
PD
PD
08/27/12 13:29
08/27/12 13:29
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 38%
D
MDL
26.6
0.574
Serial_No:09111209:35
Page 14 of 76 Page 203 of 296
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
09/11/12
SAMPLE RESULTS
MC002SG-000012-20120821Client ID:08/21/12 14:26Date Collected:08/21/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1215002-19Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Iron, Total
Manganese, Total
13600
97.9
mg/kg
mg/kg
20
20
154
1.54
08/29/12 10:12
08/29/12 10:12
1,6020A
1,6020A
PD
PD
08/27/12 13:29
08/27/12 13:29
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 61%
D
MDL
15.9
0.342
Serial_No:09111209:35
Page 15 of 76 Page 204 of 296
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
09/11/12
SAMPLE RESULTS
EB008SG-000015-20120821Client ID:08/21/12 15:01Date Collected:08/21/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1215002-21Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Iron, Total
Manganese, Total
14400
71.7
mg/kg
mg/kg
20
20
505
5.05
08/29/12 10:13
08/29/12 10:13
1,6020A
1,6020A
PD
PD
08/27/12 13:29
08/27/12 13:29
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 19%
D
MDL
52.1
1.12
Serial_No:09111209:35
Page 16 of 76 Page 205 of 296
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
09/11/12
SAMPLE RESULTS
EB006SG-000015-20120821Client ID:08/21/12 15:32Date Collected:08/21/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1215002-23Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Iron, Total
Manganese, Total
35600
174
mg/kg
mg/kg
20
20
542
5.42
08/29/12 10:15
08/29/12 10:15
1,6020A
1,6020A
PD
PD
08/27/12 13:29
08/27/12 13:29
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 17%
D
MDL
55.9
1.21
Serial_No:09111209:35
Page 17 of 76 Page 206 of 296
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
09/11/12
SAMPLE RESULTS
EK021SG-000015-20120821Client ID:08/21/12 16:07Date Collected:08/21/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1215002-25Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Iron, Total
Manganese, Total
17900
174
mg/kg
mg/kg
20
20
204
2.04
08/29/12 10:16
08/29/12 10:16
1,6020A
1,6020A
PD
PD
08/27/12 13:29
08/27/12 13:29
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 46%
D
MDL
21.0
0.453
Serial_No:09111209:35
Page 18 of 76 Page 207 of 296
FF
Parameter ResultDilution FactorQualifier Units RL
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
09/11/12
Iron, Total
Manganese, Total
J2.39
ND
mg/kg
mg/kg
2
2
20.0
0.200
08/29/12 09:57
08/29/12 09:57
1,6020A
1,6020A
PD
PD
08/27/12 13:29
08/27/12 13:29
Total Metals - Mansfield Lab for sample(s): 01,03,05,07,09,11,13,15,17,19,21,23,25 Batch: WG557278-1
EPA 3050BDigestion Method:
Prep Information
MDL
2.06
0.045
Serial_No:09111209:35
Page 19 of 76 Page 208 of 296
Iron, Total
Manganese, Total
114
113
-
-
75-125
75-125
-
-
20
20
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,11,13,15,17,19,21,23,25 Batch: WG557278-2 SRM Lot Number: S1SPIKE
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
09/11/12
Qual Qual Qual
Serial_No:09111209:35
Page 20 of 76 Page 209 of 296
Iron, Total
Manganese, Total
38700
468.
42000
842
193
109
-
-
-
-
75-125
75-125
-
-
20
20
ParameterNative Sample
MS Found
MS%Recovery
MSD Found
MSD %Recovery
RecoveryLimits RPD
RPD Limits
Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,11,13,15,17,19,21,23,25 QC Batch ID: WG557278-4 QC Sample: L1215002-15 Client ID: NC046SG-000015-20120821
1710
342
MS Added
Matrix Spike AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
09/11/12
Qual
Q
Qual Qual
Serial_No:09111209:35
Page 21 of 76 Page 210 of 296
Iron, Total
Manganese, Total
38700
468.
40400
488
mg/kg
mg/kg
4
4
20
20
Units RPDParameter Native Sample Duplicate Sample RPD Limits
Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,11,13,15,17,19,21,23,25 QC Batch ID: WG557278-3 QC Sample: L1215002-15 Client ID: NC046SG-000015-20120821
NEWTOWN CREEK RI
120782-01.01
Project Name:
Project Number:
L1215002Lab Number:
Report Date:
Lab Duplicate AnalysisBatch Quality Control
09/11/12
Qual
Serial_No:09111209:35
Page 22 of 76 Page 211 of 296
Iron, Total
Manganese, Total
38700
468.
38900
462
mg/kg
mg/kg
1
1
10
10
Units % DParameter Native Sample Serial Dilution RPD Limits
Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,11,13,15,17,19,21,23,25 QC Batch ID: WG557278-5 QC Sample: L1215002-15 Client ID: NC046SG-000015-20120821
NEWTOWN CREEK RI
120782-01.01
Project Name:
Project Number:
L1215002Lab Number:
Report Date:
Lab Serial Dilution Analysis
Batch Quality Control 09/11/12
Qual
Serial_No:09111209:35
Page 23 of 76 Page 212 of 296
INORGANICS&
MISCELLANEOUS
Serial_No:09111209:35
Page 24 of 76 Page 213 of 296
FF
EK002SG-000015-20120821Client ID:08/21/12 09:06Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-01Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Nitrogen, Ammonia
Solids, Total
7.54
9.28
250
26.2
%
%
mg/kg
%
1
1
1
1
0.010
0.010
27
0.100
08/28/12 09:00
08/28/12 09:00
08/31/12 16:53
08/23/12 11:45
1,9060
1,9060
30,4500NH3-BH
30,2540G
SF
SF
AT
KB
Date Prepared
-
-
08/30/12 13:03
-
09/11/12
MDL
0.010
0.010
4.8
0.100
Serial_No:09111209:35
Page 25 of 76 Page 214 of 296
FF
EK002SG-000015-20120821Client ID:08/21/12 09:06Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-01Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabSulfide 15000 mg/kg 400760 08/25/12 13:22 1,9030B MP
Date Prepared
08/25/12 11:45
09/11/12
D
MDL
170
Serial_No:09111209:35
Page 26 of 76 Page 215 of 296
FF
EK001SG-000015-20120821Client ID:08/21/12 09:31Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-03Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Nitrogen, Ammonia
Solids, Total
6.67
6.05
170
22.3
%
%
mg/kg
%
1
1
1
1
0.010
0.010
31
0.100
08/28/12 09:00
08/28/12 09:00
08/31/12 16:54
08/23/12 11:45
1,9060
1,9060
30,4500NH3-BH
30,2540G
SF
SF
AT
KB
Date Prepared
-
-
08/30/12 13:03
-
09/11/12
MDL
0.010
0.010
5.6
0.100
Serial_No:09111209:35
Page 27 of 76 Page 216 of 296
FF
EK001SG-000015-20120821Client ID:08/21/12 09:31Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-03Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabSulfide 12000 mg/kg 200450 08/25/12 13:14 1,9030B MP
Date Prepared
08/25/12 11:45
09/11/12
D
MDL
100
Serial_No:09111209:35
Page 28 of 76 Page 217 of 296
FF
EK010SG-000015-20120821Client ID:08/21/12 10:14Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-05Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Nitrogen, Ammonia
Solids, Total
8.86
8.66
240
21.6
%
%
mg/kg
%
1
1
1
1
0.010
0.010
35
0.100
08/28/12 09:00
08/28/12 09:00
08/31/12 16:55
08/23/12 11:45
1,9060
1,9060
30,4500NH3-BH
30,2540G
SF
SF
AT
KB
Date Prepared
-
-
08/30/12 13:03
-
09/11/12
MDL
0.010
0.010
6.2
0.100
Serial_No:09111209:35
Page 29 of 76 Page 218 of 296
FF
EK010SG-000015-20120821Client ID:08/21/12 10:14Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-05Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabSulfide 13000 mg/kg 200460 08/25/12 13:14 1,9030B MP
Date Prepared
08/25/12 11:45
09/11/12
D
MDL
100
Serial_No:09111209:35
Page 30 of 76 Page 219 of 296
FF
NC071SG-000015-20120821Client ID:08/21/12 10:49Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-07Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Nitrogen, Ammonia
Solids, Total
6.21
6.20
280
25.0
%
%
mg/kg
%
1
1
1
1
0.010
0.010
28
0.100
08/28/12 09:00
08/28/12 09:00
08/31/12 16:56
08/23/12 11:45
1,9060
1,9060
30,4500NH3-BH
30,2540G
SF
SF
AT
KB
Date Prepared
-
-
08/30/12 13:03
-
09/11/12
MDL
0.010
0.010
5.0
0.100
Serial_No:09111209:35
Page 31 of 76 Page 220 of 296
FF
NC071SG-000015-20120821Client ID:08/21/12 10:49Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-07Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabSulfide 12000 mg/kg 200400 08/25/12 13:15 1,9030B MP
Date Prepared
08/25/12 11:45
09/11/12
D
MDL
90.
Serial_No:09111209:35
Page 32 of 76 Page 221 of 296
FF
NC059SG-000015-20120821Client ID:08/21/12 11:06Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-09Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Nitrogen, Ammonia
Solids, Total
5.09
5.00
71
29.2
%
%
mg/kg
%
1
1
1
1
0.010
0.010
24
0.100
08/28/12 09:00
08/28/12 09:00
08/31/12 16:56
08/23/12 11:45
1,9060
1,9060
30,4500NH3-BH
30,2540G
SF
SF
AT
KB
Date Prepared
-
-
08/30/12 13:03
-
09/11/12
MDL
0.010
0.010
4.2
0.100
Serial_No:09111209:35
Page 33 of 76 Page 222 of 296
FF
NC059SG-000015-20120821Client ID:08/21/12 11:06Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-09Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabSulfide 5200 mg/kg 100170 08/25/12 13:15 1,9030B MP
Date Prepared
08/25/12 11:45
09/11/12
D
MDL
38.
Serial_No:09111209:35
Page 34 of 76 Page 223 of 296
FF
NC1059SG-000015-20120821Client ID:08/21/12 11:06Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-11Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Nitrogen, Ammonia
Solids, Total
5.48
5.48
80
29.6
%
%
mg/kg
%
1
1
1
1
0.010
0.010
24
0.100
08/28/12 09:00
08/28/12 09:00
08/31/12 16:57
08/23/12 11:45
1,9060
1,9060
30,4500NH3-BH
30,2540G
SF
SF
AT
KB
Date Prepared
-
-
08/30/12 13:03
-
09/11/12
MDL
0.010
0.010
4.3
0.100
Serial_No:09111209:35
Page 35 of 76 Page 224 of 296
FF
NC1059SG-000015-20120821Client ID:08/21/12 11:06Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-11Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabSulfide 7200 mg/kg 200340 08/25/12 13:22 1,9030B MP
Date Prepared
08/25/12 11:45
09/11/12
D
MDL
76.
Serial_No:09111209:35
Page 36 of 76 Page 225 of 296
FF
NC058SG-000015-20120821Client ID:08/21/12 11:33Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-13Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Nitrogen, Ammonia
Solids, Total
3.95
3.79
110
25.4
%
%
mg/kg
%
1
1
1
1
0.010
0.010
28
0.100
08/28/12 09:00
08/28/12 09:00
08/31/12 16:58
08/23/12 11:45
1,9060
1,9060
30,4500NH3-BH
30,2540G
SF
SF
AT
KB
Date Prepared
-
-
08/30/12 13:03
-
09/11/12
MDL
0.010
0.010
5.0
0.100
Serial_No:09111209:35
Page 37 of 76 Page 226 of 296
FF
NC058SG-000015-20120821Client ID:08/21/12 11:33Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-13Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabSulfide 2800 mg/kg 100200 08/25/12 13:16 1,9030B MP
Date Prepared
08/25/12 11:45
09/11/12
D
MDL
44.
Serial_No:09111209:35
Page 38 of 76 Page 227 of 296
FF
NC046SG-000015-20120821Client ID:08/21/12 11:57Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-15Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Nitrogen, Ammonia
Solids, Total
3.77
3.86
48
28.1
%
%
mg/kg
%
1
1
1
1
0.010
0.010
26
0.100
08/28/12 09:00
08/28/12 09:00
08/31/12 17:02
08/23/12 11:45
1,9060
1,9060
30,4500NH3-BH
30,2540G
SF
SF
AT
KB
Date Prepared
-
-
08/30/12 13:03
-
09/11/12
MDL
0.010
0.010
4.6
0.100
Serial_No:09111209:35
Page 39 of 76 Page 228 of 296
FF
NC046SG-000015-20120821Client ID:08/21/12 11:57Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-15Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabSulfide 2500 mg/kg 200360 08/25/12 15:21 1,9030B MP
Date Prepared
08/25/12 11:45
09/11/12
D
MDL
80.
Serial_No:09111209:35
Page 40 of 76 Page 229 of 296
FF
MC006SG-000015-20120821Client ID:08/21/12 13:48Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-17Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Nitrogen, Ammonia
Solids, Total
6.27
6.26
230
37.6
%
%
mg/kg
%
1
1
1
1
0.010
0.010
18
0.100
08/28/12 09:00
08/28/12 09:00
08/31/12 17:04
08/23/12 11:45
1,9060
1,9060
30,4500NH3-BH
30,2540G
SF
SF
AT
KB
Date Prepared
-
-
08/30/12 13:03
-
09/11/12
MDL
0.010
0.010
3.3
0.100
Serial_No:09111209:35
Page 41 of 76 Page 230 of 296
FF
MC006SG-000015-20120821Client ID:08/21/12 13:48Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-17Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabSulfide 10000 mg/kg 400530 08/25/12 15:31 1,9030B MP
Date Prepared
08/25/12 11:45
09/11/12
D
MDL
120
Serial_No:09111209:35
Page 42 of 76 Page 231 of 296
FF
MC002SG-000012-20120821Client ID:08/21/12 14:26Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-19Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Nitrogen, Ammonia
Solids, Total
3.52
3.12
53
61.0
%
%
mg/kg
%
1
1
1
1
0.010
0.010
12
0.100
08/28/12 09:00
08/28/12 09:00
08/31/12 17:05
08/23/12 11:45
1,9060
1,9060
30,4500NH3-BH
30,2540G
SF
SF
AT
KB
Date Prepared
-
-
08/30/12 13:03
-
09/11/12
MDL
0.010
0.010
2.2
0.100
Serial_No:09111209:35
Page 43 of 76 Page 232 of 296
FF
MC002SG-000012-20120821Client ID:08/21/12 14:26Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-19Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabSulfide 4200 mg/kg 200160 08/25/12 15:22 1,9030B MP
Date Prepared
08/25/12 11:45
09/11/12
D
MDL
37.
Serial_No:09111209:35
Page 44 of 76 Page 233 of 296
FF
EB008SG-000015-20120821Client ID:08/21/12 15:01Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-21Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Nitrogen, Ammonia
Solids, Total
11.9
11.0
500
19.4
%
%
mg/kg
%
1
1
1
1
0.010
0.010
38
0.100
08/28/12 09:00
08/28/12 09:00
08/31/12 17:06
08/23/12 11:45
1,9060
1,9060
30,4500NH3-BH
30,2540G
SF
SF
AT
KB
Date Prepared
-
-
08/30/12 13:03
-
09/11/12
MDL
0.010
0.010
6.8
0.100
Serial_No:09111209:35
Page 45 of 76 Page 234 of 296
FF
EB008SG-000015-20120821Client ID:08/21/12 15:01Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-21Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabSulfide 12000 mg/kg 200520 08/25/12 15:22 1,9030B MP
Date Prepared
08/25/12 11:45
09/11/12
D
MDL
120
Serial_No:09111209:35
Page 46 of 76 Page 235 of 296
FF
EB006SG-000015-20120821Client ID:08/21/12 15:32Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-23Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Nitrogen, Ammonia
Solids, Total
8.96
8.75
450
17.4
%
%
mg/kg
%
1
1
1
1
0.010
0.010
40
0.100
08/28/12 09:00
08/28/12 09:00
08/31/12 17:07
08/23/12 11:45
1,9060
1,9060
30,4500NH3-BH
30,2540G
SF
SF
AT
KB
Date Prepared
-
-
08/30/12 13:03
-
09/11/12
MDL
0.010
0.010
7.3
0.100
Serial_No:09111209:35
Page 47 of 76 Page 236 of 296
FF
EB006SG-000015-20120821Client ID:08/21/12 15:32Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-23Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabSulfide 19000 mg/kg 200570 08/25/12 15:23 1,9030B MP
Date Prepared
08/25/12 11:45
09/11/12
D
MDL
130
Serial_No:09111209:35
Page 48 of 76 Page 237 of 296
FF
EK021SG-000015-20120821Client ID:08/21/12 16:07Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-25Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Nitrogen, Ammonia
Solids, Total
3.84
3.78
44
45.5
%
%
mg/kg
%
1
1
1
1
0.010
0.010
15
0.100
08/28/12 09:00
08/28/12 09:00
08/31/12 17:08
08/23/12 11:45
1,9060
1,9060
30,4500NH3-BH
30,2540G
SF
SF
AT
KB
Date Prepared
-
-
08/30/12 13:03
-
09/11/12
MDL
0.010
0.010
2.8
0.100
Serial_No:09111209:35
Page 49 of 76 Page 238 of 296
FF
EK021SG-000015-20120821Client ID:08/21/12 16:07Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-25Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabSulfide 4900 mg/kg 200220 08/25/12 15:23 1,9030B MP
Date Prepared
08/25/12 11:45
09/11/12
D
MDL
49.
Serial_No:09111209:35
Page 50 of 76 Page 239 of 296
FF
SRM1650BClient ID:08/21/12 12:00Date Collected:08/21/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1215002-27Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield LabTotal Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
1.78
1.82
%
%
1
1
0.010
0.010
08/28/12 09:00
08/28/12 09:00
1,9060
1,9060
SF
SF
Date Prepared
-
-
09/11/12
MDL
0.010
0.010
Serial_No:09111209:35
Page 51 of 76 Page 240 of 296
FF
Parameter ResultDilution FactorQualifier Units RL
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
09/11/12
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Sulfide
Nitrogen, Ammonia
ND
ND
ND
ND
%
%
mg/kg
mg/kg
1
1
1
1
0.010
0.010
0.50
7.5
08/28/12 09:00
08/28/12 09:00
08/25/12 13:12
08/31/12 16:50
1,9060
1,9060
1,9030B
30,4500NH3-BH
SF
SF
MP
AT
-
-
08/25/12 11:45
08/30/12 13:03
Total Organic Carbon - Mansfield Lab for sample(s): 01,03,05,07,09,11,13,15,17,19,21,23,25,2 Batch: WG556725-1
General Chemistry - Westborough Lab for sample(s): 01,03,05,07,09,11,13,15,17,19,21,23,25 Batch: WG557078-1
General Chemistry - Westborough Lab for sample(s): 01,03,05,07,09,11,13,15,17,19,21,23,25 Batch: WG558038-1
MDL
0.010
0.010
0.11
0.01
Serial_No:09111209:35
Page 52 of 76 Page 241 of 296
Sulfide
Nitrogen, Ammonia
80
105
-
-
75-125
83-115
-
-
25
20
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,11,13,15,17,19,21,23,25 Batch: WG557078-2
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,11,13,15,17,19,21,23,25 Batch: WG558038-2
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
09/11/12
Qual Qual Qual
Serial_No:09111209:35
Page 53 of 76 Page 242 of 296
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Sulfide
Nitrogen, Ammonia
3.77
3.86
2500
48.
5.81
5.55
2700
1500
120
115
430
109
-
-
-
-
-
-
-
-
75-125
75-125
70-130
55-144
-
-
-
-
25
25
25
20
ParameterNative Sample
MS Found
MS%Recovery
MSD Found
MSD %Recovery
RecoveryLimits RPD
RPD Limits
Total Organic Carbon - Mansfield Lab Associated sample(s): 01,03,05,07,09,11,13,15,17,19,21,23,25,2 QC Batch ID: WG556725-4 QC Sample: L1215002-15 Client ID: NC046SG-000015-20120821
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,11,13,15,17,19,21,23,25 QC Batch ID: WG557078-4 QC Sample: L1215002-15 Client ID: NC046SG-000015-20120821
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,11,13,15,17,19,21,23,25 QC Batch ID: WG558038-4 QC Sample: L1215002-15 Client ID: NC046SG-000015-20120821
1.7
1.54
46.8
1300
MS Added
Matrix Spike AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
09/11/12
Qual
Q
Qual Qual
Serial_No:09111209:35
Page 54 of 76 Page 243 of 296
Solids, Total
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Sulfide
Nitrogen, Ammonia
28.1
3.77
3.86
2500
48.
28.7
3.79
3.92
2500
47
%
%
%
mg/kg
mg/kg
2
1
2
0
2
10
25
25
25
20
Units RPDParameter Native Sample Duplicate Sample RPD Limits
General Chemistry - Mansfield Lab Associated sample(s): 01,03,05,07,09,11,13,15,17,19,21,23,25 QC Batch ID: WG556644-1 QC Sample: L1215002-15 Client ID: NC046SG-000015-20120821
Total Organic Carbon - Mansfield Lab Associated sample(s): 01,03,05,07,09,11,13,15,17,19,21,23,25,2 QC Batch ID: WG556725-3 QC Sample: L1215002-15 Client ID: NC046SG-000015-20120821
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,11,13,15,17,19,21,23,25 QC Batch ID: WG557078-3 QC Sample: L1215002-15 Client ID: NC046SG-000015-20120821
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,11,13,15,17,19,21,23,25 QC Batch ID: WG558038-3 QC Sample: L1215002-15 Client ID: NC046SG-000015-20120821
NEWTOWN CREEK RI
120782-01.01
Project Name:
Project Number:
L1215002Lab Number:
Report Date:
Lab Duplicate AnalysisBatch Quality Control
09/11/12
Qual
Serial_No:09111209:35
Page 55 of 76 Page 244 of 296
S.R.M. Standard Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1215002
Parameter
09/11/12
% Recovery QC CriteriaTotal Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
96
100
75-125
75-125
Standard Reference Material (SRM): WG556725-2
Qual
Serial_No:09111209:35
Page 56 of 76 Page 245 of 296
*Values in parentheses indicate holding time in days
L1215002-01A
L1215002-01E
L1215002-01F
L1215002-01X
L1215002-02A
L1215002-03A
L1215002-03E
L1215002-03F
L1215002-03X
L1215002-04A
L1215002-05A
L1215002-05E
L1215002-05F
L1215002-05X
L1215002-06A
L1215002-07A
L1215002-07E
L1215002-07F
L1215002-07X
L1215002-08A
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 500ml unpreserved
Amber 500ml unpreserved
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 500ml unpreserved
Amber 500ml unpreserved
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 500ml unpreserved
Amber 500ml unpreserved
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 500ml unpreserved
Amber 500ml unpreserved
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
B
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
A
B
C
Absent
Absent
Absent
CoolerCustody SealCooler Information
NEWTOWN CREEK RI
120782-01.01
A2-FE-6020T(180),A2-TS(7),A2-MN-6020T(180),A2-TOC-9060-2REPS(28)
NH3-4500(28)
SULFIDE-9030(7)
A2-FE-6020T(180)
SUB-GEOTESTING(28)
A2-FE-6020T(180),A2-TS(7),A2-MN-6020T(180),A2-TOC-9060-2REPS(28)
NH3-4500(28)
SULFIDE-9030(7)
A2-FE-6020T(180)
SUB-GEOTESTING(28)
A2-FE-6020T(180),A2-TS(7),A2-MN-6020T(180),A2-TOC-9060-2REPS(28)
NH3-4500(28)
SULFIDE-9030(7)
A2-FE-6020T(180)
SUB-GEOTESTING(28)
A2-FE-6020T(180),A2-TS(7),A2-MN-6020T(180),A2-TOC-9060-2REPS(28)
NH3-4500(28)
SULFIDE-9030(7)
A2-FE-6020T(180)
SUB-GEOTESTING(28)
Project Name:
Project Number:
L1215002Lab Number:
Report Date:
Sample Receipt and Container Information
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
09/11/12
Were project specific reporting limits specified? YES
Reagent H2O Preserved Vials Frozen on: NA
Serial_No:09111209:35
Page 57 of 76 Page 246 of 296
*Values in parentheses indicate holding time in days
L1215002-09A
L1215002-09E
L1215002-09F
L1215002-09X
L1215002-10A
L1215002-11A
L1215002-11E
L1215002-11F
L1215002-12A
L1215002-13A
L1215002-13E
L1215002-13F
L1215002-13X
L1215002-14A
L1215002-15A
L1215002-15E
L1215002-15F
L1215002-15F1
L1215002-15X
L1215002-16A
L1215002-16D
L1215002-17A
L1215002-17E
L1215002-17F
L1215002-17X
L1215002-18A
L1215002-19A
L1215002-19E
L1215002-19F
L1215002-19X
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 500ml unpreserved
Amber 500ml unpreserved
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 500ml unpreserved
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 500ml unpreserved
Amber 500ml unpreserved
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Glass 60mL unpreserved
Amber 500ml unpreserved
Amber 500ml unpreserved
Amber 500ml unpreserved
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 500ml unpreserved
Amber 500ml unpreserved
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 500ml unpreserved
A
A
A
A
A
C
C
C
C
A
A
A
A
A
C
C
C
C
C
C
C
A
A
A
A
A
A
A
A
A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
4.1
4.1
4.1
4.1
4.1
5.1
5.1
5.1
5.1
4.1
4.1
4.1
4.1
4.1
5.1
5.1
5.1
5.1
5.1
5.1
5.1
4.1
4.1
4.1
4.1
4.1
4.1
4.1
4.1
4.1
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
NEWTOWN CREEK RI
120782-01.01
A2-FE-6020T(180),A2-TS(7),A2-MN-6020T(180),A2-TOC-9060-2REPS(28)
NH3-4500(28)
SULFIDE-9030(7)
A2-FE-6020T(180)
SUB-GEOTESTING(28)
A2-FE-6020T(180),A2-TS(7),A2-MN-6020T(180),A2-TOC-9060-2REPS(28)
NH3-4500(28)
SULFIDE-9030(7)
SUB-GEOTESTING(28)
A2-FE-6020T(180),A2-TS(7),A2-MN-6020T(180),A2-TOC-9060-2REPS(28)
NH3-4500(28)
SULFIDE-9030(7)
A2-FE-6020T(180)
SUB-GEOTESTING(28)
A2-FE-6020T(180),A2-TS(7),A2-MN-6020T(180),A2-TOC-9060-2REPS(28)
NH3-4500(28)
SULFIDE-9030(7)
SULFIDE-9030(7)
A2-FE-6020T(180)
SUB-GEOTESTING(28)
SUB-GEOTESTING(28)
A2-FE-6020T(180),A2-TS(7),A2-MN-6020T(180),A2-TOC-9060-2REPS(28)
NH3-4500(28)
SULFIDE-9030(7)
A2-FE-6020T(180)
SUB-GEOTESTING(28)
A2-FE-6020T(180),A2-TS(7),A2-MN-6020T(180),A2-TOC-9060-2REPS(28)
NH3-4500(28)
SULFIDE-9030(7)
A2-FE-6020T(180)
Project Name:
Project Number:
L1215002Lab Number:
Report Date:
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
09/11/12
Serial_No:09111209:35
Page 58 of 76 Page 247 of 296
*Values in parentheses indicate holding time in days
L1215002-20A
L1215002-21A
L1215002-21E
L1215002-21F
L1215002-21X
L1215002-22A
L1215002-23A
L1215002-23E
L1215002-23F
L1215002-23X
L1215002-24A
L1215002-25A
L1215002-25E
L1215002-25F
L1215002-25X
L1215002-26A
Amber 500ml unpreserved
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 500ml unpreserved
Amber 500ml unpreserved
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 500ml unpreserved
Amber 500ml unpreserved
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 500ml unpreserved
Amber 500ml unpreserved
A
A
A
A
A
A
C
C
C
C
C
B
B
B
B
B
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
4.1
4.1
4.1
4.1
4.1
4.1
5.1
5.1
5.1
5.1
5.1
3.7
3.7
3.7
3.7
3.7
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
NEWTOWN CREEK RI
120782-01.01
SUB-GEOTESTING(28)
A2-FE-6020T(180),A2-TS(7),A2-MN-6020T(180),A2-TOC-9060-2REPS(28)
NH3-4500(28)
SULFIDE-9030(7)
A2-FE-6020T(180)
SUB-GEOTESTING(28)
A2-FE-6020T(180),A2-TS(7),A2-MN-6020T(180),A2-TOC-9060-2REPS(28)
NH3-4500(28)
SULFIDE-9030(7)
A2-FE-6020T(180)
SUB-GEOTESTING(28)
A2-FE-6020T(180),A2-TS(7),A2-MN-6020T(180),A2-TOC-9060-2REPS(28)
NH3-4500(28)
SULFIDE-9030(7)
A2-FE-6020T(180)
SUB-GEOTESTING(28)
Project Name:
Project Number:
L1215002Lab Number:
Report Date:
Sent to GeoTesting Express
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Sent to GeoTesting Express
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L1215002-02A
L1215002-04A
L1215002-06A
L1215002-08A
L1215002-10A
L1215002-12A
L1215002-14A
L1215002-16A
L1215002-16D
L1215002-18A
L1215002-20A
L1215002-22A
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
09/11/12
Container Comments
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*Values in parentheses indicate holding time in days
NEWTOWN CREEK RI
120782-01.01
Project Name:
Project Number:
L1215002Lab Number:
Report Date:
Sent to GeoTesting Express
Sent to GeoTesting Express
L1215002-24A
L1215002-26A
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
09/11/12
Container Comments
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Report Format: DU Report with "J" Qualifiers
GLOSSARY
Project Name:
Project Number:
Lab Number:
Report Date:
L1215002NEWTOWN CREEK RI
120782-01.01 09/11/12
Acronyms
EPA
LCS
LCSD
LFB
MDL
MS
MSD
NA
NC
NI
RL
RPD
SRM
Environmental Protection Agency.
Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes.Laboratory Control Sample Duplicate: Refer to LCS.
Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes.Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any adjustments from dilutions, concentrations or moisture content, where applicable.Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. Matrix Spike Sample Duplicate: Refer to MS.
Not Applicable.
Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit.Not Ignitable.
Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL includes any adjustments from dilutions, concentrations or moisture content, where applicable.Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precisionof analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report.Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples.
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Terms
Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum.
Data Qualifiers
A
B
C
D
E
G
H
I
M
NJ
-
-
-
-
-
-
-
-
-
-
Spectra identified as "Aldol Condensation Product".
The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte at less than five times (5x) the concentration found in the blank. For MCP-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ-Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit.Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted analyses.Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations of the analyte.Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument.
The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should be considered estimated.The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.
The RPD between the results for the two columns exceeds the method-specified criteria; however, the lower value has been reporteddue to obvious interference.Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte.
Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where the identification is based on a mass spectral library search.
1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the originalmethod.
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Footnotes
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Report Format: DU Report with "J" Qualifiers
Project Name:
Project Number:
Lab Number:
Report Date:
L1215002NEWTOWN CREEK RI
120782-01.01 09/11/12
Data Qualifiers
P
Q
R
RE
-
-
-
-
The RPD between the results for the two columns exceeds the method-specified criteria.
The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing CalibrationStandard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoverieswhen the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are lessthan 5x the RL. (Metals only.)Analytical results are from sample re-analysis.
Analytical results are from sample re-extraction.
J
ND
-
-
Estimated value. The Target analyte concentration is below the quantitation limit (RL), but above the Method Detection Limit (MDL). This represents an estimated concentration for Tentatively Identified Compounds (TICs).Not detected at the method detection limit (MDL) for the sample.
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Alpha Analytical performs services with reasonable care and diligence normal to the analytical testinglaboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analyticalshall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liablefor any incidental, consequential or special damages, including but not limited to, damages in any wayconnected with the use of, interpretation of, information or analysis provided by Alpha Analytical.
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,containers, sampling procedures, holding time and splitting of samples in the field.
LIMITATION OF LIABILITIES
1
30
Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates I - IIIA, 1997.
Standard Methods for the Examination of Water and Wastewater. APHA-AWWA-WPCF. 18th Edition. 1992.
Project Name:
Project Number:
Lab Number:
Report Date:
L1215002NEWTOWN CREEK RI
120782-01.01
REFERENCES
09/11/12
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Certificate/Approval Program SummaryLast revised August 3, 2012 – Mansfield Facility
The following list includes only those analytes/methods for which certification/approval is currently held.For a complete listing of analytes for the referenced methods, please contact your Alpha Customer Service Representative.
Connecticut Department of Public Health Certificate/Lab ID: PH-0141.
Wastewater/Non-Potable Water (Inorganic Parameters: pH, Turbidity, Conductivity, Alkalinity, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Strontium, Thallium, Tin, Titanium, Vanadium, Zinc, Total Residue (Solids), Total Suspended Solids (non-filterable). Organic Parameters: PCBs, Organochlorine Pesticides, Technical Chlordane, Toxaphene, Acid Extractables, Benzidines, Phthalate Esters, Nitrosamines, Nitroaromatics & Isophorone, PAHs, Haloethers, Chlorinated Hydrocarbons, Volatile Organics.)
Solid Waste/Soil (Inorganic Parameters: pH, Aluminum, Antimony, Arsenic, Barium, Beryllium, Cadmium,Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Thallium, Titanium, Vanadium, Zinc, Total Organic Carbon, Corrosivity, TCLP 1311, SPLP 1312. Organic Parameters: PCBs, Organochlorine Pesticides, Technical Chlordane, Toxaphene, Volatile Organics, Acid Extractables, Benzidines, Phthalates, Nitrosamines,Nitroaromatics & Cyclic Ketones, PAHs, Haloethers, Chlorinated Hydrocarbons.)
Florida Department of Health Certificate/Lab ID: E87814. NELAP Accredited.
Non-Potable Water (Inorganic Parameters: SM2320B, SM2540D, SM2540G.)
Solid & Chemical Materials (Inorganic Parameters: 6020, 7470, 7471, 9045. Organic Parameters: EPA 8260,8270, 8082, 8081.)
Air & Emissions (EPA TO-15.)
Louisiana Department of Environmental Quality Certificate/Lab ID: 03090. NELAP Accredited.
Non-Potable Water (Inorganic Parameters: EPA 180.1, 245.7, 1631E, 3020A, 6020A, 7470A, 9040, 9050A, SM2320B, 2540D, 2540G, 4500H-B, Organic Parameters: EPA 3510C, 3580A, 3630C, 3640A, 3660B, 3665A,5030B, 8015D, 3570, 8081B, 8082A, 8260B, 8270C, 8270D.)
Solid & Chemical Materials (Inorganic Parameters: EPA 1311, 3050B, 3051A, 3060A, 6020A, 7196A, 7470A,7471B, 7474, 9040B, 9045C, 9060. Organic Parameters: EPA 3540C, 3570, 3580A, 3630C, 3640A, 3660,3665A, 5035, 8015D, 8081B, 8082A, 8260B, 8270C, 8270D.)
Biological Tissue (Inorganic Parameters: EPA 6020A. Organic Parameters: EPA 3570, 3510C, 3610B, 3630C, 3640A, 8270C, 8270D.)
Air & Emissions (EPA TO-15.)
New Hampshire Department of Environmental Services Certificate/Lab ID: 2206. NELAP Accredited.
Non-Potable Water (Inorganic Parameters: EPA 180.1, 1631E, 6020A, 7470A, 9040B, 9050A, SM2540D, 2540G, 4500H+B, 2320B, 3020A, . Organic Parameters: EPA 3510C, 3630C, 3640A, 3660B, 8081B, 8082A, 8270C, 8270D, 8015D.)
Solid & Chemical Materials (Inorganic Parameters: SW-846 1311, 3050B, 3051A, 6020A, 7471B, 9040B, 9045C. Organic Parameters: SW-846 3540C, 3580A, 3630C, 3640A, 3660B, 3665A, 8270C, 8015D, 8082A, 8081B.)
New Jersey Department of Environmental Protection Certificate/Lab ID: MA015. NELAP Accredited.
Non-Potable Water (Inorganic Parameters: SW-846 1312, 3020A, SM2320B, SM2540D, 2540G, 4500H-B, EPA 180.1, 1631E, SW-846 7470A, 9040C, 6020A, 9050A. Organic Parameters: SW-846 3510C, 3580A, 3630C, 3640A, 3660B, 3665A, 8015D, 8081B, 8082A, 8270C, 8270D)
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Solid & Chemical Materials (Inorganic Parameters: SW-846 1311, 1312, 3050B, 3051A, 6020A, 7471B, 7474,9040B, 9040C, 9045C, 9045D, 9060. Organic Parameters: SW-846 3540C, 3570, 3580A, 3630C, 3640A, 3660B, 3665A, 8081B, 8082A, 8270C, 8270D, 8015D.)
Atmospheric Organic Parameters (EPA 3C, TO-15, TO-10A, TO-13A-SIM.)
Biological Tissue (Inorganic Parameters: SW-846 6020A. Organic Parameters: SW-846 8270C, 8270D, 3510C, 3570, 3610C, 3630C, 3640A)
New York Department of Health Certificate/Lab ID: 11627. NELAP Accredited.
Non-Potable Water (Inorganic Parameters: SM2320B, SM2540D, 6020A, 1631E, 7470A, 9050A, EPA 180.1, 3020A. Organic Parameters: EPA 8270C, 8270D, 8081B, 8082A, 3510C.)
Solid & Hazardous Waste (Inorganic Parameters: EPA 6020A, 7471B, 7474, 9040C, 9045D. Organic Parameters: EPA 8270C, 8270D, 8081B, 8082A, 1311, 3050B, 3580A, 3570, 3051A.)
Air & Emissions (EPA TO-15, TO-10A.)
Pennsylvania Certificate/Lab ID: 68-02089 NELAP Accredited
Non-Potable Water (Inorganic Parameters: 1312, 1631E, 180.1, 3020A, 6020A, 7470A, 9040B, 9050A, 2320B, 2540D, 2540G, SM4500H+-B. Organic Parameters: 3510C, 3580A, 3630C, 3640A, 3660B, 3665A, 8015D, 8081B, 8082A, 8270C, 8270D .)
Solid & Hazardous Waste (Inorganic Parameters: EPA 1311, 3051A, 6020A, 7471B, 7474 9040B, 9045C, 9060.Organic Parameters: EPA3050B, 3540C, 3570, 3580A, 3630C, 3640A, 3660B, 3665A, 8270C, 8270D, 8081B,8015D, 8082A.)
Rhode Island Department of Health Certificate/Lab ID: LAO00299. NELAP Accredited via NJ-DEP.
Refer to NJ-DEP Certificate for Non-Potable Water.
Texas Commission of Environmental Quality Certificate/Lab ID: T104704419-08-TX. NELAP Accredited.
Solid & Chemical Materials (Inorganic Parameters: EPA 6020, 7470, 7471, 1311, 9040, 9045, 9060. Organic Parameters: EPA 8015, 8270, 8081, 8082.)
Air (Organic Parameters: EPA TO-15)
Virginia Division of Consolidated Laboratory Services Certificate/Lab ID:460194. NELAP Accredited.
Non-Potable Water (Inorganic Parameters:EPA 3020A, 6020A, 245.7, 9040B. Organic Parameters: EPA 3510C,3640A, 3660B, 3665A, 8270C, 8270D, 8082A, 8081B, 8015D.)
Solid & Chemical Materials (Inorganic Parameters: EPA 6020A,7470A,7471B,9040B,9045C,3050B,3051, 9060.Organic Parameters: EPA 3540C, 3580A, 3630C, 3640A, 3660B, 3665A, 3570, 8270C, 8270D, 8081B, 8082A,8015D.)
Washington State Department of Ecology Certificate/Lab ID: C954. Non-Potable Water (InorganicParameters: SM2540D, 180.1, 1631E.)
Solid & Chemical Materials (Inorganic Parameters: EPA 6020, 7470, 7471, 7474, 9045C, 9050A, 9060. OrganicParameters: EPA 8081, 8082, 8015, 8270.)
U.S. Army Corps of Engineers
Department of Defense, L-A-B Certificate/Lab ID: L2217.01.
Non-Potable Water (Inorganic Parameters: EPA 6020A, SM4500H-B. Organic Parameters: 3020A, 3510C,8270C, 8270D, 8270C-ALK-PAH, 8270D-ALK-PAH, 8082A, 8081B, 8015D-SHC, 8015D.)
Solid & Hazardous Waste (Inorganic Parameters: EPA 1311, 3050B, 6020A, 7471A, 9045C, 9060, SM 2540G, ASTM D422-63. Organic Parameters: EPA 3580A, 3570, 3540C, 8270C, 8270D, 8270C-ALK-PAH, 8270D-ALK-PAH 8082A, 8081B, 8015D-SHC, 8015D.
Air & Emissions (EPA TO-15.)
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Analytes Not Accredited by NELAP Certification is not available by NELAP for the following analytes: 8270C: Biphenyl. TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene, 3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 2-Methylnaphthalene, 1-Methylnaphthalene.
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Certificate/Approval Program Summary
Last revised August 16, 2012 - Westboro Facility
The following list includes only those analytes/methods for which certification/approval is currently held. For a complete listing of analytes for the referenced methods, please contact your Alpha Customer Service Representative.
Connecticut Department of Public Health Certificate/Lab ID: PH-0574. NELAP Accredited Solid Waste/Soil. Drinking Water (Inorganic Parameters: Color, pH, Turbidity, Conductivity, Alkalinity, Chloride, Free Residual Chlorine, Fluoride, Calcium Hardness, Sulfate, Nitrate, Nitrite, Aluminum, Antimony, Arsenic, Barium, Beryllium, Cadmium, Calcium, Chromium, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Nickel, Selenium, Silver, Sodium, Thallium, Zinc, Total Dissolved Solids, Total Organic Carbon, Total Cyanide, Perchlorate. Organic Parameters: Volatile Organics 524.2, Total Trihalomethanes 524.2, 1,2-Dibromo-3-chloropropane (DBCP) 504.1, Ethylene Dibromide (EDB) 504.1, 1,4-Dioxane (Mod 8270). Microbiology Parameters: Total Coliform-MF mEndo (SM9222B), Total Coliform – Colilert (SM9223, Enumeration and P/A), E. Coli. – Colilert (SM9223, Enumeration and P/A), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform-EC Medium (SM 9221E). Wastewater/Non-Potable Water (Inorganic Parameters: Color, pH, Conductivity, Acidity, Alkalinity, Chloride, Total Residual Chlorine, Fluoride, Total Hardness, Silica, Sulfate, Sulfide, Ammonia, Kjeldahl Nitrogen, Nitrate, Nitrite, O-Phosphate, Total Phosphorus, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Strontium, Thallium, Tin, Titanium, Vanadium, Zinc, Total Residue (Solids), Total Dissolved Solids, Total Suspended Solids (non-filterable), BOD, CBOD, COD, TOC, Total Cyanide, Phenolics, Foaming Agents (MBAS), Bromide, Oil and Grease. Organic Parameters: PCBs, Organochlorine Pesticides, Technical Chlordane, Toxaphene, Acid Extractables (Phenols), Benzidines, Phthalate Esters, Nitrosamines, Nitroaromatics & Isophorone, Polynuclear Aromatic Hydrocarbons, Haloethers, Chlorinated Hydrocarbons, Volatile Organics, TPH (HEM/SGT), CT- Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH. Microbiology Parameters: Total Coliform – MF mEndo (SM9222B), Total Coliform – MTF (SM9221B), E. Coli – Colilert (SM9223 Enumeration), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform – A-1 Broth (SM9221E), Enterococcus - Enterolert. Solid Waste/Soil (Inorganic Parameters: pH, Sulfide, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Thallium, Tin, Vanadium, Zinc, Total Cyanide, Ignitability, Phenolics, Corrosivity, TCLP Leach (1311), SPLP Leach (1312 metals only), Reactivity. Organic Parameters: PCBs, PCBs in Oil, Organochlorine Pesticides, Technical Chlordane, Toxaphene, CT-Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH, Dicamba, 2,4-D, 2,4,5-T, 2,4,5-TP(Silvex), Dalapon, Volatile Organics (SW 8260), Acid Extractables (Phenols) (SW 8270), Benzidines (SW 8270), Phthalates (SW 8270), Nitrosamines (SW 8270), Nitroaromatics & Cyclic Ketones (SW 8270), PAHs (SW 8270), Haloethers (SW 8270), Chlorinated Hydrocarbons (SW 8270). ) Maine Department of Human Services Certificate/Lab ID: 2009024. Drinking Water (Inorganic Parameters: SM9215B, 9222D, 9223B, EPA 180.1, 353.2, SM2130B, 2320B, 2540C, 4500Cl-D, 4500CN-C, 4500CN-E, 4500F-C, 4500H+B, 4500NO3-F, EPA 200.7, EPA 200.8, 245.1, EPA 300.0. Organic Parameters: 504.1, 524.2.) Wastewater/Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 350.1, 351.1, 353.2, 410.4, 420.1, SM2320B, 2510B, 2540C, 2540D, 426C, 4500Cl-D, 4500Cl-E, 4500CN-C, 4500CN-E, 4500F-B, 4500F-C, 4500H+B, 4500Norg-B, 4500Norg-C, 4500NH3-B, 4500NH3-G, 4500NO3-F, 4500P-B, 4500P-E, 5210B, 5220D, 5310C, 9010B, 9040B, 9030B, 7470A, 7196A, 2340B, EPA 200.7, 6010B, 200.8, 6020, 245.1, 1311, 1312, 3005A, Enterolert, 9223D, 9222D. Organic Parameters: 608, 624, 625, 8081A, 8082, 8330, 8151A, 8260B, 8270C, 3510C, 3630C, 5030B, ME-DRO, ME-GRO, MA-EPH, MA-VPH.) Solid Waste/Soil (Inorganic Parameters: 9010B, 9012A, 9014A, 9030B, 9040B, 9045C, 6010B, 7471A, 7196A, 9050A, 1010, 1030, 9065, 1311, 1312, 3005A, 3050B. Organic Parameters: ME-DRO, ME-GRO, MA-EPH, MA-VPH, 8260B, 8270C, 8330, 8151A, 8081A, 8082, 3540C, 3546, 3580A, 3630C, 5030B, 5035.) Massachusetts Department of Environmental Protection Certificate/Lab ID: M-MA086. Drinking Water (Inorganic Parameters: (EPA 200.8 for: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,Tl) (EPA 200.7 for: Ba,Be,Ca,Cd,Cr,Cu,Na,Ni) 245.1, (300.0 for: Nitrate-N, Fluoride, Sulfate); (EPA 353.2 for: Nitrate-N, Nitrite-N); (SM4500NO3-F for: Nitrate-N and Nitrite-N); 4500F-C, 4500CN-CE, EPA 180.1, SM2130B, SM4500Cl-D, 2320B, SM2540C, SM4500H-B. Organic Parameters: (EPA 524.2 for: Trihalomethanes, Volatile Organics); (504.1 for: 1,2-Dibromoethane, 1,2-Dibromo-3-Chloropropane), EPA 332. Microbiology Parameters: SM9215B; ENZ. SUB. SM9223; ColilertQT SM9223B; MF-SM9222D.) Non-Potable Water (Inorganic Parameters:, (EPA 200.8 for: Al,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,Tl,Zn); (EPA 200.7
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for: Al,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,Tl,V,Zn); 245.1, SM4500H,B, EPA 120.1, SM2510B, 2540C, 2340B, 2320B, 4500CL-E, 4500F-BC, 426C, SM4500NH3-BH, (EPA 350.1 for: Ammonia-N), LACHAT 10-107-06-1-B for Ammonia-N, SM4500NO3-F, 353.2 for Nitrate-N, SM4500NH3-BC-NES, EPA 351.1, SM4500P-E, 4500P-B,E, 5220D, EPA 410.4, SM 5210B, 5310C, 4500CL-D, EPA 1664, SM14 510AC, EPA 420.1, SM4500-CN-CE, SM2540D. Organic Parameters: (EPA 624 for Volatile Halocarbons, Volatile Aromatics),(608 for: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT,Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs-Water), (EPA 625 for SVOC Acid Extractables and SVOC Base/Neutral Extractables), 600/4-81-045-PCB-Oil. Microbiology Parameters: (ColilertQT SM9223B; Enterolert-QT: SM9222D-MF.) New Hampshire Department of Environmental Services Certificate/Lab ID: 200307. NELAP Accredited. Drinking Water (Inorganic Parameters: SM 9222B, 9223B, 9215B, EPA 200.7, 200.8, 300.0, SM4500CN-E, 4500H+B, 4500NO3-F, 2320B, 2510B, 2540C, 4500F-C, 5310C, 2120B, EPA 332.0. Organic Parameters: 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM9222D, 9221B, 9222B, 9221E-EC, EPA 3005A, 200.7, 200.8, 245.1, SW-846 6010B, 6010C, 6020, 6020A, 7196A, 7470A, SM3500-CR-D, EPA 120.1, 300.0, 350.1, 350.2, 351.1, 353.2, 410.4, 420.1, 426C, 1664A, SW-846 9010B, 9030B, 9040B, SM2120B, 2310B, 2320B, 2540B, 2540D, 4500H+B, 4500CL-E, 4500CN-E, 4500NH3-H, 4500NO3-F, 4500NO2-B, 4500P-E, 4500-S2-D, 5210B, 5220D, 2510B, 2540C, 4500F-C, 5310C, 5540C, LACHAT 10-204-00-1-A, LACHAT 10-107-06-2-D, 3060A. Organic Parameters: SW-846 3510C, 3630C, 5030B, 8260B, 8270C, 8270D, 8330, EPA 624, 625, 608, SW-846 8082, 8082A, 8081A, 8081B, 8151A, 8330, 8270C-SIM, 8270D-SIM.) Solid & Chemical Materials (Inorganic Parameters: SW-846 6010B, 6010C, 7196A, 7471A, 1010, 1030, 9010, 9012A, 9014, 9030B, 9040B, 9045C, 9050, 9065,1311, 1312, 3005A, 3050B, 3060A. Organic Parameters: SW-846 3540C, 3546, 3050B, 3580A, 3630C, 5030B, 5035, 8260B, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330, 8151A, 8015B, 8015C, 8082, 8082A, 8081A, 8081B.) New Jersey Department of Environmental Protection Certificate/Lab ID: MA935. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9222B, 9221E, 9223B, 9215B, 4500CN-CE, 4500NO3-F, 4500F-C, EPA 300.0, 200.7, 200.8, 245.1, 2540C, SM2120B, 2320B, 2510B, 5310C, SM4500H-B. Organic Parameters: EPA 332, 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM5210B, EPA 410.4, SM5220D, 4500Cl-E, EPA 300.0, SM2120B, 2340B, SM4500F-BC, EPA 200.7, 200.8, 351.1, LACHAT 10-107-06-2-D, EPA 353.2, SM4500NO3-F, 4500NO2-B, EPA 1664A, SM5310B, C or D, 4500-PE, EPA 420.1, SM510ABC, SM4500P-B5+E, 2540B, 2540C, 2540D, 2540G, EPA 120.1, SM2510B, SM2520B, SM15 426C, 9222D, 9221B, 9221C, 9221E, 9222B, 9215B, 2310B, 2320B, 4500NH3-H, 4500-S D, EPA 350.1, 350.2, SW-846 1312, 7470A, 5540C, SM4500H-B, 4500SO3-B, SM3500Cr-D, 4500CN-CE, EPA 245.1, SW-846 9040B, 3005A, 3015, EPA 6010B, 6010C, 6020, 6020A, 7196A, 3060A, SW-846 9010B, 9030B. Organic Parameters: SW-846 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3510C, EPA 608, 624, 625, SW-846 3630C, 5030B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 1,4-Dioxane by NJ Modified 8270, 8015B, NJ EPH.) Solid & Chemical Materials (Inorganic Parameters: SW-846, 6010B, 6010C, 6020, 6020A, 7196A, 3060A, 9010B, 9030B, 1010, 1030, 1311, 1312, 3005A, 3050B, 7471A, 7471B, 9014, 9012A, 9040B, 9040C, 9045C, 9045D, 9050A, 9065, 9251. Organic Parameters: SW-846 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3540C, 3546, 3580A, 3630C, 5030B, 5035L, 5035H, NJ OQA-QAM-025 Rev.7, NJ EPH.) New York Department of Health Certificate/Lab ID: 11148. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9223B, 9222B, 9215B, EPA 200.8, 200.7, 245.2, SM5310C, EPA 332.0, SM2320B, EPA 300.0, SM2120B, 4500CN-E, 4500F-C, 4500NO3-F, 2540C, SM 2510B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: SM9221E, 9222D, 9221B, 9222B, 9215B, 5210B, 5310C, EPA 410.4, SM5220D, 2310B-4a, 2320B, EPA 200.7, 300.0, SM4500CL-E, 4500F-C, SM15 426C, EPA 350.1, SM4500NH3-BH, EPA 351.1, LACHAT 10-107-06-2, EPA 353.2, SM4500-NO3-F, 4500-NO2-B, 4500P-E, 2540C, 2540B, 2540D, EPA 200.8, EPA 6010B, 6010C, 6020, 6020A, EPA 7196A, SM3500Cr-D, EPA 245.1, 245.2, 7470A, SM2120B, LACHAT 10-204-00-1-A, 4500CN-CE, EPA 1664A, EPA 420.1, SM14 510C, EPA 120.1, SM2510B, SM4500S-D, SM5540C, EPA 3005A, 3015, 9010B, 9030B. Organic Parameters: EPA 624, 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 625, 608, 8081A, 8081B, 8151A, 8330, 8082, 8082A, EPA 3510C, 5030B.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010, 1030, EPA 6010B, 6010C, 7196A, 7471A, 7471B, 9012A, 9014, 9065, 9050A, EPA 1311, 1312, 3005A, 3050B, 9010B, 9040C, 9045D. Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8015B, 8015C, 8081A, 8081B, 8151A, 8330, 8082 8082A, 3540C, 3546, 3580, 3580A, 5030B, 5035A-H, 5035A-L.)
Serial_No:09111209:35
Page 68 of 76 Page 257 of 296
North Carolina Department of the Environment and Natural Resources Certificate/Lab ID : 666. (Inorganic Parameters: SM2310B, 2320B, 4500Cl-E, 4500Cn-E, 9014, Lachat 10-204-00-1-X, 1010A, 1030, 4500NO3-F, 353.2, 4500P-E, 4500SO4-E, 300.0, 4500S-D, 5310B, 5310C, 6010C, 6020A, 200.7, 200.8, 3500Cr-B, 7196A, 245.1, 7471A, 7471B, 1311,1312. Organic Parameters: 608, 8081B, 8082A, 624, 8260B, 625, 8270D, 8151A, 8015C, 504.1, MA-EPH, MA-VPH.) Drinking Water Program Certificate/Lab ID: 25700. (Inorganic Parameters: Chloride EPA 300.0. Organic Parameters: 524.2) Pennsylvania Department of Environmental Protection Certificate/Lab ID : 68-03671. NELAP Accredited. Drinking Water (Inorganic Parameters: 200.7, 200.8, 245.2, 300.0, 332.0, 2120B, 2320B, 2510B, 2540C, 4500-CN-CE, 4500F-C, 4500H+-B, 4500NO3-F, 5310C. Organic Parameters: EPA 524.2, 504.1) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1312, 3005A,3015, 3060A, 200.7, 200.8, 410.4, 1664A, SM2540D, 5210B, 5220D, 4500-P,BE, 245.1, 300.0, 3501., 350.2, 353.2, 420.1, 6010B, 6010C, 6020, 6020A, 7196A, 7470A, 9010B, 9030B, 9040B, Lachat 10-107-06-2-D, NJ-EPH, 2120B, 2310B, 2320B, 2340B, 2510C, 2540B, 2540C, 3500Cr-D, 436C, 4500CN-CE, 4500Cl-E, 4500F-B, 4500F-C, 4500H+-B, 4500NO2-B, 4500NO3-F, 4500S-D, 4500SO3-B, 5310BCD, 5540C. Organic Parameters: EPA 3510C, 3630C, 5030B, 625, 624, 608, 8081A, 8081B, 8082, 8082A, 8151A, 8260B, 8270C, 8270D, 8330, 8015B, ) Solid & Hazardous Waste (Inorganic Parameters: EPA 350.1, 1010, 1030, 1311, 1312, 3005A, 3050B, 3060A, 6010B, 6010C, 6020A, 7196A, 7471A, 7471B, 9010B, 9012A, 9014, 9040B, 9045C, 9050, 9065, SM 4500NH3-BH, 9030B, 9038, 9251. Organic Parameters: 3540C, 3546, 3580A, 3630C, 5035, 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8260B, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330, NJ-EPH.) Rhode Island Department of Health Certificate/Lab ID: LAO00065. NELAP Accredited via NJ-DEP. Refer to MA-DEP Certificate for Potable and Non-Potable Water. Refer to NJ-DEP Certificate for Potable and Non-Potable Water. Texas Commisson on Environmental Quality Certificate/Lab ID: T104704476-09-1. NELAP Accredited. Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664, 200.7, 200.8, 245.1, 245.2, 300.0, 350.1, 351.1, 353.2, 410.4, 420.1, 6010, 6020, 7196, 7470, 9040, SM 2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 2540D, 426C, 4500CL-E, 4500CN-E, 4500F-C, 4500H+B, 4500NH3-H, 4500NO2B, 4500P-E, 4500 S2¯D, 510C, 5210B, 5220D, 5310C, 5540C. Organic Parameters: EPA 608, 624, 625, 8081, 8082, 8151, 8260, 8270, 8330.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1311, 1312, 9012, 9014, 9040, 9045, 9050, 9065.) Virginia Division of Consolidated Laboratory Services Certificate/Lab ID: 460195. NELAP Accredited. Drinking Water (Inorganic Parameters: EPA 200.7, 200.8, 300.0, 2510B, 2120B, 2540C, 4500CN-CE, 245.2, 2320B, 4500F-C, 4500F-C, 4500NO3-F, 5310C. Organic Parameters: EPA 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 200.7, 2..08, 245.1, 300.0, 3005A, 3015, 1312, 6010B, 6010C, 3060A, 353.2, 420.1, 6020, 6020A, SM4500S-D, SM4500-CN-CE, Lachat 10-204-00-1-X, 7196A, 7470A, 9010B, 9040B, 2310B, 2320B, 2510B, 2540B, 2540C, 3500Cr-D, 426C, 4500Cl-E, 4500F-B, 4500F-C, 4500PE, 510AC, 5210B, 5310B 5310C, 5540C. Organic Parameters: EPA 3510C, 3630C, 5030B, 8260B, 608, 624, 625, 8081A, 8081B, 8082, 8082A, 8151A, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330, ) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010A, 1030, 3060A, 3050B, 1311, 1312, 6010B, 6010C, 6020, , 7196A, 7471A, 7471B, 6020A, 9030B, 9010B, 9012A, 9014 9040B, 9045C, 9050A, 9065. Organic Parameters: EPA 5035, 3540C, 3546, 3550, 3580, 3630C, 8260B, 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330.) Department of Defense, L-A-B Certificate/Lab ID: L2217. Drinking Water (Inorganic Parameters: SM 4500H-B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: EPA 200.7, 200.8, 6010B, 6010C, 6020, 6020A, 245.1, 245.2, 7470A, 9040B, 9010B, 180.1. 300.0, 332.0, 6860, 353.2, 410.4, 9060, 1664A, SM 4500CN-E, 4500H-B, 4500NO3-F, 4500CL-D, 5220D, 5310C, 2130B, 2320B, 2540C, 3005A, 3015, 9010B, 9056. Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330A, 8082, 8082A, 8081A, 8081B, 3510C, 5030B, MassDEP EPH, MassDEP VPH.)
Serial_No:09111209:35
Page 69 of 76 Page 258 of 296
Solid & Hazardous Waste (Inorganic Parameters: EPA 200.7, 6010B, 6010C, 7471A, 6860, 1311, 1312, 3050B, 7196A, 9010B, 9012A, 9040B, 9045C, 3500-CR-D, 4500CN-CE, 2540G, Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330A/B-prep, 8082, 8082A, 8081A, 8081B, 3540C, 3546, 3580A, 5035A, MassDEP EPH, MassDEP VPH.) The following analytes are not included in our current NELAP/TNI Scope of Accreditation: EPA 8260B: Freon-113, 1,2,4,5-Tetramethylbenzene, 4-Ethyltoluene. EPA 8330A: PETN, Picric Acid, Nitroglycerine, 2,6-DANT, 2,4-DANT. EPA 8270C: Methyl naphthalene, Dimethyl naphthalene, Total Methylnapthalenes, Total Dimethylnaphthalenes, 1,4-Diphenylhydrazine (Azobenzene). EPA 625: 4-Chloroaniline, 4-Methylphenol. Total Phosphorus in a soil matrix, Chloride in a soil matrix, TKN in a soil matrix, NO2 in a soil matrix, NO3 in a soil matrix, SO4 in a soil matrix. EPA 9071: Total Petroleum Hydrocarbons, Oil & Grease.
Serial_No:09111209:35
Page 70 of 76 Page 259 of 296
L 12 I~O()2.
305 W Grand Ave Suite 300, Montvale, New Jersey 07645; ph: 201.930.9690
Client: Newtown Creek Group
* "ft. AN. CH OR\I..;, OE A ::::::::::; ENVIRONMENTAL SAMPLE CHAIN OF CUSTODY
Project: Newtown Creek
COCID:
Sample Custodian:
Lab:
AAL-20120821-163510
dp
Alpha Analytical Labs
CDCCollected # LabSample Field Sample ID Matrix Containers Analytical Program ac'Number Date Time
001 EK002SG.000015.20120821 SE 08/21/2012 09:06 5 Newtown Creek Surface Sediment 0002 EK001SG.000015.20120821 SE 08/21/2012 09:31 5 Newtown Creek Surface Sediment 0003 EK010SG.000015.20120821 SE 08/21/2012 10:14 5 Newtown Creek Surface Sediment 0004 NC071SG.000015.20120821 SE 08/21/2012 10:49 5 Newtown Creek Surface Sediment 0
0 005 NC059SG-000015.20120821 SE 08/21/2012 11:06 5 Newtown Creek Surface Sediment 0'l- 006 NC1059SG.000015-20120821 SE 08/21/2012 11:06 4 Newtown Creek Surface Sediment 0y 007 NC058SG-000015-20120821 SE 08/21/2012 11:33 5 Newtown Creek Surface Sediment 0(., 008 NC046SG-000015.20120821 SE 08/21/2012 11:57 7 Newtown Creek Surface Sediment [!]If 009 MC006SG-000015.20120821 SE 08/21/2012 13:48 5 Newtown Creek Surface Sediment 0
010 MC002SG.000012-20120821 SE 08/21/2012 14:26 5 Newtown Creek Surface Sediment 0'L 011 EB008SG-000015-20120821 SE 08/21/2012 15:01 5 Newtown Creek Surface Sediment 0<f 012 EB006SG.000015-20120821 SE 08/21/2012 15:32 5 Newtown Creek Surface Sediment 0
013 EK021SG-000015.20120821 SE 08/21/2012 16:07 5 Newtown Creek Surface Sediment 0
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Page 1 of 1
Serial_No:09111209:35
Page 71 of 76 Page 260 of 296
FIELD _SAMPLE_IDEB006SG-0000 15-20 121EB006SG-0000 15-20 121EB006SG-0000 15-20 12(EB006SG-000015-2012(EB006SG-000015-2012(EB006SG-000015-2012(EB008SG-000015-2012(EB008SG-000015-2012(EB008SG-0000 15-20 12(EB008SG-000015-2012(EB008SG-000015-2012(EB008SG-000015-2012(EKOO1SG-OOOO15-20 121EK001 SG-000015-2012(EK001 SG-000015-20121EK001 SG-000015-20121EK001 SG-000015-20121EK001 SG-000015-20121EK002SG-000015-2012(EK002SG-000015-2012(EK002SG-000015-2012(EK002SG-000015-2012(EK002SG-000015-2012(EK002SG-000015-2012(EK010SG-000015-2012(EK010SG-000015-2012(EK010SG-000015-2012(EK010SG-000015-2012(EK010SG-000015-2012(EK010SG-000015-2012(EK021 SG-OOOO15-20 121EK021 SG-000015-20121EK021 SG-OOOO15-20 121EK021 SG-OOOO15-20 121EK021 SG-000015-20121EK021 SG-000015-20121MC002SG-000012-2012MC002SG-000012-2012MC002SG-000012-2012MC002SG-000012-2012MC002SG-000012-2012MC002SG-000012-2012MC006SG-000015-2012
MATRIXSESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESE
SAMPLE SAMPLE_DATE _TIME TEST_REQUEST8/21/2012 15:32 Ammonia8/21/2012 15:32 Archive8/21/2012 15:32 Grainsize8/21/2012 15:32 Iron & manganese8/21/2012 15:32 Sulfide8/21/2012 15:32 TOC8/21/2012 15:01 Ammonia8/21/2012 15:01 Archive8/21/2012 15:01 Grainsize8/21/2012 15:01 Iron & manganese8/21/2012 15:01 Sulfide8/21/2012 15:01 TOC8/21/2012 9:31 Ammonia8/21/2012 9:31 Archive8/21/2012 9:31 Grainsize8/21/2012 9:31 Iron & manganese8/21/2012 9:31 Sulfide8/21/2012 9:31 TOC8/21/2012 9:06 Ammonia8/21/2012 9:06 Archive8/21/2012 9:06 Grainsize8/21/2012 9:06 Iron & manganese8/21/2012 9:06 Sulfide8/21/2012 9:06 TOC8/21/2012 10:14 Ammonia8/21/2012 10:14 Archive8/21/2012 10:14 Grainsize8/21/2012 10:14 Iron & manganese8/21/2012 10:14 Sulfide8/21/2012 10:14 TOC8/21/2012 16:07 Ammonia8/21/2012 16:07 Archive8/21/2012 16:07 Grainsize8/21/2012 16:07 Iron & manganese8/21/2012 16:07 Sulfide8/21/2012 16:07 TOC8/21/2012 14:26 Ammonia8/21/2012 14:26 Archive8/21/2012 14:26 Grainsize8/21/2012 14:26 Iron & manganese8/21/2012 14:26 Sulfide8/21/2012 14:26 TOC8/21/2012 13:48 Ammonia
METHODSM4500NH3HNAASTM 0422EPA 6010B/6020EPA 9030BEPA 9060SM4500NH3HNAASTM 0422EPA 6010B/6020EPA 9030BEPA 9060
, SM4500NH3HNAASTM 0422EPA 601OB/6020EPA 9030BEPA 9060SM4500NH3HNAASTM 0422EPA 601 OB/6020EPA 9030BEPA 9060SM4500NH3HNAASTM 0422EPA 601 OB/6020EPA 9030BEPA 9060SM4500NH3HNAASTM 0422EPA 601 OB/6020EPA 9030BEPA 9060SM4500NH3HNAASTM 0422EPA 601 OB/6020EPA 9030BEPA 9060SM4500NH3H
Page 1 of 2
TURN_A CONTAINROUND_ TAT_UN ER_COUTIME IT NT30 DAYS 0-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0
SAMPLE_CUSTO
LAB_QC COC_ID DIANNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL -20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dp
Serial_No:09111209:35
Page 72 of 76 Page 261 of 296
MATRIXSESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESESE
FIELD_SAMPLE_IDMC006SG-000015-2012MC006SG-000015-2012MC006SG-000015-2012MC006SG-000015-2012MC006SG-000015-2012NC046SG-000015-2012'NC046SG-000015-2012'NC046SG-000015-2012'NC046SG-000015-2012'NC046SG-000015-2012'NC046SG-0000 15-20 12'NC058SG-000015-2012'
; NC058SG-000015-2012' ;NC058SG-000015-2012'NC058SG-000015-2012'NC058SG-000015-2012'NC058SG-000015-2012'NC059SG-0000 15-20 12'NC059SG-000015-2012'NC059SG-000015-2012'NC059SG-000015-2012'NC059SG-000015-2012'NC059SG-000015-2012'NC071 SG-000015-2012'NC071 SG-000015-2012'NC071 SG-OOOO15-20 12'NC071 SG-000015-2012'NC071 SG-000015-2012'NC071 SG-000015-2012'NC1 059SG-000015-201;NC1 059SG-000015-201;NC 1059SG-0000 15-201:NC1 059SG-000015-201,NC1 059SG-000015-201,
SAMPLE SAMPLE_DATE _TIME TEST_REQUEST8/21/2012 13:48 Archive8/21/2012 13:48 Grainsize8/21/2012 13:48 Iron & manganese8/21/2012 13:48 Sulfide8/21/2012 13:48 TOC8/21/2012 11 :57 Ammonia8/21/2012 11 :57 Archive8/21/2012 11 :57 Grainsiie8/21/2012 11 :57 Iron & manganese8/21/2012 11 :57 Sulfide8/21/2012 11 :57 TOC8/21/2012 11 :33 Ammonia8/21/2012 11:33 Archive8/21/2012 11 :33 Grainsize8/21/2012 11 :33 Iron & manganese8/21/2012 11 :33 Sulfide8/21/201211:33 TOC8/21/2012 11 :06 Ammonia8/21/2012 11 :06 Archive8/21/2012 11 :06 Grainsize8/21/2012 11 :06 Iron & manganese8/21/2012 11 :06 Sulfide8/21/2012 11:06 TOC8/21/2012 10:49 Ammonia8/21/2012 10:49 Archive8/21/2012 10:49 Grainsize8/21/2012 10:49 Iron & manganese8/21/2012 10:49 Sulfide8/21/2012 10:49 TOC8/21/2012 11 :06 Ammonia8/21/2012 11 :06 Grainsize8/21/2012 11 :06 Iron & manganese8/21/2012 11 :06 Sulfide8/21/2012 11 :06 TOC
METHODNAASTM 0422EPA 60108/6020EPA 90308EPA 9060SM4500NH3HNAASTM 0422EPA 60108/6020EPA 90308EPA 9060SM4500NH3HNAASTM 0422EPA 60108/6020EPA 90308EPA 9060SM4500NH3HNAASTM 0422EPA 60108/6020EPA 90308EPA 9060SM4500NH3HNAASTM 0422EPA 60108/6020EPA 90308EPA 9060SM4500NH3HASTM 0422EPA 60108/6020EPA 90308EPA 9060
Page 2 of 2
TURN_A CONTAINROUND_ TAT_UN ER_COUTIME IT NT-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0-1 DAYS 130 DAYS 230 DAYS 130 DAYS 230 DAYS 130 DAYS 0-1; DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 0-1 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 130 DAYS 030 DAYS 130 DAYS 130 DAYS 130 DAYS 1
SAMPLE_CUSTO
LA8_QC COC_ID DIANNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpYES AAL-20120821-163510 dpYES AAL-20120821-163510 dpYES AAL-20120821-163510 dpYES AAL-20120821-163510 dpYES AAL-20120821-163510 dpYES AAL-20120821-163510 dpNO AAL-20120821-163510 dp
; NO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dpNO AAL-20120821-163510 dp
Serial_No:09111209:35
Page 73 of 76 Page 262 of 296
CHAIN OF CUSTODY PAGE1 OF'1 Date Rec'd in Lab:
!-iA.ANALYTICAL
Project Name: Newtown CreekWestborough,MATEL: 508-898-9220
FAX: 508-898-9193
Mansfield,MATEL: 508-822-9300
FAX: 508-822-3288
••..••• ra .1iut:U['
""
.'."IeI.
o FAX
o ADEx
-r:r.mF.ll'i1'i'lll:(:lo
Add'i Deliverables
al.""_.!"I.l.I.
Please provide ANCHOR EQUIS EDD and reference Newtown Creek
Other Project Specific Requirements/CommentslDetection Limits:
IS YOUR PROJECTMA MCP or CT RCP?
Client: Alpha Analytical
Address: 320 Forbes Blvd,Mansfield, MA 02048
Phone: 508-844-4122
Fax: 508-822-3288:,Email: [email protected]
o Thesesampleshavebeenpr~viOUSlyanalyzedbyAlpha
Sample SpecificComments •L1215002-02 1
L1215002-04 1
L1215002-06 1
L1215002-08 1
L1215002-10 1
SAMPLEHANDLINGFiltration
o Doneo Nol Neededo LabIa doPresetVation
o Lablodo(Please specifybelow)
L1215002-12
L1215002-14
L1215002-16
L1215002-18
L1215002-20
'~Il~~~"lurryai1:i(;rii;ltj~9~ willnot ,'.". fll!.r1'~~I,.,~nY.¥!Ji9jgUitieSa~~o;;r"S()!,ve(j,A1I.s~,~ples\> :':~u9!"itt.••d,i:I~,,-S,ub~I~'"-Alpha'sPaymenlTeims:' "
0 0 00 0 00 0 00 0 00 0 00 0 00 0 00 0 00 0 00 0 0. . .
. - .
Datemme
Criteria
Received By:
-"ml~'m.tJ=rn-1.RMiI!"ler.l"I::II.l~"[eI::II~:I.}i'.IiI.Are MCPAnalytical Methods Reguired?Are CT RCP (Reasonable Confidence Protocolsl Reauired?
o No
o No
ANALYSIS
DYes
DYes
MCP PRESUMPTIV
State/Fed Prooram
\
I I I I I I I I,
NN"!'I:)
:2I- W(/) I-« «w <..>N ::::iu; Q.
::>z I:)
~ 0Cl a
I I I I I I I
[gI 0 0 0 0 0 0 0 0[gI 0 0 0 0 0 0 0 0[gI 0 0 0 0 0 0 0 0[gI 0 0 0 0 0 0 0 0[gI 0 0 0 0, 0 0 0 0!Xl 0 0 0 0 D 0 0 0[gI 0 0 0 0 0 0 0 0[gI [gI 0- 0 0 0 0 0 0[gI 0 0 0 0 0 0 0 0[gI 0 0 0 0 0 0 0 0
. . .
- I--, .
ished By:
Time:
Sample I Sampler'sMatrix Initials
8/21112 0906 se'diment
8/21/12 0931 sediment
8/21/12 1014 sediment
8/21/12 1049 sediment
8/21/12 1106 sediment
8/21/12 1106 sediment
8/21/12 1133 sediment
8/21/12 1133 sediment
8/21/12 1348 sediment
8/21112 1426 sedimenti
Container Type
• Preservative
Due Date:
ALPHA Quote #.
Turn-Around Time
~ Standard 0 Rush (ONLYIF PRE-APPROVED)
Project Location:
Project#:
Proiect Manaaer: Chris Anderson
Sample ID-
ALPHA Lab ID.-.(L~b'U~'eon!~)A
FORM NO; 01-01(1)(reY.30-JUl-07)
EK002SG-000015-20120821
EK001 SG-000015-20120821
EK010SG-000015-20120821
NC071 SG-000015-20120821
NC059SG-000015-20120821
NC1059SG-000015-20120821
NC058SG-000015-20120821
NC046SG-000015-20120821
MC006SG-000015-20120821
MC002SG-000012-20120821
PLEASE ANSWER QUESTIONS ABOVE!
Serial_No:09111209:35
Page 74 of 76 Page 263 of 296
Sample SpecificComments
SAMPLE HANDLING
Filtrationo Done
o Nol Neededo Lilblodo
Preservation
o Lablodo(Please specifybelow)
L1215002-22
L1215002-24
L1215002-26
DYesDYes
ANALYSIS
Time:
NNv0:2I-U)«wN
Sampler'sCi5Z
Initials ~C>
sediment ~ 0 0 0 0 0 0 0 0 0 0 0sediment ~ 0 0 0 0 0 0 0 0 0 0 0sediment ~ 0 0 0 0 0 0 0 0 0 0 0
0 0 0 0 0 0 0 0 0 0 0 0.0 0 0 0 0' 0 0 0 0 0 0 00 0 0 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 0 0 0 0
Container Type
Preservative
Receive.d By: DaterTime
o Rush (ONLY IF PRE.APPROVED)
1607
1532
15018/21/12
8/21/12
8/21/12
~ Standard
ALPHAQ t #
Due Date:
Project Location:
Pro'ect#:
• ¥. ~ , .' : ' - ~ '" .'. .."
ifurn-Around Time ,,' ."A,~'''',,',
CHAIN OF CUSTODY
Sample 10
EB008SG-000015-20120821
EB006SG-000015-20120821
EK021 SG-000015-20120821
I-iANAlYT1CAL
Please provide ANCHOR EQUIS EDO and reference Newtown Creek
Fax: 508-824-3288
Email: [email protected]
o These samples have been Previously analyzed by Alpha
Other Project Specific Requirements/Comments/Detection Limits:
Address: 320 Forbes Blvd
Mansfield, MA 02048
Phone: 508-844-4122
ALPHALabID;(Lab Use Oilly)'
FORM NO: 01-01(1)(re ••..30-JUL.Qr)
PLEASE ANSWER QUESTIONS ABOVE!
IS YOUR PROJECTMA MCP or CT RCP?
Serial_No:09111209:35
Page 75 of 76 Page 264 of 296
Serial_No:09111209:35
Page 76 of 76 Page 265 of 296
Alpha Summary
Forms
Page 266 of 296
Inorganic Summary Forms
Page 267 of 296
U.S. EPA - CLP
COVER PAGE
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Client Sample No. Lab Sample ID.EK002SG-000015-20120821 L1215002-01EK001SG-000015-20120821 L1215002-03EK010SG-000015-20120821 L1215002-05NC071SG-000015-20120821 L1215002-07NC059SG-000015-20120821 L1215002-09
NC1059SG-000015-20120821 L1215002-11NC058SG-000015-20120821 L1215002-13NC046SG-000015-20120821 L1215002-15MC006SG-000015-20120821 L1215002-17MC002SG-000012-20120821 L1215002-19EB008SG-000015-20120821 L1215002-21EB006SG-000015-20120821 L1215002-23EK021SG-000015-20120821 L1215002-25
Prep Blank WG557278-1LCS WG557278-2
NC046SG-000015-20120821D WG557278-3NC046SG-000015-20120821S WG557278-4
NC046SG-000015-20120821SER WG557278-5
ICP-AES ICP-MS
Were ICP-AES and ICP-MS interelement Yes/No NA Yescorrections applied?
Yes/No NA YesWere ICP-AES and ICP-MS background correctionsapplied?
If yes-were raw data generated before application of background corrections? Yes/No NA No
Comments:
Page 268 of 296
U.S. EPA - CLP1-IN CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Matrix (soil/water ): SOIL Lab Sample ID: L1215002-01
Analytical Method: 6020A Date Received: 08/21/12
% Solids: 26.2 Date Analyzed: 8/29/12 9:59
Concentration Units: mg/kg
CAS No. Analyte Concentration C
7429-90-5 Aluminum7440-36-0 Antimony7440-38-2 Arsenic7440-39-3 Barium7440-41-7 Beryllium7440-43-9 Cadmium7440-70-2 Calcium7440-47-3 Chromium7440-48-4 Cobalt7440-50-8 Copper7439-89-6 Iron 343007439-92-1 Lead7439-95-4 Magnesium7439-96-5 Manganese 2197439-97-6 Mercury7439-98-7 Molybdenum7440-02-0 Nickel7440-09-7 Potassium7782-49-2 Selenium7440-22-4 Silver7440-23-5 Sodium7440-24-6 Strontium7440-28-0 Thallium7440-62-2 Vanadium7440-66-6 Zinc7440-31-5 Tin7440-42-8 Boron57-12-5 Cyanide*END*
Comments:
FORM I-IN ILM05.0
EK002SG-000015-20120821
Page 269 of 296
U.S. EPA - CLP1-IN CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Matrix (soil/water ): SOIL Lab Sample ID: L1215002-03
Analytical Method: 6020A Date Received: 08/21/12
% Solids: 22.3 Date Analyzed: 8/29/12 10:00
Concentration Units: mg/kg
CAS No. Analyte Concentration C
7429-90-5 Aluminum7440-36-0 Antimony7440-38-2 Arsenic7440-39-3 Barium7440-41-7 Beryllium7440-43-9 Cadmium7440-70-2 Calcium7440-47-3 Chromium7440-48-4 Cobalt7440-50-8 Copper7439-89-6 Iron 335007439-92-1 Lead7439-95-4 Magnesium7439-96-5 Manganese 2197439-97-6 Mercury7439-98-7 Molybdenum7440-02-0 Nickel7440-09-7 Potassium7782-49-2 Selenium7440-22-4 Silver7440-23-5 Sodium7440-24-6 Strontium7440-28-0 Thallium7440-62-2 Vanadium7440-66-6 Zinc7440-31-5 Tin7440-42-8 Boron57-12-5 Cyanide*END*
Comments:
FORM I-IN ILM05.0
EK001SG-000015-20120821
Page 270 of 296
U.S. EPA - CLP1-IN CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Matrix (soil/water ): SOIL Lab Sample ID: L1215002-05
Analytical Method: 6020A Date Received: 08/21/12
% Solids: 21.6 Date Analyzed: 8/29/12 10:01
Concentration Units: mg/kg
CAS No. Analyte Concentration C
7429-90-5 Aluminum7440-36-0 Antimony7440-38-2 Arsenic7440-39-3 Barium7440-41-7 Beryllium7440-43-9 Cadmium7440-70-2 Calcium7440-47-3 Chromium7440-48-4 Cobalt7440-50-8 Copper7439-89-6 Iron 329007439-92-1 Lead7439-95-4 Magnesium7439-96-5 Manganese 2007439-97-6 Mercury7439-98-7 Molybdenum7440-02-0 Nickel7440-09-7 Potassium7782-49-2 Selenium7440-22-4 Silver7440-23-5 Sodium7440-24-6 Strontium7440-28-0 Thallium7440-62-2 Vanadium7440-66-6 Zinc7440-31-5 Tin7440-42-8 Boron57-12-5 Cyanide*END*
Comments:
FORM I-IN ILM05.0
EK010SG-000015-20120821
Page 271 of 296
U.S. EPA - CLP1-IN CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Matrix (soil/water ): SOIL Lab Sample ID: L1215002-07
Analytical Method: 6020A Date Received: 08/21/12
% Solids: 25.0 Date Analyzed: 8/29/12 10:02
Concentration Units: mg/kg
CAS No. Analyte Concentration C
7429-90-5 Aluminum7440-36-0 Antimony7440-38-2 Arsenic7440-39-3 Barium7440-41-7 Beryllium7440-43-9 Cadmium7440-70-2 Calcium7440-47-3 Chromium7440-48-4 Cobalt7440-50-8 Copper7439-89-6 Iron 375007439-92-1 Lead7439-95-4 Magnesium7439-96-5 Manganese 3047439-97-6 Mercury7439-98-7 Molybdenum7440-02-0 Nickel7440-09-7 Potassium7782-49-2 Selenium7440-22-4 Silver7440-23-5 Sodium7440-24-6 Strontium7440-28-0 Thallium7440-62-2 Vanadium7440-66-6 Zinc7440-31-5 Tin7440-42-8 Boron57-12-5 Cyanide*END*
Comments:
FORM I-IN ILM05.0
NC071SG-000015-20120821
Page 272 of 296
U.S. EPA - CLP1-IN CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Matrix (soil/water ): SOIL Lab Sample ID: L1215002-09
Analytical Method: 6020A Date Received: 08/21/12
% Solids: 29.2 Date Analyzed: 8/29/12 10:05
Concentration Units: mg/kg
CAS No. Analyte Concentration C
7429-90-5 Aluminum7440-36-0 Antimony7440-38-2 Arsenic7440-39-3 Barium7440-41-7 Beryllium7440-43-9 Cadmium7440-70-2 Calcium7440-47-3 Chromium7440-48-4 Cobalt7440-50-8 Copper7439-89-6 Iron 333007439-92-1 Lead7439-95-4 Magnesium7439-96-5 Manganese 3067439-97-6 Mercury7439-98-7 Molybdenum7440-02-0 Nickel7440-09-7 Potassium7782-49-2 Selenium7440-22-4 Silver7440-23-5 Sodium7440-24-6 Strontium7440-28-0 Thallium7440-62-2 Vanadium7440-66-6 Zinc7440-31-5 Tin7440-42-8 Boron57-12-5 Cyanide*END*
Comments:
FORM I-IN ILM05.0
NC059SG-000015-20120821
Page 273 of 296
U.S. EPA - CLP1-IN CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Matrix (soil/water ): SOIL Lab Sample ID: L1215002-11
Analytical Method: 6020A Date Received: 08/21/12
% Solids: 29.6 Date Analyzed: 8/29/12 10:06
Concentration Units: mg/kg
CAS No. Analyte Concentration C
7429-90-5 Aluminum7440-36-0 Antimony7440-38-2 Arsenic7440-39-3 Barium7440-41-7 Beryllium7440-43-9 Cadmium7440-70-2 Calcium7440-47-3 Chromium7440-48-4 Cobalt7440-50-8 Copper7439-89-6 Iron 326007439-92-1 Lead7439-95-4 Magnesium7439-96-5 Manganese 3007439-97-6 Mercury7439-98-7 Molybdenum7440-02-0 Nickel7440-09-7 Potassium7782-49-2 Selenium7440-22-4 Silver7440-23-5 Sodium7440-24-6 Strontium7440-28-0 Thallium7440-62-2 Vanadium7440-66-6 Zinc7440-31-5 Tin7440-42-8 Boron57-12-5 Cyanide*END*
Comments:
FORM I-IN ILM05.0
NC1059SG-000015-20120821
Page 274 of 296
U.S. EPA - CLP1-IN CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Matrix (soil/water ): SOIL Lab Sample ID: L1215002-13
Analytical Method: 6020A Date Received: 08/21/12
% Solids: 25.4 Date Analyzed: 8/29/12 10:07
Concentration Units: mg/kg
CAS No. Analyte Concentration C
7429-90-5 Aluminum7440-36-0 Antimony7440-38-2 Arsenic7440-39-3 Barium7440-41-7 Beryllium7440-43-9 Cadmium7440-70-2 Calcium7440-47-3 Chromium7440-48-4 Cobalt7440-50-8 Copper7439-89-6 Iron 371007439-92-1 Lead7439-95-4 Magnesium7439-96-5 Manganese 4337439-97-6 Mercury7439-98-7 Molybdenum7440-02-0 Nickel7440-09-7 Potassium7782-49-2 Selenium7440-22-4 Silver7440-23-5 Sodium7440-24-6 Strontium7440-28-0 Thallium7440-62-2 Vanadium7440-66-6 Zinc7440-31-5 Tin7440-42-8 Boron57-12-5 Cyanide*END*
Comments:
FORM I-IN ILM05.0
NC058SG-000015-20120821
Page 275 of 296
U.S. EPA - CLP1-IN CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Matrix (soil/water ): SOIL Lab Sample ID: L1215002-15
Analytical Method: 6020A Date Received: 08/21/12
% Solids: 28.1 Date Analyzed: 8/29/12 10:08
Concentration Units: mg/kg
CAS No. Analyte Concentration C
7429-90-5 Aluminum7440-36-0 Antimony7440-38-2 Arsenic7440-39-3 Barium7440-41-7 Beryllium7440-43-9 Cadmium7440-70-2 Calcium7440-47-3 Chromium7440-48-4 Cobalt7440-50-8 Copper7439-89-6 Iron 387007439-92-1 Lead7439-95-4 Magnesium7439-96-5 Manganese 4687439-97-6 Mercury7439-98-7 Molybdenum7440-02-0 Nickel7440-09-7 Potassium7782-49-2 Selenium7440-22-4 Silver7440-23-5 Sodium7440-24-6 Strontium7440-28-0 Thallium7440-62-2 Vanadium7440-66-6 Zinc7440-31-5 Tin7440-42-8 Boron57-12-5 Cyanide*END*
Comments:
FORM I-IN ILM05.0
NC046SG-000015-20120821
Page 276 of 296
U.S. EPA - CLP1-IN CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Matrix (soil/water ): SOIL Lab Sample ID: L1215002-17
Analytical Method: 6020A Date Received: 08/21/12
% Solids: 37.6 Date Analyzed: 8/29/12 10:11
Concentration Units: mg/kg
CAS No. Analyte Concentration C
7429-90-5 Aluminum7440-36-0 Antimony7440-38-2 Arsenic7440-39-3 Barium7440-41-7 Beryllium7440-43-9 Cadmium7440-70-2 Calcium7440-47-3 Chromium7440-48-4 Cobalt7440-50-8 Copper7439-89-6 Iron 225007439-92-1 Lead7439-95-4 Magnesium7439-96-5 Manganese 1097439-97-6 Mercury7439-98-7 Molybdenum7440-02-0 Nickel7440-09-7 Potassium7782-49-2 Selenium7440-22-4 Silver7440-23-5 Sodium7440-24-6 Strontium7440-28-0 Thallium7440-62-2 Vanadium7440-66-6 Zinc7440-31-5 Tin7440-42-8 Boron57-12-5 Cyanide*END*
Comments:
FORM I-IN ILM05.0
MC006SG-000015-20120821
Page 277 of 296
U.S. EPA - CLP1-IN CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Matrix (soil/water ): SOIL Lab Sample ID: L1215002-19
Analytical Method: 6020A Date Received: 08/21/12
% Solids: 61.0 Date Analyzed: 8/29/12 10:12
Concentration Units: mg/kg
CAS No. Analyte Concentration C
7429-90-5 Aluminum7440-36-0 Antimony7440-38-2 Arsenic7440-39-3 Barium7440-41-7 Beryllium7440-43-9 Cadmium7440-70-2 Calcium7440-47-3 Chromium7440-48-4 Cobalt7440-50-8 Copper7439-89-6 Iron 136007439-92-1 Lead7439-95-4 Magnesium7439-96-5 Manganese 97.97439-97-6 Mercury7439-98-7 Molybdenum7440-02-0 Nickel7440-09-7 Potassium7782-49-2 Selenium7440-22-4 Silver7440-23-5 Sodium7440-24-6 Strontium7440-28-0 Thallium7440-62-2 Vanadium7440-66-6 Zinc7440-31-5 Tin7440-42-8 Boron57-12-5 Cyanide*END*
Comments:
FORM I-IN ILM05.0
MC002SG-000012-20120821
Page 278 of 296
U.S. EPA - CLP1-IN CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Matrix (soil/water ): SOIL Lab Sample ID: L1215002-21
Analytical Method: 6020A Date Received: 08/21/12
% Solids: 19.4 Date Analyzed: 8/29/12 10:13
Concentration Units: mg/kg
CAS No. Analyte Concentration C
7429-90-5 Aluminum7440-36-0 Antimony7440-38-2 Arsenic7440-39-3 Barium7440-41-7 Beryllium7440-43-9 Cadmium7440-70-2 Calcium7440-47-3 Chromium7440-48-4 Cobalt7440-50-8 Copper7439-89-6 Iron 144007439-92-1 Lead7439-95-4 Magnesium7439-96-5 Manganese 71.77439-97-6 Mercury7439-98-7 Molybdenum7440-02-0 Nickel7440-09-7 Potassium7782-49-2 Selenium7440-22-4 Silver7440-23-5 Sodium7440-24-6 Strontium7440-28-0 Thallium7440-62-2 Vanadium7440-66-6 Zinc7440-31-5 Tin7440-42-8 Boron57-12-5 Cyanide*END*
Comments:
FORM I-IN ILM05.0
EB008SG-000015-20120821
Page 279 of 296
U.S. EPA - CLP1-IN CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Matrix (soil/water ): SOIL Lab Sample ID: L1215002-23
Analytical Method: 6020A Date Received: 08/21/12
% Solids: 17.4 Date Analyzed: 8/29/12 10:15
Concentration Units: mg/kg
CAS No. Analyte Concentration C
7429-90-5 Aluminum7440-36-0 Antimony7440-38-2 Arsenic7440-39-3 Barium7440-41-7 Beryllium7440-43-9 Cadmium7440-70-2 Calcium7440-47-3 Chromium7440-48-4 Cobalt7440-50-8 Copper7439-89-6 Iron 356007439-92-1 Lead7439-95-4 Magnesium7439-96-5 Manganese 1747439-97-6 Mercury7439-98-7 Molybdenum7440-02-0 Nickel7440-09-7 Potassium7782-49-2 Selenium7440-22-4 Silver7440-23-5 Sodium7440-24-6 Strontium7440-28-0 Thallium7440-62-2 Vanadium7440-66-6 Zinc7440-31-5 Tin7440-42-8 Boron57-12-5 Cyanide*END*
Comments:
FORM I-IN ILM05.0
EB006SG-000015-20120821
Page 280 of 296
U.S. EPA - CLP1-IN CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Matrix (soil/water ): SOIL Lab Sample ID: L1215002-25
Analytical Method: 6020A Date Received: 08/21/12
% Solids: 45.5 Date Analyzed: 8/29/12 10:16
Concentration Units: mg/kg
CAS No. Analyte Concentration C
7429-90-5 Aluminum7440-36-0 Antimony7440-38-2 Arsenic7440-39-3 Barium7440-41-7 Beryllium7440-43-9 Cadmium7440-70-2 Calcium7440-47-3 Chromium7440-48-4 Cobalt7440-50-8 Copper7439-89-6 Iron 179007439-92-1 Lead7439-95-4 Magnesium7439-96-5 Manganese 1747439-97-6 Mercury7439-98-7 Molybdenum7440-02-0 Nickel7440-09-7 Potassium7782-49-2 Selenium7440-22-4 Silver7440-23-5 Sodium7440-24-6 Strontium7440-28-0 Thallium7440-62-2 Vanadium7440-66-6 Zinc7440-31-5 Tin7440-42-8 Boron57-12-5 Cyanide*END*
Comments:
FORM I-IN ILM05.0
EK021SG-000015-20120821
Page 281 of 296
U.S. EPA - CLP2A-IN
INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Concentration Units: mg/L
Initial Calibration Continuing Calibration VerificationVerification M
Analyte True Found %R(1) True Found %R(2) Found %R(2)AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIron 5.05 5.324 105 5.05 5.320 105 5.298 105LeadMagnesiumManganese 0.05 0.0511 102 0.05 0.0522 104 0.0517 103MercuryMolybdenumNickelPotassiumSeleniumSilverSodiumStrontiumThalliumVanadiumZincTinBoronCyanide***
(1) ICV Control Limits: Mercury 90-110; Other Metals 90-110; Cyanide 85-115(2) CCV Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
ILM05.0
Page 282 of 296
U.S. EPA - CLP2A-IN
INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Concentration Units: mg/L
Initial Calibration Continuing Calibration VerificationVerification M
Analyte True Found %R(1) True Found %R(2) Found %R(2)AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIron 5.05 5.288 105 5.311 105LeadMagnesiumManganese 0.05 0.0518 104 0.0520 104MercuryMolybdenumNickelPotassiumSeleniumSilverSodiumStrontiumThalliumVanadiumZincTinBoronCyanide***
(1) ICV Control Limits: Mercury 90-110; Other Metals 90-110; Cyanide 85-115(2) CCV Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
ILM05.0
Page 283 of 296
U.S. EPA - CLP2A-IN
INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Concentration Units: mg/L
Initial Calibration Continuing Calibration VerificationVerification M
Analyte True Found %R(1) True Found %R(2) Found %R(2)AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIron 5.05 5.118 101 5.218 103LeadMagnesiumManganese 0.05 0.0503 101 0.0504 101MercuryMolybdenumNickelPotassiumSeleniumSilverSodiumStrontiumThalliumVanadiumZincTinBoronCyanide***
(1) ICV Control Limits: Mercury 90-110; Other Metals 90-110; Cyanide 85-115(2) CCV Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
ILM05.0
Page 284 of 296
U.S. EPA - CLP3-IN
BLANKS
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Preparation Blank Matrix (soil/water): SOIL
Preparation Blank Concentration Units: mg/kg
InitialCalibration Continuing Calibration PreparationBlank(mg/L) Blank (mg/L) Blank
Analyte C 1 C 2 C 3 C C MAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIron 0.020612 U 0.020612 U 0.020612 U 0.020612 U 2.39 JLeadMagnesiumManganese 0.000445 U 0.000445 U 0.000445 U 0.000445 U 0.045 UMercuryMolybdenumNickelPotassiumSeleniumSilverSodiumStrontiumThalliumVanadiumZincTinBoronCyanide***
FORM III - IN ILM05.0
Page 285 of 296
U.S. EPA - CLP3-IN
BLANKS
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Preparation Blank Matrix (soil/water): SOIL
Preparation Blank Concentration Units:
InitialCalibration Continuing Calibration PreparationBlank(mg/L) Blank (mg/L) Blank
Analyte C 1 C 2 C 3 C C MAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIron 0.020612 U 0.020612 U 0.020612 ULeadMagnesiumManganese 0.000445 U 0.000445 U 0.000445 UMercuryMolybdenumNickelPotassiumSeleniumSilverSodiumStrontiumThalliumVanadiumZincTinBoronCyanide***
FORM III - IN ILM05.0
Page 286 of 296
U.S. EPA - CLP4A-IN
ICP-AES INTERFERENCE CHECK SAMPLE
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
ICP-AES Instrument ID: ICPMS2
Concentration Units: mg/l
True Initial Found Final FoundSol. Sol. Sol. Sol. Sol. Sol.
Analyte A AB A %R AB %R A %R AB %R
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIron 250.0 250.0 248.20771 99 246.84223 99LeadMagnesiumManganese 0.1 0.0035564 0.1048574 105MercuryMolybdenumNickelPotassiumSeleniumSilverSodiumStrontiumThalliumVanadiumZincTinBoron***
FORM IVA - IN ILM05.0
Page 287 of 296
U.S. EPA - CLP5A-IN EPA SAMPLE NO.
MATRIX SPIKE SAMPLE RECOVERY
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Matrix (soil/water): SOIL
% Solids for Sample: 28.1
Concentration Units: mg/kg
Control Spiked Sample Sample SpikeAnalyte Limit Result (SSR) Result (SR) Added (SA)
%R C C %RAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIron 75-125 42000 38700 1710 193LeadMagnesiumManganese 75-125 842. 468 342.0 109MercuryMolybdenumNickelPotassiumSeleniumSilverSodiumStrontiumThalliumVanadiumZincTinBoronCyanide
Comments:
FORM VA -IN ILM05.0
NC046SG-000015-20120821S
Page 288 of 296
U.S. EPA - CLP6-IN EPA SAMPLE NO.
DUPLICATES
Lab Name: Alpha Analytical
Lab Code: AAL Case No.:
Matrix (soil/water): SOIL
% Solids for Sample: 28.1 % Solids for Duplicate: 28.1
Concentration Units: mg/kg
Control Sample (S) Duplicate (D)Analyte Limit C C RPD
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIron 20 38700 40400 4LeadMagnesiumManganese 20 468 488. 4MercuryMolybdenumNickelPotassiumSeleniumSilverSodiumStrontiumThalliumVanadiumZincTinBoronCyanide
FORM VI - IN ILM05.0
NC046SG-000015-20120821D
Page 289 of 296
U.S. EPA - CLP7-IN
LABORATORY CONTROL SAMPLE
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002SOIL
Aqueous (mg/L) Solid (mg/kg)Analyte True Found %R Limits True Found C Limits %R
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIron 1000 1140 75-125 114LeadMagnesiumManganese 200 226. 75-125 113MercuryMolybdenumNickelPotassiumSeleniumSilverSodiumStrontiumThalliumVanadiumZincTinBoronCyanide
FORM VII - IN ILM05.0
Page 290 of 296
U.S. EPA - CLP8-IN EPA SAMPLE NO.
ICP-AES AND ICP-MS SERIAL DILUTIONS
Lab Name: Alpha Analytical SDG No.: L1215002
Lab Code: AAL
Matrix (soil/water): SOIL
Concentration Units: mg/Kg
Serial %Initial Sample Dilution Difference
Analyte Result (I) C Result (S) C Q M
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIron 38700 38900 1LeadMagnesiumManganese 468. 462. 1MercuryMolybdenumNickelPotassiumSeleniumSilverSodiumStrontiumThalliumVanadiumZincTinBoronCyanide
FORM VIII-IN ILM05.0
NC046SG-000015-20120821SER
Page 291 of 296
U.S. EPA - CLP12-IN
PREPARATION LOG
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Preparation Method: EPA 3050B
EPASample Preparation Weight VolumeNo. Date (gram) (mL)
L1215002-01 08/27/12 2.080 50L1215002-03 08/27/12 2.050 50L1215002-05 08/27/12 2.030 50L1215002-07 08/27/12 2.010 50L1215002-09 08/27/12 2.070 50L1215002-11 08/27/12 2.070 50L1215002-13 08/27/12 2.120 50L1215002-15 08/27/12 2.130 50L1215002-17 08/27/12 2.060 50L1215002-19 08/27/12 2.130 50L1215002-21 08/27/12 2.040 50L1215002-23 08/27/12 2.120 50L1215002-25 08/27/12 2.160 50WG557278-1 08/27/12 1.000 50WG557278-2 08/27/12 1.000 50WG557278-3 08/27/12 2.020 50WG557278-4 08/27/12 2.080 50WG557278-5 08/27/12 2.130 50
FORM XII-IN ILM05.0
Page 292 of 296
U.S. EPA - CLP13-IN
Analysis Run Log
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Instrument ID: ICPMS2 Analysis Method: 6020A
Start Date: 08/29/12 End Date: 08/29/12
AnalytesLab
Sample D/F Time A S A B B C C C C C F P M M H M N K S A N S T V Z SID L B S A E D A R O U E B G N G O I E G A R L N N
A1-ICV 1 9:31 X XA1-ICB 1 9:32 X XA1-ICSA 1 9:34 X XA1-ICSAB 1 9:35 X XA1-CCV 1 9:41 X XA1-CCB 1 9:42 X XA1-CCV 1 9:52 X XA1-CCB 1 9:53 X XWG557278-1 2 9:57 X XWG557278-2 2 9:58 X XL1215002-01 20 9:59 X XL1215002-03 20 10:00 X XL1215002-05 20 10:01 X XL1215002-07 20 10:02 X XA1-CCV 1 10:03 X XA1-CCB 1 10:03 X XL1215002-09 20 10:05 X XL1215002-11 20 10:06 X XL1215002-13 20 10:07 X XL1215002-15 20 10:08 X XWG557278-3 20 10:09 X XWG557278-5 100 10:09 X XWG557278-4 20 10:10 X XL1215002-17 20 10:11 X XL1215002-19 20 10:12 X XL1215002-21 20 10:13 X XA1-CCV 1 10:14 X XL1215002-23 20 10:15 X XA1-CCB 1 10:15 X XL1215002-25 20 10:16 X XA1-CCV 1 10:24 X XA1-CCB 1 10:25 X X
Page 293 of 296
U.S. EPA - CLP13-IN
Analysis Run Log
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
Instrument ID: ICPMS2 Analysis Method: 6020A
Start Date: 08/29/12 End Date: 08/29/12
AnalytesLab
Sample D/F Time A S A B B C C C C C F P M M H M N K S A N S T V Z SID L B S A E D A R O U E B G N G O I E G A R L N N
A1-CCV 1 10:31 X XA1-CCB 1 10:32 X X
FORM XIII-IN ILM02.0
Page 294 of 296
U.S. EPA - CLP14-IN
ICP-MS TUNE
Lab Name: Alpha Analytical
Lab Code: AAL SDG No.: L1215002
ICP-MS Instrument ICPMS Date: 08/29/12
Element - MassAvg. Measured Mass (amu) Avg. Peak Width at10% Peak Height (amu)
%RSD
9Be 8.975 0.724 0.87259Co 58.975 0.697 0.907115In 114.875 0.676 0.845205Tl 205.025 0.733 0.719238U 238.125 0.717 0.565
Comments:
FORM XIV-IN ILM05.0
Page 295 of 296
U.S. EPA - CLP15-IN
ICP-MS Internal Standards Relative Intensity Summary
Lab Name: Alpha Analytical SDG No.: L1215002
Lab Code: AAL
ICP Instrument ID: ICPMS2 Start Date: 8/29/2012 End Date: 8/29/2012
EPA Sample Time Internal Standards %RI For:
No. Lithium Q Scandium Q Germanium Q Indium Q Bismuth Q Q
ICV 9:31 101
ICB 9:32 101
ICSA 9:34 77
ICSAB 9:35 76
CCV 9:41 101
CCB 9:42 101
CCV 9:52 102
CCB 9:53 103
WG557278-1 9:57 104
WG557278-2 9:58 99
L1215002-01 9:59 102
L1215002-03 10:00 103
L1215002-05 10:01 102
L1215002-07 10:02 102
CCV 10:03 102
CCB 10:03 102
L1215002-09 10:05 101
L1215002-11 10:06 102
L1215002-13 10:07 101
L1215002-15 10:08 101
WG557278-3 10:09 101
WG557278-5 10:09 103
WG557278-4 10:10 102
L1215002-17 10:11 104
L1215002-19 10:12 102
L1215002-21 10:13 103
CCV 10:14 102
L1215002-23 10:15 104
CCB 10:15 102
L1215002-25 10:16 104
CCV 10:24 105
CCB 10:25 105
CCV 10:31 102
CCB 10:32 102
Page 296 of 296