Air Sampling...2011/07/19 · WDNR LAB lD: 113133790 NELAP LAB lD: E37658 EPA LAB W100007 Supplement to test report#: 9391658 Amended Report WSLH Sample: OV003833 D,F Kurrycz, M,D

4631 County Road A • Oregon, Wisconsin 53575 Phone: 608.576.3001 • Fax: 608.835.3542

July 19, 2011 Mr. Michael Schmoller Wisconsin Department of Natural Resources 3911 Fish Hatchery Road Fitchburg, Wisconsin 53711 RE: Soil and Groundwater Sampling Properties Adjacent to Madison‐Kipp Corporation Dear Mr. Schmoller:

Soil and soil vapor samples have recently been collected and analyzed from several properties adjacent to the eastern property line of Madison‐Kipp Corporation (“MKC”). This work was performed in cooperation with requests from the Wisconsin Department of Natural Resources (“WDNR”). Work was completed by RJN Environmental Services, LLC (“RJN”).

Soil Vapor and Air Sampling

Soil vapor samples were collected from back yard probes at 142, 150, 154 and 202 South Marquette Street. Sub‐slab vapor samples were collected at 150, 154 and 162 South Marquette Street, and indoor (basement) air samples were collected at those locations, as well. Finally, a single ambient air sample was collected in the back yard of the residence at 150 South Marquette Street.

Back yard wells were sampled through soil vapor wells, which were installed in 2005 and in June of 2011. Soil vapor wells were installed at 150, 154 and 162 South Marquette Street (the home owner at 162 South Marquette Street has removed his). RJN installed wells at 142 and 202 South Marquette Street in June 2011. The initial installation of soil vapor probes was conducted at 150, 154 and 162 South Marquette Street because these properties are adjacent to the area of the MKC property which was impacted by fallout from a vapor degreasing vent, which had been located on the east wall of the MKC building. The wells installed in June 2011 were to verify that the extent of the presence of soil vapor has been defined.

A sample pump was used to purge the wells for approximately 10 minutes prior to sample collection. Samples were collected in a Summa Canister, provided by the Wisconsin State Laboratory of Hygiene (“WSLH”).

Sub‐slab samples were collected using a “helium shroud” method. Components of the sub‐slab vapor probes are shown on Figure 1; Figure 2 shows the setup of the helium shroud. Helium is

Mr. Michael Schmoller Wisconsin Department of Natural Resources

July 9, 2011 Page 2

pumped into the shroud, and a sample is drawn from the vapor probe. The vapor is screened using a helium‐detecting field instrument. If no helium is detected, it is assumed that the probe is properly sealed, and a sample is collected. As with the well sampling, samples were collected in Summa Canisters, provided by the WSLH.

Basement air samples were collected in Summa Canisters. Sampling was conducted in the same area in which the sub‐slab probes were installed. An ambient outdoor air sample was also collected. This was collected in the back yard of the residence at 150 South Marquette Street. After sample collection, all samples were delivered to the WSLH for analyses of tetrachloroethene (“PCE”) and its breakdown compounds.

The results from the soil vapor and air samples are summarized in the attached Table 1; laboratory reports are provided in Appendix A. Soil vapor well results for PCE ranged from 0.341 parts per billion by volume (“ppb”) at 202 South Marquette Street to 188 at 154 South Marquette Street. The assumption that the three properties adjacent to the MKC release (150, 154 and 162) represent the core of the soil vapor plume is supported by the results of the sampling. PCE concentrations at 150 and 154 South Marquette Street were 5.78 ppb and 188 ppb, respectively, and the most recent sample collected at 162 South Marquette Street (September 2009) contained 56 ppb of PCE. The two wells installed in 2011 yielded 1.87 ppb of PCE (142 South Marquette Street) and 0.341 ppb (202 South Marquette Street). No breakdown compounds (cis‐ & trans‐1,2‐dichloroethene, trichloroethene and vinyl chloride) were detected in any samples.

The soil vapor wells are completed in clay; however, the basements of the residences are, as well. Consequently, the results from the well sampling should be considered to be an accurate representation of the soil vapor concentrations present at those locations.

Soil Sampling

Soil samples were collected in the back yards of the properties at 150, 154 and 162 South Marquette Street in the winter of 2003. A sample collected from 162 South Marquette Street produced a concentration of 2.68 mg/kg (parts per million) of PCE, which exceeded the USEPA direct contact exposure limit of 1.23 mg/kg (calculated using the USEPA soil screening website with Wisconsin Department of Natural Resources default parameters for non‐industrial sites). The concentrations detected in samples from 154 and 162 were below the USEPA standard.

Based on the results at 162 South Marquette Street, arrangements were made to apply an oxidation compound (Biox – Deep Earth Technologies) to the soil on that property. This work was completed in 2003.

Soil samples were collected in May 2011 in the three yards noted above, in the approximate locations and depths from which samples were collected in February 2003. Sample locations are shown on Figure 3. Samples were forwarded to TestAmerica for analyses of volatile organic

Mr. Michael Schmoller Wisconsin Department of Natural Resources

July 9, 2011 Page 3

compounds (“VOCs”); laboratory reports are provided in Appendix B. PCE was detected in five of the samples, as follows:

SAMPLE PCE (mg/kg)

HA 101 <0.031

HA 102 0.033

HA 103 0.180

HA 104 0.610

HA 105 0.110

HA 106 0.092

No other VOCs were detected in any of the samples collected. These data show that the injection completed in 2003 was effective in the remediation of the soil on the property at 162 South Marquette Street, and that no further remedial activities are necessary for these soils.

Conclusions

The extent of soil vapor impacts appears to be defined to the north and south of the properties on the west side of South Marquette Street. Radon systems have been installed in the basements of five properties, removing PCE vapors from beneath the basement, and discharging them to the atmosphere.

Soil sampling in February 2003 indicated the exceedance of the USEPA’s direct contact exposure limit for PCE at a single location, on the property at 162 South Marquette Street. 2011 sampling confirmed that the injection completed in 2003 brought those concentrations to below the exposure limit. No further soil sampling or remediation is anticipated at this time. Sincerely, RJN ENVIRONMENTAL SERVICES, LLC

Robert J. Nauta, P.G. Hydrogeologist

cc: Mark Meunier – Madison‐Kipp Corporation

142 S. Mar. 202 S. Mar.

Well Indoor Sub‐slab Well Indoor Sub‐slab Well Indoor Sub‐slab Well

cis‐1,2‐Dichloroethene <0.085 <0.085 <20 <0.085 <0.085 <53.22 <20 <0.085 <10 <0.085 <0.085

trans‐1,2‐Dichloroethene <0.085 <0.085 <20 <0.085 <0.085 <53.22 <20 <0.085 <10 <0.085 <0.085

Trichloroethene <0.085 <0.085 <20 <0.085 <0.085 <53.22 <20 <0.085 <10 <0.085 <0.085

Tetrachloroethene 1.87 <0.085 108 5.78 0.668 470 188 <0.085 31 0.341 <0.085

Vinyl chloride <0.085 <0.085 <20 <0.085 <0.085 <53.22 <20 <0.085 <10 <0.085 <0.085

All quantities in parts per billion.1 Collected in back yard at 150 South Marquette Street.2 Level of detect not achievalbe due to dilution.

See lab reports for additional qualifications.

TABLE 1

AIR AND SOIL VAPOR SAMPLE RESULTS

SOUTH MARQUETTE STREET

MADISON, WISCONSIN

150 South Marquette 154 South Marquette 162 South MarquetteOutdoor

1PARAMETER

TUBE

COMPRESSIONNUT

COMPRESSIONFITTING

CAP

DRAWN BY PROJ. No. DATE FILE

RN 09-101 14 JUL 11 PROBE DETAIL4631 COUNTY ROAD A OREGON, WISCONSIN 53575 (608) 576-3001

Surface Water StudiesGroundwater StudiesSite Investigations

MADISON-KIPP CORPORATIONMADISON, WISCONSIN

SUB-SLAB PROBE CONSTRUCTIONNOTE: ALL COMPONENTS ARESTAINLESS STEEL.


RN 09-101 14 JUL 11 GAS PROBE4631 COUNTY ROAD A OREGON, WISCONSIN 53575 (608) 576-3001


MADISON-KIPP CORPORATIONMADISON, WISCONSIN

SUB-SLAB SAMPLING APPERATUS

CONCRETEFILLER

HELIUM INTO SHROUD

HEL

IUM

TA

NK

AIRPUMP

RIGIDPLASTICSHROUD


MADISON KIPP CORPORATIONMADISON, WISCONSIN

MAY 2011 SOIL SAMPLE LOCATIONS

RN 09-101 18 JUL 11 SOIL SAMP4631 COUNTY ROAD A OREGON, WISCONSIN 53575 (608) 576-3001


150

154

162

AREA OFDETAIL

0 25 50

SCALE IN FEET

MA

RQ

UET

TE S

TREE

T

HA 101

HA 102

HA 104HA 103

HA 106HA 107

SOIL SAMPLE LOCATION

APPENDIX A

AIR AND SOIL GAS LABORATORY REPORTS

Wisconsin State Laboratory of Hygiene2601 Agriculture Drive, PO Box7996Madison, Wl53707-7996(800)442-46 1 8 . F AX (608)224-6213http://www.slh.wisc.edu

Laboratory Report

Field #: 150 SOIL

Collection Start: 0210312011

Collection End:

Collected By: BOB NAUTA

County:

Sample Source: AIR

Sample Depth:

Sample Information:

Sample Location:

Sample Description:

Analyses and Results:

Environmental Health Division

WDNR LAB lD: 113133790 NELAP LAB lD: E37658 EPA LAB W100007Supplement to test report#: 9391658

Amended Report WSLH Sample: OV003833

RJN ENVIRONMENTAL SVC., LLC

4631 COUNTY ROAD A

oREGON, Wt53575

D,F. Kurtycz, M.D., Medical Director. Charles D Brokopp, Dr.P.H,, Director

Organic Chemistry

Wl DATCP lD: 105-415

Bi l lTo

Bi l l ing lD: 7305879

Customer lD: 320225

TRACKING 4920

2601 AGRICULTURAL DRIVE

MADISON WI 53718

tD#:

Waterbody/Outfall lD:

PointANell:

Account #: LH034

Project No:

Date Received: 0210412011

Date Reported: 0410712011

Sample Reason:

Analysis Date0210912011

Lab Comment

Method

PROPENE

DICHLORODI FLUOROMETHANE

CHLOROMETHANE

1 .2.DICHLOROTETRAFLUOROETHANE

VINYL CHLORIDE

1,3-BUTADIENE

BROMOMETHANE

CHLOROETHANE

ACETONE

HALOCARBON 1 1

1 .1-DICHLOROETHENE

METHYLENE CHLORIDE

CARBON DISULFIDE

Result

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD LOQ Report Limit

20.

20.

20.

20.

20.

20.

2Q.

20.

20.

20.

20.

20.

20.

Page 1 of4

Wisconsin State Laboratory of Hygiene2601 Agnculfure Drive, PO Box 7996Madison, W I 5370'7 -7996(800x42-461 8 . FAX (608)224-6213httD://w$,v slh wisc edu

Laboratory Report


WDNR LAB lD: 113133790 NELAP LAB lD: E37658 EPA LAB W100007Supplement to test report#: 9391658


D,F Kurrycz, M,D , Medical Director. Charles D Brokopp, Dr P H , Director

Organic Chemistry


lvsis Method

1, 1,2-TRICHLOROTRI FLUOROETHANE

TRANS-1,2-DICHLOROETHYLENE

1,1-DICHLOROETHANE

TERT-BUTYL METHYL ETHER

VINYL ACETATE

METHYL ETHYL KETONE

CIS-1 .2.DICHLOROETHYLENE

HEXANE

CHLOROFORM

ETHYL ACETATE

TETMHYDROFURAN,1,2-DICHLOROETHANE

1, 1, l .TRICHLOROETHANE

BENZENE

CARBON TETRACHLORIDE

CYCLOHEXANE

1,2-DICHLOROPROPANE

BROMODICHLOROMETHANE

TRICHLOROETHYLENE

1,4-DIOXANE

HEPTANE

CIS-l ,3.DICHLOROPROPENE

METHYL ISOBUTYL KETONE

TRANS-1 .3-DICHLOROPROPENE

1, 1,2-TRICHLOROETHANE

TOLUENE

METHYL N-BUTYL KETONE

DIBROMOCHLOROMETHANE

1,2-DIBROMOETHANE

T.ETRA€FJ L€ RO ETH YL ENE

CHLOROBENZENE

Result

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

108.

<20.

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V


20.

20.

20.

zv .

zv .

20.

20.

20.

20.

20.

zv .

zv .

20.

20.

20.

20.

20.

20.

zv .

20.

20.

zu .

20.

zv.

20

20.

20.

zu .

20.

20.

20.

Page 2 of 4

Wisconsin State Laboratory of Hygiene2601 Agriculture Drive, PO Box 7996Madison, WI 53707-7996(800)442-4618 . F Ax (608)224-6213http : //www. slh.wi sc.edu

Laboratory ReportD.F. Kurtycz, M.D., Medical Director. Charles D Brokopp, Dr.p,H , Director

Environmental Health Division Organic Chemistry

WDNR LAB lD: 113133790 NELAP LAB lD: E37658 EPA LAB W100007 Wl DATCP lD: 105-415

Supplement to test report#: 9391658


Method

ETHYLBENZENE

M/P-XYLENE

BROMOFORM

STYRENE

1, 1,2,2-TETMCHLOROETHANE

O-XYLENE

1 -ETHYL-4.METHYL BENZENE

1,3,s-TRIMETHYL BENZENE

1,2,4-TRIMETHYL BENZENE

CHLOROMETHYL BENZENE (ALPHA)

l ,3.DICHLOROBENZENE

1,4-DICHLOROBENZENE

l,2.DICHLOROBENZENE

1,2,4-TRICHLOROBENZENE

HEXACH LORO-1 . 3-BUTADI EN E

Result

<20.

<40.

<20,

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

Report Limil

20.

20.

20.

20.

20.

20.

20.

20.

20.

20.

20.

20.

20.

20.

2Q.

LOD LOQ

Method Result Units LOD LOO Report Limit

TOXIC ORGANIC COMPOUNDS IN COMPLETE 1AMBIENT AIR TO15 - PREP

Page 3 of 4

Wisconsin State l,aboratory of Hygiene260 I Agriculture Drive, PO Box 7996Madison, Wl53701-7996(800)44246 I 8 . FAX (608)224-621 3httF, : //wuv.slh.wisc. edu

Laboratory Report


D F Kurtycz, M D, Medical Director . Char lesD. Brokopp, Drp H, Director

Organic ChemistryWDNR LAB lD: 113133790 NELAP LAB lD: E37658 EPA LAB Wl000O7 Wl DATCP lD: 105-415

Supplementtotestreport#: 9391658


Test results for NELAP accredited tests are certified to meet the requirements of the NELAC standards. For a list of accredited analytes seehttp://www. slh wisc edu/nelap/

List of Abbreviations:

LOD = Level of detectionLOQ = Level of quantiflcationND = None detected. Results are less than the LOD

Responsible Party: +{ .-4<"D

lf there are questions about this report, please contact Steve Geis at608-224-6269.

The results in this report apply only to the sample specifically listed above. This report is not to be reproduced except in full.

Report #: 9404841 Page 4 of4

Wisconsin State Laboratory of llygiene2601 Agriculture Drive. P0 Box 7996Madison. WI 53707-799(r(8f i ) )442-46| 8 . FAX (608)224_62l - lhttp://www.slh.u'isc-edu

Laboratory ReportD.F. Kurtycz, M.D.. Medical Dircctor . Char les D. Brokopp. Dr.P.H.. Dirsctor

Environmental Health Division Organic ChemistryWDNR LAB lD: 113133790 NELAP LAB lD: E37658 EPA LAB W100007 Wt DATCp tD: 105-415

F ie ld # : 150 WELL


Col lect ion End:


County.

Sample Source: AIR

Sample Depth:

Sample Information:

Sample Locat ion:

Sample Descript ion:


WSLH Sample: OV003834


4631 COUNTY ROAD A

oREGON, Wt 53575

B i l l T o


Customer lD: 320225

TRACKING 4920


MADISON WI 537,I8

rD#.


PoinVWell:

Account #: LH034

Project No:DateReceived: 0210412011


Sample Reason:

Analysis Date02t09t2010

Lab CommentUPPER QC LIMIT FOR CALIBRATION CHECK EXCEEDED--QU.

s Method

PROPENE


CHLOROMETHANE

1,2.D IC HLOROTETRAFLUOROETHAN E

VINYL CHLORIDE,I,3-BUTADIENE

BROMOMETHANE

CHLOROETHANE

ACROLEIN

ACETONE

HALOCARBON 1 1

Result

N D

0.509

ND

ND

N D

N D

N D

ND

ND

"QU 0.522

0.262

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.085

0.085

0.085

0 . 1 0

0.085

0.085

0.085

0,085

0.400

0.400

0.085

LOQ Report Limit

0.280

0.280

0.280

0.330

0.280

0.280

0.280

0.280

1 . 3 2

1 . 3 2

0.280

Note: The reported value above is equal to or greater than the LOD and less than the LOQ

1., I-DICHLOROETHENE ND PPB V 0.085 0.280

Page 1 of4

Wisconsin Stale Laboratory of tlygiene2601 Agriculture Drive. PO Box 7996Madison, WI 53707-7996(800)442-461 U . FAX (608)224-62 l lhttp ://wwrv.slh.wisc.edu

Laboratory Report


WDNR LAB lD: 113133790 NELAP LAB tD: E37658

D.F. Kurtycz, M.D.. Mcdical Direcror . Char les D. Brokopp. Dr.p_H.. Director

Organic Chemistry

EPA LAB WIOOOOT Wl DATCP lD: 105-4'15


lysis Method

METHYLENE CHLORIDE

CARBON DISULFIDE,I, 1,2-TRICHLOROTRI FLUOROETHANE

TRANS- 1,2-DICHLOROETHYLENE

1,1-DICHLOROETHANE


VINYL ACETATE

METHYL ETHYL KETONE

CIS-1,2-DICHLOROETHYLENE

HEXANE

CHLOROFORM

ETHYL ACETATE

TETRAHYDROFURAN

1 ,2.DICHLOROETHANE

1 . 1 . 1 -TRICHLOROETHANE

BENZENE


CYCLOHEXANE

1,2-DICHLOROPROPANE


TRICHLOROETHYLENE

1,4-DIOXANE

HEPTANE

CIS-1,3-DICHLOROPROPENE


TRANS-1,3-DICHLOROPROPENE

1 . 1 .2-TRICHLOROETHANE

TOLUENE



1,2-DIBROMOETHANE

Result

ND

ND

ND

N D

N D

ND

ND

ND

N D

N D

ND

N D

ND

ND

ND

N D

N D

ND

ND

ND

ND

ND

ND

ND

ND

N D

ND

0.464

N D

N D

ND

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.400

0.085

0.085

0.085

0.085

0.085

0.085

0 . 1 0

0.085

0.400

0.085

0.085

0.400

0.085

0.085

0.085

0.400

0.085

0.085

LOQ

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

t . J z

0.280

0.280

0.280

0.280

0.280

0.280

0.33

0.280

1 . 3 2

0.280

0.280

1 . 3 2

0.280

0.280

0.280

1 . 3 2

0.280

0.280

Report Limit

Page 2 of 4

Wisconsin State Laboratory of' Hygiene2601 Agriculture t)rive, P0 Box 7996Madison. Wl 53707-7996(flu))4.+2-46 | 8 . FAX (608)224-62 I 3http:iiwww.slh.*'isc.edu

Laboratory Report


WDNR LAB lD: 1 13133790 NELAP LAB lD: E37658

D.F. Kurtycz, M.D.. Medical Director . Char les D. Brokopp, f ) r .p.H.. Director

Organic Chemistry

EPA LAB W100007 Wl DATCP lD: 105-415


Analysis Method

TETRACHLOROETHYLENE

CHLOROBENZENE

ETHYLBENZENE

M/P-XYLENE

BROMOFORM

STYRENE

1,1,2,2-T ETRACH LOROETHAN E

O-XYLENE

1 -ETHYL-4-METHYL BENZENE


1.2.4-TRIMETHYL BENZENE


1,3-DICHLOROBENZENE

1,4-DICHLOROBENZENE

1,2-DICHLOROBENZENE,I,2,4-TRICHLOROBENZENE

HEXACHLORO-1,3-BUTADIENE

Result

5.78

ND

ND

0.726

ND

ND

ND

v .26J

0.379

N D.QU 0 .519

ND

ND

ND

ND

ND

N D

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.08s

0.085

0.085

o.170

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

LOQ

0.280

0.280

0.280

0.561

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

Report Limil


Lab Comment

Analysis Method Result Units LoD Loe Report Limit

SCREENING TEST FOR HIGH EPA TO15 COMPLETE 1SAMPLES


Lab Comment

Analysis Method Resutt Units LoD Loe Report Limit


Page 3 of 4

Wisconsin State Laboratory of Ilvgiene2601 Agriculture Drive. PO Box 7996Madison, WI 5-1707-7996(800)442-4618 . FAX (608)224_621 3http: //u'wu,.slh. wisc.edu

Laboratory ReportD.F. Kurtycz, M.D.. Medical Director . Char lcs D. Brokopp. Dr.p.H.. Direcror


WDNR LAB lD: 113133790 NELAP LAB lD: E37658 EPA LAB W100007 Wl DATCP tD: 105-415


Test results for NELAP accredited tests are certified to meet the requirements of the NELAC standards. For a list of accredited analytes seehttp:/ /www.slh.wisc.edu/nelap/


LOD = Level of detectionLOQ = Level of quantification

ND = None detected. Results are less than the LOD

Responsible Party. *fr_ . -A<rD

lf there are questions about this report, please contact Steve Geis aI608-224-6269.


Reoort #: 9391659 Page 4 of 4

Wisconsin State Laboratorv of Ilygicnc2601 Agriculture Dlive, PO Box 7996Madison, WI 53707-7996(800),+42-461 8 - FAX (608)224-621 3http://www.s lh.wisc.cdu

Laboratory ReportD.F. Kurtycz, M.D.. Medical [ ) r rector . Char les D. Brokopp. Dr.P.H., Director


WDNR LAB lD: 1 13133790 NELAP LAB lD: E37658 EPA LAB W100007 Wl DATCP lD: 105-415

F ie ld # : 150 INDOOR


Col lect ion End:


County:

Sample Source: AIR

Sample Depth:

Sample Information:

Sample Locat ion:

Sample Description:




4631 COUNTY ROAD A

oREGON. Wt5357s

B i l l T o


Cuslomer lD: 320225

TRACKING 4920


MADISON WI 53718

rD#:


PoinUWell:

Account #. LH034

Project No.

DateReceived: 0210412011


Sample Reason:

Analysis Date02t07 t2011

Lab CommentSEE OVOO3B32.MM1

s Method

PROPENE

DICH LORODI FLUOROMETHANE

CHLOROMETHANE

1,2-D ICHLOROTETRAFLUOROETHAN E

VINYL CHLORIDE

1,3-BUTADIENE

BROMOMETHANE

CHLOROETHANE

ACROLEIN

ACETONE

HALOCARBON 11

1,1-DICHLOROETHENE

METHYLENE CHLORIDE

Result

" l < 1 . 2 0

ND

N D

ND

N D

ND

ND

ND

N D. Q U 1 1 . 0

0.526

ND

1 . 4

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.085

0.085

0.085

0 . 1 0

0.085

0.085

0.085

0.085

0.400

0.400

0.085

0.085

0.085

LOQ

0.280

0.280

0.280

0.330

0.280

0.280

0.280

0.280

1 . 3 2

1 . 3 2

0.280

0.280

0.280

Report Limit

Page 1 of4

Wisconsin Statc Laboratory of Hygiene2601 Agriculture Drive, PO Box 7996Madison, Wl 53707-7996(800)4'12-46r ri . FAX {60t{)224-62 | 3http :1/tvww.slh.wisc.cdu

Laboratory Report


WDNR LAB lD: 1 '13133790 NELAP LAB lD: E37658

D.F. Kurtycz, M.D., Medical Director . Char les D. Fl rokopp. Dr.P.FL. Dircctor

Organic Chemistry



nalysis Method

CARBON DISULFIDE

1 . 1 .2-TRICHLOROTRI FLUOROETHANE


l , l .D ICHLOROETHANE


VINYL ACETATE

METHYL ETHYL KETONE

CIS-1,2-D ICHLOROETHYLENE

HEXANE

CHLOROFORM

ETHYL ACETATE

TETRAHYDROFURAN

l,2.DICHLOROETHANE,1, 1, 1 -TRICHLOROETHANE

BENZENE


CYCLOHEXANE

1,2-DICHLOROPROPANE


TRICHLOROETHYLENE

1,4-DIOXANE

HEPTANE

CIS-1,3-D ICHLOROPROPENE




TOLUENE



Result

N D

N D

N D

ND

ND

0.609

1 . 1 4

N D

0 . 5 1 4

ND

ND

0.580

N D

N D

0.411

ND

ND

ND

ND

N D

ND

0.464

N D

ND

ND

ND

0.862

ND

ND

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.085

0.085

0.085

0.08s

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.400

0.085

0.085

0.085

0.085

0.085

0.085

0 . 1 0

0.085

0.400

0.085

0.085

0.400

0.085

0.085

0.085

0.400

0.085

LOQ

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

t . 5 z

0.280

0.280

0.280

0.280

0.280

0.280

0.33

0.280

1 . 3 2

0.280

0.280

t . J z

0.280

0.280

0.280

1 . 3 2

0.280

Report Limit

Note: The reported value above is equal to or greater than the LOD and less than the LOQ.

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

Page 2 of 4

Wisconsin State Laboratory of [lygiene2601 Agriculture Drive, PO Box 7996Madison. Wl 53707-7996(8t [ )442-461 8 . FAX (608)224-621 ]http://*rvw.slh.rvisc.edu

Laboratory Report



D.F. Kurtycz, M.D., Medical Director . Char les D. Brokopp. Dr.P.H.. Director

Organic Chemistry



\nalysis Method

1,2-DIBROMOETHANE

TETRACHLOROETHYLENE

CHLOROBENZENE

ETHYLBENZENE

M/P.XYLENE

BROMOFORM

STYRENE

1,1,2,2-T ET RAC HLOROETHAN E

O-XYLENE


1 .3.s.TRIMETHYL BENZENE


CHLOROMETHYL BENZENE (ALPHA),I ,3.DICHLOROBENZENE

l,4.DICHLOROBENZENE

1,2-DICHLOROBENZENE

1 .2.4-TRICHLOROBENZENE

HEXACHLORO-1 .3-BUTADIENE

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.085

0.085

0.085

0.085

0.1 70

0.085

0.08s

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

LOQ

0.280

0.280

0.280

0.280

0.56' l

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

Report Limil

N D

N D

0.667

ND

o.432

ND

ND

ND

N D.QU 0.369

N D

N D

ND

ND

ND

ND

o v O 0 3 B 3 2 . M M 1 :

WISCONSIN STATE LABORATORY OF HYGIENE SAMPLE OVOO3B32 CONTAINS THEFOLLOWING FLAGS.

INTERFERENCE INDICATED BY * I .

UPPER QC L IMIT FOR CALIBRATION CHECK EXCEEDED - *QU.

I F Y O U H A V E A N Y Q U E S T I O N S , C O N T A C T S T E V E G E I S A T ( 6 0 8 ) 2 2 4 _ 6 2 6 9 .


Lab Comment

Analysis Method Result Units LOD LOQ Report Limit


Page 3 of 4

Wisconsin State Laboratory of Hygienc2601 Agnculture Drive. PO Box 7996Madison, WI 53707-7996(ft00)442-46 I 8 . r.AX (608)224-62 r 3http :i,/wwrv.slh.wisc.edu

Laboratory Report



D.F. Kurtycz, M.D.. Medical Director . Char les D. tsrokopp, Dr.P. I I . . Director

Organic Chemistry

EPA LAB WIOOOOT Wl DATCP lD: 105-415

Test results for NELAP accredited tests are certified to meet the requirements of the NELAC standards. For a list of accredited analytes seehttp. / /www.slh.wisc.edu/nelap/


LOD = Level of detection

LOQ = Level of quantif ication


Responsible Party: ffi7 _AoD


The results in this report apply only to the sample specifically listed above. This report is not to be reproduced except in full


alvsis Date Lab Commentt2011

lysis Method Result Units LOD LOQ Report Limit


Reoort #. 939'1657 Page 4 ot 4

Wisconsin State Laboratory of Hygrene2601 Agnculture Drivc. PO Box 7996Madison, Wl 53707-7996(n00)442-46I 8 . FAX (608)22,{-62I3http :,'/ulvw.slh.w,isc.edu

Laboratory ReportD.F. Kurtycz, M.t) . , Medical Director . Char les D. Brokopp. I ) r .P. t l . . Director


WDNRLABID: 1 '13133790 NELAPLABID: E37658 EPALAB W100007 Wl DATCPID: 105-415

Field #: 154 INDOOR


Col lect ion End:


County:

Sample Source: AIR

Sample Depth:

Sample lnformation:

Sample Location:

Sample Description:




4631 COUNTY ROAD A

oREGON. Wt 53575

B i l l T o


Customer lD: 320225

TRACKING 4920


MADISON WI 53718

rD#:


PoinUWell:

Account #. LH034

Project No.



Sample Reason:


Lab CommentSEE OVOO3836.MM1

alvsis Method

PROPENE


CHLOROMETHANE

1,2-D ICHLOROTETRAFLUOROETHAN E

VINYL CHLORIDE

1,3-BUTADIENE

BROMOMETHANE

CHLOROETHANE

ACROLEIN

ACETONE

HALOCARBON 1 1

1 ,1-DICHLOROETHENE

METHYLENE CHLORIDE

Result

- t< 10.7

0.528

0.455

ND

N D

ND

ND

N D

ND.QU 6.73

o.347

ND

N D

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.085

0.085

0.085

0 . 1 0

0.085

0.085

0.085

0.085

0.400

0.400

0.085

0.085

0.085

LOQ

0.280

0.280

0.280

0.330

0.280

0.280

0.280

0.2B0

1 . 3 2

1 . 3 2

0.280

0.280

0.280

Report Limit

Page 1 of4

Wisconsin State Laboratory of Flygiene2601 Agnculture Drive. PO Box 7996Madison, Wl -s-1707-7996(800)442-46r 8 . FAX (608)22.1-6213http ://wrvw.slh.wisc.edu

Laboratory Report


WDNR LAB lD: 113133790 NELAP LAB lD: E37658

D.F. Kurtycz, M.D., Medical Director . Char les D. t l rokopp. Dr.P. l l . . Director

Organic Chemistry



Method

CARBON DISULFIDE

1 . .1 .2-TRICHLOROTRI FLUOROETHANE

TRANS-1,2-D ICHLOROETHYLENE

l , l .D ICHLOROETHANE


VINYL ACETATE

METHYL ETHYL KETONE


HEXANE

CHLOROFORM

ETHYL ACETATE

TETRAHYDROFURAN

1,2-DICHLOROETHANE

1 . 1 . 1 -TRICHLOROETHANE

BENZENE


CYCLOHEXANE

1,2-DICHLOROPROPANE


TRICHLOROETHYLENE

1,4-DIOXANE

HEPTANE

CIS-l ,3.DICHLOROPROPENE




TOLUENE


Result

N D

N D

ND

ND

N D

0.572

0.480

0.271

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.085

0.085

0.08s

0,085

0.085

0.085

0.085

0.085

LOQ

0.280

0.280

0.2B0

0.280

0.280

0.280

0.280

0.280

Report Limit


0.726

0 . 2 1 1

0.085

0.085

0.280

0.280

Note: The reported value above is equal to or grealer than the LOD and less than the LOQ.

0.93

ND

ND

0.312

0.408

ND

0.442

N D

N D

ND

ND

0.404

ND

ND

ND

N D

0.570

ND

0.085

0.400

0.085

0.085

0.085

0.085

0,085

0.085

0 . 1 0

0.085

0.400

0.085

0.085

0.400

0.085

0.085

0.085

0.400

0.280

1 . 3 2

0.280

0.280

0.280

0.280

0.280

0.280

0.33

0.280

1 . 3 2

0.280

0.280

1 . 3 2

0.280

0.280

0,280

1 . 3 2

Page 2 of 4

Wisconsin State Laboratory of tlygicne2601 Agriculture Drive, PO Box 7996Madison. Wl 53707-7996t800)442-461 8 . FAX (608)224-621 -lhttp:,t/www.slh.rvisc.edu

Laboratory Report


WDNR LAB lD: 1 13133790 NELAP LAB

I ) .F. Kurtycz, M.D.. Medical Director . Char les D. Brokopp. Dr.P.H.. Director

Organic Chemistry

lD: E37658 EPA LAB W100007 Wl DATCP lD: 105-415


Analysis Method


1,2-DIBROMOETHANE

TETRACHLOROETHYLENE

CHLOROBENZENE

ETHYLBENZENE

M/P-XYLENE

BROMOFORM

STYRENE

1,1,2,2-T ET RAC H LO ROETHAN E

O-XYLENE

1 -ETHYL.4-METHYL BENZENE

1 .3.5-TRIMETHYL BENZENE



1,3-DICHLOROBENZENE

1,4-DICHLOROBENZENE

1,2-DICHLOROBENZENE



Result

N D

N D

0.668

ND

0.361

0"912

ND

0.333

N D

0.341

N D

N D.QU 0.331

ND

ND

ND

N D

N D

N D

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.08s

0.085

0.085

0.085

0.085

0.1 70

0.085

0.085

0.085

0.085

0.085

0.085

0.08s

0.085

0.085

0.085

0.085

0.085

0.085

LOQ

0.280

0.280

0.280

0.280

0.280

0.s61

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

U.ZUU

0.280

0.280

0.280

0.280

Report Limit

o v O 0 3 B 3 6 . M M 1 :

WISCONSIN STATE LABORATORY OF HYGIENE SAMPLE OVOO3836 CONTA]NS THEFOLLOWING FLAGS.


UPPER QC L IMIT FOR CALIBRATION CHECK EXCEEDBD "QU.

I F Y O U H A V E A N Y Q U E S T I O N S , C O N T A C T S T E V E G E I S A T ( 6 0 8 ) 2 2 4 . 6 2 6 9 .


Lab Comment

Analysis Method Result Units LOD LOQ Report Limit


Page 3 of4

Wisconsin State Laboratory of Hygienc2601 Agriculture Drive, PO Box 7996Madison, Wl 53707-7996(ti00)4.{2-46r n . FAX (608)224-62 I lhttp:,//www.slh.wisc.edu

Laboratory Report



D.F. Kurtycz. M.D., Medical Director . Char les D. Brokopp. Dr.P.H., Director

Organic Chemistry

EPA LAB WIOOOOT Wl DATCP lD: 105-4'15

Test results for NELAP accredited tests are certified to meet the requirements of the NELAC standards. For a list of accredited analytes seehtto:/iwww. slh.wisc.edu/nelap/


LOD = Level of detectionLOQ = Level of quantificationND = None detected. Results are less than the LOD

Responsible Party: ffi: *,4&D

lf there are questions about this report, please contact Steve Geis at 608-224-6269.

The results in this report apply only to the sample specifically listed above. This report is not to be reproduced except in full


ysis Method Result Units LOD LOQ Report Limit


lysis Date Lab Commenl1 1

is Method Result Units LOD LOO Report Limit


R e o o r t # : 9 3 9 1 6 6 1 Page 4 of 4

Wisconsin State Laboratory of [lygiene2601 Agricullure Drive, PO Box 7996Madison. Wl 51707-7996(800)442-461 rJ . r .AX (608)224-621 3http :/iu'wu'.slh.wisc.edu

Laboratory ReportD.F. Kurtycz, M.D.. Medical Director . Char les D. Brokopp. f ) r .P.H.. Director


WDNR LAB lD: 1 '13133790 NELAP LAB lD: E37658 EPA LAB W100007 Wt DATCp tD: 105-4'15

F ie ld # : 154 SOIL


Col lect ion End.


County.

Sample Source: AIR

Sample Depth:

Sample Information:

Sample Locat ion:




RJN ENVIRONMENTAL SVC.. LLC

4631 COUNTY ROAD A

oREGON, Wt 53575

B i l l T o


Customer lD: 320225

TRACKING 4920


MADISON WI 53718

tD#:


PoinVWell:

Account #: 1H034

Project No:Date Received: 0210412011


Sample Reason:


Lab CommentSEE OVOO3B3B.MMl

Result

.D< 53.2

"D< 53.2*D< 53.2*D< 53.2*D< 53.2

"D< 53.2*D< 53.2*D< 53.2*D< 53.2*D< 53.2*D< 53.2*D< 53.2*D< 53.2

Method

PROPENE


CHLOROMETHANE

1,2-DICHLOROTETRAFLUOROETHANE

VINYL CHLORIDE

1,3-BUTADIENE

BROMOMETHANE

CHLOROETHANE

ACROLEIN

ACETONE

HALOCARBON 1 1

1 ,1-DICHLOROETHENE

METHYLENE CHLORIDE

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.085

0.085

0.085

0 . 1 0

0.085

0.085

0.085

0.085

0.400

0.400

0.085

0.085

0.085

LOQ

0.280

0.280

0.280

0.330

0.280

0.280

0.280

0.280

1 . 3 2

1 . 3 2

0.280

0.280

0.280

Report Limit

Page 1 of4

Wisconsin State Laboratory of llygienc2601 Agriculture Drive, PO Box 7996Madison. Wl 5-1707-7996(800)4.+2-46r 8 . FAX (608)224-621 3http://rwl,w.slh.wisc-edu

Laboratory Report


WDNR LAB lD: 1 13133790 NELAP LAB tD: E37058

D.F. Kurtycz. M.D.. Medical Director . Char lcs D. Brokopp, Dr.p.Fl . . Director

Organic Chemistry



Method

CARBON DISULFIDE,I, ,1,2-TRICHLOROTRI FLUOROETHANE

TRANS-1,2-DICHLOROETHYLENE,I,1-DICHLOROETHANE


VINYL ACETATE

METHYL ETHYL KETONE


HEXANE

CHLOROFORM

ETHYL ACETATE

TETRAHYDROFURAN

l,2.DICHLOROETHANE

1, 1 , 1 -TRICHLOROETHANE

BENZENE


CYCLOHEXANE

1,2-DICHLOROPROPANE


TRICHLOROETHYLENE,I,4-DIOXANE

HEPTANE

CIS.1,3-DICHLOROPROPENE


TRANS.1,3-DICHLOROPROPENE

1, 1,2-TRICHLOROETHANE

TOLUENE



1,2-DIBROMOETHANE

TETRACHLOROETHYLENE

Result

"D< 53.2-D< 53.2.D< 53.2*D< 53.2*D< 53.2

"D< 53.2

"D< 53.2-D< 53.2

"D< 53.2-D< 53.2-D< 53.2

"D< 53.2-D< 53.2.D< 53.2'D< 53.2*D< 53.2*D< 53.2*D< 53.2-D< 53.2*D< 53.2*D< 53.2-D< 53.2*D< 53.2*D< 53.2*D< 53.2*D< 53.2* u 3 1 4

*D< 53.2

"D< 53.2*D< 53.2-u 470

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.08s

0.085

0.085

0.085

0.085

0.085

0.085

0.085

U.Ud3

0.085

0.085

0.400

0.085

0.085

0.085

0.085

0.085

0.085

0 . 1 0

0.085

0.400

0.085

0.085

0.400

0.085

0.085

0.085

0.400

0"085

0.085

0.085

LOQ

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

1 . 3 2

0.280

0.280

0.280

0.280

0.280

0.280

U . J J

0.280

1 . 3 2

0.280

0.280

1 . 3 2

0.280

0.280

0.280

1 . 3 2

0.280

0.280

0.280

Report Limit

Page 2 of 4

Wisconsin State Laboratory of Ilygiene2601 Agriculture Drivc, PO Box 7996Madison, Wl -s-3707-7996(800)442-46r 8 . f .AX (608)224-621 3http:i/wwrv.slh.u'isc-edu

Laboratory Report



D.F. Kur lvcz. M.D., Medical Director . Char les D. Brokopp. Dr.p. l l . . Director

Organic Chemistry



Analysis Method

CHLOROBENZENE

ETHYLBENZENE

M/P-XYLENE

BROMOFORM

STYRENE

1,1,2,2-T ET RACHLOROETHAN E

O-XYLENE


1,3,s-TRIMETHYL BENZENE

1,2.4-TRIMETHYL BENZENE


1,3-DICHLOROBENZENE

1,4-DICHLOROBENZENE

1,2-DICHLOROBENZENE



Result

*D< 53.2-D< 53.2*D< 53.2.D< 53.2*D< 53.2-D< 53.2

"D< 53.2.D< 53.2*D< 53.2

"D< 53.2*D< 53.2-D< 53.2

"D< 53.2-D< 53.2*D< 53.2*D< 53.2

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.085

0.085

0 . 1 7 0

0.085

0.085

0.085

0.085

0.08s

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

Report LimilLOQ

0.280

0.280

0.561

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

o v O 0 3 B 3 8 . M M 1 :

WISCONSIN STATE LABORATORY OF HYGIENE SAMPLE OVOO3838 CONTAINS THEFOLLOWING FLAGS.

LOD NOT ACHIEVABLE DUE TO DILUTION *D.

RESULTS ARE APPROXIMATE, ABOVE UPPER CALIBRATION RANGE - *U.

IF YOU I IAVE ANY QUESTTONS, CONTACT STEVE GEIS AT (608) 224 6269.


Lab Comment

Analysis Method Resutt Units LoD Loe Report Limit


Page 3 of4

Wisconsin State Laborarory of Hygiene2601 Agnculture Drivc, PO Box 7996Madison, Wl 53707-7996(800)442-461 8 . FAX (608)224-621 3http:,r/wwrv.slh. wisc.edu

Laboratory Report



D,f'. Kurtycz, M.D., Medical Director . Charles D. Brokopp, Dr.p.H.. Director

Organic Chemistry




Lab Comment

alysis Method Result

COMPLETE

Units LOD LOQ Report Limrr

TOXIC ORGANIC COMPOUNDS INAMBIENT A IR TO15 - PREP

Test results for NELAP accredited tests are certified to meet the requirements of the NELAC standards. For a list of accredited analvtes seehttp: / /www.slh.wisc.edu/nelap/



Responsible Party: ffi;* *,4&D




\4 ' rsconsin State I .aboratory o l Hy,giene2601 Agr icu)t r . r re l ) r i r e. I )O Box 7996Madison, WI 53707-7996(800)4.11-461 8 . t -AX (60E)224-621 3ht tp: ,1 ' rvww.slh,wisc.edu

Laboratory Report

Fie ld # : 154 WELL

Col lect ionStart : 0210412011

Col lect ion End:

Col lected By: BOB NAUTA

County:

Sample Source: AIR

Sample Depth:

Sample Information:

Sample Locat ion:

Sample Descript ion.


Environmental Health Divis ion

WDNR LAB lD: 113133790 NELAP LAB lD: E37658 EpA LAB Wt00007Supplement to test report#: 9391662



4631 COUNTY ROAD A

oREGON. Wt 53575

D.F. Kurtycz, M.D., Medical Director . Char les D. Brokopp, Dr.p.H.. Dircctor

Organic Chemistry


B i l l T o


Customer lD: 320225

TRACKING 4920


MADISON WI 53718

tD#:


PoinUWell :

Account #: 1H034

Project No:Date Received: 0210412011


Sample Reason:


Lab CommentSEE OVOO3B37.MM1

ysis Method

PROPENE

DICHLORODIFLUOROMETHANE

CHLOROMETHANE,1,2-DICHLOROTETRAFLUOROETHANE

VINYL CHLORIDE

1,3-BUTADIENE

BROMOMETHANE

CHLOROETHANE

ACETONE

HALOCARBON 1 1

1 ,1-DICHLOROETHENE

METHYLENE CHLORIDE

CARBON DISULFIDE

Resull

<20.

<20.

<20.

<20.

<20.

<20 .

<20.

<20.

<20.

<20.

<20.

<20.

<20.

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

Report Limit

20 .

20.

20.

20.

20.

20.

20.

20

20.

20 .

20.

20.

20.

LOD LOQ

Page 1 o f4

\ \ rsconsrn Srare Labor.aror ; of Hygrcnc2601 Agncul turc Dr ive. PO Box 7996Madison. WI 53707-7996(800)442-461 8 . FAX (608)22.1_62 I 3http:,r wurv.slh. rl,rsc. edu

Laboratory Report


WDNR LAB lD: 1 13133790 NELAP LAB tD:


Amended Report

D.F Kunycz. N, l .D. , Nledical Director . Char les D Brokopp. Dr p.H.. Director

Organic Chemistry

E37658 EPA LAB W100007 Wl DATCP lD: '105-415


Method

1, 1 ,2 -TRICHLOROTRIFLUOROETHANE

TRANS-.I ,2-DICHLOROETHYLENE, I ,1 -DICHLOROETHANE


VINYL ACETATE

METHYT ETHYL KETONE

CI S.,1,2-DICH LOROETHYLENE

HEXANE

CHLOROFORM

ETHYL ACETATE

TETRAHYDROFURAN

1,2-DICHLOROETHANE


BENZENE


CYCLOHEXANE

l,2.DICHLOROPROPANE


TRICHLOROETHYLENE

1,4-DIOXANE

HEPTANE

CIS.1 ,3-DICHLOROPROPENE


TRANS-l,3.DICHLOROPROPENE

1, 1 ,2 -TRICHLOROETHANE

TOLUENE



1,2-DIBROMOETHANE

TETRACHLOROETHYLENE

CHLOROBENZENE

Resul t

<20 .

<20.

<20 .

<20 .

<20 .

<20 .

<20 .

<20.

<20.

<20 ,

<20 .

<20 .

<20.

<20.

<20 .

<20.

<20.

<20.

<20 .

<20 .

<20 .

<20 .

<20 .

<20 .

<20 .

<20.

<20 .

<20 .

<20 .-u 188.

<20.

Uni ts

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

Report Limit

20 .

20

20

z v .

20.

2 0 .

2 0 .

2 0 .

2 0 .

20.

2 0 .

20 .

20.

20 .

20 .

20 .

20 .

20.

2 0 .

20 .

2 0 .

20.

20.

2 0 .

20

20.

2 0 .

20 .

2 0 .

2 0 .

20

LOD LOQ

Page 2 ot 4

Wisconsin State Laborarory of Hygrene2601 Agr icul ture Dr ive. PO Box 7996Madison, WI 53707-7996(800)442-461 8 . r -AX (608)224-62 I 3hnp :,'iu'rvw. slh. wisc. eclu

Laboratory ReportD F. Kurtycz, M D. Medical Director . Char les D. Brokopp. Dr p.H.. Drrector

Environmental Health Divis ion Organic Chemistry

WDNR LAB lD: '113133790 NELAP LAB lD: E37658 EPA LAB W100007 Wl DATCP tD: i05-415Supplement to test report#: 9391662


Analysis Method

ETHYLBENZENE

M/P-XYLENE

BROMOFORM

STYRENE

1,1 ,2 ,2 -T ET RACH LO ROETHAN E

O-XYLENE


1,3 ,5-TRIMETHYL BENZENE



1,3-DICHLOROBENZENE

1,4-DICHLOROBENZENE

1,2-DICHLOROBENZENE

1,2 ,4-TRICHLOROBENZENE

H EXACH LORO-1, 3-BUTADI EN E

Resul t

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20 .

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V


20.

20 .

20.

20

20.

20

20.

20.

20.

20.

2 0 .

20.

20

o v 0 0 3 8 3 7 . M M 1 :


LOD NOT ACHIEVABLE DUE TO DILUTION _ *D.

RESULTS ARE APPROXIMATE, ABOVE UPPER CALIBRATION RANGE _ *U.

I F Y O U H A V E A N Y Q U E S T I O N S , C O N T A C T S T E V E G E I S A T ( 6 0 8 ) 2 2 4 _ 6 2 6 9 .


Lab Comment

\na lys is Method Resul t Uni ts LOD LOe Report L imi t

TOXIC ORGANIC COMPOUNDS IN COMPLETE 1AMBIENT A IR TO15 - PREP

Page 3 of 4

Wisconsin State Laboratorv of H.vgiene2601 Agr icul ture Dr ive, PO Box ?996Madison. \ \ ' l 53707-7996(800)442-{6 I 8 . FAX (608)224-6: t 3ht tp: 'usav s ih.* ' rsc.edu

Laboratory Reportt ) F Kurr ! 'cz. M.D.. N, ledrcal Direcror . Char les D Brokopp, Dr p.H.. Direcror

Environmental Health Drvision Organic Chemistry

WDNR LAB lD: 113133790 NELAP LAB lD: E37658 EPA LAB W100007 Wt DATCp tD: ' t05-415


Amended Report WSLH Sampte: OV0O3837

Test results for NELAP accredited tests are cert i f ied to meet the requirements of the NELAC standards. For a l ist of accredited analvtes seehtto ://www. slh.wisc. edu/nelaol



Responsible Party: *tr . A<"D



Report #: 9404842 Page 4 ol 4

Wisconsin State Laboratory of Hyriene2601 Agnculture Drive, PO Box 7996Madison. Wl 53707-7996(800)442-46 r 8 . r-AX (608)224-62 1 3http :i/wrvw-slh.u isc.edu

Laboratory Report


WDNR LAB lD: 1 '13133790 NELAP LAB lD: E37658

D.F. Kurtycz. M.D.. Metlical Director . C'harles D. Brokopp. Dr.P.l1.. Director

Organic Chemistry


Field #: 162 INDOOR

Collect ion Start : 0210712011 12.37.12

Collection End:

Collected By, BOB NAUTA

County:

Sample Source: AIR

Sample Depth:

Sample Information:

Sample Location.

Sample Description:



RJN ENVIRONMENTAL SVC.LLC

4631 COUNTY ROAD A

oREGON, Wt 53575

B i l l T o

Bi l l ing lD; 7305879

Customer lD: 320225

TRACKING 4920


MADISON WI 53718

lD#:


PoinUWell :

Account #: LH034

Project No.Date Received: 0210712011


Sample Reason:


Lab CommentSEE OVOO3853.MM1

Resultysis Method

PROPENE


CHLOROMETHANE


VINYL CHLORIDE

1,3-BUTADIENE

BROMOMETHANE

CHLOROETHANE

ACROLEIN

ACETONE

HALOCARBON 1 1

1 ,1-DICHLOROETHENE

METHYLENE CHLORIDE

- l< 1 .3 '1

0.506

0.452

ND

ND

ND

ND

ND

ND

"QU 2 .17

0 . 3 1 6

ND

ND

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.085

0.085

0.085

0 . 1 0

0.085

0.085

0.085

0.085

0.400

0.400

0.085

0.085

0.085

LOQ

0.280

0.280

0.280

0.330

0.280

0.280

0.280

0.280

t . 3 z

1 . 3 2

0.280

0.280

0.280

Report Limit

Page 1 of 4

Wisconsin Stale Laboratory of llygienc2601 Agriculture Dnve, PO Box 7996Madison, WI 53707-7996(800)442-46t 8 . FAX (608)224-62 I 3http:i /rvwrv.sl h.wisc-edu

Laboratory Report


WDNR LAB lD: 1 13133790 NELAP LAB tD:

D.F. Kurrycz. M.D., Medical Director . Char les D. Urokopp, Dr.p. l l . , Director

Organic Chemistry

E37658 EPA LAB W100007 Wl DATCP tD: 105-415


alvsis Method

CARBON DISULFIDE

1, 1,2-TRICHLOROTRIFLUOROETHANE


1,1-DICHLOROETHANE


VINYL ACETATE

METHYL ETHYL KETONE


HEXANE

CHLOROFORM

ETHYL ACETATE

TETRAHYDROFURAN

l,2.DICHLOROETHANE

1, 1, 1 -TRICHLOROETHANE

BENZENE


CYCLOHEXANE

1,2-DICHLOROPROPANE


TRICHLOROETHYLENE

1,4-DIOXANE

HEPTANE

CIS-1,3-DICHLOROPROPENE


TRANS- 1,3-DICHLOROPROPENE


TOLUENE



Result

N D

ND

ND

ND

N D

N D

o.432

ND

N D

N D

ND

0.481

N D

ND

0.347

N D

N D

ND

ND

ND

ND

N D

N D

N D

N D

ND

0.307

ND

N D

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.0B5

0.085

0.085

0.085

0.085

0.085

0.085

0.08s

0.085

0.085

0.085

0.400

0.085

0.085

0.085

0.085

0.085

0.085

0 . 1 0

0.085

0.400

0.085

0.085

0.400

0.085

0.085

0.085

0.400

0.085

LOQ

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

1 . 3 2

0.280

0.280

0.280

0.280

0.280

0.280

0.33

0.280

1 . 3 2

0.280

0.280

1 . 3 2

0.280

0.280

0.280

1 . 3 2

0.280

Report Limit


PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

Page 2 of 4

Wisconsin State Laboratory of Ilygiene2601 Agriculture Drivc. PO Box 7996Madison, Wl 53707-799(r(800)442-46t 8 . FAX (608)224_621 lhttp: //www.slh.wisc.edu

Laboratory Report



D.F' . Kurtycz, M.D., Medical Director . Char les D. Brokopp, Dr.p.H.. Director

Organic Chemistry



Analysis Method

1,2-DIBROMOETHANE

TETRACHLOROETHYLENE

CHLOROBENZENE

ETHYLBENZENE

M/P-XYLENE

BROMOFORM

STYRENE

1, 1,2,2-TETRACHLOROETHANE

O-XYLENE,I -ETHYL-4-METHYL BENZENE




1,3-DICHLOROBENZENE

1,4-DICHLOROBENZENE

1,2-DICHLOROBENZENE



Result

N D

ND

ND

ND

N D

ND

ND

ND

N D

N D

ND

ND

ND

ND

N D

N D

N D

ND

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.085

0.085

0.085

0.085

0.170

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.08s

0.085

LOQ

0.280

0.280

0.280

0.280

0.561

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.2B0

Report Limil

o v O 0 3 B 5 3 . M M 1 :

WISCONSIN STATE LABORATORY OF HYGIENE SAMPLE OVOO3B53 CONTAINS THEFOLLOWING FLAGS.

UPPER QC L IM]T FOR CALIBRATION CHECK EXCEEDED *QU.

I F Y O U H A V E A N Y Q U E S T I O N S . C O N T A C T S T E V E G E I S A T ( 6 0 8 ) 2 2 4 6 2 6 9 .


Lab Comment

\nalysis Method Result Units LOD LOe Report Limit


Page 3 of 4

Wisconsin State Laboratory of tlygiene2601 Agriculture Drive. PO Box 7996Madison, WI 53707-7996(nt)0)442-461 1l . t-AX (608)224-62 I 3http :i/wwrv.slh.wisc.cdu

Laboratory Report



I).F. Kurtycz, M.D.. Mcdical Director. Charlcs D. t3rokopp, Dr.p.H., Director

Organic Chemistry



Analysis Date Lab Comment02t09t2011

is Method Result Units LOD LOe Report Limit

TOXIC ORGANIC COMPOUNDS IN COMPLETE . IAMBIENT AIR TO15 - PREP

Test results for NELAP accredited tests are certified to meet the requirements of the NELAC standards. For a list of accredited analytes seehttp:/ /www.slh.wisc.edu/nelao/


LOD = Level of detectionLOQ = Level of ouantificationND = None detected. Results are less than the LOD

Responsible Party: #-* _.4<"p

lf there are questions about this report, please contact Steve Geis a|608-224-6269.


R e o o r t # : 9 3 9 1 6 6 5 Page 4 ot 4

Wisconsin State Laboratory of Hygiene2601 Agr icul ture Dr ive, PO Box 7996Madison, WI 53707-7996(800)442-461 8 . r -AX (608)224-6213http :/iur'w. slh.wi sc.edu

Laboratory ReportD.F. Kunycz, M.D., Medical Director . Char les D, Brokopp, Dr.P.H., Direcror


WDNR LAB lD: 1 13133790 NELAP LAB lD: E37658 EPA LAB W100007 Wl DATCP lD: 105-415



RJN ENVIRONMENTAL SVC.LLC

4631 COUNTY ROAD A

oREGON, W153575

B i l l T o

Bi l l ing lD : 7305879

Customer lD; 320225

TRACKING 4920


MADISON WI 53718

tD#:


PoinUWell ;

Accounl #; LH034

Project No:

Date Received: 0210712011


Sample Reason:

F ie ld # : 162 SOIL

Collection Start: 0210712011 12.36:42

Col lect ion End:

Col lected By: BOB NAUTA

County:

Sample Source; AIR

Sample Depth:

Sample Information:

Sample Locat ion;




Lab Comment

sis Method Resul t

<20.

<20.

<20.

<20.

<20.

<20 .

<20 .

<20.

<20.

<20.

<20.

<20 .

<20.

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD t r ) n Report Limi l

20.

20.

20.

20.

PROPENE

DICHLORODIFLUOROMETHANE

CHLOROMETHANE,1,2-DICHLOROTETRAFLUOROETHANE

VINYL CHLORIDE

1,3-BUTADIENE

BROMOMETHANE

CHLOROETHANE

ACETONE

HALOCARBON 11

1,1-DICHLOROETHENE

METHYLENE CHLORIDE

CARBON DISULFIDE

2 0 .

20.

20 .

20.

20.

20 .

20.

20 .

20.

Page '1 of 4

Wisconsrn State Laborarory of Hygrene2601 Agnculnrre Dr ive. PO Box 7996Madrson , WI 53707 -7996(800)442-461 8 . FAX (608)224-62 I 3http t/,'wrw .slh,wrsc. edu

Laboratory Report

Environmental Health

WDNR LAB lD: 1 13133790

Supplement to test report#:

Amended Report

D.i" . Kurtycz. M.D., Medical Director . Char les D. Brokopp. Dr.P.H., Director

Division Organic Chemistry

NELAP LAB lD: E37658 EPA LAB W100007 Wl DATCP lD: 105-415

9391 664


alysis Method

1. 1 .2 -TRICHLOROTRI FLUOROETHANE

TRANS-1,2-DICHLOROETHYLEN E

1,1-DICHLOROETHANE


VINYL ACETATE

METHYL ETHYL KETONE

CIS-1,2-DICH LOROETHYLEN E

HEXANE

CHLOROFORM

ETHYL ACETATE

TETRAHYDROFURAN

1,2-DICHLOROETHANE


BENZENE


CYCLOHEXANE

l ,2 .DICHLOROPROPANE


TRICHLOROETHYLENE

1,4-DIOXANE

HEPTANE

CIS-1 ,3-DICHLOROPROPENE




TOLUENE


DIBROMOCHLOROMETHANE,1,2-DIBROMOETHANE

TETRACHLOROETHYLENE

CHLOROBENZENE

Resul t

<20.

<20 .

<20 .

<20 .

<20 .

<20 .

<20 .

<20 .

<20.

<20 .

<20.

<20 .

<20 .

<20.

<20 .

<20.

<20 .

<20.

<20.

<20.

<20 .

<20 .

<20 .

<20.

<20 .

<20.

<20.

<20 .

<20.

3 1 .

<20 .

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

Report Llmit

2 0 .

20.

20.

20.

20.

20 .

20.

2 0 .

20.

20.

2 0 .

20.

2 0 .

2 0 .

20 .

2 0 .

20 .

20

20.

20

20.

20.

2 0 .

20.

20

20.

20 .

20.

2 0 .

20.

2 0 .

LOD toQ

Page 2 of 4

Wisconsin State Laboratory of Hygiene2601 Agr iculrure Dr ive, PO Box 7996Madrson, WI 53707-7996(800)4,12-461 8 . FAX (608)224-621 3ht tp: / lwww.slh.wisc.edu

Laboratory Report


D.F. Kurrycz, M.D., Medical Director . Char les D. Brokopp, Dr.p.H.. Director

Organic Chemistry

WDNR LAB lD: 1 '13133790 NELAP LAB lD: E37658 EPA LAB W100007 Wl DATCP lD: 105-415Supplement to test report#: 9391664


lys is Method

ETHYLBENZENE

M/P-XYLENE

BROMOFORM

STYRENE

1,1,2,2-T ET RAC H LOROETHAN E

O-XYLENE,I -ETHYL-4-METHYL BENZEN E


1,2 ,4 .TRIMETHYL BENZENE


1,3-DICHLOROBENZENE

1,4-DICHLOROBENZENE

1,2-DICHLOROBENZENE

1,2 ,4-TRICHLOROBENZENE

HEXACHLORO-1 . 3 -BUTADIENE

Analysis Date Lab Comment02t09t2011

Method Units LOD LOQ

Resul t

<20.

<40 .

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

<20.

Uni ts

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V


20 .

20.

20.

20.

20.

20 .

20.

20 .

20 .

20.

20.

20.

20.

20.

20 .

Report L imi t

1

Result

COMPLETETOXIC ORGANIC COMPOUNDS INAMBIENT AIR TO15 - PREP

Page 3 of 4

\tr'isconsin State LaborarotJ of Hygrene2601 Agnculrure Dr ive, PO Box 7996Madison, WI 5370?-7996(800)442-461 8 . FAX (608)224-621 3http :,/'wur',slh.wisc.edu

Laboratory ReportD.F. Kurtycz. N' t .D. , Medical Director . Char les D. Brokopp. Dr.P.H, Drrecror

Environmental Health

WDNR LAB lD: 113133790

Supplement to test report#:

Amended Report

Division Organic ChemistryNELAP LAB lD: E37658 EPA LAB W100007

939 1 664


Wl DATCP lD: 105-4 '15

Test results for NELAP accredited tests are certified to meet the requirements of the NELAC standards. For a list of accredited anal\4es seehtto:/ /www.slh.wisc.edu/nelao/


LOD = Level of detectionLOQ = Level of ouantificationND = None detected. Results are less than the LOD

Responsible Party: *E , A<,,D




Wisconsin State Laboratory of [Jygiene2601 Agriculture Drivc, PO Box 7996Madrson, WI -53707-7996(800)442-4618 . FAX (608)224_621 3http:/iwwrv.slh.wisc-edu

Laboratory ReportD.F. Kurtycz, M.D.. Medical Director . Char les D. L l rokopo. Dr.P. l l . . Dircctcx

Environmental Health Division Organic ChemistryWDNR LAB lD. 113133790 NELAP LAB lD: E37658 EPA LAB W100007 Wl DATCP tD: 105-415

Field #: OUTDOOR AIR

Collection Start: O2lO4l2O11

Col lect ion End:


County:

Sample Source: AIR

Sample Depth:

Sample Information:

Sample Location.

Sample Description:




4631 COUNTY ROAD A

oREGON, Wt 53575

B i l l T o


Customer lD: 320225

TRACKING 4920


MADISON WI 53718

rD#:


PoinUWell:

Account #: LH034

Project No.DateReceived. 0210412011


Sample Reason:


Lab Comment

SEE OVOO3B35.MM1

s Method

PROPENE


CHLOROMETHANE


VINYL CHLORIDE

1,3-BUTADIENE

BROMOMETHANE

CHLOROETHANE

ACROLEIN

ACETONE

HALOCARBON 1 1

1 ,1-DICHLOROETHENE

METHYLENE CHLORIDE

Result

- t< 0.770

0.655

0.681

ND

ND

ND

N D

N D

N D-B"QU 1.4'1

0 . 3 1 1

ND

ND

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.085

0.085

0.085

0 . 1 0

0.085

0.085

0.085

0.085

0.400

0.400

0.085

0.085

0.085

LOQ

0.280

0.280

0.280

0.330

0.280

0.280

0.280

0.280

1 . 3 2

1 . 3 2

0.280

0.280

0.280

Report Limit

Page 1 of4

Wisconsin Slate Laboratory of Hygiene2601 Agriculture Drive. PO Box 7996Madison, Wl 53707-7996(rrc)0)442-4618 . t -AX (608)224_62 t3http ://www.slh.wisc.edu

Laboratory Report



D.F. Kurtycz, M.D.. Medical Director . Charles D. tlrokopp. Dr.p.fl.. Director

Organic Chemistry



Method

CARBON DISULFIDE

1, 1,2-TRICHLOROTRIFLUOROETHANE

TRANS-,I ,2-DICHLOROETHYLENE

1,1-DICHLOROETHANE


VINYL ACETATE

METHYL ETHYL KETONE

CIS- 1,2-DICHLOROETHYLENE

HEXANE

CHLOROFORM

ETHYL ACETATE

TETRAHYDROFURAN

l,2.DICHLOROETHANE


BENZENE


CYCLOHEXANE

1,2-DICHLOROPROPANE


TRICHLOROETHYLENE

1,4-DIOXANE

HEPTANE

CIS-1,3-DICHLOROPROPEN E


TRANS- 1,3-DICHLOROPROPENE

1, 1 .2-TRICHLOROETHANE

TOLUENE



1,2-DIBROMOETHANE

TETRACHLOROETHYLENE

Result

ND

N D

ND

ND

N D

ND

0.347

N D

ND

ND

ND

N D

ND-IS ND

.ts 0.343- I S N D- IS ND- IS ND* IS ND- IS ND

" IS ND- IS ND* IS ND- I S N D* IS ND

" IS ND.ts 0.307* IS ND* IS ND- IS ND* IS ND

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.08s

0.085

0.085

0.085

0.400

0.08s

0.085

0,085

0.085

0.085

0.085

0 . 1 0

0.085

0.400

0.085

0.085

0.400

0.085

0.085

0.085

0.400

0.085

0.085

0.085

LOQ

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

1 . 3 2

0.280

0.280

0.280

0.280

0.280

0.280

0.33

0.280

1 . 3 2

0.280

0.280

1 . 3 2

0.280

0.280

0.280

1 . 3 2

0.280

0.280

0.280

Report Limit

Page 2 of 4

Wisconsin State Laboratory of tlygiene2601 Agriculturc Ddve. PCt flox 7996Madison, WI 53707-7996(ti00)442-46 I 8 . r.AX (608)224-62 I 3http :i,lwww.slh.wisc.edu

Laboratory Report



D.F. Kurtycz, M.D.. Mcdical Dircctor . Char les I ) . Brokopp. Dr.p.H.. Director

Organic Chemistry



Analysis Method

CHLOROBENZENE

ETHYLBENZENE

M/P-XYLENE

BROMOFORM

STYRENE


O-XYLENE



1,2,4.TRIMETHYL BENZENE


1,3-DICHLOROBENZENE

1,4-DICHLOROBENZENE

1 ,2 -DICHLOROBENZENE


HEXACHLORO.l,3-BUTADIENE

Result

" I IS ND

"I IS ND-I IS ND-I lS ND- l13 ND

"l l3 ND-I IS ND

"l l i ND-[ i ND.[ i ND.[ i ND.t { i ND.t { i ND. l { i ND.t { i ND. l { i ND

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.085

0.085

0 . 1 7 0

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.08s

0.085

0.085

0.085

LOQ

0.280

0.280

0.561

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

Report Limit

o v O 0 3 8 3 5 . M M 1 :

WISCONSIN STATE LABORATORY OF HYGIENE SAM-PLE OVOO3B35 CONTAINS THEFOLLOWING FLAGS.


COMPOT]}TD DETECTED IN LAV BLANK INDICATED I3Y *8.THE INTERNAL STANDARD QC L IMIT IS EXCEEDE] ] * IS .UPPER QC L IMIT FOR CALTBRATION CHECK EXCE] IDED *QU.

IF YOU I {AVE ANY QUESTIONS, CONTACT STEVE GEIS AT (608) 224 6269.


Lab Comment

\nalysis Method Resutt Units LOD LOe Report Limit


Page 3 of 4

Wisconsin State Laboratory of llygiene2601 Agriculture Drive, PO Box 7996Madison. Wl 53707-7996(800)442-46 I 8 . FAX (6crt3)224-62 r -lhttp :/,'www.slh.wisc.edu

Laboratory ReportD.F. Kurtycz, M.D., Medical Direclor . Char les D. Brokorrp. Dr.p. lJ . . Director



Organic Chemistry


Test results for NELAP accredited tests are certified to meet the requirements of the NELAC standards. For a list of accredited analytes seehttp:/iwww. slh.wisc.edu/nelap/



Responsible Party: HE: _.A<rD

lf there are questions about this report, please contact Steve Geis al608-224-6269.The results in this report apply only to the sample specifically listed above. This report is not to be reproduced except in full


Analysis Date Lab Comment0210712011

is Method Result Units LOD LOe Report Limit


Report #: 9391660Page 4 of 4

Wisconsin State Laboralor"- of Hygrene260i Agr icul ture Dr ive, PO Box 7996N' ladison, Wl 53707-7996(800)442-46r8 . FAX (60E)22.1-6213http : / /xw.s lh.* isc.edu

Laboratory Report

D.I j Kurtycz, M.D., Medical Director Char les D. Brokopp, Dr 'P.H, Dlrector


WDNR LAB ID: 1 13133790 NELAP LAB ID: E37658 EPA LAB WIOOOOT WI DATCP ID: 105-415

WSLH Sample: ovo05796

RJN ENV. SERVICES LLC

4631 COUNW ROAD A

oREGON. Wr 53s75

Bi l l To

Bi l l ing lD : 7305879

Customer lD; 320225

TRACKING 4920


M A D I S O N W I 5 3 7 1 8

lD#:

Waterbody/Outfal l lD:

PoinWVell :

Account #: 1H034

Project No:



Sample Reason:

Field #: 142


Collection End:

Collected By:

County:

Sample Source: AIR

Sample DePth:

Sample lnformation:

Sample Location:

Sample DescriPtion:


Analysis Date0611512011 01:00:00

lysis Method

PROPENE

DICHLORODIFLUOROMETHAN E

CHLOROMETHANE

l,2.DICHLOROTETRAFLUOROETHAN E

VINYL CHLORIDE

1,3-BUTADIENE

BROMOMETHANE

CHLOROETHANE

ACROLEIN

ACETONE

HALOCARBON 11

Note: The rePorted value above is

l , l .D ICHLOROETHENE

equal to or greater than the LOD and less than the LOQ

PPB V 0 .085 0 .280

Lab Comment

SEE OVOO5796 .MM1

Result

N D

0.570

N D

N D

N D

N D

N D

N D

N D

"B.QU0.620

0 . 1 3 8

Units

PPB V

PPB V

P P B V

PPB V

P P B V

P P B V

P P B V

PPB V

PPB V

P P B V

PPB V

LOD

0.085

0.085

0.085

0 . 1 0

0.085

0.085

0.085

0.085

0.085

0.085

0.085

LOQ

0.280

0.280

0.280

0.330

0 280

0.280

0.280

0.280

0.280

0.280

0.280

Report Limit

ND

P a a a 1 a f 4

\ \ ' isconsin Str te Labor l ton or ' H) crcn(260i Agr icul ture Dr ive, PO Box 7996Madison. Wl 53707- i996(800)4,+2-46 l 8 . FAX (608)21.{-61 r lht tp: i / *urv.sLh.wisc.edu

Laboratory Report



D.l i . Kuf tycz, M.D.. Medical l l i rector Char ies D. Brokopp, Dr. l ' .H. , Director

Organic Chemistry



Method

METHYLENE CHLORIDE

CARBON DISULFIDE

1, 1,2-TRICHLOROTRI FLUOROETHAN E

TMNS-1,2-DICHLOROETHYLENE

1.1-DICHLOROETHANE


VINYL ACETATE

METHYL ETHYL KETONE


HEXANE

CHLOROFORM

ETHYL ACETATE

TETMHYDROFURAN

1,2-DICHLOROETHANE

1, 1,, I -TRICHLOROETHANE

BENZENE


CYCLOHEXANE

1,2-DICHLOROPROPANE


TRICHLOROETHYLENE

1,4-DIOXANE

HEPTANE

CIS-1 .3-DICHLOROPROPENE

Result

0 . 1 0 8

0 . 3 6 1

N D

0.235

0 . 3 1 7

N D

N D

0 . 2 7 1

Units LOD LOQ Report Limit

PPB V 0 .08s 0 .280

PPB V O.OB5 O.2BO

PPB V O.OB5 O.2BO

PPB V 0 .085 0 .280

PPB V O.OB5 O.2BO

PPB V O.OB5 O,2BO

PPB V O.OB5 O.2BO

PPB V O.OB5 O.2BO

PPB V 0 .085 0 .280

PPB V 0 .085 0 .280

Note: The repor ted value above is equal to or greater than the LOD and less than the LOQ.

ND PPB V 0 .08s 0 .280

0 . 1 1 9 PPB V 0 .085 0 .280


N D

N D

N D

0.260




ND PPB V 0 .085 0 .280

ND PPB V O.OB5 O.2BO

PPB V 0 .085 0 .280

P P B V 0 . 1 0 0 . 3 3

PPB V 0 .085 0 .280

ND PPB V 0 .085 O.2BO

ND PPB V O.OB5 0 .280



ND PPB V 0 .085 O.2BO

PPB V 0 .085 0 .280

PPB V O.OB5 O.2BO

N D

N D

N D

Page 2 of 4

\ \ isconsin Stare Labururon ol H) gruns2601 Agriculrure Dnle. PO Box 7996Madrson, Wl 53707-7996(800)442-461 8 . FAX (608)22;1-61 l lhttp: i,'rvurv.sih.rvi sc.edu

Laboratory Report



D.1. . Kurtvcz. M.D., Medical Dircctor . Char les D. Brokopp, Dr.P.H., Dircctor

Organic Chemistry



alvsis Method


TRANS-1 .3-DICHLOROPROPENE


TOLUENE



1,2-DIBROMOETHANE

TETRACHLOROETHYLENE

CHLOROBENZENE

ETHYLBENZENE

M/P-XYLENE

BROMOFORM

SryRENE


O-XYLENE

1.ETHYL4-METHYL BENZEN E

1 .3.s-TRIMETHYL BENZENE,1 .2.4.TRIMETHYL BENZENE


1,3-DICHLOROBENZENE

1,4-DICHLOROBENZENE

1,2-DICHLOROBENZENE


HEXACHLORO-1,3-BUTADI EN E


Result

3 .38

N D

N D

| . o z

0.779

N D

N D

1 . 8 7

N D

0.459

1 . 5 4

N D

0.270

N D

0.630

0.577

0.450

2 . 1 0

N D

N D

N D

N D

N D

N D

Unr ts

P P B V

PPB V

PPB V

PPB V

PPB V

PPB V

P P B V

P P B V

PPB V

P P B V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

P P B V

PPB V

PPB V

PPB V

PPB V

PPB V

LOD

0.085

0.08s

0.085

0.085

0.085

0.085

0.085

0.085

0.08s

0.085

0. '1 70

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

LOQ

0.280

0 280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.56'1

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

Report Limit

Page 3 of 4

\ \ rscorrs in Statc L i rburatory of Hvgicne2601 Agrrcui ture Dr ive, [ 'O Box 7996Madison, Wl 53701-7996(800)4.12-46 l 8 . FAX (608)224-62 I lhttp:ii *'w'.slh. *'isc.edu

Laboratory Report

Environmental Heal th Div is ion

WDNR LAB lD : ' 113133790 NELAP LAB lD : E37658

D.F Kurtycz, M.D., i \ , ledtcal Director Char les D. Brokopp, Dr.P.H., Drrector

Organic Chemistry



o V O 0 5 7 9 6 . M M 1 :


COMPOUND DETECTED IN I,AB BLANK INDICATED BY *B.

UPPER QC L IMIT FOR CALIBRATION CHECK EXCEEDED _ *QU.

] F Y O U H A V E A N Y Q U E S T I O N S , C O N T A C T S T E V E G E I S A T ( 6 O B ) 2 2 4 - 6 2 6 9 .

Analys is Date Lab Comment

0611512011 01:00:00

ralysis Method Result Units LOD LOQ Repo( Limit


Test results for NELAP accredited lests are certified to meet the requirements of the NELAC standards. For a list of accredited analytes see

http://www.slh.wisc.edu/nelaP/




Responsible Party: ffi -.AL'D Steve Geis, Chemist SuPervisor

lf there are questions about this report, please contact Steve Geis aI 608-224-6269.

The results in this report apply only to the sample specifically listed above, This report is not to be reproduced except in full '

Report#: 9425892 Page 4 of 4

Wise onsin State Lubor:r tory of Higicne260i Agnculrure Dr ive, PO Box 7996Madrson, Wl 53707-7996(800)4,12-46 r E . FAX (608)22.1-62 r 3http :,1.1wv'.slh.wisc.cdu

Laboratory Report


WDNR LAB lD: 113133790 NELAP LAB lD: E37658 EPA LAB W100007

D.F Kurt-vcz, M.D., lv lcdrcal Director Char les D. Brokopp, Dr.P.H , Director


WSLH Sample:

RJN ENV. SERVICES LLC

4631 COUNTY ROAD A

oREGON. Wl 53575

ovo05795

Field #: 202


Collection End:

Collected By:

County:

Sample Source: AIR

Sample DePth:

Sample Information:

Sample Locat ion:

Sample DescriPt ion:


B i l l T o

Bi l l ing lD : 7305879

Customer lD: 320225

TRACKING 4920


MADISON WI 53718

tD#:

WaterbodY/Outfal l lD:

PoinUWell :

Account #. 1H034

Project No.

Date Received. 0611412011


Sample Reason:

Analysis Date06t1512011

Lab CommentSEE OVOO5795.MM,1

alysis Method Result

"B . l<0 .579

0.243

Units

PPB V

PPB V

LOD LOQ RePort L imi t

PROPENE 0.085

0.085

0.280

0.280DICHLORODI FLUOROMETHAN E

Note: The rePorted value above is

CHLOROMETHANE

equal to or greater than the LOD and less than the LOQ'

1,2-DICHLOROTETRAFLUOROETHAN E

VINYL CHLORIDE

1,3-BUTADIENE

BROMOMETHANE

CHLOROETHANE

ACROLEIN

ACETONE

N D

N D

N D

N D

N D

N D

N D

" B . Q U 1 . 1 7

PPB V

P P B V

P P B V

PPB V

PPB V

PPB V

PPB V

PPB V

0.085 0 .280

0 . 1 0 0 . 3 3 0

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

Page 1 of 4

Wisconsin State Laboraton of Hi 'g icnc260i Agr iculrure Drrve, PO Box 7996Madison, wl 53707-1996(800)4.+2-.16 r8 . FAX (608)22.1-62 I lhttp : i,'uuv. slh.*'i sc. edr-r

Laboratory Report


WDNR LAB lD : 113133790 NELAP LAB lD : E37658

D.l- . Kurqcz, M.D., Nledical Director Char les D. tsrokopp, Dr.P.H, Director

Organic ChemistrY



Result

0 . ' 1 5 1

Units

PPB VHALOCARBON 1 1

Note: The reoor ted value above is equal to or qreater than the LOD and less than the LOQ.

Method

1 ,1 -DICHLOROETHENE

METHYLENE CHLORIDE

CARBON DISULFIDE

1 . 1 .2-TRICHLOROTRIFLUOROETHAN E


1 ,1 -DICHLOROETHANE

TERT-BUWL METHYL ETHER

VINYL ACETATE

METHYL ETHYL KETONE

CIS-1 ,2-DICHLOROETHYLENE

HEXANE

CHLOROFORM

ETHYL ACETATE

TETRAHYDROFURAN

1,2-DICHLOROETHANE


BENZENE


CYCLOHEXANE

1.2-DICHLOROPROPANE


TRICHLOROETHYLENE

1,4-DIOXANE

HEPTANE

CIS-1 ,3-DICHLOROPROPENE


LOD LOQ

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

0 . 1 0 0 . 3 3

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

Report Limit

N D

N D

N D

N D

N D

N D

N D

0.312

0.373

N D

N D

0 . 1 6 4

N D

N D

N D

N D

0.277

PPB V

P P B V

PPB V

PPB V

PPB V

PPB V

P P B V

PPB V

PPB V

PPB V

PPB V

PPB V

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280

0.085 0 .280



PPB V

P P B V

PPB V

PPB V

P P B V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

N D

N D

N D

N D

N D

N D

N D

N D

N D

P a n o ) a f A

\ \ isconsin Statc Laborr tor ; of Hvu.rene2601 Agnculrure Dr ive. PO Bor ?996Madison, Wl 53707-7996(800)4,+2-46 I 8 . FAX (608)224-62 i lhnp: , / i ww. s lh.wisc. edu

Laboratory Report



D.lr . Kurrycz, M.D., Medical Direclor Char les D. Brokopp, Dr.P.H, Director

Organic Chemistry



nalysis Method

TRANS-1,3-DICHLOROPROPEN E

1, l ,2.TRICHLOROETHAN E

TOLUENE



1,2-DIBROMOETHANE

TETRACHLOROETHYLENE

CHLOROBENZENE

ETHYLBENZENE

M/P-XYLENE

BROMOFORM

STYRENE

1, 1,2,2-TETMCHLOROETHANE

O-XYLENE

1 -ETHYL4-METHYL BENZENE

1,3 ,s -TRIMETHYL BENZENE



1,3-DICHLOROBENZENE

1,4-DICHLOROBENZENE

1,2-DICHLOROBENZENE




0.085

0.085

0.08s

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

Result

N D

N D

z . t l

N D

N D

N D

0.341

N D

0.532

2.05

N D

0.268

N D

0.824

0.726

0.489

2.68

N D

N D

N D

N D

N D

N D

Units

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

P P B V

PPB V

PPB V

PPB V

PPB V

PPB V

PPB V

P P B V

PPB V

PPB V

PPB V

PPB V

P P B V

P P B V

PPB V

PPB V

LOD

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0.085

0 . ' 1 7 0

0.085

0.085

I na\

0.280

0.280

0 280

0.280

0.280

0.280

0.280

0.280

0.280

0 . 5 6 1

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

0.280

Report Limit

Page 3 of 4

\ ! isconsrn State Laborr t . , rv of H1 grenc2601 Agncul ture Dr ive. i )O Box 7996Madrson, Wl 53707-7996(800 )#2 -4618 . FAX (608 )221 -6213http :"/wr'.slh.wisc.cdu

Laboratory Report

D.ir . Kurry 'cz, M.D ' Medical Director Char les D Brokopp' Dr 'P H , Dtrector


WDNR LAB lD: 113133790 NELAP LAB lD: E37658 EPA LAB W100007 Wl DATCP lD: 105-415

WSLH Sample: ovo05795

0 0 5 7 9 5 . M M 1 :

WISCONSIN STATE LABORATORY OF HYGIENE SAMPLE OVOO5795 CONTAINS THE

FOLLOWING FLAGS.


COMPOTIND DETECTED IN LAB BLANK INDICATED BY *8.

U P P E R Q C L I M I T F O R C A L I B R A T I O N C H E C K E X C E E D E D - " Q U .

I F Y O U H A V E A N Y Q U E S T I O N S , C O N T A C T S T E V t r G E I S A T ( 6 0 8 ) 2 2 4 - 6 2 6 9 .

Analysis Date Lab Comment

0611512011

is Method Result Units LOD LOQ Report Limit

TOXIC ORGANIC COMPOUNDS lN COMPLETE I

AMBIENT AIR TO15 . PREP

Test results for NELAp accredited tests are certified to meet the requirements of the NELAC standards. For a list Of accredited analytes see

htto://www.slh.wisc.edu/nelaP/




Responsible PartY: ffi. -41rD Steve Geis, Chemist SuPervisor

lf there are questions about this report, please contact Steve Geis al608'224-6269'

The results in this report apply only to the sample specifically listed above. This report is not to be reproduced except in full '

Report #: 9425891 Page 4 ol 4

X P

z - -, i

l -

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va l(-lc4

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h * l a i tv f v l . = w

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ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Watertown1101 Industrial Drive, Suites 9 & 10Watertown, WI 53094Tel: 800-833-7036

TestAmerica Job ID: WUF0165Client Project/Site: [none]Client Project Description: Madison Kipp

For:RJN ENVIRONMENTAL SERVICES, LLC4631 County Road AOregon, WI 53575

Attn: Mr. Robert Nauta

Authorized for release by:06/15/2011 06:32:10 AMBrian DeJongOrganics [email protected]

Designee for

Dan F. MilewskyProject [email protected]

This report has been electronically signed and authorized by the signatory. Electronic signatureis intended to be the legally binding equivalent of a traditionally handwritten signature.

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https://secure.testamericainc.com/TotalAccess/login.aspx

http://www.testamericainc.com/AskTheExpert/Expert_index.htm

http://www.testamericainc.com

mailto:[email protected]

mailto:[email protected]

Table of Contents

Client: RJN ENVIRONMENTAL SERVICES, LLCProject/Site: [none]

TestAmerica Job ID: WUF0165

Page 2 of 30TestAmerica Watertown

06/15/2011

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22

Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29

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Definitions/GlossaryTestAmerica Job ID: WUF0165Client: RJN ENVIRONMENTAL SERVICES, LLC

Project/Site: [none]

Qualifiers

GCMS Volatiles

Qualifier Description

J Estimated value. Analyte detected at a level less than the Reporting Limit (RL) and greater than or equal to the Method Detection Limit

(MDL). The user of this data should be aware that this data is of limited reliability.

Qualifier

Glossary

These commonly used abbreviations may or may not be present in this report.

☼ Listed under the "D" column to designate that the result is reported on a dry weight basis.

Abbreviation

EPA United States Environmental Protection Agency

ND Not Detected above the reporting level.

MDL Method Detection Limit

RL Reporting Limit

RE, RE1 (etc.) Indicates a Re-extraction or Reanalysis of the sample.

%R Percent Recovery

RPD Relative Percent Difference, a measure of the relative difference between two points.

TestAmerica Watertown

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Detection SummaryTestAmerica Job ID: WUF0165Client: RJN ENVIRONMENTAL SERVICES, LLC


Client Sample ID: HA 101 Lab Sample ID: WUF0165-01

No Detections.


Analyte Result Qualifier Unit Method Prep TypeD

☼

Dil Fac

Tetrachloroethene 33 J

RL

130 ug/kg dry SW 8260B Total1.0

MDL

31



☼

Dil Fac

Tetrachloroethene 180

RL


MDL

30



☼

Dil Fac

Tetrachloroethene 610

RL


MDL

29



☼

Dil Fac


RL


MDL

31



☼

Dil Fac


RL


MDL

31

Client Sample ID: MeOH Blank Lab Sample ID: WUF0165-07

No Detections.


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Client Sample ResultsTestAmerica Job ID: WUF0165Client: RJN ENVIRONMENTAL SERVICES, LLC


Lab Sample ID: WUF0165-01Client Sample ID: HA 101Matrix: SoilDate Collected: 06/07/11 07:00

Percent Solids: 81.5Date Received: 06/07/11 11:47

Method: SW 8260B - VOCs by SW8260B

Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac

Benzene <31 120 31 ug/kg dry ☼ 06/09/11 14:31 06/09/11 20:32 1.0

Analyte

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Bromobenzene <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Bromochloromethane <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Bromodichloromethane <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Bromoform <31

310 120 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Bromomethane <120

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼n-Butylbenzene <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼sec-Butylbenzene <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼tert-Butylbenzene <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Carbon Tetrachloride <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Chlorobenzene <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Chlorodibromomethane <31

120 61 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Chloroethane <61

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Chloroform <31

120 61 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Chloromethane <61

120 61 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼2-Chlorotoluene <61


120 61 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼1,2-Dibromo-3-chloropropane <61

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼1,2-Dibromoethane (EDB) <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Dibromomethane <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼1,2-Dichlorobenzene <31



120 61 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Dichlorodifluoromethane <61

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼1,1-Dichloroethane <31


120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼1,1-Dichloroethene <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼cis-1,2-Dichloroethene <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼trans-1,2-Dichloroethene <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼1,2-Dichloropropane <31



120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼1,1-Dichloropropene <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼cis-1,3-Dichloropropene <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼trans-1,3-Dichloropropene <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Isopropyl Ether <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Ethylbenzene <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Hexachlorobutadiene <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Isopropylbenzene <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼p-Isopropyltoluene <31

120 61 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Methylene Chloride <61

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Methyl tert-Butyl Ether <31

120 61 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Naphthalene <61

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼n-Propylbenzene <31

120 61 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Styrene <61

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼1,1,1,2-Tetrachloroethane <31


120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Tetrachloroethene <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Toluene <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼1,2,3-Trichlorobenzene <31


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Method: SW 8260B - VOCs by SW8260B (Continued)


1,2,4-Trichlorobenzene <31 120 31 ug/kg dry ☼ 06/09/11 14:31 06/09/11 20:32 1.0

Analyte

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼1,1,1-Trichloroethane <31


120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Trichloroethene <31

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Trichlorofluoromethane <31

120 61 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼1,2,3-Trichloropropane <61

120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼1,2,4-Trimethylbenzene <31


120 31 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Vinyl chloride <31

370 92 ug/kg dry 06/09/11 14:31 06/09/11 20:32 1.0☼Xylenes, total <92

Qualifier Prepared Analyzed Dil Fac % Recovery Limits

Dibromofluoromethane 100 80 - 120 06/09/11 14:31 06/09/11 20:32 1.0

Surrogate

Toluene-d8 99 06/09/11 14:31 06/09/11 20:32 1.080 - 120

4-Bromofluorobenzene 98 06/09/11 14:31 06/09/11 20:32 1.080 - 120





Benzene <31 130 31 ug/kg dry ☼ 06/09/11 14:31 06/09/11 20:59 1.0

Analyte






























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1,2-Dichloropropane <31 130 31 ug/kg dry ☼ 06/09/11 14:31 06/09/11 20:59 1.0

Analyte















130 63 ug/kg dry 06/09/11 14:31 06/09/11 20:59 1.0☼Styrene <63



130 31 ug/kg dry 06/09/11 14:31 06/09/11 20:59 1.0☼Tetrachloroethene 33 J

130 31 ug/kg dry 06/09/11 14:31 06/09/11 20:59 1.0☼Toluene <31














Surrogate

Toluene-d8 99 06/09/11 14:31 06/09/11 20:59 1.080 - 120






Benzene <30 120 30 ug/kg dry ☼ 06/09/11 14:31 06/09/11 21:26 1.0

Analyte









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tert-Butylbenzene <30 120 30 ug/kg dry ☼ 06/09/11 14:31 06/09/11 21:26 1.0

Analyte




































120 60 ug/kg dry 06/09/11 14:31 06/09/11 21:26 1.0☼Styrene <60



120 30 ug/kg dry 06/09/11 14:31 06/09/11 21:26 1.0☼Tetrachloroethene 180

120 30 ug/kg dry 06/09/11 14:31 06/09/11 21:26 1.0☼Toluene <30











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Vinyl chloride <30 120 30 ug/kg dry ☼ 06/09/11 14:31 06/09/11 21:26 1.0

Analyte




Surrogate

Toluene-d8 99 06/09/11 14:31 06/09/11 21:26 1.080 - 120






Benzene <29 120 29 ug/kg dry ☼ 06/09/11 14:31 06/09/11 21:53 1.0

Analyte






































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Hexachlorobutadiene <29 120 29 ug/kg dry ☼ 06/09/11 14:31 06/09/11 21:53 1.0

Analyte







120 59 ug/kg dry 06/09/11 14:31 06/09/11 21:53 1.0☼Styrene <59



120 29 ug/kg dry 06/09/11 14:31 06/09/11 21:53 1.0☼Tetrachloroethene 610

120 29 ug/kg dry 06/09/11 14:31 06/09/11 21:53 1.0☼Toluene <29














Surrogate

Toluene-d8 97 06/09/11 14:31 06/09/11 21:53 1.080 - 120






Benzene <31 120 31 ug/kg dry ☼ 06/09/11 14:31 06/09/11 22:20 1.0

Analyte

















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4-Chlorotoluene <31 120 31 ug/kg dry ☼ 06/09/11 14:31 06/09/11 22:20 1.0

Analyte




























120 61 ug/kg dry 06/09/11 14:31 06/09/11 22:20 1.0☼Styrene <61




120 31 ug/kg dry 06/09/11 14:31 06/09/11 22:20 1.0☼Toluene <31














Surrogate

Toluene-d8 98 06/09/11 14:31 06/09/11 22:20 1.080 - 120



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Benzene <31 120 31 ug/kg dry ☼ 06/10/11 10:44 06/10/11 15:45 1.0

Analyte












































120 62 ug/kg dry 06/10/11 10:44 06/10/11 15:45 1.0☼Styrene <62




120 31 ug/kg dry 06/10/11 10:44 06/10/11 15:45 1.0☼Toluene <31



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1,2,4-Trichlorobenzene <31 120 31 ug/kg dry ☼ 06/10/11 10:44 06/10/11 15:45 1.0

Analyte












Surrogate

Toluene-d8 99 06/10/11 10:44 06/10/11 15:45 1.080 - 120


Lab Sample ID: WUF0165-07Client Sample ID: MeOH BlankMatrix: methanolDate Collected: 06/07/11 00:00

Date Received: 06/07/11 11:47



Benzene <25 100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0

Analyte

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Bromobenzene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Bromochloromethane <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Bromodichloromethane <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Bromoform <25

250 100 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Bromomethane <100

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0n-Butylbenzene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0sec-Butylbenzene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0tert-Butylbenzene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Carbon Tetrachloride <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Chlorobenzene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Chlorodibromomethane <25

100 50 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Chloroethane <50

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Chloroform <25

100 50 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Chloromethane <50

100 50 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.02-Chlorotoluene <50

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.04-Chlorotoluene <25

100 50 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.01,2-Dibromo-3-chloropropane <50

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.01,2-Dibromoethane (EDB) <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Dibromomethane <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.01,2-Dichlorobenzene <25



100 50 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Dichlorodifluoromethane <50

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.01,1-Dichloroethane <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.01,2-Dichloroethane <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.01,1-Dichloroethene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0cis-1,2-Dichloroethene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0trans-1,2-Dichloroethene <25


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Lab Sample ID: WUF0165-07Client Sample ID: MeOH BlankMatrix: methanolDate Collected: 06/07/11 00:00




1,2-Dichloropropane <25 100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0

Analyte

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.01,3-Dichloropropane <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.02,2-Dichloropropane <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.01,1-Dichloropropene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0cis-1,3-Dichloropropene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0trans-1,3-Dichloropropene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Isopropyl Ether <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Ethylbenzene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Hexachlorobutadiene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Isopropylbenzene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0p-Isopropyltoluene <25

100 50 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Methylene Chloride <50

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Methyl tert-Butyl Ether <25

100 50 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Naphthalene <50

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0n-Propylbenzene <25

100 50 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Styrene <50

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.01,1,1,2-Tetrachloroethane <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.01,1,2,2-Tetrachloroethane <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Tetrachloroethene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Toluene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.01,2,3-Trichlorobenzene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.01,2,4-Trichlorobenzene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.01,1,1-Trichloroethane <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.01,1,2-Trichloroethane <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Trichloroethene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Trichlorofluoromethane <25

100 50 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.01,2,3-Trichloropropane <50

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.01,2,4-Trimethylbenzene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.01,3,5-Trimethylbenzene <25

100 25 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Vinyl chloride <25

300 75 ug/kg wet 06/10/11 10:44 06/10/11 15:18 1.0Xylenes, total <75



Surrogate

Toluene-d8 98 06/10/11 10:44 06/10/11 15:18 1.080 - 120



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Surrogate SummaryTestAmerica Job ID: WUF0165Client: RJN ENVIRONMENTAL SERVICES, LLC


Method: SW 8260B - VOCs by SW8260BPrep Type: TotalMatrix: methanol

Lab Sample ID Client Sample ID (80-120) (80-120) (80-120)

DBFM TOL BFB

102 98 100WUF0165-07

Percent Surrogate Recovery (Acceptance Limits)

MeOH Blank

Surrogate Legend

DBFM = Dibromofluoromethane

TOL = Toluene-d8

BFB = 4-Bromofluorobenzene

Method: SW 8260B - VOCs by SW8260BPrep Type: TotalMatrix: Soil


DBFM TOL BFB

100 99 98WUF0165-01


HA 101

100 99 98WUF0165-02 HA 102

98 99 98WUF0165-03 HA 103

100 97 99WUF0165-04 HA 104

104 98 98WUF0165-05 HA 105

99 99 99WUF0165-06 HA 106

Surrogate Legend


TOL = Toluene-d8


Method: SW 8260B - VOCs by SW8260BPrep Type: TotalMatrix: Solid/Soil


DBFM TOL BFB

99 99 9811F0129-BLK1


Method Blank

106 99 9911F0129-BS1 Lab Control Sample

98 100 9911F0155-BLK1 Method Blank

104 99 9911F0155-BS1 Lab Control Sample

Surrogate Legend


TOL = Toluene-d8



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QC Sample ResultsTestAmerica Job ID: WUF0165Client: RJN ENVIRONMENTAL SERVICES, LLC



Client Sample ID: Method BlankLab Sample ID: 11F0129-BLK1

Matrix: Solid/Soil Prep Type: Total

Analysis Batch: U000789 Prep Batch: 11F0129_P

Result Qualifier Unit D Prepared Analyzed Dil FacRL MDL

Benzene <25 100 25 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00

Blank Blank

Analyte

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Bromobenzene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Bromochloromethane

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Bromodichloromethane

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Bromoform

<100 100250 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Bromomethane

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00n-Butylbenzene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00sec-Butylbenzene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00tert-Butylbenzene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Carbon Tetrachloride

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Chlorobenzene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Chlorodibromomethane

<50 50100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Chloroethane

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Chloroform

<50 50100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Chloromethane

<50 50100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.002-Chlorotoluene


<50 50100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.001,2-Dibromo-3-chloropropane

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.001,2-Dibromoethane (EDB)

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Dibromomethane

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.001,2-Dichlorobenzene



<50 50100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Dichlorodifluoromethane

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.001,1-Dichloroethane


<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.001,1-Dichloroethene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00cis-1,2-Dichloroethene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00trans-1,2-Dichloroethene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.001,2-Dichloropropane



<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.001,1-Dichloropropene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00cis-1,3-Dichloropropene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00trans-1,3-Dichloropropene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Isopropyl Ether

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Ethylbenzene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Hexachlorobutadiene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Isopropylbenzene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00p-Isopropyltoluene

<50 50100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Methylene Chloride

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Methyl tert-Butyl Ether

<50 50100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Naphthalene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00n-Propylbenzene

<50 50100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Styrene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.001,1,1,2-Tetrachloroethane


<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Tetrachloroethene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Toluene


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1,2,3-Trichlorobenzene <25 100 25 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00

Blank Blank

Analyte

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.001,2,4-Trichlorobenzene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.001,1,1-Trichloroethane


<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Trichloroethene

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Trichlorofluoromethane

<50 50100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.001,2,3-Trichloropropane

<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.001,2,4-Trimethylbenzene


<25 25100 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Vinyl chloride

<75 75300 ug/kg wet 06/09/11 10:19 06/09/11 13:21 1.00Xylenes, total

% Recovery Qualifier Prepared Analyzed Dil FacLimits

Dibromofluoromethane 99 80 - 120 06/09/11 13:21 1.00

Blank Blank

Surrogate

06/09/11 10:19

99 06/09/11 10:19 06/09/11 13:21 1.00Toluene-d8 80 - 120

98 06/09/11 10:19 06/09/11 13:21 1.004-Bromofluorobenzene 80 - 120

Client Sample ID: Lab Control SampleLab Sample ID: 11F0129-BS1


Analysis Batch: U000789 Prep Batch: 11F0129_PSpike

Added Result Qualifier Unit % Rec

% Rec.

Limits

Benzene 2500.0 2410 ug/kg 96 80 - 120

LCS LCS

DAnalyte

Bromobenzene 2500.0 2390 ug/kg 95 80 - 120

Bromochloromethane 2500.0 2430 ug/kg 97 80 - 120

Bromodichloromethane 2500.0 2420 ug/kg 97 80 - 120

Bromoform 2500.0 2370 ug/kg 95 80 - 120

Bromomethane 2500.0 2500 ug/kg 100 60 - 140

n-Butylbenzene 2500.0 2440 ug/kg 97 80 - 120

sec-Butylbenzene 2500.0 2440 ug/kg 97 80 - 120

tert-Butylbenzene 2500.0 2410 ug/kg 96 80 - 120

Carbon Tetrachloride 2500.0 2530 ug/kg 101 60 - 140

Chlorobenzene 2500.0 2330 ug/kg 93 80 - 120

Chlorodibromomethane 2500.0 2380 ug/kg 95 80 - 120

Chloroethane 2500.0 2470 ug/kg 99 60 - 140

Chloroform 2500.0 2500 ug/kg 100 80 - 120

Chloromethane 2500.0 2450 ug/kg 98 60 - 140

2-Chlorotoluene 2500.0 2380 ug/kg 95 80 - 120


1,2-Dibromo-3-chloropropane 2500.0 2340 ug/kg 94 60 - 140

1,2-Dibromoethane (EDB) 2500.0 2270 ug/kg 91 80 - 120

Dibromomethane 2500.0 2370 ug/kg 95 80 - 120

1,2-Dichlorobenzene 2500.0 2280 ug/kg 91 80 - 120



Dichlorodifluoromethane 2500.0 2440 ug/kg 98 60 - 140

1,1-Dichloroethane 2500.0 2520 ug/kg 101 80 - 120


1,1-Dichloroethene 2500.0 2500 ug/kg 100 80 - 120


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% Rec.

Limits

cis-1,2-Dichloroethene 2500.0 2480 ug/kg 99 80 - 120

LCS LCS

DAnalyte

trans-1,2-Dichloroethene 2500.0 2450 ug/kg 98 80 - 120

1,2-Dichloropropane 2500.0 2430 ug/kg 97 80 - 120



1,1-Dichloropropene 2500.0 2560 ug/kg 102 80 - 120

cis-1,3-Dichloropropene 2500.0 2460 ug/kg 98 80 - 120

trans-1,3-Dichloropropene 2500.0 2420 ug/kg 97 80 - 120

Isopropyl Ether 2500.0 2520 ug/kg 101 80 - 120

Ethylbenzene 2500.0 2370 ug/kg 95 80 - 120

Hexachlorobutadiene 2500.0 2320 ug/kg 93 60 - 140

Isopropylbenzene 2500.0 2400 ug/kg 96 80 - 120

p-Isopropyltoluene 2500.0 2450 ug/kg 98 80 - 120

Methylene Chloride 2500.0 2440 ug/kg 98 80 - 120

Methyl tert-Butyl Ether 2500.0 2440 ug/kg 98 80 - 120

Naphthalene 2500.0 2210 ug/kg 89 60 - 140

n-Propylbenzene 2500.0 2440 ug/kg 97 80 - 120

Styrene 2500.0 2390 ug/kg 96 80 - 120

1,1,1,2-Tetrachloroethane 2500.0 2440 ug/kg 97 80 - 120


Tetrachloroethene 2500.0 2380 ug/kg 95 80 - 120

Toluene 2500.0 2360 ug/kg 94 80 - 120

1,2,3-Trichlorobenzene 2500.0 2250 ug/kg 90 80 - 120


1,1,1-Trichloroethane 2500.0 2570 ug/kg 103 80 - 120


Trichloroethene 2500.0 2400 ug/kg 96 80 - 120

Trichlorofluoromethane 2500.0 2510 ug/kg 101 80 - 120

1,2,3-Trichloropropane 2500.0 2260 ug/kg 90 80 - 120

1,2,4-Trimethylbenzene 2500.0 2410 ug/kg 96 80 - 120


Vinyl chloride 2500.0 2530 ug/kg 101 80 - 120

Xylenes, total 7500.0 7130 ug/kg 95 80 - 120

Qualifier % Recovery Limits

Dibromofluoromethane 106 80 - 120

LCS LCS

Surrogate

99Toluene-d8 80 - 120

994-Bromofluorobenzene 80 - 120





Benzene <25 100 25 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00

Blank Blank

Analyte

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Bromobenzene

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Bromochloromethane

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Bromodichloromethane

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Bromoform


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Bromomethane <100 250 100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00

Blank Blank

Analyte

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00n-Butylbenzene

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00sec-Butylbenzene

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00tert-Butylbenzene

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Carbon Tetrachloride

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Chlorobenzene

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Chlorodibromomethane

<50 50100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Chloroethane

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Chloroform

<50 50100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Chloromethane



<50 50100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.001,2-Dibromo-3-chloropropane

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.001,2-Dibromoethane (EDB)

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Dibromomethane




<50 50100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Dichlorodifluoromethane



<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.001,1-Dichloroethene

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00cis-1,2-Dichloroethene

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00trans-1,2-Dichloroethene




<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.001,1-Dichloropropene

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00cis-1,3-Dichloropropene

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00trans-1,3-Dichloropropene

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Isopropyl Ether

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Ethylbenzene

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Hexachlorobutadiene

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Isopropylbenzene

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00p-Isopropyltoluene

<50 50100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Methylene Chloride

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Methyl tert-Butyl Ether

<50 50100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Naphthalene

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00n-Propylbenzene

<50 50100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Styrene



<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Tetrachloroethene

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Toluene





<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Trichloroethene

<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Trichlorofluoromethane


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1,2,3-Trichloropropane <50 100 50 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00

Blank Blank

Analyte



<25 25100 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Vinyl chloride

<75 75300 ug/kg wet 06/10/11 10:44 06/10/11 13:31 1.00Xylenes, total

% Recovery Qualifier Prepared Analyzed Dil FacLimits

Dibromofluoromethane 98 80 - 120 06/10/11 13:31 1.00

Blank Blank

Surrogate

06/10/11 10:44

100 06/10/11 10:44 06/10/11 13:31 1.00Toluene-d8 80 - 120

99 06/10/11 10:44 06/10/11 13:31 1.004-Bromofluorobenzene 80 - 120





% Rec.

Limits

Benzene 2500.0 2460 ug/kg 98 80 - 120

LCS LCS

DAnalyte

Bromobenzene 2500.0 2370 ug/kg 95 80 - 120

Bromochloromethane 2500.0 2430 ug/kg 97 80 - 120

Bromodichloromethane 2500.0 2450 ug/kg 98 80 - 120

Bromoform 2500.0 2350 ug/kg 94 80 - 120

Bromomethane 2500.0 2480 ug/kg 99 60 - 140

n-Butylbenzene 2500.0 2470 ug/kg 99 80 - 120

sec-Butylbenzene 2500.0 2440 ug/kg 98 80 - 120

tert-Butylbenzene 2500.0 2400 ug/kg 96 80 - 120

Carbon Tetrachloride 2500.0 2580 ug/kg 103 60 - 140

Chlorobenzene 2500.0 2360 ug/kg 95 80 - 120

Chlorodibromomethane 2500.0 2410 ug/kg 96 80 - 120

Chloroethane 2500.0 2420 ug/kg 97 60 - 140

Chloroform 2500.0 2490 ug/kg 99 80 - 120

Chloromethane 2500.0 2460 ug/kg 98 60 - 140



1,2-Dibromo-3-chloropropane 2500.0 2240 ug/kg 89 60 - 140

1,2-Dibromoethane (EDB) 2500.0 2310 ug/kg 92 80 - 120

Dibromomethane 2500.0 2340 ug/kg 94 80 - 120




Dichlorodifluoromethane 2500.0 2450 ug/kg 98 60 - 140



1,1-Dichloroethene 2500.0 2540 ug/kg 102 80 - 120

cis-1,2-Dichloroethene 2500.0 2510 ug/kg 101 80 - 120

trans-1,2-Dichloroethene 2500.0 2500 ug/kg 100 80 - 120




1,1-Dichloropropene 2500.0 2600 ug/kg 104 80 - 120


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% Rec.

Limits

cis-1,3-Dichloropropene 2500.0 2450 ug/kg 98 80 - 120

LCS LCS

DAnalyte

trans-1,3-Dichloropropene 2500.0 2450 ug/kg 98 80 - 120

Isopropyl Ether 2500.0 2500 ug/kg 100 80 - 120

Ethylbenzene 2500.0 2440 ug/kg 98 80 - 120

Hexachlorobutadiene 2500.0 2350 ug/kg 94 60 - 140

Isopropylbenzene 2500.0 2450 ug/kg 98 80 - 120

p-Isopropyltoluene 2500.0 2430 ug/kg 97 80 - 120

Methylene Chloride 2500.0 2410 ug/kg 96 80 - 120

Methyl tert-Butyl Ether 2500.0 2400 ug/kg 96 80 - 120

Naphthalene 2500.0 2200 ug/kg 88 60 - 140

n-Propylbenzene 2500.0 2450 ug/kg 98 80 - 120

Styrene 2500.0 2400 ug/kg 96 80 - 120



Tetrachloroethene 2500.0 2450 ug/kg 98 80 - 120

Toluene 2500.0 2400 ug/kg 96 80 - 120





Trichloroethene 2500.0 2450 ug/kg 98 80 - 120

Trichlorofluoromethane 2500.0 2550 ug/kg 102 80 - 120

1,2,3-Trichloropropane 2500.0 2250 ug/kg 90 80 - 120



Vinyl chloride 2500.0 2530 ug/kg 101 80 - 120

Xylenes, total 7500.0 7300 ug/kg 97 80 - 120

Qualifier % Recovery Limits

Dibromofluoromethane 104 80 - 120

LCS LCS

Surrogate

99Toluene-d8 80 - 120

994-Bromofluorobenzene 80 - 120


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QC Association SummaryTestAmerica Job ID: WUF0165Client: RJN ENVIRONMENTAL SERVICES, LLC


GCMS Volatiles

Analysis Batch: U000789

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Total Solid/Soil SW 8260B 11F0129_P11F0129-BS1 Lab Control Sample

Total Solid/Soil SW 8260B 11F0129_P11F0129-BLK1 Method Blank

Total Soil SW 8260B 11F0129_PWUF0165-01 HA 101





Analysis Batch: U000795


Total Solid/Soil SW 8260B 11F0155_P11F0155-BS1 Lab Control Sample

Total Solid/Soil SW 8260B 11F0155_P11F0155-BLK1 Method Blank

Total methanol SW 8260B 11F0155_PWUF0165-07 MeOH Blank


Prep Batch: 11F0129_P


Total Solid/Soil SW 503511F0129-BS1 Lab Control Sample

Total Solid/Soil SW 503511F0129-BLK1 Method Blank

Total Soil SW 5035WUF0165-01 HA 101







Total Solid/Soil SW 503511F0155-BS1 Lab Control Sample

Total Solid/Soil SW 503511F0155-BLK1 Method Blank

Total methanol SW 5035WUF0165-07 MeOH Blank


WetChem

Analysis Batch: 11F0133


Total Soil SM 2540G 11F0133_PWUF0165-01 HA 101








Total Soil NO PREP -

WET CHEM

WUF0165-01 HA 101


WET CHEM

WUF0165-02 HA 102


WET CHEM

WUF0165-03 HA 103


WET CHEM

WUF0165-04 HA 104


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QC Association SummaryTestAmerica Job ID: WUF0165Client: RJN ENVIRONMENTAL SERVICES, LLC


WetChem (Continued)

Prep Batch: 11F0133_P (Continued)



WET CHEM

WUF0165-05 HA 105


WET CHEM

WUF0165-06 HA 106


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Lab ChronicleClient: RJN ENVIRONMENTAL SERVICES, LLC TestAmerica Job ID: WUF0165


Client Sample ID: HA 101 Lab Sample ID: WUF0165-01Matrix: SoilDate Collected: 06/07/11 07:00


Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared

Or Analyzed Analyst LabPrep Type

Total Prep SW 5035 06/09/11 14:31 ABA1.0 11F0129_P TAL WT

Total Analysis SW 8260B 1.0 U000789 06/09/11 20:32 ABA TAL WT

Total Prep NO PREP - WET

CHEM

1.0 11F0133_P 06/09/11 11:11 MMP TAL WT

Total Analysis SM 2540G 1.0 11F0133 06/10/11 12:41 MMP TAL WT



Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared





CHEM

1.0 11F0133_P 06/09/11 11:11 MMP TAL WT




Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared





CHEM

1.0 11F0133_P 06/09/11 11:11 MMP TAL WT




Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared





CHEM

1.0 11F0133_P 06/09/11 11:11 MMP TAL WT




Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared





CHEM

1.0 11F0133_P 06/09/11 11:11 MMP TAL WT


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Lab ChronicleClient: RJN ENVIRONMENTAL SERVICES, LLC TestAmerica Job ID: WUF0165




Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared


Total Analysis SM 2540G 06/10/11 12:41 MMP1.0 11F0133 TAL WT



Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared





CHEM

1.0 11F0133_P 06/09/11 11:11 MMP TAL WT


Client Sample ID: MeOH Blank Lab Sample ID: WUF0165-07Matrix: methanolDate Collected: 06/07/11 00:00


Batch

Type

Batch

Method Run

Dilution

Factor

Batch

Number

Prepared




Laboratory References:

TAL WT = TestAmerica Watertown, 1101 Industrial Drive, Suites 9 & 10, Watertown, WI 53094, TEL 800-833-7036


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Certification SummaryTestAmerica Job ID: WUF0165Client: RJN ENVIRONMENTAL SERVICES, LLC


Laboratory Program Certification IDAuthority EPA Region

TestAmerica Watertown 105-266WI Dept of Agriculture (Micro)

TestAmerica Watertown 100453NELACIllinois 5

TestAmerica Watertown 294State ProgramIowa 7

TestAmerica Watertown 055-999-366NELACMinnesota 5

TestAmerica Watertown 128053530State ProgramWisconsin 5

Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory’s

current list of certified methods and analytes.


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Method SummaryTestAmerica Job ID: WUF0165Client: RJN ENVIRONMENTAL SERVICES, LLC


Method Method Description LaboratoryProtocol

SW 8260B VOCs by SW8260B TAL WT

SM 2540G General Chemistry Parameters TAL WT

Protocol References:

Laboratory References:

TAL WT = TestAmerica Watertown, 1101 Industrial Drive, Suites 9 & 10, Watertown, WI 53094, TEL 800-833-7036


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Sample SummaryTestAmerica Job ID: WUF0165Client: RJN ENVIRONMENTAL SERVICES, LLC


Lab Sample ID Client Sample ID ReceivedCollectedMatrix

WUF0165-01 HA 101 Soil 06/07/11 07:00 06/07/11 11:47

WUF0165-02 HA 102 Soil 06/07/11 09:10 06/07/11 11:47

WUF0165-03 HA 103 Soil 06/07/11 09:22 06/07/11 11:47

WUF0165-04 HA 104 Soil 06/07/11 09:32 06/07/11 11:47

WUF0165-05 HA 105 Soil 06/07/11 09:48 06/07/11 11:47

WUF0165-06 HA 106 Soil 06/07/11 09:55 06/07/11 11:47

WUF0165-07 MeOH Blank methanol 06/07/11 00:00 06/07/11 11:47


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Documents

Air Sampling...2011/07/19 · WDNR LAB lD: 113133790 NELAP LAB lD: E37658 EPA LAB W100007 Supplement to test report#: 9391658 Amended Report WSLH Sample: OV003833 D,F Kurrycz, M,D