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CaRPORATIONEnvironmental Services
Public Ledger BuildingIndependence Square6th and Chestnut StreetsSuite 872Philadelphia, PA 19106
Telephone: 215-440-7340Fax: 215-440-7346
July 17, 1991
HAND DELIVERY
Ms. Christine ChulickU.S. Environmental Protection Agency841 Chestnut BuildingPhiladelphia, PA 19107
RE: Data Validation ReportsSaegertown SiteWork Assignment No. C03045
Dear Ms. Chulick:
Enclosed are copies of the data summary forms for case # 15741 SDGs MCBB99 andMCDP 87, and # 15536 SDGs MCDP 80 and CCBOO. The validation for these cases hasbeen completed and sent to Diann Sims in Region HI Central Laboratory. Also enclosedare copies of a completed case #15741 SDG CAU93 which was approved by Region HICentral Laboratory for distribution.
Should you have any questions, please do not hesitate to call me at (215) 440-7340.
Sincerely,
Camille Costa JE.Project Manager
cc: Mr. Robert E. Stecik, Dynamac, Philadelphia Operations (letter only)Ms. Donna McGowan, EPA, Regional Project Officer (letter only)
Enclosure
AB302502
Corporate Headquarters: The Dynamac Building, 2275 Research Boulevard, Suite 500, Rockville, MD 20850-3268
Attachment 2Data Summary Fo
flR302503
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Attachment 2Data Summary Forms
AR302506
n
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Quanti.tatl.oi
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l-Olchloroethane j
o9oroforw
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H
*l-Dlchloroethane |
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r»•rbon Disul fide
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rryl CM or Id*
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location
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ws
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Dilution Factor
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8a
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I
I
rW
rt
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\[li-l.J-Olchloropropene i 1 location
•
\ Holtture
x»
i*"
V
^
-*
Dilution factor
X,
C
*
C
X\
VI
!
1
1
x-
rCN"tfco.^
^
fp>&o
T «•••*•
SfrvXN,
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o
>
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me Chloride
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o
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o
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i
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LocationDilution Factor
xCi
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a
t?
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o^
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i
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u,
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S0
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u.
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a
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o
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c
*•iit
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vn
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wt
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n3"
e>
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OE
Ul
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Dlbromochtorome thane |
Ul
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n
o
o
Ul
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3-
T
Oo
o
1 T 5TV
LocationDilution Factor
0
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vt
I
o
rs
0U/
PiCNoOs
I
I
a caa fta a
3
ca
Hca
o»n
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rt
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o
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o
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M
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rx
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o
o
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8.
o
a
<=
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o
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n
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o
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oroethene |
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i
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9
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o
I
f
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o
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o
1
Alcohol ]
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|
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R^
or*
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41
location |
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k
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Dilution Factor
^
J
x
O
7s0
m
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O
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eaniline |
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o
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3
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o
f?
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1
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i
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s
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o
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Dilution Factor
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XO
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r\sJ.
o
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itts
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il O M• fta a
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on Vs V•o 3* 1 'B ?<a (oJ ^
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j* 5
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ta
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o
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rtor
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i
<
i L0 O S
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o
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o
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o
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o
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o
er
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ny
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o o
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i
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1
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I
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i
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o
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o
Phenanthrene |
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o
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o
j
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g
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^
s
§
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£
Sample No.Dilution Factor
X Moltturelocation
C*Ql COMPOUND
^
^ % 4
" Vr*
— =
"sj
-f•
V
5
s
5
3=
0
x,fv
X
c
X.
0
1c11*>^
To calculate* aaajpl* quantitjrt?lon limit i
(CRQi, • Dilution Factor) /
((100 - % axO?tura)/100)
«CC
o•a
S
ca
-3H-3
aft
x
xX
V.
^
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25
e
az
|
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ta
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az>en
a
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• Contractb Require*)
Quanititatior
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C9eaE NARRA
H
1
§£HEPINITI
i
|
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S
L7~*
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iu
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MUl*•
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ro
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I Aroclor-
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o
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rsirvj
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eot
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a
o
°
af
0
1
o
r§
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49
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*>V
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•
^
^
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|
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V
*
Endoiull
o
n2
*
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*
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c
a
n
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at
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m
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a
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a
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—H
o
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a
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a
99
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M
«.4
n0r~
1
•41
^W ^
r-
i"
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f
tt
f
*
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>3
X
1
Dilution Factor |
^
X
>.
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O
f
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i
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0x
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rv
§
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B n» nfl Bft M0 ••1 ft"- a^* a-* •
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hAR3025U
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Attachment 2Data Summary Forms
SM
ops-
taaartanfti—o
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a fta a
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rt9
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I
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e H-<t ft
0 5-ft B;>.'t IHIon 3R3025 r-
0Ht^
Attachment 2Data Summary Fo
AR3025I7
o
fIM
fc
j
rsVj
N
G»
2.
oba
N
1
Vi
§
Vi>^o
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S
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en
02518"2 •i HIo MIH- aMl 0H- ft" f• A
Date : June 14, 1991
Subject : Organic Data Validation Case 15741,SDG:CAU93Site: Saegertown Industrial r t
From : Ting-Ting Chang, Darline F. Terrell'Data Reviewer, Project Manager
To: :Diann SimsEPA Region III TES Contract Coordinator
Overview
Case 15741, SDG CAU93 contained two (2) soil samples and six (6)water samples for full organic analyses, and two (2) water samplesfor volatile analysis only. All these samples were analyzedthrough the Contract Laboratory Program Routine AnalyticalServices.
summary
All compounds were successfully analyzed. Areas of concern withrespect to usability are listed according to the seriousness of theproblem.
Ma-1 or Problems
2-butanone in all the water samples would not have beendetected even if this compound were present in the samples.The reported detection limits for this compound has beenqualified as unreliable (R) due to the very poor instrumentresponse factors (0.023 and 0.024).
Minor Issues
Estimate (J) the positive results and (UJ) all the non-detected sample results for both BNA and pesticide/PCB data insamples CAU97 and CAU98 due to the sample extraction holdingtime were exceeded for two days.
AR302519
Low level blank contaminations affected the reported resultsfor the following compounds in the samples indicated. Theywere all qualified "B".
Compound SamplesMethylene Chloride All samplesAcetone CAU97, CAU98Bis(2-Ethylhexyl)Phthalate All Samples
The following TICs were crossed off of the TIC forms : Unknownat retention time 4.81 and 22.83, Sulfur, Unknown Hydrocarbonat retention time 6.23, Hexane (DOT 8CI9CI), and 1,1,2-Trichloro-l,2,2-Trifluoroethane. The above mentioned TICs werealso detected in the associated blanks.
The TICs which were not blank contaminations were flagged "J"(estimated) to reflect the quantitative error inherent in theanalysis of compounds without corresponding calibrationstandards.
Notes
All other compounds with a HJ" qualifier were detected attrace levels.
All data was reviewed according to the National FunctionalGuildlines for evaluating Organic Analyses. The text of thisreport addresses only those problems affecting usability.
Attachments:
1. Glossary of data qualifier codes.2. Data Summary. This includes:
a) All positive results for the target analytes withqualifier codes, if applicable.b) All unusable detection limits (qualified NRM).
3. Appendix A - Results as reported by the laboratory for alltarget analytes (no corrections were made during datavalidation).
4. Appendix B - Results of all tentatively identified compounds(TIC) which have been corrected to exclude method artifactsand laboratory contaminants.
5. Appendix C - DPO report addresses laboratory compliance tothe statement of work.
6. Appendix D - Support Documentation includes details tosupport the statements in this report.
7. Appendix E - Telephone log.
AR3025
Attachment 1Data Qualifier Codes
SR302521
Glossary of Data Qualifier Codes (Organic)
Codes Relating to Identification(Confidence concerning presence or absence of compounds):
U = Not detected. The associated number indicatesapproximate sample concentrations necessary to bedetected.
(NO CODE) - Confirmed identification.
B — Not detected substantially above the level reported inlaboratory or field blanks.
R = Unreliable results. Analyte may or may not be presentin the sample. Supporting data necessary to confirmresults.
Codes Related to Ouantitation(can be used for both positive results and sample quantitationlimit):
J = Analyte Present. Reported value may not be accurate orprecise.
K = Analyte present. Reported value may be biased high.Actual value is expected to be lower.
L = Analyte present. Reported value may be biased low.Actual value is expected to be higher.
UJ = Not detected. Quantitation limit may be inaccurate orimprecise.
UL » Not detected. Quantitation limits is probably higher.
Other Codes
Q - No analytical result.
HR3G2522
Attachment 2Data Summary Forms
AR302523
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n
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at
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rt
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Appendix ALaboratory Results of all Target Analytes
A83G2536
1A EPA S A M P L E NOV O L A T I L E ORGANICS A N A L Y S I S DATA SHEET
I CAUS3Lab Name: NET C o n t r a c t : 63090031 I
Lab Code: NET Case No.: 15741 S A S N o . : S D G N o . : C A U 9 3
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) ML Lab F i l e ID: F3700
L e v e l : (low/med) LOW Date Received: 1/24/31
% Moisture: not dec. 100. Date A n a l y z e d : 1/29/91
Column: (pack/cap) CAP D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3-------Ch1orometbane ____74-83-9-------Bromomet hane______75-01-4-------Vinyl chloride____75-00-3-------Ch1oroe thane______75-03-2-------Methylene chloride,67 - 64 - 1 -- -- - --Acetone __________75-15-0-------Carbon d i s u l f i d e__75-35-4-------1 , l - D i c h 1 o r o e t h e n e _7 5 - 3 4 - 3 - - - - - - - 1 , 1 - D i c h l o r o e t h a n e
540-5'3-0-------l,2-Dich1oroethene (total) __S7-66-3-------Ch1orofor m__________________
107-06-2-------1 , 2 - D i c h l o r o e t h a n e__________78-93-3-------2-8u tan one_________________7 1 - 5 5 - l s - - - - - - - l , l , l - T r i c h l o r o e t h a n e _____56-23-5-------Carbon t e t r a c h l o r i de_______108-05-4-------Vinyl acetate _____________75-27-4-------8romodi chloromethane_______78-87-5-------l,2-Oichloropropane _______
10061-Ql-5-------ci s - 1 , 3 - D i c h l o r o p r o p e n e79-01 - 6-------Trichloroethene _______
124-48-1-------Oi bromochloromethane_79-00-5-------1,1,2-Tri c h l o r o e t h a n e71-43-2-------Benzene ____________
10061-02-6-------trans-l ,3-Di c h l o r o p r o p e n e -75-25 - 2 - - -----Bromoform
108-10-l-------4-Methyl-2-pen tan one_____531-78-6-------2-Hex an one_______________127-18-4-------Tetrachloroethene _______79-34-5-------1,1,2,2-Tetrachloroethane108-88-3-------To1uene _________________108-90-7-------Ch1orobenzene __________100-4l-4-------Etny1benzene_____________100-42-5-------Styrene
10. |U10. |U10. |U10. j U11 . I B10. | U5 . I U5. |U5. |U5. |U5. |U5. |U
10. | U5. |U5. |U10. |U5. |U5. |U5. |U1. | J5. |U5. |U5. |U5. '|U5. |U10. | U10. |U5. |U5. |U
5. |U5. |U* w w ^ w «•* ^ v r i w i c ^ v <-* * \ •*• |
1330-20-7-------Xy1ene (total)_____________| 5. |U | C J
1A EPA SAMPLE NO.V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ___________
II CAUS4
Lab Name: NET C o n t r a c t : 68090031 I
Lab Code: NET Case No.: 15741 3AS No.: SOG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) ML Lab F i l e ID: F3703
Level: (low/med) LOW Date Received: 1/24/91
% M o i s t u r e : not dec. 100. Date A n a l y z e d : 1/29/91
Column: (pack/cap) CAP D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---74-83-9---75-01-4---75-00-3----? er n Q •? »
67-64-1 ---75-15-0---75-35-4---75-34-3---
540-59-0---67-66-3---107-06-2---
71-55-6---56-23-5---108-05-4---75-27-4---/ O O / v
10061-01-5---79-01 -6---
124-48-1 ---79-00-5---71-43-2---
10061-02-6---75-25-2---
108-10-1 ---O 7 i / O O127-13-4---79-34-5---
108-88-3---108-90-7---100-41-4---100-42-5---
1330-20-7---
----Chl oromethane----Bromomethane- - - - V i n y l c h l o r i d e----Chl oroethane- - --Me t hy 1 ene c h l o r i d e----Acetone----Carbon d i s u l f i d e----1 , 1-Dichloroethene----1 , 1 - D i c h l o r o e t h a n e- --- 1 , 2 -Di c hi oroet hen e (total) __----Chl orofo rm----1 , 2 - O i c h l o r o e t h a n e----2-8utanone----1 , 1 , 1 - T r i c h l o r o e t h a n e----Carbon t e t r a c h 1 o r i de- - - - V i n y l acetate- -- -8 r omodi chl oromethane----1 , 2 - O i c h l o r o p r o p a n e- - - -c i s - 1 , 3 - Oi c h 1 o r op r open e ____----Trichloroethene----Di bromochl oromethane----1 , 1 ,2-Trichl oroethane----Benzene- - - - t r ans- 1 , 3 - Oi c h 1 o r op r opene __- -- -8 r omof o rm----4-Methyl -2-pentanone----2-Hexanone----Tetrachloroethene- - - - 1 , 1 , 2 , 2 -Te t r achl o r oet hane __----Toluene----Chl orobenzene----Ethyl benzene----Styrene----Xy 1 ene (total )
10.10.10.10.10.10.5 .5 .5 .5 .5 .5 .10.5 .5 .10.5 .5 .
. 5 .1 .5 .5 .5 .5 .5 .10.10.5 .
AB3C5 .5.5.5 .
1
I|U|U|U|UI B|U|U|U|U|U|U|U|U|U|U|U|U|U|U1 J|U|U[U|U|U|U|U|U
1 538|U|U|U|U1
37
1A EPA SAMPLE NO.V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET
I CAU95Lab Name: NET $ C o n t r a c t : 68090031 I___
Lab Code: NET Case No.: 15741 3AS No.: SDG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5.0 (g/mt.) ML Lab F i l e ID: F3704
Level: (low/med) LOW Date Re c e i v e d : 1/24/91
% M o i s t u r e : not dec. 100. Date Analyzed: 1/29/91
Column: (pack/cap) CAP D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3-------Chloromethane ____74-83-9-------Br omomethane______75-01-4-------Vinyl chloride____75-00-3-------Chloroe thane______75-03-2-------Methylene chloride,67-64-1-------Acetone __________75-15-0-------Carbon disulfide__75-35-4-------1,l-0ichloroethene_7 5 - 3 4 - 3 - - - - - - - 1 , 1 - O i c h l o r o e t h a n e
540-59-0-------1,2-Dichloroethene (total)__67-66-3-------Chlorof orm__________________
107-06-2-------1 ,2-Dichloroethan e_________78-33-3-------2-Butanone__________________71-55-6-------1 , 1 , 1 - T r i c h l o r o e t h a n e ______56-23-5-------Carbon t e t r a c h l o r i de_______108-05-4-------Vinyl acetate _____________75-27-4-------Bromodi chl orome thane________78-87-5-------l,2-Dichloropropane ________
10061 -01-5-------cis-1,3-Dichloropropene79-01 - 6-----~-Trichl oroethene _____
1 24-43-1-------Di bromochl oromethane_79-00-5-------1,1,2-Trichloroethane7 1-43-2-------Benzene ______ ___
10061-02-6-------trans-l ,3-Di chloropropene __75 - 25 - 2 --- - ---Bromoform _______________
108-10-1-------4-Methyl -2-pentan one_____59 1-73-&-------2-Hexanone______________127-13-4-------Tetrachloroethene _______79-34-5-------1 , 1,2,2-Tetrachloroethane
•To 1uene1 08-90-7-------Ch1orobenzene100-41-4-------Ethyl benzene__100-42-5-------Styrene ______
1330-20-7-------Xy1ene (total).
10. |U10. JU10. JU10. |U12. | B10. | U5. |U5. |U5. |U5. |U5. |U5. |U10. | U5. |U5 . | U10. |U5. |U5 . |U5. |U5. |U5. |U5. |U5. |U5. |U5 . U10. U10, U5. U5. U
5 . U5 . |U5. U
1A EPA SAMPLE NO.V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET
I ———;I CAU96 j
Lab Name: NET C o n t r a c t : 68030031 |__________ \\
Lab Code: NET Case No.: 15741 S A S N o . : S D G N o . : C A U 9 3
M a t r i x : ( s o i l / w a t e r ) WATER Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) ML Lab F i l e ID: F3705
L e v e l : (low/med) LOW Date Received: 1/24/91
% M o i s t u r e : not dec. 100. Date Analyzed: 1/29/91
Column: (pack/cap) CAP D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. • COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3----74-83-9----75-01-4----75-00-3----75-09-2----67-64- 1 - - - -75-15-0----75-35-4----75-34-3----
540-53-0----67-66-3----
107-06-2----78-93-3----71-55-6----56-23-5----
1 U O U 3 *+
75-27-4----78-37-5----
10061 -01 -5----79-01-6----
124-43-1----79-00-5----71-43-2----
10061-02-6----75-25-2----
108-10-1 ----C Q 1 7 Q _ C - _ _ -
127-18-4----79-34-5----
i U w w w O
I U o a U /100-41 -4----100-42-5----
1330-20-7----
- --Ch 1 oromethane---Bromomethane---Vinyl c h loride---Chloroethane---Methylene c h l o r i d e---Acetone---Carbon d i s u l f i d e---1 , 1 - D i c h l o r o e t h e n e---1 , 1 - O i c h l o r o e t h a n e- - - 1 , 2 -Di c hi o r oe t hen e (total) __---Chloroform---1 , 2 - D i c h l o r o e t h a n e---2-8utanone---1 , 1 , 1-Trichl oroethane---Carbon t e t rachl o r i de- - - V i n y l acetate- --Bromodi chl o r ome thane---1 , 2-Oichloropropane- - -e i s-1 ,3-Oi chl oropropene---Trichloroethene- - - Oi b r omoc hi o r ome thane---1 , 1 ,2-Trichl oroethane---Benzene- - - t r ans- 1 , 3 -Oi c hi o r op r op ene __- - - 8 r omof o rm---4-Methyl -2-oentanone---2-Hexanone---Tetrachloroethene---!-, 1,2,2- Tetrachloroethane __---Toluene---Chlorobenzene---Ethylbenzene---Styrene---Xy 1 ene (tota 1 )
110. U10. U10. U10. U14. B10. U5. U5. |U5 . U5. U5 . U5. U
10. U5 . U5. JU10. |U5. U5 . U5. U5. U5 . U5 . U5. U5 . U5 . U
10. U10. U5. |U
A5R3Cl|5l4i5'. |u5. |U5 . U
1A EPA SAMPLE NO,VOLATILE ORGANICS A N A L Y S I S DATA SHEET
| CAU97Lab Name: NET C o n t r a c t : 68D90031 I
Lab Code: NET Case No.: 15741 SAS No.: SOG No.: CAU33
M a t r i x : (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 5.1 (g/mL) G Lab F i l e ID: F3724
Level: (low/med) LOW Date Received: 1/24/91
% Moisture: not dec. 37. Date A n a l y z e d : 1/31/91
Column: (pack/cap) CAP D i l u t i o n Factor? 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3----7 A O "* Q
75-01-4----75-00-3----75-03-2----67-64- i - - - -75-15-0----75-35-4----75-34-3----
540-53-0----67-66-3----
107-06-2----/ O J O J71 C C C.
56-23-5----108-05-4----75-27-4----78-87-5----
10061-01-5----73-01-6----
124-48-1----79-00-5----71-43-2---
10061-02-6----75-25-2----108-10-1---591-78-6---127-18-4---79-34-5---
108-90-7---100-41-4---100-42-5---
1330-20-7---1
---Chl oromethane• - - - 8 r omome thane• - - - V i n y l c h l o r i d e•---Chl oroethane- - - -Me t hy 1 ene c h l o r i d e•---Acetone•---Carbon d i s u l f i d e•---1 , 1 - D i c h l o r o e t h e n e•---1 , 1 - D i c h l o r o e t h a n e•---1 , 2-Di chl oroethene (total) __•---Chl orofo rm•---1 , 2-Di chl oroethane•---2-Butanone----1 , 1 , 1-Trichl oroethane•---Carbon te t rachl o r i de•---Vinyl acetate
•---1 , 2-Oichloropropane•---ci s-1.3-Dichloropropene•---Tri chl oroethene•---Di br omoc hi oromethane•---1 , 1 ,2-Trichl oroethane----Benzene• --- t r an s- 1 , 3 -Di c hi o r op r opene __- - -- B r omof o rm----4-Methyl -2-pentanone----2-Hexanone----Tetrachl oroethene- --- 1 , 1 , 2 , 2 -Te t r ac h 1 o roe t hane __----To! uene----Chl orobenzene----Ethyl benzene----Styrene- - - - X y l e n e (total)
15. U15. U15. U15. U9. B18. B8. U8. U8. U8. U3. U8. U
15 . U8. U8. U
15. U3. U8. U8. U8. U8. U8. U8. U8. |U3. |U
15 . |U15. |U8. |U8. |U
A|;30|?5l»l8. (U8. | U
1 8. |U1
95
1A EPA S A M P L E NOV O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ____________
\ CAU38Lab Name: NET C o n t r a c t : 68090031 I
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 5.3 (g/mL) G Lab F i l e ID: F3725
L e v e l : (low/med) LOW Date Received: 1/24/91
% Moisture: not dec. 22. Date A n a l y z e d : 1/31/91
Column: (pack/cap) CAP D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3----74-83-9----75-01 -4----75-00-3----75-03-2----67-64-1----75-15-0----75-35-4----7 c _ - 3 4 _ 3 - _ _ .' J V ** J
540-59-0----67-66-3----
107-06-2----/ O J J J
71-55-6----5f 1 *^ C6-23-5----108-05-4----75-27-4----/ o O / 3
10061-01-5----73-01-6----
124-43-1----79-00-5----71-43-2----
10061 -02-6----T C * ff *575-25-2----
108-10-1----b3l~/o"b"*""127-13-4----7<9_-54_c.__.1 J sP ** -J
iuo o o J1 U O J U /
100-41-4----100-42-5----
1330-20-7----
----Chl oromethane----Bromomethane- - - - V i n y l c h l o r i d e----Chloroethane- -- -Me t hy 1 ene c h l o r i d e----Acetone•---Carbon d i s u l f i d e----1 , 1 - D i c h l o r o e t h e n e•---1 , 1-Dichloroethane- - -- 1 , 2 -Oi c hi or o e t hen e (total) __- - - - C h l o r o f o r m•---1 , 2 - D i c h l o r o e t h a n e• ---2-Butanone•---1 , 1 , 1 - T r i c h l oroethane----Carbon t e t r achl o r i de•---Vinyl acetate•---Bromodi chl oromethane----1 , 2 - D i c h l o r o p r o p a n e• - - -c i s - 1 , 3 - Di c h 1 o r op r open e ____•---Tri chl oroethene•---Di bromochl oromethane----1 , 1 ,2-Trichl oroethane•---Benzene• -- - t r an s - 1 , 3 - Di c h 1 o r op r op en e __• -- - 8 r omof o rm----4-Methyl -2-pentanone•---2-Hexanone•---Tetrachl oroethene• - -- 1 , 1 , 2 , 2 -Te t r ac hi o r oe t hane __• - - -To 1 uene•---Chlorobenzene•---Ethylbenzene- - - - S t y r e n e•---Xy 1 ene (total )
12.12 .12.12 .7.
1 1 .6.6 •6.6.6.6.
12.6.6.
12.6.6.6.6.6.6.6.6.6.
12.12.6.
6.6.6.3.
UUUUBBJUUUUUUUUUUUUUUUUUuuuuu
*5«,2UuJ
Ul
IA EPA S A M P L E NO.VOLATILE ORGANICS A N A L Y S I S DATA SHEET _____________^
II CAU99
Lab Name: NET Contract: 68090031 I
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) WATER Lao Sample ID:
Sample wt/vol: 5.0 (g/mL) ML Lab F i l e 10: F3706
L e v e l : (low/med) LOW Date Received: 1/24/91
% M o i s t u r e : not dec. 100. Date A n a l y z e d : 1/23/31
Column: (pack/cap) CAP D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-37-3----/*»"*O.53
75-01-4----75-00-3----75-09-2----67-64-1----75-15-0----75-35-4----75-34-3----
540-53-0----67-66-3----
107-06-2----73-93-3----71-55-6----5C. - -" -5 -. C _ _ _ .
108-05-4----75-27-4----/ o - o / — 0
10061-01-5----73-01-6---
1 24-43-1----79-00-5----71 _ 4 - 5 _ - > _ - _/I *+ '^ la,
i U U O l U l . O
75-25-2---108-10-1---531-73-6---127-13-4---73-34-5---
i U O s ? t 3 j108-30-7---100-41-4---100-42-5---
1330-20-7---
• ---Ch 1 oromethane•---Bromomethane• - - - V i n y l c h l o r i d e•---Chl oroethane• ---Me t hy 1 ene c h l o r i d e•---Acetone•---Carbon d i s u l f i d e•---1 , 1 - O i c h l o r o e t h e n e•---1 , 1 - D i c h l o r o e t h a n s•---1 , 2-Di c h l o r o e t h e n e (total ) __•---Chl oroform•---1 , 2 - D i c h l o r o e t h a n e•---2-Sutanone•---1 , 1 , 1 - T r i c h l oroethane•---Carbon t et r achl o r i de- - - - V i n y l acetate- - --B r omodi chl oromethane----1 , 2-Oichloropropane- -- -c i s - 1 1 3 -Oi c h I o r op r open e ____----Tri chl oroethene----Oi br omoch lor orne thane----1 . 1 ,2-Trichl oroethane•---Benzene- - -- t r ans- 1 , 3 -Di c h 1 o r op r op ene __- - - - 8 r omof o rm----4-Methyl -2-pentanone----2-Hexanone----Tetrachloroethene- --- 1 , 1 , 2 , 2 -Te t r ac hi o r oe t hane __- -- -To 1 uen e----Chl orobenzene----Ethylbenzene----Styrene- - - - X y l e n e (total)
10.10.10.10.14.12 .5 .5 .5 .5 .5.5 .10.5 .5.10.5 .5 .5 .5 .5 .5 .5.5.5 .10.10.5 .
^R3<5 .5.5.5 .
UUUuB
UUUUuUuuuu|Uuu|U|U|U|U|U|Uu|U
ii-si^|U|U|U|U1
1A EPA SAMPLE NO.VOLATILE ORGANICS ANA L Y S I S DATA SHEET
I 1I CC612 |
Lab Name: NET ' C o n t r a c t : S8DS0031 I___ i
Lab Cod*: NET Case No.: 15741 SAS No.: SDG No.: CAU33
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) ML Lab F i l e ID: F3637
L e v e l : (low/med) LOW Date Received: 1/24/31
% M o i s t u r e : not dec. 100. Date A n a l y z e d : 1/23/31
Column: (pack/cap) CAP D i l u t i o n F a c t o r : 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
I74-87-3-------Chloromethane74-83-3-------Br omome thane75-01-4-------Vinyl chloride____75-00-3-------Chloroethane______75-09-2-------Methylene chloride,67-64-1-------Acetone ___________75-15-0-------Carbon disulfide__7 5 - 3 5 - 4 - - - - - - - 1 , 1 - D i c h l o r o e t h e n e
10. |U10. |U10. JU10. | U10. | B10. | U5. JU5. |U
75-34-3-------1 , 1-Di chl oroethane__________| 5. |U540-53-0-------1 ,2-Dichloroethene (total)__| 5. |U67-66-3-------Ch 1 oroform_________________| 5- I U
107-06-2-------1 , 2-Di chl oroethane_________| 5. |U10. | U5 . |U5. |U10. |U5. |U5 . | U5. |U5. |U5. |U5. |U5. |U5. |U .5. |U10. |U4. | J5. |U5. |U
73-93-3-------2-Bu tanone___________7 1 - 5 5 - 6 - - - - - - - l , l , l - T r i c h l o r o e t h a n e56-23-5-------Carbon tetrachlori de_
103-05-4-------Vinyl acetate _______75-27-4-------8r omodi chloromet hane_78-87-5-------1,2-Dichloropropane _
10061-01-5-------ci s-1,3-Oichloropropene79-01 -6-------Triohloroethene _______
124-48-l-------Dib romochlo r omet hane_79-00-5-------1,1,2-Trichloroethane7 1-43-2 -------Benzene __________________
10061-02-6-------trans-l ,3-Di chloropropene __75 - 25 - 2 -------8romoform _________________108-10-l-------4-Methyl-2-pentanone_______591-78-6-------2-Hexanone_________________127-18-4-------Tetrachloroethene _________79-34-5-------1,1,2,2-Tetrachloroethane __108-33-3 -------To 1uene ___________________108-90-7-------Ch1orobenzene _____________100-41-4-------Ethyl benzene_______________100-42-5-------Styrene ___________________
1330-20-7-------Xylene (total)_____________
5. |U5. |U5. IU
144
IA EPA S A M P L E NO.V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET
| CCB13Lab Name: NET C o n t r a c t : 68D30031 I
Lab Code: NET Case No.: 15741 SAS No.: SOG No.: CAU33
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) ML Lab F i l e ID: F3638
Lev e l : (low/med) LOW Date Received: 1/24/31
% Moisture: not dec. 100. Date Analyzed: 1/23/31
Column: (pack/cap) CAP D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3----74-33-3----75-01-4----7 5 - UU - J - - -75-09-2----67-64-1----75-15-0----75-35-4----75-34-3----
540-53-0----67-66-3----
107-06-2----78-93-3----71 -55-6----56-23-5----108-05-4----75-27-4----
10061-01-5----73-01-6----
124-48-1----73-00-5----71-43-2----
10061-02-6---75-25-2----
108-10-1---531-78-6---127-18-4---73-34-5---l u o o o oI U <3 j \J f100-41-4---
| 100-42-5---| 1330-20-7---1
•---Chloromethane• - - - B r omome thane•---Vinyl c h l o r i d e•---Chl oroethane• -- -Me t hy 1 ene c h l o r i d e•---Acetone----Carbon d i s u l f i d e•---1 , 1 - D i c h l o r o e t h e n e•---1 , 1 - D i c h l o r o e t h a n e•--- 1 , 2-Di c hi or oethene (total) __•---Chloroform•---1 ,2-Dichloroethane•---2-Butanone•---1 , 1 , 1-Trichl oroethane•---Carbon te t r a chl o r i de- - - - V i n y l acetate- - - - B r omodi chl oromethane----1 , 2-Di chl oropropane•- --c i s- 1 , 3 -Di ch 1 orop r open e ____----Tri chl oroethene•---Di bromochl oromethane•---1 , 1 ,2-Trichl oroethane----Benzene-- -- t r ans - 1 , 3-Oi c hi o ropr opene __- ---B r omof o rm----4-Methyl -2-pentanone----2-Hexanone----Tetrachl oroethene- - -- 1 , 1 , 2 , 2 -Te t r achl o r oe t hane __-- --To 1 uene----Chl orobenzene----Ethyl benzene----Styrene----Xy 1 ene ( tota 1 )
101010101210555555
10551055555555510to55
si555
1. |U. |U. |U. |U• 18• |U
|U. |U• |U. |U. |U. |U. |U. |U. |U. |U. |U. |U. |U. |U. |U- |U. |U. !U. |U. |U• |U. |U. |U
30$5 if 5. |U• |U. |U
1
1A ERA S A M P L E NO.V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET _____________
II CC814
Lab Name: NET C o n t r a c t : 68090031 |_____________
L a b C o a e : N E T Case No.: 15741 SAS No.: S D G N o . : C A U 3 3
M a t r i x : (soil/water) WATER Lab S a m p l e ID:
Sample wt/vol: 5.0 (g/mL) ML Lab F i l e ID: F3699
L e v e l : (low/med) LOW Date R e c e i v e d : 1/24/91
% M o i s t u r e : not dec. 100. Date A n a l y z e d : 1/23/31
Column: (pack/cap) CAP D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3----74-83-9----75-01-4---75-00-3----75-03-2----67-64-1 ---75-15-0----75-35-4---75-34-3----
540-59-0----67-66-3----
107-06-2----' O ™" J sj J
71 C C r"1-55-6----56-23-5----108-05-4----75-27-4----o o / D
10061-01-5----73-01 -6----
124-43-1----79-00-5----71 -43-2----
10061-02-6----75-25-2----108-10- 1 - - - -
127-13-4----73-34-5----
I U 8 3 U /100-41 -4----100-42-5----
1330-20-7----1
- - - - C h l oromethane- -- - 8 r omome thane- - - - V i n y l c h l o r i d e- - - - C h l oroethane• - - -Me t hy 1 ene c h l o r i d e----Acetone----Carbon d i s u l f i d e•---1 , 1 - D i c h l o r o e t h e n e•---1 , 1 - D i c h l o r o e t h a n e• - - - 1 , 2 - D i c h l o r o e t h e n e (total) __•---Chlorofo rm----1 , 2 - D i c h l o r o e t h a n e•---2-Butanone•---1 , 1 , 1 - T r i c h l oroethane•---Carbon t e t r a c h l o r i d e•---Vinyl acetate
•---1 , 2-Di chl oropropane• - - -c i s - 1 , 3 -Oi c h 1 o r op ropen e ___•---Trichloroethene•---Oi bromochl oromethane•---1 , 1 ,2-Trichl oroethane•---Benzene• - - - t r an s- 1 , 3 -Di ch 1 o r op r op ene __• -- -B r omof o rm•---4-Methyl -2-pentanone•---2-Hexanone•---Tetrachl oroethene• -- - 1 , 1 , 2 , 2 -Te t r ac h 1 o r oe t hane __•---Toluene•---Chl orobenzene•---Ethylbenzene•---Styrene•---Xy 1 ene (tota 1 )
10.10.10.10.12.10.5 .5 .5 .5 .5.5 .
10.5,5 .10.5 .5.5.5.5 .5.5 .5.5 .10.10.5.
ftilSG5.5.5.5.
11
u lu tu l8 Iu l
U |u lu 1u lu iu lu lu iu 1u iu iu lu iu lu lu lu 1^en*^djDHOju !u Iu lu li
179
18 EPA SAMPLE NOS E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET
I CAU93Lab Name: NET C o n t r a c t : 68090031 I
Lab Code: NET Case No.: 15741 SAS No.: SOG No.: CAU93
M a t r i v : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000.0 (g/mL) ML Lab F i l e ID: D8561
L e v e l : (low/med) LOW Date Received: 1/24/91
% Moisture: not dec. 100. dec. 0. Date Extracted: 1/28/31
E x t r a c t i o n : (SepF/Cont/Sone) CONT Date A n a l y z e d : 2/ 7/91
GPC C l e a n u p : (Y/N) N PH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
1 1 i-44-4----9C C "7 O
541 -73-1----106-46-7----100-51-6----35-50-1 ----95-48-7----103-60-1 ----106-44-5----621 -64-7----
/ - / _ ~ i - - - -
O J O O
O O '3 J
105-67-9----65-35-0----
1 1 1 - 31-1----
120-32- 1 ----31-20-3----106-47-8----37-63-3----53-50-7----31-57-6----77-47-4----83-06-2----35-35-4---31-58-7----38-74-4---
131-1 1 - 3 - - - -203-36-8---S06-20-2---
1---Phenol•---bi s(2-Chl oroethyl )ether ____---2-Chl orophenol
• - - - 1 ,3-Dichlorobenzene---1 , 4-Di chl orobenzene•---Benzyl a l c o h o l---1 , 2-Di chl orobensene---2-Methyl phenol---bi s(2-chloroi sopropyl )ether._,_4_Ma,thyl phenol- - -N -N i troso-di - n - p r o p y l ami n e __•---Hexachl oroethane- - -N i trobenzene•---Isophorone---2-Ni trophenol•---2, 4-Dimethyl phenol•---Benzoic acid•---bi s ( 2-Chloroethoxy)met hane __•---2 , 4-Oi chl orophenol•---1,2,4-Trichlorobenzene•---Naphtha! ene----4-Chl oroani 1 i ne•---Hexachl orobutadi ene- - - -4- Chl or o-3 -me t hy 1 pheno 1 ____- - - - 2 - M e t h y l n a p h t h a l e n e- - --He xachl o r ocy c 1 open t adi ene __- - - - 2 , 4 , 6 - T r i c h l o r o p h e n o l----2.4,5-Trichl orophenol- - - - 2 - C h 1 o r o n a D h t h a 1 e n e- - - - 2 - N i troani 1 i ne- - - - D i m e t h y l p h t h a l a t e- - - - A c e n a p h t h y l ene- - - - 2 . 6 - D i n i t r o t o l u e n e
10.10.10.10.10.10.10 .'10.10.10 .10 .10.10 .10.10.10.50.10.10.10.10.10.10 .10.10.10.10.50.
10.10.10.
1|U|U|U|U|U|U|U|U|UI1-1|U|U|U|U|U|U|U|U|U|U|U|U
|U|U|U|U|U
fl25^^|U|U|U1
286
1C EPA SAMPLE NOS E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ____________
I I| CAU93 |
Lab Name: NET C o n t r a c t : S8D90031 | ______________ i
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000.0 (g/mL) ML Lab F i l e ID: D8561
L e v e l : (low/med) LOW Date Received: 1/24/91
% M o i s t u r e : not dec. 100. dec. 0. Date E x t r a c t e d : 1/28/91
E x t r a c t i o n : (SepF/Cont/Sone) CONT Date A n a l y z e d : 2/ 7/91
GPC C l e a n u p : (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND Og/L or ug/Kg) UG/L Q
99-09-2---->J 3 £ J
51 -28-5----100-02-7----132-64-3----1 2 1 - 1 4 - 2 - - - -
7005-72-3----36-73-7----
100-01-6----534-52-1----86-30-6----
101 -55-3----
37-36-5----85-01-8----
120-12-7----84-74-2----
206-44-0----129-00-0----35-63-7----31 -34- 1 ----56-55-3----
218-01-3----1 17-81-7----1 1 7-fid-fi----
207-08-9---50-32-8----
193-39-5---53-70-3----
191-24-2----
- - - 3 - N i t r o a n i l i n e•---Acenaohthene---2 , 4-Oi ni trophenol
• ---4-Ni trophenol- - -Di benz of u r an- - - 2 , 4 - D i n i t r o t o l u e n e---Di e t h y l p h t h a l ate---4-Chl orophenyl - p h e n y l erthe r __- - - F l uorene---4-Ni troani 1 i ne---4, 6-Di ni t r o - 2 - m e t h y l p h e n o l __
• - - -N -N i t r o sodi p hen y 1 ami ne (1) __
•---Hexachl orobenzene---Pentachl orophenol•---Phenanthrene•---Anthracene•---Di - n - b u t y l p h t h a l a t e•---Fl uoranthene•---Pyrene•---Butyl benzy! ph t h a l ate----3,3'-Dichlorobenzidine•---Benzo(a')anthracene----Chrysene•---bi s(2-Ethylhexyl ) p h t h a 1 a t e __----Oi -n-octyl p h t h a l ate•---Benzo(b)fluoranthene•---Benzo(k)fluoranthene•---Benzo(a)oyrene- - - - I n d e n o f l ,2.3-cd)pyrene----Dibenzfa.h)anthracene- ---Benzo (g . h . i ) per y 1 ene
50.10.50.50.10.10.10.10.10.50.50.10.10.10.50.10.10.10.10.10 .10.20.10.10.4.10.10.10.10a rlO*?*10.10.
1 1|U 1
|U ||U !|U |
|U i|U i
|U I|U i
iu' i|U 1|U ||U ||U |
|U ||U I|U 1IM 1|U ||U i1 BJ ||U 1|U 1|U
|U1 1____ 237(1) - Cannot be separated from d i p h e n y 1 amine
FORM I SV-2 1/37 Rev.
IB EPA SAMPLE NOSEMIVOLATILE ORGANICS A N A L Y S I S DATA SHEET ______________
I| CAU94
Lab Name: NET C o n t r a c t : 68D30031 I
Lab Code: NET Case No.: 15741 • SAS No.: SOG No.: CAUS3
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample w t / v o l : 1000.0 (g/rnL) ML Lab F i l e ID: 08564
L e v e l : (low/med) LOW Date Received: 1/24/91
% M o i s t u r e : not dec. 100. dec. 0. Date E x t r a c t e d : 1/28/91
E x t r a c t i o n : (SepF/Cont/Sonc ) CONT Date A n a l y z e d : 2/ 7/91
GPC C l e a n u p : (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-95-2----1 l l -44-4----
541 -73-1----106-46-7----100-51-6----35-50- 1 ----95-43-7----
108-60- 1 ----106-44-5----621 -64-7----67-72-1----93-95-3----/ O J J 1
08" /3-D----105-67-3----65-85-0----
1 1 1 - 3 1 - 1 - - - -120-S3-2----120-32- 1----91 -20-3----106-47-8----
53-50-7----31 -57-6----77-47-4----
35-35-4----31-53-7----88-74-4----
131-1 1-3----203-36-8----606-20-2----
i---Phenol i- --bi s ( 2 -Chl oroet hy 1 ) e the r _____---2-Chl orophenol---1 , 3-Oi chl orobenzene---1 ,4-Oichlorobenzene---Benzyl alcohol- - - 1 , 2 - D i c h l o r o b e n z e n e- - - 2 - M e t h y l phenol- - - b i s(2-chl oroi s o p r o p y l )ether---4-Methyl phenol
---Hexachl oroethane---Ni trobenzene---Isophorone---2-Ni trophenol•---2.4-Oimethyl phenol•---Benzoic a c i d•---bi s(2-Chloroethoxy)met hane __•---2,4-Oichlorophenol•---1 . 2.4-Tri chl orobenzene•---Naphthalene•---4-Chloroani 1 ine•---Hexachl o r o b u t a d i ene• - - - 4 - Ch 1 o r o - 3 -me t hy 1 pheno 1 _____•--- 2 - M e t h y l n a p h t h a l ene•---He'xachl orocycl opentadi ene _•---2.4,6-Trichlorophenol•---2 , 4.5-Tri chl orophenol•---2-Chl oronaphthal ene•---2-Ni troani 1 i ne•---Dimethylphthal ate•---Acenaohthyl ene•---2, 6-Di ni trotol uene
10.10 .10.10.10.10 .10 .10.10.10.10.10 .10.10.10.10.50.10.10 .10.10.10.10.10.10.10.10.50.
$8310.10.10.
1'-' 1
'u |
u |
|U1FORM I SV- 1 1 /S7
1C EPA SAMPLE NO.S E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ___________
I| CAU94
Lab Name: NET C o n t r a c t : 68D30031
Lab Cod*: NET Case No.: 15741 SAS No.: SDG No.: CAU33«
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample w t / v o l : 1000.0 (g/mL) ML Lab F i l e 10: OS564
L e v e l : (low/med) LOW Date R e c e i v e d : 1/24/31
% M o i s t u r e : not dec. 100. dec. 0. Date E x t r a c t e d : 1/28/91
E x t r a c t i o n : ( S e p F/C o n t /S on c ) CONT Date A n a l y z e d : Z/ 7/91
GPC C l e a n u p : (Y/N) N pH: .0 D i l u t i o n F a c t o r ; 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L 0
39-09-2----o ~> -j c j5 1-28-5----100-02-7----132-64-9----1 2 1 - 1 4 - 2 - - - -84-66-2----
7005-72-3----86-73-7----
100-01-6----5 3 4 - 5 2 - 1 - - - -3f "j f*\ C6-JO-6----101 -55-3----i t o / ** I
/ O O J
3 - l J l O120-12-7----34-74-2----
206-44-0----129-00-0----35-63-7----91-94-1----56-55-3----
218-01 -9----117-81-7----1 17-84-0----205-99-2----C U / U O J50-32-8----
193-39-5----53-70-3----
191 -24-2----
- - - 3 - N i t r o a n i 1 i ne•---Acenaphthene---2 , 4-Di ni trophenol•---4-Ni trophenol---Di benzofuran---2 , 4-Di ni t r o t o l uene---Di e t h y l p h t h a l a t e---4-Chlorophenyl -phenyl ether---Fl uorene---4-Ni t r o a n i 1 i ne---4 , 6-Di ni t r o - 2 - m e t h y l phenol __- - -N -N i t r o sod i p hen y 1 ami ne (1) __- - - 4- B r omophen y 1 - p hen y 1 e t he r __---Hexachl orobenzene---Pentachl orophenol---Phenanthrene---Anthracene•---Di -n-butyl phthal ate---Fl uoranthene•---Pyrene---Butyl benzyl p h t h a l ate•---3,3'-Dichlorobenzidine---Benzo(a)anthracene
• - - -Ch r y sen e- - - b i s ( 2 - E t h y l h e x y l ) p h t h a l a t e __•---Di - n - o c t y l p h t h a l ate---Benzo(b)fl uoranthene•---Benzo(k)fluoranthene•---Benzo(a)pyrene•---Indenofl.2.3-cd')pyrene•---Oibenz(ath")anthracene•---8enzo(q.h.i "Jperylene
50 .10 .50.50.10.10.10 .10 .10 .50.50.10.10.10.50.10.10.10.10.10.10.20.10 .10.8.10.10.10.10.
10.
1I'J|U|U|U|U|U|UIUm|U|UI'J|U|U|UI'J|U|UI'J|UI'JI'J|U|U| BJI'J|U|U|U
q§25^|U1
(1) - Cannot be separated from d i p h e n y 1 amine
FORM I SV-2 1/37 Rev
18 EPA S A M P L E NOS E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ______________'
II C A U 9 S
Lab Name: NET C o n t r a c t : 68090031 |_________
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) WATER Lao Sample ID:
Sample wt/vol: 1000.0 (g/mL) ML Lab F i l e ID: 08565
L e v e l : (low/med) LOW Date Received: 1/24/31
% M o i s t u r e : not dec. 100. dec. 0. Date E x t r a c t e d : 1/28/31
E x t r a c t i o n : (SepF/Cont/Sonc) CONT Date A n a l y z e d : 2/ 7/91
GPC C l e a n u p : (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
11 1-44-4----j O O / O
541-73-1 ----106-46-7----100-51 -6----95-50- 1 ----35-48-7----103-60-1 ----106-44-5----621-64-7----67-72-1 ----90 o c ^
38-75-5----105-67-3----o D o O U
1 1 1 - 9 1 - 1 - - - •120-33-2----120-82-1----31-20-3----106-47-8---87-63-3----59-50-7---31 -57-6----77-47-4----33-06-2----35-35-4---91-58-7----33-74-4---
131-1 1 - 3 - - - -
606-20-2----
• ---Phenol |•---bis(2-Chloroethyl.) ether ___•---2-Chl orophenol•---1 ,3-Dichlorobenzene---1 , 4-Di chl orobenzene•---Benzyl alcohol•---1 , 2 - D i o h l o r o b enzene• - - - 2 - M e t h y l phenol---bi s(2-chl oroi sopropyl )ether
- - - -4-Me t hy 1 phenol- - - N - N i troso-di - n - p r o p y l a m i ne _•---Hexachl oroethane•---Ni trobenzene• -- - I sophor one•---2-Ni trophenol•---2,4-Oi met hy 1 phenol•---Benzoic acid•---bi s(2-Chloroethoxy)rnet hane __•---2,4-Dichlorophenol•---1 , 2,4-Tri chl orobenzene----Naphtha! ene•---4-Ch!oroanil ine•---Hexachl orobutadi ene----4- Chl or o-3 -methyl phenol• - - - 2 - M e t h y l n a p h t h a l ene--- -Hexachl o rocyc 1 open tadi ene __----2, 4,6-Tri chl orophenol----2.4,5-Trichlorophenol• - - - 2 - C h l o r o n a p h t h a l e n e•---2-Ni troani 1 i ne• - - - D i m e t h y l p h t h a l ate- - - - A c e n a p h t h y l ene----2 . 6-Di ni trotol uene
10.10.10.10.10 .10.10.10 .10.10.10.10.10.10.10.10.50.10.10.10.10.10.10.10.10.10.10.
50.10.10.10.
1|U|U|U|U|UItJ|U|UI'J|U|U|U|U|U|UI'J|U|U 1|U 1|UI'J 1I'J|U 1I'J|U ||U|U3^25^
I
|U|U|U|U1
IC EPA S A M P L E NOS E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET _______________'
I_ | CAU96Lab Name: NET C o n t r a c t : 63090031 I
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU33
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol : 1000.0 (g/mL) ML Lab F i l e ID: D8565
L e v e l : (low/med) LOW ' Date Received:. 1/24/91
% M o i s t u r e : not dec. 100. dec. 0. Date Extracted: 1/23/31
E x t r a c t i o n : (SepF/Cont/Sonc) CONT Date A n a l y z e d : 2/ 7/31
GPC C l e a n u p : (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
93-09-2-------3-N1 t r o a n i 1 i ne____83-32-9-------Acenapht hene______51-28-5-------2,4-Dinitrophenol
1 00-02-7-------4-Nitropheno1 ____132-64-9-------Di benzofu ran______1 2 1 - 1 4 - 2 - - - - - - - 2 , 4 - O i n i t r o t o l u e n e _84-66-2-------Di et h y l p h t h a l a t e__
7005-72-3-------4-Chlorophenyl-phenylethe r__86-73-7-------F1uoren e___________________
100-01-6-------4-Ni t r o a n i 1 i n e_____________534-52-l-------4,6-Dinitro-2-methylphenol__36-30-6-------N-Nitrosodipheny1amine (1)__
101-5 5 - 3 - - - - - - - 4 - B r o m o p h e n y l - p h e n y l e t h e r __113-74-l-------Hexachlorobenzene _________87-36-5-------Pentachlorophenol _________85-01-8-------Phenant hrene_______________120-12-7-------Anthracene_________________84-74-2-------Di-n-butylphthalate _______
206-44-0-------Fluoran thene_______________1 29-00-0-------Pyrene_____________________35-68-7-------Butylbenzylphthala te_______91-34-l-------3,3'-Oichlorobenzidi ne______56-55-3-------6enzo(a)anthracen e_________213-01-3-------Chrysene___________________M7-81-7-------bis(2-Ethylhexyl)phthalat e__117-84-0-------Di-n-octylphthalate _______205-99-2-------Benzo(b)fluoranthen e_______207-08-3-------Benzo(k)fluoranthen e_______50-32-8-------Benzo(a)py rene_____________193-39-5-------Indeno(1,2,3-cd)pyrene_____53-70-3-------Dibenz(a,h)anthracene ______131-24-2-------Benzo(g,h,i)perylene_______
50. |U10. |U50. |U50. |U10. |U10. |U10. |U10. |U10. |U50. |U50. |U10. |U10. |U10. |U50. |U10. ID10. |U10. I U10. |U10. |U10. |U20. |U10. |U10. |U3 . I BJ10. |U10. |U10. IU
10. |U10. |U
o «j(1) - Cannot be separated from d i p h e n y l a m i n e
FORM I SV-2 1/87 Rev
IB EPA S A M P L E NOS E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ____________
I| CAU97
Lab Name: NET Contract: 63D90031 I
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU33
M a t r i x : (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 30.1 (g/mL) G Lab F i l e ID: D8574
L e v e l : (low/med) LOW Date Received: 1/24/91
% M o i s t u r e : not dec. ,34. dec. 0. Date Extracted: 2/ 1/91
E x t r a c t i o n : (SepF/Cont/Sonc) SONC Date A n a l y z e d : 2/ 8/91
GPC Cleanup: (Y/N) Y pH: 6.7 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
i U O j 3 L1 l 1-44-4-9C —— C 7 a. O ——D-D / - o -
541 -73-1-106-46-7-100-51 -6-35-50-1-95-43-7-103-60- 1 -106-44-5-621 -64-7-67-72-1-O - IT O ~ -> ~
/ O 3 5 I
'jo / J -3
105-67-3-/- c o c _ n _b D o O u
1 1 1 - 9 1 - 1 -1 *> t"l —— Q "5 a. *> ——1 * _ U O - » - .
120-32-1-91-20-3-106-47-8-37-63-3-59-50-7-31-57-6-77-47-4-a Q - n c - '-s o - u b iSe Q C A
91 C O - "7 —l o o /38-74-4-
1 3 1 - 1 1-3-i U o j O o
606-20-2-
1------Phenol |------bi s(2-Chloroethyl )ether------2-Chl orophenol------1 ,3-Dichlorobenzene------ 1 , 4-Di chl orobenzene- - - - - - B e n z y l a l c o h o l_ _ _ _ _ _ 1 , 2-Dichlorobenzene- - - - - - 2 - M e t h y l p h e n o l- - - - - _ t ) i 3 ( 2 - c h l o r o i s o p r o p y l ) e t h e r_ _ - - - _ 4 _ M f t t | n y l phenol------N-Ni troso-di - n - p r o p y l a m i ne __------Hexachl oroethane------Ni trobenzene------Isophorone------2-Ni trophenol------2, 4-Dimethyl phenol------ Benz o i c a c i d------bi s(2-Chloroethoxy)met hane __------ 2 , 4-Di chl orophenol------ 1 , 2,4-Tri chl orobenzene_ _ . _ _ _ N a p h t h a l ene- - - - - - 4 - C h l o r o a n i l ine------Hexachl o r o b u t a d i ene_---__4_Ch'Ioro_3-me(:hyTpheno-|------2-Methyl naphtha! ene------Hexachl orocycl opentadi ene _------2. 4. 6-Trich! orophenol------2, 4, 5-Trichl orophenol------2-Chl oronaphthal ene------2-Ni troani 1 i ne- - - - - - O i m e t h y l p h t h a l ate------Acenaphthy! ene_ _ - . _ - 2 , 6 - O i n i t r o t o l u e n e
1000.1000.1000.1000.1000.1000.1000 .1000.1000.1000 .1000.1000.1000.1000.1000.1000.4900 .1000.1000.1000.1000.1000.1000.1000.1000.1000.1000.
i!ol33o4900.1000.1000.1000.
uuuuuuuuuuuuuuuuuu'JI'Juu|UI UI'Juu
$553uuuu
o D o
1C EPA SAMPLE NOSEMIVOLATILE ORGANICS A N A L Y S I S DATA SHEET ___________
I ~I CAU97
Lao Name: NET C o n t r a c t : 6 8 D 9 0 0 3 1 | ______
Lab C o d e : N £ T Case No.: 15741 SAS No.: S D G N o . : C A U 9 3
M a t r i x : (soil/water) SOIL Lab S a m p l e ID:
Sample wt/vol: 30.1 (g/mL) G Lab F i l e ID: 08574
Level : (low/med) LOW Date Received: 1/24/91
% M o i s t u r e : not dec. 34. dec. 0. Date Extracted: 2/ 1/91
E x t r a c t i o n : (SepF/Cont/Sonc) SONC Date Analyzed: 2/ 8/31
GPC Cl e a n u p : (Y/N)Y pH: 6.7 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2-----5 O t J
51-28-5----100-02-7----132-64-3----121 - 1 4 - 2 - - - -84-66-2----
7005-72-3----86-73-7----
100-01-6----534-52- 1 - - - -86-30-6----
101 -55-3----1 18-74-1----O / O O v
35-01-8----l _ ij i - /34-74-2----
206-44-0----123-00-0----
3 b o /3 1 -94- 1 ---•56-55-3----
21 3-01-9---1 17-81-7---1 17-34-0---->Q 5 _qq _ 2 - - -207-03-3---50-32-8---
193-39-5---53-70-3---1Q1.74-2---
•---3-Ni troani 1 i ne- ---Acenaphthene•---2 , 4-Oi ni trophenol•---4-Ni trophenol•---Oi benzofuran•---2, 4 - O i n i trotol uene• - - - D i e t h y l p h t h a l a t e- - - - 4 - C h l o r o p h e n y l - p h e n y l e t h e r __•---Fl uorene•---4-Ni troani 1 i ne•---4 , 6-Di ni tro-2-methyl phenol __• - --N -Ni t r o sodi p hen y 1 ami n e (1) __• - - -4- 8 r omophen y 1 -pheny 1 e t he r __•---Hexachl orobenzene•---Pentachl orophenol----Phenanthrene•---Anthracene----Di -n-butyl p h t h a l ate•---F! uoranthene•---Pyrene----Butylbenzy! p h t h a l ate----3,3'-Oichlorobenzidine•---Benzo(a)anthracene•---Chrysene----bi s ( 2 - E t h y l h e x y l )phthalat e __----Di - n - o c t y l p h t h a l a t e• - - - B e n z o C b ^ f l uoranthene----Benzofk If 1 uoranthene- - --Benzo (a)pyrene----Indeno(l .2.3-cd)pyrene----Dibenz(afh")anthracene- - - - B e n z o ( g . h . i 1 p e r y 1 e n e
4900.1000.4300.4300 .1000.1000.1000.1000.130.
4300.4900.1000.1000.1000.4900.1400 .380.330.
2200 .1400 .1000.2000.850.870.460.1000.680.720.7 WDf* <35W «1000.260.
1 1
IU |I'J 1
1 J 1|U |IU iIU i
IU |IU |1 11 J 11 J 11 11 1IU |I'J 11 J 11 J 11 BJ |IU |1 J 1
3 55(4
1 1(1) - Cannot be separated from d i p h e n y 1 amine
F O R M I S V - 2
359
18 EPA SAMPLE NOS E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ______________
I C A U9 8Lab Name: NET C o n t r a c t : 63D90031 | _ _ _ _ _ _ _ _ _ |
Lab Code: NET Case No.: 15741 . SAS No.: SDG No.: CAU93
M a t r i x : ( s o i l / w a t e r ) SOIL Lab Sample ID:
Sample w t / v o l : 30.1 (g/mL) G Lab F i l e ID: 03577
L e v e l : (low/med) LOW Date Received: 1/24/91
% M o i s t u r e : not dec. 22. dec. 0. Date E x t r a c t e d : 2/ 1/91
E x t r a c t i o n : (SepF/Cont/Sonc) SONC Date A n a l y z e d : 2/ 8/31
GPC Clean up: (Y/N) Y pH: 6.9 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CA3 NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
In o c c "5 _» -.
1 1 1-44-4----3C C "7 O . .
541 -73-1----106-46-7----100-51 -6----95-50-1 ----95-48-7----
108-60-1----106-44-5----621 -64-7----O / / i. I
7O C & 1
38-75-5----105-67-3----65-35-0----
X i i J i, i
120-32-1----91-20-3----106-47-8----87-68-3----59-50-7----91-57-6----77-47-4----
35-95-4----j I O O /38-74-4----
1 3 1 - 1 1-3----208-96-3----606-20-2----
- - -Phenol• ---bi s(2-Chl oroethyl )ether ___---2-Chl orophenol---1 ,3-Dichlorobenzene---1 ,4-Dichlorobenzene---Benzyl a l c o h o l--- 1 , 2-Di chl orobenzene
• - --2 -Me thy 1 phen ol---bi s(2~chl oroi s o p r o p y l )ether---4-Methyl phenol---N-Ni troso-di - n - p r o p y l a m i ne __•---Hexachl oroethane---Ni trobenzene
• - - - I sopho r one•---2-Ni trophenol•---2,4-Oimethylphenol•---Benzoic acid•---bi s(2-Chloroethoxy)met hane __•---2 , 4-Di chl orophenol•---1 ,2,4-Trichloroben_ene•---Naphtha! ene•---4-Chloroani 1 ine•---Hexachl orobutadi ene-----4-Chloro-3-methyl phenol•---2-Methylnaphthal ene- - - -He x ac hi o r oc y c 1 open t a di ene __•---2,4.6-Trichlorophenol• ---2 . 4 . 5-Tri chl orophenol•---2-Chl o r o n a p h t h a l ene----2-Ni troani 1 i ne• - - - D i m e t h y l p h t h a l a t e•---Acenaphthyl ene• - - - 2 , 6 - D i n i t r o t o l u e n e
860.860.860.860.360.860 .860.360 .860 .860.860 .860.860.860.360.360.
4200.360.860.360 .360.860.860.860.860.360.860 .
4200.360.360 .360.
1u 1u lu 1u lU Iu 1u lu 1u iu 1u lu lu iu 1u 1u lu lu lu lu 1u l
I'J 1u 1I'J
IU |uu l
1^25^uuuu
£54J4
c n R M T c y - i
!C EPA SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ______________
I '| CAU98
Lab Name: NET C o n t r a c t : 63090031 I
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU33
M a t r i x : ( s o i l / w a t e r ) SOIL L a b S a m p l e I D :
Sample w t / v o l : 30.1 (g/mL) G Lab F i l e ID: D8577
L e v e l : (low/med) LOW Date R e c e i v e d : 1/24/31
% M o i s t u r e : not dec. 22. dec. 0. Date E x t r a c t e d : 2/ 1/31
E x t r a c t i o n : (SepF/Cont/Sonc) SONC Date A n a l y z e d : 2/ 8/31
GPC C l e a n u p : (Y/N) Y pH: 6.3 D i l u t i o n F actor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
93-03-2-------3-Ni troani 1 ine_83-32-9-------Acenaphthene__51-28-5-------2,4-Dinitrophenol
100-02-7-------4-Nitropheno1 ____132-64-9-------Di benzofu ran______12 1 - 1 4 - 2 - - - - - - - 2 , 4 - D i n i t r o t o l u e n e ,34-66-2-------Di ethyl p h t h a l a te__
7 0 0 5 - 7 2 - 3 - - - - - - - 4 - C h 1 o r o p h e n y 1 - p h e n y l e t h e r _36-73 - 7---- ---Fl uorene _________________
100-01-6-------4-Ni troani 1 i n e____________53 4 - 5 2 - l - - - - - - - 4 , 6 - O i n i t r o - 2 - m e t h y l p h e n o l .8 6 - 3 0 - 6 - - - - - - - N - N i t r o s o d i p h e n y l a m i n e (1).
101 -55-3-------4-Bromophenyl - p h e n y l e t h e r118-74- 1 - - - - - - - H e x a c h l orobenz ene ________87-S6-5-------Pentachloroph«nol _______35-01-8-------Phenant hr ene_____
•Anthracene84-74-2-------Oi-n-butyl p h t h a l a t e
206-44-0-------F1 uoran thene________123-00-0-------Pyrene_____________35-68-7-------Butyl benzyl p h t h a l a te__9 1 - 9 4 - l - - - - - - - 3 , 3 ' - O i c h l o r o b e n z i d i n e _56-55-3-------Benzo(a)anthracen e____
•Chrysene_l l 7 - 8 1 - 7 - - - - - - - b i s ( 2 - E t h y l h e x y l ) p h t h a l a t e .117-34-0-------Di-n-octyl p h t h a l a t e ______205-99-2-------Benzo(b)fluoranthen e______
•8enzo(k)f!uoranthene_50-32-8-------Ben_o(a)pyren e________
193-39-5-------Indeno(1,2,3-cd)pyrene.53-70-3-------Dibenz(a,h)anthracene
131-24-2-------Benzo(g,h,i)perylen e__
4200.250.
4200.4200.160.860.860.860.360.4200 .4200.860 .860.860 .
4200.2400.370 .860.
4600.3300 .360 .1700.1700.1500.310.360
1300.1500
J
BJu
560.860. |U360. | J 4:5
(1) - Cannot be separated from d i p h e n y l a m i n e
FORM I SV-2 1/87 Rev.
18 EPA SAMPLE N'.S E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET
I CAU93Lab Name: NET C o n t r a c t : 68090031 I
Lab Code: NET Case No.: 1574] SAS No.: S O G N o . : C A U 3 3
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample w t / v o l : 1000.0 (g/mL) ML Lab F i l e ID: D8566
L e v e l : (low/med) LOW Date Received: 1/24/31
% M o i s t u r e : not dec. 100. dec. 0. Date E x t r a c t e d : 1/28/91
E x t r a c t i o n : (SepF/Cont/Sonc) CONT Date A n a l y z e d : 2/ 7/31
GPC C l e a n up: (Y/N)N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L 0
l U O - J O t1 l l -44-4----9r- c •— Q
541 -73-1----106-46-7----100-51-6----95-50-1----95-43-7----108-60- 1----106-44-5----621 -64-7----67-72- 1 ----G -^ O K .. __3 O 3 D - J "
/ O O J 1
83-75-5----105-67-9----65-35-0----
1 1 1 -91-1---.120-83-2----L h. U O i. 1
31-20-3----106-47-8----87-68-3----53-50-7---31-57-6----77-47-4---88-06-2----95-95-4---91-58-7----38-74-4----
13 1 - 1 1-3----_.Uo3b-o"~"'606-20-2----
---Phenol•---bi s (2-Chloroethyl )ether---2-Chl orophenol
•---1 ,3-Dichlorobenzene---1 , 4-Oi chl orobenzene•---Benzyl a l c o h o l- - - 1 , 2-Oi chl orobenrene
• - - - 2 - M e t h y l phenol---bi s(2-chloroi s o p r o p y l ) e t h* r
• ---4-Methyl phenol
•---Hexachl oroethane•---Ni trobenzene•---Isophorone•---2-Ni trophenol• ---2. 4-Dime thy! phenol•---Benzoic acid•---bi s(2-Chloroethoxy)methan e __•---2 , 4-Di chl orophenol----1,2,4-Trichlorobenzene----Naphtha! ene
•---Hexachl orobutadi en<?- - - - 4 -Chl o r o - 3 -me t h y ! p h en o 1 _______• - - - 2 - M e t h y l n a p h t h a l ene----Hexachl orocycl opentadi ene __•---2,4,6-Trichloropheno!----2.4.5-Trichl orophenol•---2-Chl o r o n a p h t h a l ene----2-Ni troani 1 i ne- - - - D i m e t h y l p h t h a l ate- - - - A c e n a p h t h y l ene----2. 6-Di ni t r o t o l uene
10.10.10.10 .10.10.10.10.10.10.10.10 .10.10.10.10.50.10.10.10 .10 .10.10.10.10.10.10.D'Mu
50.10 .10.10.
1|U|UIU1 u|U1 uI U1 'JIU1 u|U1 uIUI'J|UI'JIU|UI UI'J|U|UIUI'J|U|U
ifessIU|UI UIU1
443
IC EPA SAMPLE NO.S E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ___________
I ~I CAU99
Lab Name: NET C o n t r a c t : S3D30031 I
Lab Code: NET Case No.: 15741 SAS No.: S O G N o . : C A U 9 3
M a t r i x : ( s o i l / w a t e r ) WATER L a b Sample I D :
Sample w t / v o l : 1000.0 (g/mL) ML Lab F i l e ID: 08566
L e v e l : (low/med) LOW Date Received: 1/24/91
% M o i s t u r e : not dec. 100. dec. 0. Date E x t r a c t e d : 1/28/31
E x t r a c t i o n : (SepF/Cont/Sone) CONT Date A n a l y z e d : 2/ 7/31
GPC C l e a n u p : (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2----83-32-3----51-28-5----
100-02-7----132-64-3----1 2 1 - 1 4 - 2 - - - -
7005-72-3----86-73-7----100-01 -6----534-52- 1 ----36-30-6----
1f\ 1 C C •*»OI -55-^----
87-36-5----O U l o
120-12-7----84-74-2----
206-44-0----123-00-0----
31-34-1----56-55-3----
117-31-7----1 1 7-84-0----
L U / U O j
U -5 C OIQ •_. "5 O C
53-70-3----131 -24-2----
1- - - 3 - N i t r o a n i l i n e |
• - - - Ac enap h t hen e |- - - 2 , 4 - Di n i t r op hen o 1 |
• - - -4 -N i t r o pheno 1 |- - - D i b e n z o f u r a n |
• - - - 2 , 4 -Di n i t r o t o 1 uen e 1- - -Di e thy 1 ph t ha 1 a te 1---4-Chloropheny! - p h e n y l e t h e r __ |- - - F l u o r e n e |
---4, 6-Di ni t r o - 2 - m e t h y l phenol __ |• - - -N -N i t r o sodi p hen y 1 ami ne (1) __ |- - -4- B r omophen y 1 -phen y 1 e t he r __ |•---Hexachl orobenzene 1- - - Pen tac h 1 o r op henol 1•---Phenanthrene |---Anthracene 1
• - - -Oi -n-bu t y 1 ph t ha 1 a t e |- - - Fl uo r an t hen e |•---Pyrene 1•---Butyl benzyl p h t h a l ate 1•---3,3'-Dichlorobenzidine 1- - -Benzo ( a ) an t h r acen e 1•---Chrysene |---bi s ( 2 - £ t h y l h e x y l ) p h t h a l ate _ |
- - - - Di -n -oc t y 1 ph t ha 1 a t e 1• - - - Be nz o ( b ) f 1 uo r an t h en e 1• - - - Ben z o ( k ) f 1 uo r an t hen e |• - - - Benzo ( a ) py r ene 1• - - - I n deno ( 1 , 2 . 3 -cd 1 p y r ene 1• - - -Di benz ( a . h 1 an t h r acene 1•-- -Benzo (g . h . i ) per y 1 ene J
1 -
150. |
. 10. |50. |50. |10. |10. |10. |10. '110. |50. |50. |10. |10. |10. |50. |10. |10. |10. |10. |.0. |10. |20. |10. |10. |3. |10.10.10.
ft 8-3010.10.10.
uuuuuuuuuuU'uuuuuuuuuuuuuBOuuuuuu
11111111ii11i111I111111111i1
>58i1i
(1) - Cannot be separated from d i p h e n y l a m i n e
FORM I SV-2 1/3
18 EPA S A M P L E NOS E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SnEET ___________
l" "——I C CB12
Lab Name: NET C o n t r a c t : b3D30031 I
Lab Code: NET Case No.: 1 5 7 4 1 . SAS No.; S D G N o . : C A U 3 3
M a t r i x : ( s o i l / w a t e r ) WATER L a b Sample I D :
Sample *t/vo1: 1000.0 (g/mL) ML Lab F i l e ID: D8553
L e v e l : (low/med) LOW Date Received: 1/24/91
% M o i s t u r e : not dec. 100. dec. 0. Date E x t r a c t e d : 1/28/31
E x t r a c t i o n : (SepF/Cont/Sonc) CONT Date A n a l y z e d : 2/ 7/91
GPC C l e a n u p : (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
1/1 f*t Q _ *5
1 1 1 -44-4----J 3 O / O
541-73-1----106-46-7----100-51 -&----95-50-1----95-48-7----
108-60-1 ----106-44-5----621-64-7----67-72- 1 ----38-95-3----"7O CO 1
83-75-5----105-67-9----65-35-0----
1 1 1 - 9 1 - 1 ----120-83-2----120-82- 1----91-20-3----106-47-3----
53-50-7----31-57-6----77-47-4---88-06-2----35-95-4---91-58-7----88-74-4---
1 3 1 - 1 1-3---
606-20-2----
---Phenol• ---bi s ( 2-Chl or oe thy 1 ) et he r ___---2-Chl orophenol•---1 , 3-Oichlorobenzene---1 ,4-Dichlorobenzene•---Benzyl alcohol---1 , 2-Di ch! orobenzene•---2-Methyl phenol---bi s(2-chloroi sopropyl )ether•---4-Methylpheno!- - -N -N i troso-di -n-propyl ami ne __•---Hexachl oroethane•---Ni trobenzene• - - - I sophor one•---2-Ni trophenol• ---2 , 4-Dimethyl pheno 1•---Benzoic acid----bi s(2-Chloroethoxy)methan e __•---2, 4-Di chlorophenol•---1 , 2,4-Trichl orobenzene•---Naphthalene----4-Chloroani ! ine•---Hexachl orobutadi ene-- --4-Chl o ro-3 -me thy 1 pheno 1 ____•---2-Methylnaphthalene- - - -He x ac h 1 or oc y c 1 open t a di en e __• --- 2 , 4 , 6 -Tr i chl or ophenol- - - - 2 , 4,5-Tri chl orophenol----2-Chl oronaphtha! ene•---2-Ni troani 1 i ne• - - -Di met h y l p h t h a l a t e----Acenaphthylene•---2,6-Dinitrotoluene
10.10.10.10.10.10.10.10.10. •10.10.10.10.10.10.10.50.10.10.10.10.10.10.10.10.10.10.50.
10.10.10.
1IUIUIUI'J|UI U|U|U|UI'J|UI'JIU|U|UI UI U|U|UIUIU|UIU|U|UI U|U|U
Dtijss;|U|UI U1
472
FORM I SV-1 1/37 R*v.
1C EPA S A M P L E NOS E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ___________
II CC81Z
L a b N a m e : N E T C o n t r a c t : 6809003! I
Lab Code: NET Case No.: 15741 SAS No.: S D G N o . : C A U 3 3t
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample \* t / v o 1 : 1000.0 (g/mL) ML Lab F i l e ID: D8559
L e v e l : (low/med) LOW Date Received: 1/24/91
% M o i s t u r e : not dec. 100. dec. 0. Date Ex t r a c t e d : 1/28/91
E x t r a c t i o n : (SepF/Cont/Sone) CONT Date A n a l y z e d : 2/ 7/31
GPC C l e a n u p : (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L 0
39-09-2----O -3 O t 7
i w O 3
100-02-7----1 32-64-9----1 2 1 - 1 4 - 2 - - - -34-66-2----
7005-72-3----86-73-7----
100-01-6----534-52-1----36-30-6----
101-55-3----1 13-74-1 ----87-36-5----85-01-3----
120-12-7----34-74-2----
206-44-0----123-00-0----85-68-7----3 1 -34-1 ----56-55-3----
218-01-3----117-81-7----117-84-0----205-99-2----207-03-9----50-32-3----
193-39-5----53-70-3----
i q i _ ? 4 _ 2 - - -
- - - 3 -N i troani 1 i ne
---2. 4-Oini trophenol---4-Ni trophenol---Di benzofuran- - - 2 , 4-Di ni trotol uene- - - D i e t h y l p h t h a l a t e- - - 4 - C h l o r o p h e n y l -phenyl ethe r __--- F l uorene•---4-Ni troani 1 i ne- - - 4 , 6 - D i n i t r o - 2 -met hy 1 phenol __
• - - -N -N i t r o sodi p heny 1 ami ne (1) __- - - 4 - B r omophen y 1 - phen y 1 e t he r __•---Hexachl orobenzene---Pentachlorophenol•---Phenanthrene---Anthracene•---Di - n - b u t y l p h t h a ! a t e•---Fl uoranthene•---Pyrene• ---Butyl benzyl p h t h a l ate•---3.3'-Oichlorobenzidine•---Benzo(a)anthracene- - - -Ch r y sen e- - - - b i s ( 2 - E t h y l h e x y l ) p h t h a l a t e __----Di -n-octy!phthalate•---Benzo(b)fluoranthene•---Benzo(k)fluoranthene•---Benzo(a)oyrene----Indeno(l .2,3-cd)pyrene----Dibenz(a.h)anthracene----Benzo(q.h.i)perylene
50. |U10. |U50. |U50. |U10. |U10. | U10. |U10. | U10. |U50. | U50 . |U10 . | U10 . |U10. |U50. U10. U10. U10. U10. U10. U10. U20. U10. |U10. U3 . 8010. U10. U10. Uwsq?5^10. U10. |U 473_____________ _ _ _______i__i
(1) - Cannot be separated from d i p h e n y 1 amine
FORM I SV-2 1/37 R e v .
IS EPA SAMPLE NOS E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ____________^
II C C B 1 3
Lab Name: NET C o n t r a c t : 68D30031 I
Lab Code: NET Case No.: 15741 SAS No.: SOG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000.0 (g/mL) ML Lab F i l e ID: D8560
L e v e l : (low/med) LOW Date Received: 1/24/31
% M o i s t u r e : not dec. 100. dec. 0. Date E x t r a c t e d : 1/28/31
E x t r a c t i o n : (SepF/Cont/Sonc) CONT Date A n a l y z e d : 2/ 7/31
GPC C l e a n u p : (Y/N)N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
1r"^ O Q C O
1 l 1-44-4----35-57-8----
541 -73- 1----106-46-7----100-51 -6----95-50-1----O H - O /----
l U O O U i - - — -
106-44-5----621 -64-7----67-72- 1 ----
/ O w - f l
O O / 3 J
105-67-9----65-35-0----
1 1 1 - 3 1 -1----120-33-2----120-82-1----91-20-3----106-47-8----87-63-3----59-50-7----91-57-6----77-47-4----o O 1J D -,9C Q C A
i "DO /----
38-74-4----1 3 1 - 1 1 -3----— u o j b o606-20-2----
---Phenol---bi s( 2-Chl oroe thy! ) e the r ____---2-Chl oropheno!---1 , 3-Di chl orobenzene---1 , 4-Oi chl orobenzene---Benzyl alcohol---1 , 2 - D i c h l o r o b e n z e n e---2-Methyl phenol---bi s(2-chloroi sopropyl )ether---4-Methyl phenol- - -N -N i troso-di - n - p r o p y l a m i ne __---Hexachl oroethane---Ni trobenzene- -- I sophor one- --2-Ni trophenol---2,4-Dimethy! phenol---Benzoic acid---bi s(2-Chloroethoxy)methan e __---2,4-Oichlorophenol---1 ,2,4-Trichl orobenzene---Naphthalene---4-Chloroani ! ine---Hexachl orobutadi ene- - - 4 - Chl o r o -3 -me t h y 1 p heno 1 ____- - - 2 - M e t h y l n a p h t h a l e n e- --He xachl or oc y c 1 open tadi ene __---2.4,6-Trichlorophenol---2,4,5-Trichlorophenol---2-Chl oronaphthal ene---2-Ni troani 1 i ne- - - D i m e t h y l p h t h a l a t e---Acenaphthyl ene- - - 2 . 6 - D i n i t r o t o l u e n e
10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.50.10.10.10.10.10.10.10.10.10.10.
50.10.10.10.
1 1|U ||U | IU | M|U | W|U |IU |IU |1- 1IU |I'J 1IU ||U ||U |IU |IU |IU ||U ||U |IU ||U ||U ||U ||U |IU |IU ||U I
3$>56|! AI" i ™|U ||U |1 1
1C EPA SAMPLE NO.S E M I V O L A T I L E ORGANICS A N A L Y S I S DATA SHEET ______________
II CC813
Lab Name: NET C o n t r a c t : 68D90031 I
Lab Code: NET Case No.: 15741 SAS No.: S D G N o . : C A U 9 3
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000.0 (g/mL) ML Lab F i l e ID: 08560
L e v e l : (low/med) LOW Date R e c e i v e d : 1/24/91
% Moisture: not dec. 100. dec. 0. Date E x t r a c t e d : 1/28/91
E x t r a c t i o n : (SepF/Cont/Sonc) CONT Date A n a l y z e d : 2/ 7/91
GPC Cleanup: (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2---33-32-9---51-23-5---100-02-7---132-64-9---121-14-2---84-66-2---
7005-72-3---86-73-7---100-01 -6---534-52-1---36-30-6---
101-55-3---i i O / ** A
87-86-5---
120-12-7---84-74-2---206-44-0---129-00-0---85-68-7- —91-94-1---56-55-3---
218-01 -9---117-31-7---117-84-0---205-99-2---207-03-9---50-32-8---
53-70-3---191-24-2---
1
----3-Ni t r o a n i 1 i ne- ---Acenaphthene- - - - 2 , 4 - D i n i t r o p h e n o l----4-Ni trophenol- - - - D i benzofuran----2,4-Dini trotoluene- ---Di ethyl phtha! ate----4-Chlorophenyl -phenyl ethe r __----Fl uorene----4-Ni troani 1 i ne
- - - -N -N i t r o sod i p hen y 1 ami n e (1) __- - - - 4- B r omophen y 1 -pheny 1 e t he r __----Hexachl orobenzene----Pentachl orophenol----Phenanthrene----Anthracene----.Di - n - b u t y l p h t h a l a t e----Fl uoranthene- ---Py r ene----Butyl benzyl phthal ate----3 , 3 '-Oi chl orobenz i di ne----Benzo(a)anthraoene- - --Ch r y sene- - - - b i s ( 2 - E t h y l h e x y l ) p h t h a l ate __----Di -n-octy!phthalate----Benzo(b)fluoranthene- - - - B e n z o f k l f l u o r a n t h e n e----Benzo(a)pyrene----Indeno( 1 .2.3-cd)pyrene----Oi benz(afh)anthracene- - - - 8 e n z o ( g . h . i ) p e r y ! e n e
50.10.50.50.10.10.10.10.10.50.50 .10 .10 .10.50.10.10.10.10.10.10.20.10.10.2 .10.to.
10*.10.10.
1|UIU|U|UIU|U|U|U|U|U|U|UIU|U|U|U|UI U|U|U|UIU|U|U| 80|U|U
|U|U|U1
497
(1) - Cannot be separated from d i p h e n y 1 amine
FORM I SV-2 1/87 R e v .
10 EPA SAMPLE NOPESTICIDE ORGANICS A N A L Y S I S DATA SHEET
I CAU93Lab Name: NET C o n t r a c t : 68D90031 I
Lab Code: NET Case No.: 15741 SAS No.: S D G N o . : C A U 3 3
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL)ML Lab F i l e ID: F20A2018
Level: (low/med) LOW Date Received: 1/24/91
% M o i s t u r e : not dec.100. dec. 0. Date E x t r a c t e d : 1/29/31
E x t r a c t i o n : (SepF/Cont/Sonc) SEPF Date A n a l y z e d : 2/20/31
GPC C l e a n u p : (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/- or ug/Kg) UG/L Q
313-84-6-----ALPHA-BHC313-85-7-----8ETA-BHC319-86-8-----DELTA-BHC53-89 -9-----GAMMA-BHC76-44-3-----HEPTACHLOR
309-00-2-----ALDRIN1024-57-3-----HEPTACHLOR EPOXIDE359-38-3-----ENDOSULFAN I60-57- 1 - - - - - O I E L D R I N72-S5-9-----4,4'-OOE72-20-8-----ENDRIN
33213-65-9-----ENDOSULFAN I I72-54-S-----4,4'-DDO
1031-07-3-----ENDOSULFAN SULFATE50-29-3-----4,4'-OOT72-43-5-----METHOXYCHLOR
53494-70-5-----ENORIN KETONE5103-71-9-----ALPHA-CHLORDANE5103-74-2-----GAMMA-CHLORDANE3001-35-2-----TOXAPHENE
12674-11-2-----AROCLOR-101611104-23-2-----AROCLOR-122111141-16-5-----AROCLOR-123253463-21-9-----AROCLOR-124212672-23-6-----AROCLOR-124811097-69-1-----AROCLOR-125411096-82-5-----AROCLOR-1260
.050 |U
.050 | U
.050 |U
.050 |U
.050 |U
.050 |U
.050 |U
.050 |U
.100 |U
.100 |U
.100 |U
.100 | U
. 100 |U
. 100 |U
.100 |U.50 | U
. 100 |U.50 |U.50 | U1.0 | U.50 |U.50 |U.50 |U.50 | U.50 |U1.0 |U1.0 |U
AR302563
FORM I PEST 1/87 Rev
10 ' EPA SAMPLE NO.PESTICIDE ORGANICS A N A L Y S I S DATA SHEET ______________
I| CAU94
Lab Name: NET Contract: 63D90031 I
Lab Code: NET Case No.: 15741 * SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL)ML Lab F i l e ID: F20A2013
Level: (low/med) LOW Date Received: 1/24/91
% Moisture: not dec.100. dec. 0. Date E x t r a c t e d : 1/29/31
E x t r a c t i o n : (SepF/Cont/Sonc) SEPF Date A n a l y z e d : 2/20/31
GPC Cleanup: (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND C-g/L or ug/Kg) UG/L Q
319-84-6-----ALPHA-8HC313-35-7-----8ETA-8HC319-86-8-----DELTA-8HC58-33-9-----GAMMA-BHC76-44-8-----HEPTACHLOR
303-00-2-----ALDRIN1024-57-3-----HEPTACHLOR EPOXIDE953-93-3-----ENDOSULFAN I60-57-1-----DIELDRIN72-5S-9-----4,4 '-ODE72-20-8-----ENDRIN
33213-65-3-----ENDOSULFAN II72-S4-8-----4,4'-OOD
1031-07-3-----ENOOSULFAN SULFATE50-29-3-----4,4'-ODT72-43-5-----METHOXYCHLOR
53494-70-5-----ENORIN KETONE5103-71-9-----ALPHA-CHLORDANE5103-74-2-----GAMMA-CHLOROANE8001-35-2-----TOXAPHENE
12674-11-2-----AROCLOR-101611104-23-2-----AROCLOR-122111 141-16-5-----AROCLOR-123253469-21-9-----AROCLOR-124212672-29-6-----AROCLOR-12481 1097-63-1-----AROCLOR-12541 1096-82-5-----AROCLOR-1260
050 |U050 |U050 |U050 |U050 |U050 |U050 |U050 | U100 |U100 1 U100 |U100 |U100 |U100 |U100 |U.50 | U100 |U.50 | U.50 | U1.0 |U.50 |U.50 |U.50 | U.50 |U.50 |UI . 0 | U1.0 IU
AR30256«»646
FORM I PEST 1/37 Rev
10 EPA SAMPLE NOPESTICIDE ORGANICS A N A L Y S I S DATA SHEET
I CAU96Lab Name: NET Co n t r a c t : 68D90031 |
Lab Code: NET Case No.: 15741 SAS No.: S D G N o . : C A U 3 3•
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample w t / v o l : 1000. (g/mL)ML Lab F ^ l e ID: F20A2023
L e v e l : (low/med) LOW Date Received: 1/24/91
% M o i s t u r e : not dec.100. dec. 0. Date E x t r a c t e d : 1/29/91
E x t r a c t i o n : (SepF/Cont/Sonc) SEPF Date A n a l y z e d : 2/21/91
GPC C l e a n u p : (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
313-84-6-----ALPHA-BHC319-85-7-----BETA-BHC319-86-8-----DELTA-BHC58-89-9-----GAMMA-BHC76-44-8-----HEPTACHLOR
309-00-2-----ALDRIN1024-57-3-----HEPTACHLOR EPOXIDE953-33-3-----ENOOSULFAN I60-57-1-----DIELDRIN72-55-9-----4,4'-DDE72-20-8-----ENDRIN
33213-S5-3-----ENOOSULFAN I I72-54-S-----4,4 '-ODD
1031-07-8-----ENDOSULFAN SULFATE50-23-3-----4,4'-ODT72-43-5-----METHOXYCHLOR
53494-70-5-----ENDRIN KETONE5103-71-9-----ALPHA-CHLOROANE5103-74-2-----GAMMA-CHLORDANE3001-35-2-----TOXAPHENE
12674-11-2-----AROCLOR-101611104-23-2-----AROCLOR-122111141-16-5-----AROCLOR-123253463-21-3-----AROCLOR-124212672-23-6-----AROCLOR-124811037-63-1-----AROCLOR-12541 1036-82-5-----AROCLOR-1260
.050
.050
.050
. 050
.050
.050
.050
.050
. 100
. 100
. 100
. 100
. 100
. 100
. 100.50
. 100.50.501 .0.50.50.50.50.501 .01 .0
8R3G256565
FORM I PEST 1/37 Rev
10 EPA SAMPLE NOPESTICIDE ORGANICS A N A L Y S I S DATA SHEET
I CAU37Lab Name: NET Contract: 68030031 I
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU33
M a t r i x : (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 30. (g/mL) G Lab F i l e ID: F20A2027
L e v e l : (!ow/med) LOW Date Received: 1/24/91
% Mo i s t u r e : not dec. 37. dec. 0. Date E x t r a c t e d : 2/ 1/91
E x t r a c t i o n : (SepF/Cont/Sone) SONC Date Analyzed: 2/21/91
GPC Cleanup: (Y/N) Y pH: 6.7 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
319-84-6-----ALPHA-8HC319-85-7-----BETA-8HC319-86-8-----DELTA-BHC58-39-9-----GAMMA-BHC76-44-8-----HEPTACHLOR
309-00-2-----ALDRIN1024-57-3-----HEPTACHLOR EPOXIDE953-93-8-----ENOOSULFAN I60-57-1-----OIELDRIN72-55-9-----4,4'-OOE72-20-8-----ENORIN
33213-65-9-----ENOOSULFAN I I72-54-S-----4,4'-DDD
1031-07-S-----ENDOSULFAN SULFATE50-23-3-----4,4'-ODT72-43-5-----METHOXYCHLOR
53434-70-5-----ENORIN KETONE5103-71-9-----ALPHA-CHLORDANE5103-74-2-----GAMMA-CHLOROANE8001-35-2-----TOXAPHENE
12674-11-2-----AROCLOR-101611104-28-2-----AROCLOR-122111141-16-5-----AROCLOR-123253469-21-9-----AROCLOR-124212672-29-6-----AROCLOR-124811097-69-1-----AROCLOR-125411096-82-5-----AROCLOR-1260
25. |U25. |ll25. |U25. |U25. |U25. |U25. |U25. |U50. | U50. |U50. |U50. |U50. |U50. |U50. |U
250. |U50. |U50. | U
250. |U500. |U250. |U250. |U250. |U250. |U250. |U500. |U500. ' IU
65G
FORM I PEST 1/37 Rev.
ID EPA SAMPLE NOPESTICIDE ORGANICS A N A L Y S I S DATA SHEET __
I| CAU98
Lab Name: NET C o n t r a c t : 63090031 I
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 30. (g/mL) G Lab F i l e ID: F20A2030
L e v e l : (low/med) LOW Date Received: 1/24/91
*o M o i s t u r e : not dec. 22. dec. 0. Date Extracted: 2/ 1/31
E x t r a c t i o n : (SepF/Cont/Sonc) SONC Date A n a l y z e d : 2/21/91
GPC Cleanup: (Y/N) Y pH: 6.9 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
1 7 O * * O
319-35-7--I T J S b o
76-44-8--303-00-2--
1024-57-3--j D .i-TO o60-57-1--/4"D5"72-20-8--
3 _ 1 3 - b b ?72-54-8--
1031-07-8--50-29-3--72-43-5--
53494-70-5--5103-71-9--5103-74-2--3001 -35-2--
12674-1 1-2--1 1 104-23-2--1 1 141-16-5--53469-21-9--12672-23-6--1 1097-69-1--1 1036-82-5--
-. _ -. A 1 D U A — B U /*
8C T __ - D U C
---DELTA-BHC---GAMMA-BHC- - - u c o T A r u i no---ALDRIN— — _-LJCDTA/~lJ( f\D IT D A Y T F\ C
---ENOOSULFAN I---01 ELDRIN---4,4'-DOE---ENORIN---ENDOSULFAN I I---4, 4'-DDD---ENDOSULFAN SULFATE---4, 4'-OOT
M_TT*LJAVV/*UI rtO
---ENDRIN KETONE---ALPHA-CHLORDANE-- -GAMMA -CHLORD AN E---TOXAPHENE---AROCLOR-1016---AROCLOR-1221---AROCLOR-1232---AROCLOR-1242---AROCLOR-1248---AROCLOR-1254---AROCLOR-1260
21 .21 .21 .2 1_ 4 •
21 .21 .21 .") 141 .H JL •
41 .41 .*+ 4 .41 .41 .
210.41 .
210.210.410.^ i n
210.210.210.210.410.410.
1IUI UIUI UIUI UIUI U|UI'JIUI'JIU|U|UIUIUI'J|UIUI'J|UI'JI'JI'JI'JIU1
FORM I PEST 1/87 Rev
• 10 EPA SAMPLE NOPESTICIDE ORGANICS ANALYSIS DATA SHEET
I CAU99Name: NET C o n t r a c t : 63D90031 I
_ab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sample 10:
Sample w f / v o l : 1000. (g/mL)ML ' Lab F i l e ID: F20A2024
Level: (low/med) LOW Date Received: 1/24/91
* M o i s t u r e : not dec.100. dec. 0. Date Extracted: 1/29/91
E x t r a c t i o n : (SepF/Cont/Sonc) SEPF Date Analyzed: 2/21/91
GPC Cleanup: (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
319-84-6---3 i J <5 O /
.$ l j 3 b o
76-44-8---303-00-2--
1024-57-3---? v ? ./ Q O
60-57-1---72-55-9---72-20-8---
^ J w l - 5 Ov J
72-54-3---1031-07-3---
50-29-3---72-43-5--.
53434-70-5---5103-71-9---5103-74-2---3001-35-2---
iCO/4* l l « *
1 1 104-23-2---1 1 1 4 1 - 1 6-5---53463-21 -9---12672-29-6---11097-63-1--11096-32-5---
MLrnnon**.C 1 n B n v_,
•--OELTA-BHC---GAMMA-BHC
Her i H v^ n — v ~---ALDRIN•--HEPTACHLOR EPOXIDE---ENDOSULFAN I---DI ELDRIN---4,4 '-DDE---ENDRIN•--ENDOSULFAN II•--4,4'-OOD•--ENDOSULFAN SULFATE• - -4 4 ' - DOT** | •* V \ti \
MC "— 'LJ— t V V — 'LJI f\C r
•--ENORIN KETONE•--ALPHA-CHLORDANE•--GAMMA-CHLORDANE•--TOXAPHENE•--AROCLOR-1016---AROCLOR-1221•--AROCLOR-1232---AROCLOR-1242•--AROCLOR-1248---AROCLOR-1254•--AROCLOR-1260
.050
.050
.050
.050
.050
. 050
.050
.050
. 100
. 100
. 100
. 100
. 100
. 100
. 100.50
. 100.50R A. 5 0
1 .0
.50
.50
.50
.50
.501 .01 .0 ,
1IUIUIUIUIUIUIUI'JI'uI'-1I UIU !I'J|UIU|U|UI U|U|UI'JIUIUIU|UI'J|U1
AR302568C,,6b
FORM I PEST 1/87 Rev.
10 EPA SAMPLE NOP E S T I C I D E ORGANICS A N A L Y S I S DATA SHEET _____________
II CC812
Lab Name: NET C o n t r a c t : 68D90031 I
Lab Code: NET Case No.: 1 5 7 4 1 * SAS No.; S D G N o . : C A U S 3
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample w t / v o l : 1000. (g/mL)ML Lab F i l e ID: F20A2016
L e v e l : (low/med) LOW Date Received: 1/24/31
*• M o i s t u r e : not dec. 100. dec. 0. Date E x t r a c t e d : 1/29/91
E x t r a c t i o n : (SepF/Cont/Sone) SEPF Date A n a l y z e d : 2/20/91
GPC C l e a n u p : (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
313-84-6--3 L ? >i y l» j o o oD 0 O 33
76-44-8--303-00-2- -
1024-57-3--D 3 3 . 5 O
60-57-1--"7 T C P O
72-20-8--33213-65-3--
72-54-3--1031-07-8--
50-23-3--72-43-5--
53434-70-5--5 103 -71 -9--5103-74-2--3001-35-2--
12674-1 1-2--11 104-23-2--1 1 141-16-5--53463-2 1-3--l _ _ O / t _ . t ; 7 O
1 1037-69-1--11 09 6-8 2 -5--
- _ _ A 1 DLJA-QUr
8C T A — D U CC 1 n " Dn (~-
---DELTA-BHC---GAMMA-BHC
C r \ rt V* — 1 L w — \
---ALDRINt _ r i n V _ . n L U K t, r U A 1 U t
---ENDOSULFAN I---DI ELDRIN---4, 4'-DDE---ENDRIN---ENDOSULFAN I I---4, 4'-DDD---ENDOSULFAN SULFATE---4,4'-DOT
tut C T t_l rt V V /^ t_l 1 /~\ D
---ENDRIN KETONE---ALPHA -CHLORD AN E---GAMMA-CHLORDANE---TOXAPHENE---AROCLOR-1016---AROCLOR-1221---AROCLOR-1232---AROCLOR-1242---AROCLOR-1248---AROCLOR-1 254---AROCLOR-1260
.050
.050
.050
.050
.050
.050
.050
.050
. 100
. 100
. 100
. 100
. 100
. 100
. 100.50
. 100.50.501 .0.50.50.50.50.501 .01 .0
1I UIUIUI UI'JI UI UIUI UI'JI UI UIUI UI UI'J|UI'JIUIUIUIUIUI'JIU|UIU1
RR302569
FORM I PEST 1/37 Rev
ID £PA SAMPLE NO.PESTICIDE ORGANICS A N A L Y S I S DATA SHEET
| CCB13•_ab Name: NET Contract: 68D30031 |________
_ab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU33•M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL)ML Lab F i l e ID: F20A2017
L e v e l : (low/med) LOW Date Received: 1/24/91
* Moisture: not dee.100. dec. 0. Date E x t r a c t e d : 1/29/91
E x t r a c t i o n : (SepF/Cont/Sonc) SEPF Date A n a l y z e d : 2/20/91
GPC Cleanup: (Y/N) N • >pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND fug/L or ug/Kg) UG/L Q
313-84-6-----ALPHA-8HC313-85-7-----8ETA-BHC319-86-8-----DELTA-BHC58-89-9-----GAMMA-BHC76-44-8-----HEPTACHLOR
309-00-2-----ALDRIN1024-57-3-----HEPTACHLOR EPOXIOE959-93-3-----ENOOSULFAN I60-57-1-----OIELDRIN72-5S-9-----4,4'-DDE72-20-3-----ENORIN
33213-65-9-----ENDOSULFAN II72-54-S-----4,4'-ODD
1031-07-8-----ENDOSULFAN SULFATE50-29-3-----4,4'-DDT72-43-5-----METHOXYCHLOR
53494-70-5-----ENDRIN KETONE5103-71-9-----ALPHA-CHLORDANE5103-74-2-----GAMMA-CHLORDANE3001-35-2-----TOXAPHENE12674-11-2-----AROCLOR-101611 104-28-2-----AROCLOR-122111 141-16-5-----AROCLOR-123253463-21-9-----AROCLOR-124212672-29-6-----AROCLOR-12481 1097-69-1-----AROCLOR-125411 096-82-5-----AROCLOR-1260
,050 |U,050 |U,050 |U,050 |U,050 |U,050 |U,050 |U,050 |U, 100 |U, 100 | U, 100 |U, 100 |U, 100 |U, 100 |U,100 |U.50 |U
, 100 |U.50 | U.50 |U1.0 |U.50 |U.50 |U.50 |U.50 |U.50 |U1.0, |U1.0 |U
8R30257Q677
FORM I PEST 1/87 Rev.
Appendix BTIC Results
AR302571
SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ________________
TENTATIVELY IDENTIFIED COMPOUNDS | ~—————————"I CAU93
Lab Name: NET Contract: 68D90031 I
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) ML Lab F i l e ID: F3700
Level: (low/med) LOW Date Received: 1/24/91
* Moisture: not dec. 100. Date Analyzed: 1/29/91
Column: (pack/cap) CAP D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 3 (ug/L or ug/Kg) UG/L
CAS NUMBER
1. 76-13-12. 110-54-33. - -4.S.6.7.8.9.10.1 1 .12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.27.28.29.30.
COMPOUND NAME
Ethan*, 1 , 1 , 2-t H ehl or o-l , 2 ,Hexane (DOT) (8CI9C I )UNKNOWN
-
-,
RT
4.326.24
22.85
-
EST. CONC.
90.5.10.
———— H D Q fl 9 fA n o u d H
Q
JJJ
L "7 9
21FORM I VOA-TIC 1/87 Rev.
IE EPA SAMPLE NO.VOLATILE ORGANICS A N A L Y S I S DATA SHEET ________________
TENTATIVELY I D E N T I F I E D COMPOUNDS |I CAU94
Lab Name: NET Contract: 68D90031 I _____________
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) ML Lab F i l e ID: F3703
Level: (low/med) LOW Date Received: 1/24/91
% Moisture: not dec. 100. Date Analyzed: 1/29/91
Column: (pack/cap) CAP D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 3 (ug/L or ug/Kg) UG/L
CAS NUMBER
1. 76-13-12. - -3. - -4.5.6.7.8 .9.10.11 .12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.27.28.29.30.
1COMPOUND NAME • | RT
E-t liana t 1 , l.-.-,r.t-f-ic.h-V«ro- r , 2 . \ 4" . 3 0UNKNOWN HYDROCARBON 1 6.22UttKfTCWN 1 22.86
111111I11I1111I111111111I111
EST. CONC..............
90.7. -10. '
1 R n • 0 f> <"» r- -i1 A n 0 U c <j* /l
Q 1L.»-••r i
u J ..— <
3 — 43=138
FORM I VOA-T1C 1/87 Rev.
IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS | ~~———————I CAU95
Lab Name: NET Contract: 68090031 |
Lab Code: NET Case No.: 1574', SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample *t/vol: 5.0 (g/mL) ML Lab F i l e ID: F3704
Level: (low/med) LOW Date Received: 1/24/9*
% Moisture: not dec. 100. Date Analyzed: 1/29/91
Column: (pack/cap) CAP Dilution Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 3 C-g/- or ug/Kg) UG/L
CAS NUMBER
1. - -2. - -3. 76-13-14.5.6.7.8.9.10.1 1 .12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.k30.'
COMPOUND NAME
UNKNOWN HYDROCARBONUNKNOWNETHANE, 1 , 1 ,2-TRICHLORO-l ,2,2
RT
6.2322.874.31
.
-
. EST. CONC.
7.5.90.
ft D tj n *> rr«H3025i
Q
JJJ
"7 f7^___________ 56
FORM I VOA-TIC 1/87 Rev.
IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ______________
TENTATIVELY IDENTIFIED COMPOUNDS | ~I CAU96
Lab Name: NET Contract: 68D90031 I
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
Matrix.'(soil/water) WATER Lab Sample ID:
Sample wt/vol: 5.0 (g/ml.) ML Lab File ID: F3705
Level: (low/med) LOW Date Received: 1/24/91
% Moisture: not dec. 100. Date Analyzed: 1/29/91
Column: (pack/cap) CAP Dilution Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 2 (ug/L or ug/Kg) UG/L
CAS NUMBER
1. 110-54-32. 76-13-13.
(4.5-6.7.8.9.10.1 1 .12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.27.28.29.
•io.•
COMPOUND NAME
Hexane (DOT) (8C I 9C I )ETHANE, 1,1 ,2-TRICHLORO-l ,2,2
-
RT
6.244.31
.
EST. CONC.
8.80.
QK3021
Q
Jj
-i -i t r*D7b— i7'
FORM I VOA-TIC 1/87 Rev.
IE EPA SAMPLEVOLATILE ORGANICS ANALYSIS DATA SHEET _______________
TENTATIVELY IDENTIFIED COMPOUNDS |I CAU97
Lab Name: NET Contract: 68090031 |
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 5.1 (g/mL) G Lab F i l e ID: F3724
Level: (low/med) LOW Date Received: 1/24/91
% Moisture: not dec. 37. Date Analyzed: 1/31/91
Column: (pack/cap) CAP D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 1 (ug/L or ug/Kg) UG/KG
CAS NUMBER
1 . - -2.3.4.5.6.7.8.9.10.11 .12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.27.28.29.30.
COMPOUND NAME.. ———— ..... ———————————————
RT
22.72
EST. CONC.———— . ———— ..
10T.
. _ ~ ~A R 3 Q £ 5
Q
*j '__ ji
i^h (i ,___..!i •
FORM I VOA-TIC 1/87 Rev.
1E EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA SHEET __________
TENTATIVELY I D E N T I F I E D COMPOUNDS ———I CAU98
Lab Name: NET Contract: 68D90031 |
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 5.3 (g/mL) G Lab Fil e ID: F3725
Level: (low/med) LOW Date Received: 1/24/91
% Moisture: not dec. 22. Date Analyzed: 1/31/91
Column: (pack/cap) CAP Di l u t i o n Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 0 C-g/L or ug/Kg) UG/KG
CAS NUMBER
1 .2 .
k 3 .1 4.
5 .6.7.8 .9 .10.1 1 .12.13.14.15 .16.17.18.19.20.21 .22 .23.24 .25 .26.27.28.
' 30.
COMPOUND NAME RT EST. CONC.
_H'R3Q__5 i
i1 Q1
.^7
FORM I VOA-TIC 1/87 Rev
IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: NET Contract: 68D90031
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) ML Lab File 10: F3706
Level: (low/med) LOW Date Received: 1/24/91
% Moisture: not dec. 100. Date Analyzed: 1/29/91
Column: (pack/cap) CAP Dilution Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 2 (ug/L or ug/Kg) UG/L
CAS NUMBER
1. 110-54-32. -3.4.5.6.7.8.9.10.11 .12.13.14.IS .16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
COMPOUND NAME
Hexane ( DOT) C8C I 9C I )UNKNOWN
r*
RT--------
6.2222.85
EST. CONC.
6.6.
•
s p o n 9 i~
Q
JJ
5 7 8
— T7.1 c.FORM I VOA-TIC 1/87 Rev
IE EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA SHEET _____ __________
TENTATIVELY IDENTIFIED COMPOUNDS | "I CCB12
Lab Name: NET Contract: 68D90031 ____
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) ML Lab F i l e ID: F3697
Level: (low/med) LOW Date Received: 1/24/91
* Moisture: not dec. 100. Date Analyzed: 1/29/91
Column: (pack/cap) CAP D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 1 (ug/L or ug/Kg) UG/L
CAS NUMBER
1. - -^2 .
k 3'1 4'^ 5.6.7.8 .9 .to.11 .12.13 .14.15.16.17.18.19.20.21 .22.23.24.25.26.27.28.
,29.MO.
COMPOUND NAME
nrjifN.nh.tt" — — "' " ~~~"~
1ii
RT
22.86
_EST. CONC.
. 1 U-T*-«
-
-
fi n i n n A h J U _. u
QL-a-?«1—9 ——— 1
"?O/ J
.145FORM I VOA-TIC 1/87 Rev.
1E EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ______
TENTATIVELY IDENTIFIED COMPOUNDS |I CCB13
Lab Name: NET Contract: 68D90031 |
Lab Code: NET Case No.: 15741 SAS No.: SOG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) ML Lab F i l e ID: F3698
Level: (low/med) LOW Date Received: 1/24/91
% Moisture: not dec. 100. Date Analyzed: 1/29/91
Column: (pack/cap) CAP Dilution Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 3 (ug/- or ug/Kg) UG/L
CAS NUMBER
1. 76-13-12. 110-54-33. - -4.5.6.7.8.9.10.1 1 .12 .13.14.15.16.17.18.19 .20.21 .22.23 .24 .25.26.27.28.29.30.
COMPOUND NAME
i-T44AN rn".T 72 - f FrrCHTOfTO' - 172 ! ,llennfl (POT) en-fr.-9e.-3 —— ' -UNKNOWN
RT
4.3T—— ••&-. 2-3 -
22.85
EST. CONC.——— ————————
• - 2ocr: —10%
._ . .
5 R 0 2 5
Q—— i--T--~ j.. j— (
RO 1l
FORM I VOA-TIC 1/87 Rev
.. *. v-.>- • .-it-'1'' •
Matrix: (901 ' /ir»ater) K*TER ... Sampl« ID:
Sampl» v»t/vol: 5,0 (9/wL) ML Lab F i * « 10; F3$»9
L e v e l ; (low/nr.«d) LOW D.t» R««»iv«_: :/24/91
% Hoi*t-r»: n«fc -•«. JOO. 0«t» Ana'y.s-; J/2V3I
Caljmn: (pi«l«/oap) CAP D i l u t i o n Factoi ; l . 00
CONCENTRATION UNITS:Numb«r TIC* r'ognd: 1 (uf/- or vig/Kg) U6/L
1j CA, MUMiEft
| 1. 7&-J3-11 2-1 3., -.1 5.r 6.' 7 .• 9.1 9.1 10.1 It.1 !_.f 13.1 14.1 IS.| 16.1 17.i 18.1 IS.I 20.i 21.; 22.1 23. .,1 24.1 25. ... ,.1 26.1 27.| 28. •1 29.1 30.1
1CCI^OUNO NAME
Elnan*, 1 , 1 , 2-fcr i chl pro -J , 2 ,
,„ ,, ... .,„.„., , .-
._
RT
-.3!
- ........
FST. CONC.
40.
»
—————————— ft
J
Ri_•»-••
k f* C*
IF EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY I D E N T I F I E D COMPOUNDS |I CAU93
Lab Name: NET Contract: 68D90031 I___
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000.0 (g/mL) ML Lab F i l e ID: 08561
L e v e l : (low/med) LOW Date Received: 1/24/91
% Moisture: not dec. 100. dee. 0. Date Extracted: 1/28/91
E x t r a c t i o n : (SepF/Cont/Sone) CONT Date Analyzed: 2/ 7/91
GPC Cleanup: (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 0 (ug/L or ug/Kg) UG/L
CAS NUMBER
1 -2.3.4.5 .6.7.8.9.10.1 1 .12 .13.14.15 .16.17.18.19.20.21 .22.23 .24.25.26.27.28.29.30.
ICOMPOUND NAME
, ——————————— , —— .,,,..»..,.RT EST. CONC.
— AR3025£
iQ 1
_A—— 1
,
if — i|_, |l1 __ _i\
FORM I SV-TIC 1/87 Rev
IF EPA SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _____ __________
TENTATIVELY I D E N T I F I E D COMPOUNDS |I CAU94
Lab Name: NET Contract: 68090031 I
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000.0 (g/mL) ML Lab F i l e ID: D8564
Level: (low/med) LOW Date Received: 1/24/91
% Moisture: not dec. 100. dec. 0. Date Extracted: 1/28/91
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 2/ 7/91
GPC Cleanup: (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 1 (ug/L or ug/Kg) UG/L
1CAS NUMBER
1 1. 10544-50-0
1 3'r 4.5 .6.7.8.9.10.1 1 .12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.
^27.28.29.| 30.1
COMPOUND NAME
SULFUR
y
RT--------22.76
•
EST. CONC.
10.
dKliOX
Q
BJ
i B .5
FORM I SV-TIC 1 /87 Rev.
IF EPA SAMPLE NO.SEMIVOLAT1LE ORGANICS ANALYSIS DATA SHEET _________
TENTATIVELY IDENTIFIED COMPOUNDS |~| CAU96
Lab Name: NET Contract: 68D9003 1 I
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000.0 (g/mL) ML Lab F i l e ID: 08565
Level: (low/med) LOW Date Received: 1/24/91
X Moisture: not dec. 100. d«c. 0. Date Extracted: 1/28/91
E x t r a c t i o n : (SepF/Cont/Sonc) CONT Date Analyzed: 2/ 7/91
GPC Cleanup: (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 0 (ug/L or ug/Kg) UG/L
CAS NUMBER
1 .2.3.4.5.6.7.8.9.10.1 1 .12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.27.28.29.30.
COMPOUND NAME RT
, ,
EST. CONC.
- -
riH:«i25
0
ai*—O •}«-• -J
FORM I SV-TIC 1/87 Rev.
1F EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALY S I S DATA SHEET ______________
TENTATIVELY IDENTIFIED COMPOUNDS |—————————————"| CAU97
'ab Name: NET Contract: 68D90031 ___
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 30.1 (g/mL) G Lab F i l e ID: 08574
Level: (1ow/med) LOW Date Received: 1/24/91
% Moisture: not dec. 34. dec. 0. Date Extracted: Z/ .1/91
Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 2/ 8/91
GPC Cleanup: (Y/N) Y pH: 6.7 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 7 (ug/L or ug/Kg) UG/KG
CAS NUMBER
1. - -2. 10544-50-03. - -4. - -5. - -6. - -7. - -8.9.10.11 .12.13.14.15.16.17.18.19. •20.21 .22.23.24.25.26.27.28.23.30.
COMPOUND NAME
tffl KNOWN ————SULFURUNKNOWN HYDROCARBONUNKNOWN AROMATICUNKNOWNUNKNOWNUNKNOWN
RT
4.7322.8126.4327.5832.2532.3235.69
EST. CONC..............
r~ -•- Am>A>~ -400<T;1000.400.800.600.400.400.
flp onnr- r,j-« 1 1 v> y c ,5 d *j
Qv-jjjjjj
FORM I SV-TIC 1/87 Rev
1F EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS | ~————'I CAU98
Lab Name: NET Contract: 68D90031 I
Lab Code: NET Case No..1 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 30.1 (g/mL) G Lab F i l e ID: 08577
Le v e l : (low/med) LOW Date Received: 1/24/91
\ Moisture: not dec. 22. dec. 0. Date Extracted: 2/ 1/91
Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 2/ 8/91
GPC Cleanup: (Y/N) Y pH: 6.9 Dilution Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 6 (ug/L or ug/Kg) UG/KG
CAS NUMBER
1. - -2. - -3. 10544-50-04. 2381-21-75. - -6. - -7.8.9.10.1 1 .12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.27.28.29.30.
COMPOUND NAME
•tfN-KNOWW-'UNKNOWNSULFURPYRENE. 1-METHYLUNKNOWN AROMATICUNKNOWN
RT
f~- 4.8622.1422.8224.0527.5929.07
.. . ..
EST. CONC.-------------—— 3000.—
300.500.500.500.400.
&R302J
Q.....J -"*"JJJJJ
L a -5c_»b ,4
FORM I SV-TIC 1/87 Rev,
IF EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET __________•
TENTATIVELY I D E N T I F I E D COMPOUNDS | — — — — —I CAU99
b Name: NET Contract: 68D90031 I
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000.0 (g/mL) ML Lab F i l e ID: D8566
Level: (low/med) LOW Date Received: 1/24/91
% Moisture: not dec. 100. dec. 0. Date Extracted: 1/28/91
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 2/ 7/91
GPC Cleanup: (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 0 (ug/L or ug/Kg) UG/L
CAS NUMBER
1 .2.
i J:5.6.7.8.9.10.1 1 .12.13.14.15.16.17.18.19.20.21 .22.23 .24.25.26.27.28.29.30.
COMPOUND NAME RT—— ————
EST. CONC.
.
0
q •?u / ^, Iik Q
FORM I SV-TIC 1/87 Rev,
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET "* SAMPLE N0-TENTATIVELY IDENTIFIED COMPOUNDS - ———————— ———— -
Lab Nam*: NET Contract: 68D90031
Lab Code: NET Case No.: 15741 SAS No.: SOG N o > .
M a t r i x : (soil/water) WATER Lab Sflmple ID;
Sample wt/vol: 1000.0 (g/mL) ML Lab Fn. IQ. 0855g
L«v«l : (low/med) LOW n . ...Date Received: 1/24/91
* Moisture: not dec. 100. dec 0 n.* - .' u' Date Extracted: 1/28/91
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 2/ 7/91
GPC Cleanup: (Y/N)N pH: .0 Di1ution Factor: , . 00
_, . -.._, . CONCENTRATION UNITS:Number TICs found: 1 (ug/_ Q_ Ug/Kg3
CAS NUMBER
1. 10544-50-02.3.4.5.6.7 8 .9.10.11.12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.27.28.29.30.
COMPOUND NAME
3ULTU* ———————————————— ..--.- 4
RT
— - £ -«p-*-*~
-
-
*
EST. CONC.
———— • • - ——— 8 —— , ,
——— frfr£K
Q
_EJ— ..
}9Cq.<_.C»u CI1 ^
t)4fI 174
FORM I SV-TIC 1/87 Rev.
IF EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY I D E N T I F I E D COMPOUNDS | — — — —I CCB13
Lab Name: NET Contract: 68090031 |__________
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000.0 (g/mL) ML Lab F i l e ID: D8560
Level: (low/med) LOW Date Received: 1/24/91
% Moisture: not dec. 100. dec. 0. Date Extracted: 1/28/91
E x t r a c t i o n : (SepF/Cont/Sonc) CONT Date Analyzed: 2/ 7/91
GPC Cleanup: (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 0 (-g/- or ug/Kg) UG/L
«
CAS NUMBER
M:* 3.4.5.6.7.8.9.10.1 1 .12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.
k 27.^28.
30.
COMPOUND NAME RT EST. CONC.
a H :i ii _> 5
Q
1 1 i
ay498
1
FORM I SV-TIC 1/87 Rev.
Appendix CDPO Report
AR30259Q
ORGANIC REGIONAL DATA ASSZSSMtNT
CASE NO. ( > f wLABORATORY ,,A/ T
SOG • CA<*. 3j>saw*DPf> ACTION _ „ FY1
DATA ASSE:
1. HOLDING TIMES2. GC/MS TUNE/INSTR. PERFORM.3. CALIBRATIONS4. BLANKS5. SURROGATES6. MATRIX SPOCE/DU?
7. OTHER OjCS. INTERNAL STANDARDS9. COMPOUND IDENTIFICATION10. SYSTEM PERFORMANCE11. OVERALL ASSESSMENT
0 * Diet had so probl«ffi*/or quaJLfi«d dueM « Dita quaJifrd dot to otjor problem.Z • D»a unacctpabi*.X • Probtoott, bos do ao( i/Tiet daa.
Ar-nrtN rrewft .S.,?1 "* --- 4-*s* u.-**«
lf_T". /Vf-* - **tL0,- cJ Jf l , /d^
. sm i-t -rz»6/NO. OF SAJU LES/MATRIX /d /
. REVIEWER (IF NOT
. REVIEWER'S NAME
. COMPLETION DATE
5SVTENT SUMVAiy
VOA 8NA
0 Q__0 05. /0' g)r0 j2 _-d- J-—^ f.n nd rj0 0-M— JL-
to minor probtems.
xt*#** -> •A'' A **
i-i_j_->-« <^— / l.vr-,-£it .fa
TV JffJ ^ -
W*ti~~, friCJ)C5D) w A-i J-f /'J'«I A>X*«-rJL . Ccrvt,.
^j/.r/
PEST OTHER
a _ /.^^- /v^_ __vc)a£a6 / •2 __ / __
5~- jsy jO«-_ T! /<K*L _**e ) pk+ll+jLA0 0 "
AREAS OF CONCERN:
ftB30259i
NOTABLE PERFORMANCE:
Appendix DSupport Doc-mentation
AR302592
6AVOLATILE ORGANICS I N I T I A L C A L I B R A T I O N DATA
Lab Name: NET Contract: 68D90031
Lab Code: NET Case No.: 15741 SAS No.: SDG No.:
Instrument ID: 7002F C a l i b r a t i o n Date(s): 1/25/91 1/25/91
Matri x: (soi I/water ) WATER Level :( 1 ov^/med ): LOW Col umn : (pac k /cap ) CAP
Min RRF for SPCC(#) - .300 (0.250 for Bromoform) Max %RSO for CCC(») - 30.OX
LAB F I L E ID: RRF020- F3663 RRF050- F3664RRF100- F3665 RRF150- F3666 RRF200- F3667
1COMPOUND |RRF020
Chl o romet hane * .609B r omome t hane 1 .879Vin y l chloride * .813Chloroethane 1 .540
LMethvlene chloride I 1.505•Acetone 1 .293'Carbon d i s u l f i d e 1 2.4911 . 1 - Di chl oroethene * 1.0201 . 1 -Di chl oroethane * 1.5451 , 2 - Di chl oroet hene (total)_| 1.270Chloroform »2.4521 . 2-Di chl oroethane | 1.3582-8utanone 1 .0171 , 1 , 1 -Tri chl or oethane _____ | .384Carbon te t rach.1 or i de j .363V i n y l acetate 1 .127B r omodi ch 1 o romet hane | .4981 . 2- Di chl or oor ooane • .255c i s- 1 , 3 -Di chl o ropropene __ | .360Trichloroethene 1 .376Di b r omochl oromethane | .5141 , 1 , 2-Tri chl oroethane ____ | .287Benzene 1 . 6 3 1t rans- 1 , 3 -Di chl oropropene _| .295Bromoform * .3664-Me thy! - 2-pen tanone 1 .2582-Hexanone | .172Te t r achl o roethene 1 .4221,1,2,2-Tetrachloroethane _* .619Toluene * .591
kChlorobenzene * .841^Ethvl benzene * .368|Styrene 1 .807IXylene (total) 1 .436
Toluene-d8 1 .880| Br omof 1 uor oben zene | .4761 , 2-Di chl oroethane-d4 ____ | 1.178
RRF050
.6361 .033.825.578
1 .340.202
2.7001 .0431.6121 .3062.5711 .471.022.437.41 1.241.561.287.411.407.592.325.689.346.449.300.206.445.698.628.905.396.857.463
1 .023.554
1 .334
RRF100
.6681 .245.878.636
1 .396.215
3 . 1241 . 1731 .7811 . 4232 . 7491 . 617.028.518.493.367.647.332.483.460.685.370.783.429.556.358.252.511.829.717
1 .042. 446.963.528
1 . 144. 619
1 . 435
RRF150
.5921 .219.781.593
1 .257.206
2.8891 .0831 .6191 .2992.4501 .460.027.499.476.399.629.319.467.440.681.358.747.424.549.367.255.494.815.687
1 .009.431.928.512
RRF200
.5421. 131.718.563
1.205.200
2.7931.0491 .5481 .2422. 2961 .410.027.492.471.417.619.317.470.431.675.349. 736.431.554.354.249.481.800.686.970m.500
RRF
.6091 . 101.803.582
1 .341.223
2.7991 .0741 . 6211 .3082.5041.4fi-t.024.466. 443.310.591.302.438.423.630.338.717.385.495.327.227.471.752.862.953
;°283M88
1.118 1.083 1.049.616| .596| .572
1.323 1.250 1.304
* 1RSD |
7.8*13. 6|7.3*6.2|8.8|17.8|8.3|5. 6*5 . 9*5.3)6. 7*6.6|
18.9|11 .8 j
10.3|10.3*
7.6|CT>
1 7 . 2ff*~14.4^16.2|7.7|
12.1*7.7*8.5*
P7.7*6.9|7.7|
-4-3&I_. w vjl10.0|10.4|7.41
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: NET Contract: 68D90031t
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
Instrument ID: 7002F C a l i b r a t i o n Date: 1/29/91 Time: 9:54
Lab F i l e ID: F3694 Init. Calib. Oate(s): 1/25/91 1/25/91
Matrix:(soi1/water) WATER Level :(1ow/med): LOW Column:(pack/cap) CAP
Min RRF50 for SPCC(*) - .300 (0.250 for Bromoform) Max %0 for CCC(») - 25.0%
COMPOUND
C h 1 o r ome thaneB r omomet han eV i n y l c h l o r i deChl oroethaneMethylene c h l o r i d eAcet oneCarbon di su 1 f i de1 ,1-Dichloroethene1 . 1-Di chloroethane1 , 2-Di chl or oethene (totalChl orofo rm1 ,2-Dichloroethane2-8utanone1 ,1 , 1-TrichloroethaneCarbon te t r ac hi o r i deV i n y l acetateB r omod i ch 1 o romet hane1 ,2-Dichloroprooanec i s - 1 , 3 -Di c hi o r opr opene __Tri chl oroet h-eneDi bromochl o romet hane1 ,1.2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneB romof orm4 -Methyl -2- pen tanone2-HexanoneTetrac hi or oethene1,1,2,2-TetrachloroethaneTo! uen eChl o robenz eneEthylbenzeneS ty r eneXyl ene (total)
To! uene-d8Bromof luorobenzene1 , 2-Di chl oroethane-d4
11
*1
1111**
*i11111*
~l1t1
*111
_****11
1111
RRF
. 6091 . 101. 803.582
1 . 341. 223
2. 7991 .0741 . 6211 .3082.5041 . 463. 024. 466. 443. 310. 591. 302. 438. 423. 630. 338. 717. 385. 495.327. 227.471. 752. 662.953. 414. 894. 488
1 .049. 572
1 . 304
RRF50
.6891 .144.988.678
1 .609.227
3.0941 .1641 .7611 .3812.6331 .4750_T].436.403.240.559.302.429.409.578.317.701.361.441.301.213.452.679.627.896.399.834.460
1 . 100.587
| 1.391
1%D |
113.1*3.8 |
23. 1 •16.4 |20.0 |1.8 |
10.5 |8.4 »8.6 *5.6 |5.2 ».8 |
5.8 |6.5 |3.1 |
22.6 |5.5 |. 1 •
2.2 |3.1 |8.2 |6.2 |2.3 |6.2 |
10.9 *8.0 |6.0 |3.9 |9.8 *5.3 »6. 1 *3.7 *6.8 I5 •#Dl'.,,,J4ty4.9 |2.6 |6.7 |
1
FORM VI I VOA 1787 Rev
IA EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ______________
I| VBLKW1
Lab Name: NET Contract: 68D90031
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) ML Lab F i l e ID: F3695
Level: (low/med) LOW Date Received: O/ O/ 0
% Moisture: not dec. 100. Date Analyzed: 1/29/91
Column: (pack/cap) CAP Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3----
75-01-4----75-00-3----75-09-2----67-64-1----75-15-0----75-35-4----75-34-3----
3 H \J J J W
67-66-3----107-06-2----
71-55-6----56-23-5----108-05-4----75-27-4----78-87-5----
10061-01-5----/ j U 1 O
124-48-1----79-00-5----71-43-2----
10061-02-6----75-25-2----
108-10-1----
127-18-4----79-34-5----l U o o o *I U O j U /100-41-4----100-42-5----
1330-20-7----
---Chl oromethane- --8r omome thane---Vinyl chloride---Chl oroethane---Methylene chloride---Acetone---Carbon disulfide---1 , 1-Dichloroethene---1 , 1-Dichloroethane--- 1 , 2-Di chl or oethene (total) __---Chloroform---1 ,2-Dichloroethane---2 -8u tanone---1 , 1 , 1 -Tri chl oroethane---Carbon tet rachl or i de---Vinyl acetate---Bromodi chl or ome thane•---1 , 2-Di chl oropropane• ---ci s-1 , 3 -Di chl or op r opene ___ _•---Trichloroethene•---Di br omochl o romet hane•---1 , 1 , 2-Tri chl oroethane• ---B«nzene- --t r ans- 1 , 3-Di chl or opr opene __
• - - -B r omof orm•---4-Methyl -2-pentanone•---2-Hexanone•---Tetrachloroethene•---1,1,2,2-Tetrachloroethane __• - --To 1 uene•---Chl orobenzene•---Ethylbenzene•---St y rene•---Xylene (total)
10.10.10.10.. .8.
10-T-5.5.5 .5.5.5.10.5.5.10.5.5.5.5.5.5.5.5.5.10.10.5.
iftR5.5.5.
UUUuuuuuuuuuuuuuuuuuuuuuuuu
$25uuu
1
35228
IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ______________
TENTATIVELY IDENTIFIED COMPOUNDS I| VBLKW1
Lab Name: NET Contract: 68D90031 |_________
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) ML Lab F i l e ID: F3695
Level: (low/med) LOW Date Received: O/ O/ 0
% Moisture: not dec. 100. Date Analyzed: 1/29/91
Column: (pack/cap) CAP D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 1 (ug/L or ug/Kg) UG/L
CAS NUMBER
1 . - -2.3.4.5.6.7.8.9.10.11 .12.13.14.15.16.17.18.19 .20.21.22.23.24.25 .26.27.28.29.30.
COMPOUND NAME
UNKNOWN
RT
22.83
EST. CONC.———————————
7.
flH3iJ/__«
Q
J
——
jrc ——in!
___ J
FORM I VOA-TIC 1/87 Rev
I* EPA SAMPLE NO.VOLATILE ORGANICS A N A L Y S I S DATA SHEET ______________
II V B L K S 1
Lab Name: NET C o n t r a c t : 68D90031 I___________
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) G Lab F i l e ID: F3723
Level: (low/med) LOW Date Received: O/ O/ 0
% Moisture: not dec. 0. Date Analyzed: 1/31/91
Column: (pack/cap) CAP D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3----74-83-9----75-01-4----75-00-3----75-09-2----67-64-1----75-15-0----
75-34-3----540-59-0----67-66-3----
107-06-2----/ O J -J J
71-55-6----5f 1 *} S6-23-5----108-05-4----75-27-4----/ O O / 3
10061-01-5----79-01-6 —— -
124-48-1----79-00-5----71-43-2----
10061-02-6----~T f? 1C •*}75-25- 2- ---U o —I U l
O3 I — / e — o127-18-4----79-34-5----
i U O J w /
100-41-4----100-42-5----
1330-20-7----
• ---Chl oromethane- - - - B r omome thane•---Vinyl chloride•---Chl oroethane• ---Me thy I ene chloride•---Acetone•---Carbon disulfide•---I , l-Dichloroethene•---I , l - D i c h l o r o e t h a n e•--- I , 2 -Di c hi oroethene (total) __•---Chloroform•---I , 2-Dichloroethane•---2-Butanone•---I , I , l - T r i c h l oroethane•---Carbon te t r achl or i de• ---Vi nyl acetate• ---8 r omodi chl o romet hane•---I , 2-Dichloropropane• -- -c i s - I , 3 -Di c h I or op ropen e ______•---Trichloroethene• - --Di bromochl o romet hane•---I , I ,2-Trichl oroethane• ---Benzene• - -- 1 r ans- I , 3-Di c hi or opr opene __• - --Br omof o rm•---4-Methyl -2-pentanone• ---2 - Hexanone•---Tetrachl oroethene•---1,1,2,2-Tetrachloroethane __• - - -To 1 uene• ---Ch 1 or obenzene•---Ethyl benz ene•---Styrene•---Xylene (total)
10.10.10.10.2.
31 .5.5.5.5.5.5.10.5.5.10.5.5.5.5.5.5.5.5.5.1 .
10.5.5.
• 5.5.5.
1|U|UI'J|U1 J1|U|U|U|U|U|U|U|UIUIUIUIU|U|U|U|U|U|U|U1 J|U|U|U^Ift^R^Jjydu^|UIU|U1 1
245
IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ______________
TENTATIVELY IDENTIFIED COMPOUNDS || VBL K S 1
Lab Name: NET Contract: 68D90031 j______________
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) G Lab F i l e ID: F3723
Level: (low/med) LOW Date Received: O/ O/ 0
% Moisture: not dec. 0. Date Analyzed: 1/31/91
Column: (pack/cap) CAP D i l u t i o n Factor! 1.00
CONCENTRATION UNITS:Number TICs found: 0 (-g/L or ug/Kg) UG/KG
CAS NUMBER
1 .2.3 .4 .5 .6.7.8 .9 .10.1 1 .12 .13 .14 .15 .16.17.18.19 .20.21 .22 .23 .24.25 .26.27.28 .29 .30.
COMPOUND NAME
*
RT EST. CONC.
ARSONS
Q
Q Q3Q
246FORM I VOA-TIC 1/87 Rev.
2CWATER SEMIVOLATILE SURROGATE RECOVERY
Lab Name: NET C o n t r a c t : 68D90031
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
123456789101 112131415161718192021222324252627282930
EPASAMPLE NO.
SBLKW1CCB12CCB13CAU93CAU93MSCAU93MSDCAU94CAU96CAU99
SI(NBZ)*
9392
1019510285953491
S2(FBP)*
898680868875917982
S3(TPH)*
917679
109941009396102
S4(PHL)*
86718397 «
— T9~139089100 *
S5(2FP)*
756479907979798197
S6(TBP)*_ _ _ _ _ _1211051 1 11211151231231 171 18
OTHER TOTOUT
000100001
QC LIMITSSI (NBZ) - Nitrobenzene-d5 (35-114)S2 (FBP) - 2-Fluorobiphenyl (43-116)S3 (TPH) - Terphenyl-d!4 (33-141)S4 (PHL) - Phenol-d6 (10- 94)S5 (2FP) =• 2-Fluorophenol (21-100)S6 (TBP) - 2,4,6-Tribromophenol (10-123)
* Column to be used to flag recovery values
» Values outside of contract required QC l i m i t s
D Surrogates d i l u t e d out c i «J
page 1 of 1
3CWATER SEMIVOLATILE MATRIX S P I K E / M A T R I X S P I K E DUPLICATE RECOVERY
Lab Name: NET Contract: 68D90031
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x S p i k e - EPA Sample No.: CAU93
COMPOUND
Phenol2-Chl or opheno 11 , 4 - Di chl o r obenzene ___N-Ni troso-di-n-prop.(l)1 ,2 ,4-Trichlorobenzen e_4-Chloro-3-methylphenolAcenaphthene4-Ni t rop henol2,4-Dinitrotol uene _____Pentachl oroohenolPy r ene
SP IKEADDED(UG/L )
200.200.100.100.100.200.100.200.100.200.100.
SAMPLECONCENTRATION
(UG/L )
0.0.0.0.0.0.0.0.0.0.0.
'
MSCONCENTRATION
(UG/L )-------------
163.157.79.94.91 .177.84.146.79.
190.83.
MS\
REC *
8279799491888473799583
QCL I M I T SREC.
12- 8927-1 2336- 9741-11639- 9823- 9746-1 1810- 8024- 969-10326-121
COMPOUND
Phenol2-Chl orophenol1 , 4 - Di chl orobenzene ___N-Ni troso-di -n-prop. (1)1,2,4-Trichl orobenzene__4-Chl oro-3 -me thy! phenolAcenaphthene4-N i t r ophenol2,4-Dini trotol uene ____Pentachl orophenolPy r ene
SPIKEADDED(UG/L )
---------200.200.100.100.100.200.100.200.100.200.100.
MSDCONCENTRATION
(UG/L )-------------
124.162.61 .88.68.
147.70.
178.77.
196.86.
MSD%REC *
------62816188687470 ,
, 89 *• -7-?- '9886
%RPD *
273
26. T--H
' 29 »~TT~"
k 1820233
QC LRPD
424028
- 3828423150385031
[HITSREC .
12- 8927-1 2336- 974 1 - 1 1 639- 9823- 9746-1 1810- 8024- 969-103
26-1 27I(1) N-Nitroso-di-n-propy1 amine
* Column to be used to flag recovery and RPO values with an asterisk
* Values outside of QC l i m i t s AR3G260Q
RPO: 1 out of 11 outside l i m i t sSpike Recovery: 1 out of 22 outside l i m i t s
COMMENTS:
3DSOIL S E M I V O L A T I L E MATRIX SPIKE/MATRIX S P I K E DUPLICATE RECOVERY
Lab Name: NET Contract:68D90031
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x S p i k e - EPA Sample No.: CAU97 Leve 1 :(1ow/med) LOW
COMPOUND
Phenol2-Chl orophenol1 , 4-Di chl orobenzeneN-Nitroso-di-n-prop.(l)1 ,2,4-Trichlorobenzene_4-Ch1oro-3-methylphenolAcenaphthene4-Ni t r ophenol2,4-Dinitrotol uene ____Pen tachl or ophenol _______Pyrene
SPIKEADDED(UG/KG)
20994.20994.10497.10497.10497.20994.10497.20994.10497.20994.10497.
SAMPLECONCENTRATION
(UG/KG)
0.0.0.0.0.0.0.0.0.0.
1416.
MSCONCENTRATION
(UG/KG)
20003.19060.7967.9999.8806.20226.8245 .22863.9162.22167.9087.
MS
REC *--------
95 »9176958496791098710673
QCLIMITSREC.------26- 9025-10228-10441-12638-10726-10331-1 371 1 - 1 1 428- 8917-10935-142
COMPOUND——— .....-....„-.--*.>--Phenol2-Chl orophenol1 , 4 - Di ch 1 orobenzene _____N-Nitroso-di-n-prop.(l)1 ,2,4-Trichlo robenzene_4 -Chl oro -3 -me thy! phenolAcenaphthene4 -N i trophenol2,4-Dinitrotol uen« ____Pen tachl or ophenol ____Pyrene
SPI K EADDED(UG/KG)
20994.20994.10497.10497.10497.20994.10497.20994.10497.20994.10497.
MSDCONCENTRATION
(UG/KG)
15977.14809.6333.8763 .7338.
13416.771 1 .
21221.9248.19623.8683.
MSD%REC *
76716083708873
101889369
%RPD *
22252313189771
125 •
QC LRPD
3550273823331950474736
[HITSREC .
26- 9025-10228-10441-12638-10726-10331-1371 1 - 1 1 428- 8917-10935-142
(1) N- N i t r o s o - d i - n - p r o p y 1 amine
* Column to be used to fla g recovery and RPD values with an asterisk
(Values outside of QC l i m i t s AR3Q26Q1
RPD: 0 out of 11 outside l i m i t sSpike Recovery: 1 out of 22 outside l i m i t s 276
COMMENTS:
FORM II I SV-2 I/87 R
78SEMIVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: NET Contract:68D90031
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93*
Instrument ID: DARYD C a l i b r a t i o n Date: 2/ 8/91 Time: 8:27
Lab F i l e ID: D8568 I n i t . C a l i b . Date(s): 2/ 7/91 2/ 7/91
Min RRF50 for SPCC(*) • .050 Max %D for CCC(*) - 25.0%
COMPOUND | RRF
Phenol_______________________« 1.452bis(2-Chloroethyl)ether ___| 1.1712-Chl orophenol_____________| 1.3071 , 3-Dichlorobenzene ______| 1.6381,4-Dichlorobenzene ______* 1.640Benzyl alcohol_____________| .7571 ,2-Dichlorobenzene _______| 1.5332-Methyl phenol_____________| 1.116bi s(2-chloroi sopropyl)ether| 2.0214-Methyl phenol_____________| 1.072N-Ni troso-di-n-propylami ne_* .943Hexachl or oe thane__________| .687Nitrobenzene _ _ _ _ _ _ _ _ ____. . I .538
RRF50 | %0
1.461 .6 *1 . 149 1.9 |1 .251 4.3 |1.506 8.0 |1.567 4.5 *.727 3.9 |
1.456 .5.0|1.061 5.0 |1.949 3.6 |1.021 4.8 |.923 2.2 *.642 6.5 |.557 3.6 |.781 5.2 ||Isophorone_________________| .823
j 2 - N i t r o p h e n o l _____________* .235| .230| 2.3| 2 , 4-Di me thy! phenol_________| .385) .381) .9| B « n z o i c aci d________________ | .238J .227| 4.8|bis(2-Chloroethoxy )me t hane__| .474| 2 , 4-Di chl or ophenol_________* .364| 1 , 2 , 4-Tr i chl or obenzene_____| .448(Naphthalene _______________| 1.069|4-Chloroani1ine __________| .266| Hexachlorobutadiene _______* .296| 4-Chloro-3-methy1 phenol ___* .324|2-Methylnaphtha!ene _______| .895| H e x a c h 1orocyclopentadi ene _* .463| 2,4,S-Trichlorophenol ____* .492| 2 , 4,5-Trichl orophenol ____| .529j2-Chloronaphthalene ________\ 1.070| 2-Ni troani 1 ine____________| .426| Dimethyl phthal ate __________\ 1.423| Acenaphthyl ene_____________| 1.491| 2 , 6-Di ni trotol uene_________| .400| 3-Ni troani 1 i ne______________\ .233| Acenaphthene________________* 1.205|2,4-Dinitrophenol ________# .210|4-Nitrophenol _____________* .181
.457 3.5
.345 5.4
.410 8.41 .054 1 .4.315 18.2.282 4.5.324 .1.873 2.5.463 .1.502 2.1.539 1.9
1.088 1 .7.471 10.4
1.405 1.31.947 30,6..381 4.6.137 "41.2
1.204 .1 *.197 6.5 *.173 4.8 *—— —W302602
FORM VII SV-1 1/87 Rev.
7CS E M I V O L A T I L E CONTINUING CALIBRATION CHECK
Name: NET Contract: 68090031
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
Instrument ID: DARYD C a l i b r a t i o n Date: 2/ 8/91 Time: 8:27
Lab F i l e ID: D8568 I n i t . C a l i b . Date(s): 2/ 7/91 2/ 7/91
Min RRF50 for SPCC(*) - .050 Max %0 for CCC(«) - 25.0%
(1) Cannot be separated from Diphenylamine
COMPOUND
Dibenzofuran2.4-DinitrotolueneDi ethyl p h t h a l ate4-Chl orophenyl -phenyl ether_Fluorene4-Ni troani 1 ine4 , 6-Di ni tro-2-methyl phenol _N -N i t r osodi phen y 1 ami n e (1) _4 -B r omophen y 1 -pheny 1 e t her _Hexachl orobenzenePentachl orophenol ^Phenan threneAnthraceneDi - n - b u t y l p h t h a l ateF 1 uoran thenePyreneB u t y l b e n z y l p h t h a l a t e3 .3'-DichlorobenzidineBenzo(a)anthraceneC hr y senebis(2- Ethyl hexyl)phthal at e_Di -n-octylphthalateBenzo(b)fluorantheneBenzo(k)fluorantheneBenzo(a)pyr ene *Indeno(l,2, 3-cd)pyr ene ______Di ben z.( a. h) anthraceneBenzo(q.h.i )perylene
Ni trobenzene-d52-Fluorobip heny 1Terpheny 1 -d 1 4P henol -d62 - Fl uo r ophenol2 . 4,6-Tribromophenol
RRF
1 .720.564.899. 686
1 .375. 192. 169
* .451. 266.386
» .2511.1161 .0581 . 440
» 1 .3241.411. 694. 224
1 .3701 . 266.978
• 1.6511.5101 . 031
> 1 . 1761 .055.947.897
. 4141 .2611 . 0841 .3551.135.374
1RRF50 |--- —— (•1.611|.522|.818|.642 |
1 .329). 184 |. 1 67 |.428 |.252).376).243|
1 .062 |1 .049|1 .333 |1.213|1 .380 |.633|. 180 |
1.32311 . 196|.909|
1 .392|1.252|.948 |
1 .094|,957|.923|.950 |
.425 |1 .305 |1 .039 |1 .344 |1.110|.3721
1
%D
6.37.59.06.43.34. 11 .45. 1 •5.52.53.5 *4.9 |.9
7.58.4 *2.28.8
19.63.45.57.015.7 *17.18.17.0 *9.32.5 .6.0
2.73.54. 1.8
2.2.5
HR302603
544FORM VII SV-2 1/87 Rev.
IB EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ______________
I| SBLKW1
Lab Name: NET Contract: 68D90031 I
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000.0 (g/mL) ML Lab F i l e ID: 08558
Level: (low/med) LOW Date Received: O/ O/ 0
% Moisture: not dec. 100. dec. 0. Date Extracted: 1/28/91
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 2/ 7/91
GPC Cleanup: (Y/N) N pH: .0 D i l u t i o n Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
i u Q y 3 £H 1-44-4----
541-73-1----106-46-7----100-51-6----95-50-1 ----95-48-7----108-60-1----106-44-5----621-64-7----67-72-1----o ~y? 3
O O / 3 3
105-67-9----65-85-0----
1 1 1-91-1----120-83-2----120-82-1----91-20-3----106-47-8----O / D O J
59-50-7----91-57-6----77-47-4----< J O U O t
95-95-4----91 K Q _ *7 _ .
88-74-4----131-1 1-3----_ C U O ; J O o
606-20-2----
- --Phenol•---bi s(2-Chloroethyl )ether ___-- -2-Chl or ophenol
•---1 ,3-Dichlorobenzene•---1 , 4-Di chl orobenzene•---Benzyl alcohol---1 ,2-Dichlorobenzene•---2-Methylphenol---bi s(2-chloroi sopropyl)ether---4-Methylphenol---N-Ni troso-di -n-propyl ami ne __•---Hexachl oroethane---Ni trobenzene• - - - I sophor one•---2-Ni trophenol•---2,4-Dimethyl phenol- - -Benzoi c acid•---bi s( 2-Chl o roe thoxy )me t hane __---2,4-Diehlorophenol
•---1 ,2,4-Trichl orobenzene•---Naphtha! ene.---4-Chl oroani 1 ine•---Hexachl orobutadi ene•- --4-Chl or o-3-met hyl pheno 1 ____---2-Methylnaphthalene
• - - -He xac hi oroc y c ! open t ad i ene __---2, 4 , 6-Tri chl orophenol•---2,4,5-Trichloropheno!---2-Chl oronaphthal ene•---2-Nitroani line- --Di me thy Iphthalate•---Acenaphthylene•---2. 6-Dini trotoluene
10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.50.10.10.10.10.10.10.10.10.10.10.50.10.50.10.10.10.
1|U|UIU|UIUIUIUIU|UIU|U|UI«JIUJU|U|U|U|UIU|UIU|UIUIU|U|U
AFJJ026IUIUIU1
*
m ii 5581
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE N0-I ——'——
ab Nam«: NET Contract: 68D90031 | S8LKW1
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x : (soil/water) WATER Lab Sflmp1e j - .
Sample wt/vol: 1000.0 (g/mL) ML Lab F,-, e IQ. D8558
Level: (low/med) LOW Datft Rccttiv<>d. 0/ Q/ Q
% Moisture: not dec. 100. dec. 0. Date Extracted: 1/28/91
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 2/ 7/91
GPC Cleanup: (Y/N) N pH: .0 Dilution Factor: 1.00
fAf un CONCENTRATION UNITS:CAS N0- COMPOUND (ug/L or ug/Kg) UG/L Q
83-32-9----51-28-5----100-02-7----132-64-9----121-14-2----84-66-2----
7005-72-3----86-73-7----100-01-6----S'34-52-1 ---•J v —r -J £. i
86-30-6----101-55-3----1 18-74-1 ----O / O O v
O 9 U 1 - o - —120-12-7----84-74-2----
4 U O ** H U
129-00-0----
91-94-1----56-55-3----
_ l O w 1 j
117-81-7----117-84-0----205-99-2----4 U / U O 3
50-32-8----193-39-5----53-70-3----191-24-2----
•---3-Ni troani 1 ine----Acenaphthene•---2,4-Dinitrophenol•---4-Ni trophenol•---Di benzofuran•---2,4-Dini trotoluene•---Di ethylphthalate•---4-Chlorophenyl -phenyle ther _•---Fl uorene•---4-Ni troaniline•---4, 6-Dini tro-2-methyl phenol __•-- -N -N i t ro sodi phenyl ami ne (1) __• -- -4- Br omopheny 1 -pheny 1 e t he r __•---Hexachl orobenzene•---Pentachlorophenol•---Phenanthrene• - - -An thr acene•---Di -n-butyl phthal ate•---Fluoranthene• ---Py r ene•---Butylbenzylphthal ate•---3,3'-Dichlorobenzidine•---Benzo(a)anthracene• - --Ch r y sene•---bis(2-Ethylhexyl)phthalat e __•---Di -n-octylphthalate•---8enzo(b)fl uoranthene----8enzo(k )fluoranthene•---Benzo(a)pyrene-~--Indeno(l,2.3-cd)pyrene•---Di benz (a . h) anthracene----8enzo(g.h.i )perylene
50.10.50.50.10.10.10.10.10.50.50.10.10.10.50.10.10.10.10.10.10.20.10.10.
10.10.10.10.10.
!Sfl
i uuuuuuuuuuuuuuuuuuuuuuuuJ
uuuu
*$G261
>559
(1) - Cannot be separated from di p h e n y l a m i n e
FORM I SV-2 1/87 Rev
3EWATER PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
b Name: NET Contract: 68D90031
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
M a t r i x S p i k e - EPA Sample No.: CAU93
COMPOUND
GAMMA-BHCHEPTACHLORALORINDIELDRINENORIN4.4 '-DOT
S P I K EADDED(UG/L )
. 20
.20
.20
.50
.50
.50
SAMPLECONCENTRATION
(UG/L )
.00
. 00
.00
.00
.00
.00
MSCONCENTRATION
(UG/L )
. 10
.09
. 10
.27
.28
.30
MS%
REC *
v. 51 •'T3-52545760
QC |L IMITS!REC. |—— ...|56-1 23)40-131 |40-120)52-126)56-121 |38-127)
1
COMPOUND
GAMMA-BHCHEPTACHLORALDRINDIELDRINENDRIN4.4 '-DOT
SPIKEADDED(UG/L )
.20
.20
.20
.50
.50
.50
MSDCONCENTRATION
(UG/L )
. 14
. 1 1
. 14
. 36
.37
.46
MSD%
REC *
685768717492
%RPD *
29 •29 »28 *28 •27 *43 »
QC LRPD
152022132127
IMITSREC.
56-1 2340-13140-1 2052-1 2656-12138-127
* Column to be used to flag recovery and RPO values with an asterisk
* Values outside of QC l i m i t s
RPD: 6 out of 6 outside l i m i t sSpike Recovery: 1 out of 12 outside l i m i t s
COMMENTS:
HR302&II 6FORM III PEST-1 1/87 Rev.
8DPESTICIDE EVALUATION STANDARDS SUMMARY
Lab Name: NET Contract: 68D90031
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
Instrument ID: SYA1 GC Column ID: DB-608
Dates of Analyses: 2/20/91 to 2/21/91
E v a l u a t i o n Cheek for L i n e a r i t y
PESTICIDE
ALDRINENDRIN4.4'-DDTDBC
| CALIBRATION| FACTOR| EVAL MIX A
| 4066134.| 2171500.| 2645825.| 2602540.1
CALIBRATIONFACTOR
EVAL MIX B
4031834.2649667.2837950.2532530.
CALI BRATIONFACTOR
EVAL MIX C
4368400.2954067.3137994.2546010.
| %RSD
| 10.0%)|. .....1 4^I -'Ts . 2 .1 i.'s1
(1) If > 10.0% RSD, plot a standard curve and determine the ngfor each sample in that set from the curve.
E v a l u a t i o n Check for 4,4'-DDT/Endrin Breakdown(percent breakdown expressed as total degradation)
11(.. ..........| INITIAL
1 | EVAL MIX B2| EVAL MIX B3| EVAL MIX B415161718191
10111 11 211 3 1141
1
DATEANALYZED
2/20/912/20/912/21/91
. . .'
TIMEANALYZED
1 1 :2323:438:26
, ,
ENDRIN
8.49100.0012.84
?•
4,4 '-DOT
.00
.0014.81
COMBINED(2) |
--"--"I1
3.687.90 |13.87 |
(1)
(2) See Form instructions AR3026I2683
FORM VII I PEST-l 1/87 Rev,
80PESTICIDE EVALUATION STANDARDS SUMMARY
ab Name: NET Contract: 68D90031
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
Instrument ID: SYA1 GC Column ID: 08-608
Dates of Ana l y s e s : 2/20/91 to 2/21/91
Evaluation Check for L i n e a r i t y
PESTICIDE
A L D R I NENDRIN4 ,4 '-DOT ____DBC
CALIBRATIONFACTOR
EVAL MIX A
4066134.2171500.2645825 .2602540.
CAL IBRATIONFACTOR
EVAL MIX B————————————
4031834.2649667.2837950.2532530.
CAL IBRATIONFACTOR
EVAL MIX C
4368400.2954067.3137994.2546010.
%RSD
10.0%)
4-rS--UL_2-8.61 .5
(1) If > 10.0% RSD, plot a standard curve and determine the ngfor each sample in that set from the curve.
Evaluation Check for 4,4 '-DDT/Endrin Breakdown(percent breakdown expressed as total degradation)
1234567891011121314
INITIALEVAL MIX BEVAL MIX BEVAL MIX B
DATEANALYZED----------
2/20/912/20/912/21/91
•TIMEANALYZED
11 :2323:438:26
-
ENDRIN
8.49100.0012.84
4,4 '-DOT
.00
.0014.81
COMBINED(2)
3.687.90
13.87
(1)
(2) See Form instructions. Hn3026f3
685FORM V I I I PEST-l 1/87 Rev.
8EPESTICIDE EVALUATION STANDARDS SUMMARY
E v a l u a t i o n of Retention Time Shift for D i b u t y 1 c h l o r e n d a t e
Lab Name: NET Contract: 68D90031
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
Instrument ID: SYA2 GC Column ID: OB-5
Dates of Ana l y s e s : 2/20/91 to 2/21/91
1234561891011121314151 617181920212223242526272829303132333435363738
EPASAMPLE NO.
EVALAEVAL8EVALCINDAINDBTOXAPHAR1016AR1221AR1232AR1242AR1248AR1254AR1260ZZZZZZZZZZZZZZZZZZZZZZZZZE V A L B 0ZZZZZZZZZZZZZZZZZZZZPBLKS1INDA 01CAU97CAU97MSCAU97MSDCAU98EVALBINDA 02INDB 01
LAB SAMPLEID
DATEANALYZED
2/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/91
TIMEANALYZED
10:401 1 :2312:0712:5013:3414:1815:0115:4516:2817:1217:5518:3919:2220:0620:4921:3322:1623:0023:430:271:111 :542:383:214:054:485:326: 156:598:269:09
. 9:52
%D .
.0
. 1
. 1
.2
.2
.2
.2
. 1
. 1
. 1
. 1
. 1
.1
. I
. 1
. 1
.1
. 1
.2
. 1
. 1
. 1
. 1
. 1
.2
. 1
.1
. 1
.1
. 1
.0
. 1
•"-
1
* Values outside of QC l i m i t s (2.0% for packed col un&S,3 0 2 6 f 0.3% for c a p i l l a r y columns)
page 1 of 1FORM V I I I PEST-2 1/87 Rev,
8EPESTICIDE EVALUATION STANDARDS SUMMARY
E v a l u a t i o n of Retention Time Shift for D i b u t y 1 c h l o r e n d a t e
b Name: NET Contract: 68D90031
Lab Code: NET Case No.: 15741 SAS No.: S D G N o . : C A U 9 3
Instrument ID: SYA2 • GC Column ID: DB-5
Dates of A n a l y s e s : 2/20/91 to 2/21/91
12345678910111213141516171 81920212223242526272829303132333435363738
EPASAMPLE NO.
EVALAEVALBEVALCINDAINDBTOXAPHAR1016AR1 221AR1 232AR1242AR1248AR1254AR1260PBLKW1CC812CCB13CAU93CAU94EVALB 0CAU93MSCAU93MSDCAU96CAU99ZZZZZINDA 01HillZZZZZZZZZZZZZZZEVALB 0INDA 02INDB 01
LAB SAMPLEID
| DATE| ANALYZED|..- —— ——— -I 2/20/91
2/20/912/20/912/20/912/20/912/20/91
| 2/20/91| 2/20/91
2/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/20/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/912/21/91
TIMEANALYZED
10:401 1 :2312:0712:5013:3414:1815:0115:451 6 :-2 817:1217:5518:3919:2220:0620:4921 :3322: 1623:0023:430:271:111 :542:383:214:054:485:326: 156:598:269:099:52
%D -
.0
. 1
. 1
.2
.2
.2
.2
.1
. 1
. 1
. 1
. 1
.1
. 1
. 1
. 1
. 1
. 1
.2
. 1
. 1
. 1
.1
. 1
.2
.1
. 1
. 1
. 1
. 1
.0
. 1
•
* Values outside of QC l i m i t s (2.0% for packed c o 1 uftiDsO fl O £ I C0.3% for c a p i l l a r y columns) ' »fvOU_:OlO 683
>age 1 of 1FORM V I I I PEST-2 1/87 Rev.
9PESTICIDE/PCS STANDARDS SUMMARY
Lab Name: NET Contract: 68090031
Lab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
Instrument ID: SYA2 GC Column ID: D8-5
COMPOUND
ALPHA-BHCBETA-BHCDELTA-BHCGAMMA-BHC ___HEPTACHLOR ___ALDRINH«pt . Epox i deENDOSULFAN I_DIELDRIN4.4'-DD£ENDRINENDOSULFAN II4,4'-OOD ____Endo . sulfate4.4 '-DOTMETHOXYCHLOR_ENDRIN KETONEa . Chl ordaneg . Chl ordaneTOXAPHENEAROCLOR-1016AROCLOR-1 221AROCLOR-1232AROCLOR-1242AROCLOR-1248AROCLOR-1 254AROCLOR-1260
DATE(S) OF FROM: 2/20/91A N A L Y S I S TO: 2/20/91TIME(S) OF FROM: 12:50ANALYSIS TO: 13:22
FRT WIls
FROM
9.85 9.7810.67 10.5911.57 11.4910.81 10.7313.04 12.9414.15 14.0515.55 15.4316.77 16.6517.69 17.5617.80 17.6718.41 18.2718.77 18.6319.27 19.1320.31 20.1520.60 20.4422.76 22.5921 .88 21 . 7116.37 16.2416.90 16.7821.77 21.6113.61 13.519.90 9.83
12.63 12.5412.63 12.5415.94 15.8218.03 17.8920.74 20.58
{TIDOW
TO
9.9310.751 1 .6610.8913.1414.2615.6616.9017.8217.9418.5518.9119.4220.4620.7522.9322.0416.4917.0321 .9313.719.9712.7212.7216.0618. 1720.90
1
CALIBRATIONFACTOR
2607700.1613675.2192075.2440650.2629150.2792550.2828450.2466725.2386775.2231950.1969000.2494650.2048775.2624400.1564700.881155 .3097300.2860225.2871750.
61756.187812.74043.80043.165279.293013.202870.240293 .
DATE OF ANALYSIS 2/21/91TIME OF ANALYSIS 9 :09EPA SAMPLE NO.(STANDARD) INDA 02
RT
10.8113.0514. 1715.5616.7917.71
18.80
I20.6322.79
1
CALIBRATIONFACTOR
2383500.2555950.2552700.2785200.2410275 .2311625.
2443300.
1285250.777785 .
1
1QNTY/N
yY\e
y
Y
YYYw
YYYvYYYYYYYYYYYY
%0
2.32.89.61 .52.33. l'
=al- —— 4
\ \1
1
Under QNT Y/N: enter Y if quantitation was performed, N if not performed.%D must be less than or equal to 15.0% for quantitation, and less thanor equal to 20.0% for confirmation.
Note: Determining that no compounds were found above the CRQL is a form ofquantitation, and therefore at least one column must meet the 15.0% c r i t e r i a
For mu1ticomponent analytes, the largest single peak that is characteristicof the component should be used to establish retention time aflf?^?19K j f\Identification of such analytes is based p r i m a r i l y on pattern recognition.
page 2 of 3FORM IX PEST 1/87 Rev
9PESTICIDE/PCS STANDARDS SUMMARY
Name: NET Contract: 68D90031
ab Code: NET Case No.: 15741 SAS No.: SDG No.: CAU93
nstrument ID: SYA2 GC Column ID: D8-5
COMPOUND
ALPHA-BHCBETA-8HCDELTA-BHCGAMMA-BHC ___HEPTACHLOR ___| ALDRIN| Hep t . Epoxi deIENOOSULFAN I_| DIELDRIN»4'-DDE
DRINDOSULFAN II
4T4'-DDOEndo. sulfate4.4 '-DOTMETHOXYCHLOR_ENDRIN KETONEa. Chlordaneg. ChlordaneTOXAPHENEAROCLOR-1016_AROCLOR-1 221AROCLOR-t 232AROCLOR-1 242AROCLOR-l 248AROCLOR-1 254| AROCLOR-1 260
DATE(S) OF FROM: 2/20/91A N A L Y S I S TO: 2/20/91TIME(S) OF FROM: 12:50ANALYSIS TO: 19:22
fRT Wlf
FROM
9 .8510.671 1 .5710.8113 .0414.1515.5516.7717.6917.8018.4118.7719 .2720.3120.6022.7621 .8816.3716.9021 .7713.619.90
12.6312.6315.9418.0320.74
9.7810.591 1 .4910. 7312.9414.0515.4316. 6517.5617.6718. 2718 . 6319.1320. 1520. 4422.5921 .7116. 2416.7821 .6113.519.83
12.5412.5415.8217.8920.58
RTJDOW
TO
9.9310.751 1 .6610.8913.1414.2615.6616.9017.821 7.9418.5518.9119.4220. 4620.7522.9322.04.16.4917.0321 .9313.719.97
12.7212.7216.0618.1720.90
1
CALIBRATIONFACTOR
-----------2607700.1613675.2192075.2440650.2629150.2846150.2828450.2466725.2386775.2231950.1969000.2494650.2048775 .2624400.1564700.881 155 .3097300.2860225 .2871750.
61756.187812.74043.80043 .165279.293013.202870.240293.
DATE OF A N A L Y S I S 2/21/91TIME OF ANALYSIS 9:09EPA SAMPLE NO.(STANDARD) INDA 02
RT
10 .8113 .0514.1715 .5616.7917,71
18 .80
20 .6322.79
CALIBRATION QNTFACTOR |Y/N
2383500.2555950.2552700.2785200.2410275.2311625.
2443300 .
1285250.777785.
YYYYYYYYYYYYYYYYYYYYYYYYYYY
%0
2. 32.8
10.31 .52.33. 1
2 . 1
.- ——— 1LJ_?.9
11.7
—————
—————
Under QNT Y/N: enter Y if quantitation was performed, N if not performed.%D must be less than or equal to 15.0% for q u a n t i t a t i o n , and less thanor equal to 20.0% for confirmation.
Note: Determining that no compounds were found above the CRQL is a form ofq u a n t i t a t i o n , and therefore at least one column must meet the 15.0% c r i t e r i a .
r mu 1 ticomponent analytes, the largest single peak that is characteristicthe component should be used to establish retention time an^f^>30 2 6 1.7t i f i c a t i o n of such analytes is based p r i m a r i l y on pattern recognitno^jC
page 2 of 3FORM IX PEST 1/87 Rev.
Appendix ETelephone Log
8R3026I8
Lib
Contact:
Call WtUt«^ By: __
In rtf«rerKt to d*t» fcr th«
-9
(1) '.w Cooy, (,} ftt^
In Jtftfts'vm to
ContractRZGK UUVLA-50RATORY COWMVNICATKN SYSTEM
T«kphone R«cord
Date o. C*il: :f
Laboratory Na/n«: ____/I/? TLab Contact: __
f SContact: ^
Call Wtiat«<i By: __ laboratory __ R«|ion
In r«fefenc« to data for th« /oUowjng sample
Summary of Qu«stion./Is_u<3 Disoj3S«d:(9 ~Zrr- Bt.s f
Summary of RtsoJution:
U.<L*J>
Oa:«AR302620
Oi.:.-.outicr>: (:; ',10 Copy, (2; R^jon Ccpy, ij) <MO C:cy
tfviiTW, ,
R_£.
NETSEMjY:.NET MJDWEST_______: 5-28-91 : 15:53 ; NETJ>_Jm£TT- 3014173
NiT MMw»«t Ine.MATIDWAI 8«ft'f<t otvl*toflINMI IWIN/AI. 850 WMt rt ,ENVIRONMENTAL *•«•«• «•601MTESTING, INC. w
F«x: (708) 289-5445
FAX TRANSMISSION NOTICE
To: 77*",? -7~/»p £6**? ______________Company: ________________ PAX NO: /- / ' VX ?• ' 2 */ f>
Sender: fflt /&**?. A/T faictr.** f 22+ < _________" " ~~~ — "
You should receiv* panes / including thi* notic«. If youdon't receive all pages, please call the sender immediately.This transmission includes:
letter/memootherproject notes (Project ID: _________ _______ .)analytic*! report (s) t
Sanple No(s)i ________ _______ ________
CCS
f n 30262I J
15:54 :
IEV O L A T I L E ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
TI« : NET Contract: 68D90031
ode: NET Case No.: 15741 SAS No.: $DG Ne.: CAU93
ix: (soil/water) WATER Lab Sample ID:
i p l e wt/vol: 5.0 (g/mL) ML L»b F i l e ID: F3699
•vel: (1ow/m«d) LOW Date R e c e i v e d : 1/24/91
'•, Moisture: not dec. 100. Date Analysed: 1/29/91
Column: (pack/cap) CAP D i l u t i o n Factor: 1,00
CONCENTRATION UNITS:Number TICt found: 1 (ug/L or -jg/Kg) UG/L
CAS NUMBER
1 . 75-13-12.3.4.5.6.7.8.9 .10.11 .12.13.14.IS.16.17.18.19.20.21 .
. 22.23 .24.25.2G.27.29.23.30.
COMPOUND NAME
Ethane, !,l,2-trieh1oro-l,2,
-... , ,.., ... ...
RT
4.31
»
FST. CONC.
40.
*
JH3Q2&;
iQj
l
— ii
1,-, 17 2 |(e
FORM I VOA-TIC 1/87