Aam °cora ve IteAam (into ° °cora five Ite bLR SCANNED FEB 1 7 2012 Prepared by: Fremont Environmental Inc. 1530 North Boise Avenue, Suite 205 Loveland, Colorado 80538 (970) 663-2301

COMPREHENSIVE IVESTIGATION

KANEB PIPE LINE OPERATING PARTNERSHIP, L. P.

ANDOVER PIPELINE RELEASE

ANDOVER, KANSAS

FREMONT PROJECT NO. CO01-031

4 COO,

Aam (into ° °cora five Ite

bLR SCANNED

FEB 1 7 2012

Prepared by:

Fremont Environmental Inc. 1530 North Boise Avenue, Suite 205

Loveland, Colorado 80538 (970) 663-2301

November 14, 2003

RECEIVED MAY 0 1 2006

BUREAU OF ENVIRONMENTAL REMEDIATION

TABLE OF CONTENTS

1.0 INTRODUCTION 1 2.0 HISTORICAL EVALUTATION AND SITE DESCIPTION 1

2.1 PROPERTY LOCATION 1 2.2 PROPERTY HISTORY 1 2.3 PREVIOUS INVESTIGATIONS 2

3.0 STUDY AREA INVESTIGATION 2 3.1 SITE SUBSURFACE CONDITIONS 2 3.2 HUMAN/TARGET POPULATIONS 3 3.3 AREA WATER WELL SURVEYS 3 3.4 ECOLOGICAL TARGET SURVEYS 3

4.0 SOURCE CHARACTERIZATION 3 4.1 CONTAMINANT SOURCE AREAS 3 4.2 IMPACTED SOIL AND GROUNDWATER 4

4.2.1 SOIL 4 4.2.2 GROUND WATER 4

5.0 NATURE AND EXTENT CHARACTERIZATION 5 5.1 SOILS AND VADOSE ZONE 5 5.2 GROUND WATER 5 5.3 CONTAMINANT FATE AND TRANSPORT 5 5.4 IDENTIFICATION OF POTENTIAL RECEPTORS AND LAND USE 5

6.0 IDENTIFICATION OF CORRECTIVE ACTION ALTERNATIVES 6 6.1 GROUND WATER REMEDIATION ALTERNATIVES 6 6.2 SOIL REMEDIATION ALTERNATIVES 7 6.3 ADDITIONAL STEPS 8

7.0 REMARKS 9

Tables

Table 1: Soil Analytical Results Table 2: Summary of Ground Water Chemistry

Figures

Figure 1: Figure 2: Figure 3: Figure 4: Figure 5: Figure 6:

Site Location General Site Layout Ground Water Table Elevation Map (October 2, 2003) Ground Water Analytical Map (October 2, 2003) Soil Chemistry Map (April 21-23 and August 5, 2003) Cross Section

Appendices

Appendix A: Fremont's Standard Sampling Methods and Procedures Appendix B: Ground Water Laboratory Reports, Quality Control Data, and Chain-of-Custody

Documentation Appendix C: Cross Section and Boring Logs

COMPREHENSIVE INVESTIGATION

KANEB PIPE LINE OPERATING PARTNERSHIP, L. P.

ANDOVER PIPELINE RELEASE

ANDOVER, KANSAS

FREMONT PROJECT NO. C001-031

1.0 INTRODUCTION

This document is Fremont Environmental Inc.'s (Fremont's) Comprehensive Investigation (CI)

for Kaneb Pipe Line Operating Partnership, L.P.'s (Kaneb's) pipeline release east of Andover,

Kansas. The objective of this report is to summarize the data generated during the site

investigation. The investigation was conducted to determine the extent of hydrocarbon impacts to

the soil and groundwater. This report discusses the findings of the CI required by the Kansas

Department of Health and Environment (KDPHE's) Bureau of Environmental

Remediation/Remedial Section and defined in the guidance document entitled Scope of Work

(SOW) for a Cl/Corrective Action Study (CAS).

2.0 HISTORICAL EVALUTATION AND SITE DESCIPTION

2.1 PROPERTY LOCATION The release site is located near the town of Andover in Butler County, Kansas in the northeast

quarter of the southeast quarter of Section 8, Township 27 South, and Range 3 East. As shown

on Figure 2, the release occurred on the private property of Mr. Charles Rector located at 1511

Capital Street in the Easter's 1st Addition.

2.2 PROPERTY HISTORY On April 20, 1990, Mr. Charles Rector reported to Kaneb the presence of petroleum staining on soil

near his garage over a subsurface petroleum transportation pipeline operated by Kaneb. Kaneb

responded by excavating and replacing the section of pipeline in the affected area. Forty-six feet of

pipeline were replaced. A hairline crack was observed in the pipeline. Soil surrounding the

pipeline showed visual contamination of gasoline and/or diesel fuel. Approximately two to three

cubic yards of visibly petroleum-contaminated soil were removed and treated by land farming at a

Kaneb facility in El Dorado, Kansas.

On December 18, 1992, Charles Rector reported possible petroleum contamination of his drinking

water well to Kaneb. Kaneb collected a water sample from his tap on the same date. Laboratory

Comprehensive Investigation Kaneb Pipe Line Operating Partnership, L.P. Andover Pipeline Release Andover, Kansas Fremont No. CO01-031 Page 2

analysis of the sample indicated the presence of 11.0 micrograms per liter (pg/L) of benzene which

exceeded the federal Maximum Contaminant Level (MCL) of 5.0 pg/L for this contaminant. Ethyl

benzene, toluene and xylenes were also present in the sample but at concentrations below their

respective MCLs. A subsequent sample of the Rector tap water, collected on December 22, 1992,

showed 4.0 pg/L of benzene as well as trace levels of toluene and xylenes.

KDHE sampled the Rector well and two other nearby residential water supply wells at 16185

Capital Road and 1701 Glenda Court on December 29, 1992. 1,2-Dichloroethane was detected at a

concentration below its MCL in the Rector well. The residential well at 1701 Glenda Court

contained 8.6 pg/L of benzene and a low concentration of xylenes. No other petroleum constituents

were detected in these samples.

Kaneb began providing bottle water to the Rector residence and the Laymon residence at 1701

Glenda Court in December 1992. Kaneb had a carbon canister filtration system installed at the

Rector residence in January 1993.

2.3 PREVIOUS INVESTIGATIONS A limited Preliminary Site Investigation was conducted in January 1994 by Superior

Environmental Company (SECO). Field activities included drilling of five boreholes and field

screening of subsurface soil samples. Four of the five boreholes did not have observable

indications of petroleum contamination. However, petroleum contamination was observed at SB-

5, which was ultimately completed as monitoring well MW-1. The other four boreholes were not

completed as monitoring wells. SECO's report recommended further investigation of the site.

3.0 STUDY AREA INVESTIGATION

3.1 SITE SUBSURFACE CONDITIONS The vadose zone soil is generally composed of clay from the surface to a depth of approximately

15 feet. Thin limestone layers were encountered in the southern-most borings at 13 to 17 feet

below grade. The clay layer is underlain by a weathered claystone containing silt and/or sand,

and/or a siltstone. The boring logs and a cross-section (Figure 6) are provided in Appendix C.

The depth to ground water is approximately 22 feet below the ground surface (bgs). Based on the

water table elevation data, the ground water flow direction is towards the south.


3.2 HUMAN/TARGET POPULATIONS The Kaneb release site is located east of Andover, Kansas in Butler County. While the release

occurred in a residential section, the land use surrounding the release site is primarily agricultural.

The 1st Addition neighborhood comprises approximately 20 acres and is surrounded by

agricultural property towards the north, south, east and west. Highway 35 is located just north of

the neighborhood. The population of Andover is approximately 7,000.

3.3 AREA WATER WELL SURVEYS There were no state or federal registered water wells or public water supply systems identified

within a half mile radius of the property. However, we are aware of several private unregistered

wells, including the wells at 1511 Capital Road, 16185 Capital Road, and 1701 Glenda Court.

3.4 ECOLOGICAL TARGET SURVEYS

As described above, the Kaneb release site is located in a rural area east of Andover. There were

no designated critical habitats for threatened or endangered wildlife species identified on or

adjacent to the site. The majority of contamination identified at the site includes petroleum-based

constituents detected in the ground water. As no surface sources of contamination exist,

ecological exposure to contaminants is not expected. •

sp-

4.0 SOURCE CHARACTERIZATION

A medial vestigation was initiated on April 21, 2003 to determine the source and extent of

impac e soil and ground water. This investigation was based on the October 4, 2002 Dr

Work Plan and subsequent modifications as agreed to with KDHE. Eight soil borings were

drilled and five were completed as ground water monitoring wells. After this initial phase of

investigation, additional monitoring wells were proposed to further define the extent of

contamination; four additional wells were installed on August 5, 2003. The results of this

investigation are described below.

4.1 CONTAMINANT SOURCE AREAS The 1992 pipeline release is considered the only source of contamination at this location. There are

no other known petroleum releases in the area. The pipeline is located approximately three feet

below ground. The release from the hairline crack in the pipeline occurred over an unknown period

of time.


4.2 IMPACTED SOIL AND GROUNDWATER

4.2.1 SOIL Soil samples were collected from the initial borings on April 21 through 23, 2003 as shown on

The samples were collected in accordance with the protocol outlined in Appendix A

and the CI Work Plan. These samples were submitted to Pace Analytical Services Inc. (Pace) of

Lenexa, Kansas for analyses of Total Petroleum Hydrocarbons (TPH) — Gasoline Range Organics

(GRO) by Method OA1; benzene, toluene, ethylbenzene and xylene (BTEX) b EPA Method

8021; and Total E xactable Hydrocarbons (TEH) by Method 0A2.

Soil samples were also ollected from the borings advanced on Au 5, 2003. These samples

were submitted to Techn logy Laboratory, Inc. of Fort Collins, C orado for analyses of TPH-

GRO using EPAModified Method 8015B, BTEX by EPA Marhod_ 8260B and TPH — Diesel

Range Organics (DRO) by EPA Method 8015B. Soil analytical data from both sampling dates

are summarized on Figure 5 and in Table 1.

4.2.2 GROUND WATER Ground water samples were collected from the initial five monitoring wells (MW-1, F1, F2, F5 and

F8) and three private wells in April 2003 and from the additional four monitoring wells (F-9

through F-12) in August 2003. Additional water samples were collected from all nine monitoring

wells, as well as the water wells at 1701 Glenda Court and 1511 Capital Street, on October 2, 2003.

The samples were collected in accordance with the protocol outlined in Appendix A. The ground

water samples collected on April 23, 2003 were sent to Pace for OA1, 0A2, and 8021. The

October 2, 2003 samples were submitted to Technology Laboratory for analyses of TPH-GRO

using EPA Modified Method 8015B, BTEX by EPA Method 8260B and TPH — DRO by EPA

Method 8015B.

The October 2, 2003 ground water chemistry is illustrated on Figure 4. Ground water analytical

data are summarized in Table 2. A copy of the laboratories' reports, quality control data, and chain-

of-custody documentation are presented in Appendix B.


5.0 NATURE AND EXTENT CHARACTERIZATION

5.1 SOILS AND VADOSE ZONE The primary contaminants present in the soil at th site include BTEX and TPH-gasoline. Soil

contamination was identified near the water table in borings F-3 and F-7. Screening of soil

samples in the field using a photoionization detector (PID) identified VOCs at or near the water

table in borings F-2, F-3, F-4, and F-7. Petroleum constituents were identified between depths of

15 and 30 feet adjacent to the release only. Contaminant concentrations identified in the

subsurface soil are presented on Figure 5 and in Table 1.

Only one soil sample (F-7) collected at 20 feet bgs exceeded the KDHE Tier 2 risk-based levels

for residential scenarios for the soil pathway. It is located approximately 5 feet north of the

release location. The concentration of TPH-GRO detected in the soil at this location was 1,300

mg/kg. The corresponding KDHE Tier 2 value for TPH-GRO is 220 mg/kg.

5.2 GROUND WATER Elevated BTEX and TPH concentrations in ground water are present at the site as shown in Table

2 and Figure 4. The extent of contamination appears to be defined and concentrated at the release

location.

5.3 CONTAMINANT FATE AND TRANSPORT Petroleum contamination is not present at the ground surface at the site. Therefore, migration of

the contamination will primarily be restricted to transport via ground water flow. Minimal

migration in the vadose zone may occur within the soil vapor. Due to the presence of the water

table in fractured sandstone with clay at the site, contaminant migration via ground water flow

may occur in the lateral direction; significant vertical migration is not expected or evident.

Excavation of contaminated soil and natural attenuation have assisted in decreasing the

magnitude and extent of contamination.

5.4 IDENTIFICATION OF POTENTIAL RECEPTORS AND LAND USE The unregistered water wells adjacent to the release location are potential receptors of the

petroleum contamination. Kaneb has supplied bottled water to the residents at 1511 Capital

Street and 1701 Glenda Court since it was determined that these wells were impacted with


petroleum hydrocarbons. In addition, Kaneb maintains a carbon canister system for the well at

1511 Capital Street.

The data collected in April and October 2003 do not indicate that the private wells are currently

impacted. A December 2002 sample from the 1701 Glenda Court well was reported to contain

low levels of benzene and ethylbenzene, which is surprising in view of the groundwater flow

direction and absence of dissolved hydrocarbons at the Rector well. Subsequent samples from

the 1701 Glenda Court well have not had petroleum constituents that exceed the laboratory

detection limits.

6.0 IDENTIFICATION OF CORRECTIVE ACTION ALTERNATIVES

Based on the data collected during the CI, several remediation alternatives may be appropriate for

soil and ground water contamination at this site. The soil contamination consists of diesel fuel .

and gasoline in a localized area and in clay soil. The ground water contamination is present in a

fractured sandstone unit and is also localized. It should be noted that, since the release occurred

in a residential neighborhood, the potential noise level and hours of operation of temporary or

permanent treatment/remediation equipment of each proposed remedy must be considered.

Fremont believes the following remedial technologies may be effective and appropriate

individually or in combination for this site.

• Chemical oxidation utilizing Fenton's Reagent chemistry via injection for ground

water/smear zone remediation

• In-situ oxygen curtain (iSOC) for ground water remediation

• Temporary soil vapor extraction (SVE) for soil/smear zone remediation

• Natural attenuation for both soil and ground water contamination

6.1 GROUND WATER REMEDIATION ALTERNATIVES For the remediation of petroleum hydrocarbons in ground water, Fremont considers the options

listed below to be feasible approaches.

• Chemical oxidation using Fenton's Reagent chemistry

• In-Situ Oxygen Curtain (iSOC)


• Monitored Natural Attenuation

A remediation approach of chemical oxidation using Fenton's Reagent chemistry would utilize

the in-situ injection of hydrogen peroxide and ferrous sulfate directly into the water-bearing

weathered sandstone unit. Injection points would likely be on 5 to 10 feet grid spacing in the

localized area of ground water contamination. Fenton's chemistry creates the hydroxyl radical

which is a strong oxidizer of organic compounds. Considering the residential setting of the

ground water contamination, a slow injection process would be required with appropriate

subsurface soil vapor monitoring to ensure that the generation of petroleum vapors would not

result in a health and safety concern at the residential dwellings. It is likely that more than one

injection event would be required.

In-situ oxygen curtain (iSOC) units can also be considered for this site. The iSOC units are

submersible devices that are connected via tubing to above-ground, industrial-grade oxygen

bottles. These units allow the diffusion of oxygen into the ground water thereby promoting the

aerobic biodegradation of petroleum hydrocarbon contamination in ground water. This

technology is fairly new to the ground water remediation industry and limited full scale treatment

data is available. However, given the limitations at this site, the use of iSOC units may be

appropriate.

Monitored natural attenuation (MNA) is also a feasible approach at this site. The ground water

contamination plume is localized and does not appear to have migrated significantly since 1990.

However, elevated concentrations of dissolved petroleum hydrocarbon constituents remain in

monitoring well MW-1, which is in close proximity to the release location. Further, the benzene

concentrations in this monitoring well have not decreased over the last two years. Therefore,

MNA does not appear to be an appropriate approach for this site at this time. However, it may be

a feasible approach after other measures are taken to lower the magnitude of dissolved

hydrocarbons near the release point.

6.2 SOIL REMEDIATION ALTERNATIVES For the remediation of the contaminated soil in the vadose zone, Fremont considers the options

listed below to be feasible approaches.


• Excavation

• Soil Vapor Extraction

• Monitored Natural Attenuation

A small amount of petroleum contaminated soil was removed during the initial excavation in

1990. Additional excavation to a deeper depth could be attempted at this time; however, it is

unlikely that a substantial mass of petroleum would be available for removal. In addition, due to

the anticipated depth of the excavation to remove most of the residual petroleum contamination

(approximately 27 feet), the integrity of the garage at 1511 Capital Street will be threatened.

Therefore, soil removal is not recommended.

Temporary SVE may have some beneficial effect at this site, particularly if there is an unsaturated

interval in the fractured water-bearing sandstone. Petroleum contamination in this interval would

likely be due to smearing caused by a fluctuating water table. SVE would have little or no effect

on residual petroleum hydrocarbons in the clay unit. A short term pilot test could be conducted

on monitoring well MW-1 to determine if significant petroleum vapor removal could be

accomplished before water table mounding sealed the fractured sandstone in the monitoring well.

If mounding did seal the fractured sandstone unit, the air flow from the SVE blower could be

reversed to determine whether fresh air could be injected into the unsaturated zone. If this

relatively oxygen-rich air can be injected into the unsaturated zone, it may stimulate aerobic

biodegradation of petroleum hydrocarbon contamination.

If air injection or removal in the unsaturated zone is possible, the operation of this equipment

would be limited by noise considerations. It may be necessary to limit the run time of this

equipment to weekdays during typical business hours to minimize or preclude the disturbance to

the residents.

6.3 ADDITIONAL STEPS In order to further define the appropriate remedial approach for this site, Fremont proposes the

following steps:


• Conduct an SVE pilot test to determine the radius of influence, petroleum hydrocarbon

mass removal opportunity and mounding effects.

• Conduct a chemical oxidation pilot test to determine radius of influence, anticipated

petroleum hydrocarbon degradation and potential health and safety concerns.

Utilizing this additional data, Fremont can make a proposal for the appropriate corrective action

for this site.

7.0 REMARKS

The discussion and recommendations contained in this report represent our professional opinions.

These opinions are based on currently available information and are arrived at in accordance with

currently accepted hydrogeologic and engineering practices at this time and location. Other than

this, no warranty is implied or intended.

This report was prepared by FREMONT ENVIRONMENTAL INC.

Joan Henehan, P.E. Senior Consultant

Reviewed by:

, I (

Date

Date l V. Henehan, P.E.

Senior Engineer

cn Gml 1-1

E•

TABLE 2 SUMMARY OF GROUND WATER CHEMISTRY

Kaneb Andover Pipeline Release Andover, Kansas

Fremont Project No. CO01-031

Rector Well 10/11/01 <0.5 <0.5 <0.5 <0.5 NA <0.5 NA NA NA NA NA NA NA NA NA

12/18/02 <2.0 <2.0 <2.0 <7.0 <10 <0.500 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 NA NA NA

04/23/03 <2.00 <2.00 <2.00 <5.00 <10.0 <0.500 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 NA NA NA

10/02/03 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 NA NA NA NA NA NA NA NA

Dodson Well 04/23/03 <2.00 <2.00 <2.00 <5.00 <10.0 <0.500 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 NA NA NA

Laymon Well 12/18/02 17 <2.0 11 <7.0 <10 <0.500 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 NA NA NA

Glenda Court 04/23/03 <2.00 <2.00 <2.00 <5.00 <10.0 <0.500 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 NA NA NA

Propedy 1W02/03 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 NA NA NA NA NA NA NA NA

MW-1 10/11/01 1,305 154 384 272 NA 8.11 NA NA NA NA NA NA 99.47 NM NA

12/18/02 69 12 4.9 8.7 <10 29.0 <0.5 NA NA NA NA NA 25.20 74.27

04/23/03 3,930 880 540 1,000 <250 21.300 21 <0.40 <0.40 <0.40 <0.40 <0.40 22.69 76.78

10/02103 5,261 1,436 258 1,473 NA 15.1 9.0 NA NA NA NA NA 23.34 76.13

F-1 04123/03 166 298 107 852 49.0 11.000 11 <0.40 <0.40 <0.40 <0.40 <0.40 100.00 2264 77.36

10102103 235 92.8 1.4 459 NA 5.93 191 NA NA NA NA NA 23.29 76.71

F-2 04/23/03 37.5 235 270 1,280 52.7 11.500 4.7 <0.40 <0.40 <0.40 <0.40 <0.40 99.83 22.81 77.02

Duplicate 04/23/03 47.0 297 313 1,620 101 12.400 4.1 <0.40 <0.40 <0.40 <0.40 <0.40 NA NA

10/02/03 358 14.8 44.8 1,130 NA 244 86.2 NA NA NA NA NA 23.55 76.28

Duplicate 10/02/03 469 19.3 23.0 995 NS 254 70.6 NA NA NA NA NA NA NA

F-5 04/23/03 <2.00 <2.00 <2.00 <5.00 <10.0 <0.500 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 98.54 21.47 77.07

10/02/03 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 NA NA NA NA NA 22.17 76.37

F-8 04/23/03 18.9 9.20 2.03 11.8 <10.0 <0.500 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 100.28 22.55 77.73

08/05/03 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 NA NA NA NA NA NM NM

10/02/03 <0.5 <0.5 <0.5 <0.5 NA <0.5 <a5 NA NA NA NA NA 23.58 76.70

F-9 08/05/03 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 NA NA NA NA NA 101.98 NM NM

10/02/03 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 NA NA NA NA NA 25.90 76.08


10/02/03 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 NA NA NA NA NA 25.20 76.07


Duplicate 08/05/03 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 NA NA NA NA NA NA NA

10/02/03 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 NA NA NA NA NA 22.42 78.09


10/02/03 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 NA NA NA NA NA 22.92 76.73

04/21/03 30 <63 <63 <63 <160 <330 <6.300 <13 <13 <13

04/21/03 25 <56 <56 <56 <150 <290 <5.600 <11 <11 <11

04/22103 20 1,300 4,200 3,900 18,000 <350 360.000 370 <14 <14

04/22/03 24 <58 <58 <58 <150 <300 <5.800 <12 <12 <12

04/22/03 24 <63 <63 <63 <160 <330 <6.300 <13 <13 <13

04/22/03 24.5 <62 <62 <62 <160 <320 <6.200 <12 <12 <12

04/22/03 20 1,600 17,000 13,000 91,000 <2900 1,300.000 1000 <11 <11

04/23/03 24 <60 75 <60 300 <12 <12 <12

08/05/03 20 <2 <2 <2 <2 <10 NA NA

08/05/03 20 <2 <2 <2 <2 <10 NA NA

08/05/03 20 <2 <2 <2 <2 <10 NA NA

08/05/03 20 <2 <2 <2 <2 <10 NA NA

<13

<11

<14

<12

<13

<12

<11

<12

NA

NA

NA

NA

KDHE Ties' 2 tink-based leitels, • residential twit pathwa

TABLE 1 SOIL ANALYTICAL RESULTS

KANEB - ANDOVER PIPELINE RELEASE ANDOVER, KANSAS

FREMONT PROJECT NUMBER: CO01-031

-

Map center is UTM 14 665824E 4175725N (NAD27)

Santa Fe Lake quadrangle Projection is UTM Zone 14 NAD83 Datum

FIGURE 1 SITE LOCATION MAP

ANDOVER RELEASE SITE ANDOVER, KANSAS

Project No. Prepared By C001-031 JH Fremont

Date Reviewed By Envionmentat 10-16-03 PVH

I HOUSE

GARAGE

q3 F1 2

CAPITAL ROAD (unsur-fcicoel)

F5

F6 •

F1

l

GARAGE SHED

F3 • •

M• 1 PPROMWat e, • ...---ResAse =ow

SECO-4 - •

F4 • SECO-3

•

DOUBLE-WIDE MANUFACTURED

HOUSE

PA110

F2

WELL HOUSE

SECO22" . •

SECO-1 •

SHED

1511 CAPITAL STREET

GRAVEL DRIVEWAYS

F8413

HOUSE

1607 GLENDA COURT

es

• 0 0

L 3

3

CC D 0 0

0

0

HOUSE

PRIVATEWELL

REMONT NVIRONMENTAL

a EXISTING MONITORING WELL LOCATION

• SOIL BORING LOCATION

oQ PRIVATE WELL LOCATION

PROPERTY BOUNDARY

FENCE LINE

LEGEND

F9

OPEN FIELD w/some laydown

0 10 20 30 40

Scale (feet)

Figure 2

GENERAL SITE LAYOUT

F10 Kaneb Pipe Line Company

Andover, Kansas

Project No. Prepared by Drawn by

C001-031 JMA

Date Reviewed by Filename

11/7/03 01031Q

CAPITAL ROAD (unourface.cd)

76.3

76.7 F8

DOUBLE—WIDE MANUFACTURED

HOUSE SHED

GARAGE SHED

F7 • • •

lAW I APPROXIMATE oe) • c nELEASE LOCATION

SECO-4 •

F4 •

SECO-3 •

F2 nuoe

HOUSE

I SHED I

SECO-1's •

SECO-1 •

OPEN FIELD wisome loydown

F6 •

I WW1IAL JUNLGI

GRAYEL DeryBuys

PATIO 76.3

HOUSE HOUSE

GARAGE

LEGEND

•

(77.36)

EXISTING MONITORING WELL LOCATION

SOIL BORING LOCATION

PRIVATE WELL LOCATION

PROPERTY BOUNDARY

FENCE LINE

GROUND WATER ELEVATION (feet above arbitrary datum)

WATER TABLE CONTOUR (feet above arbitrary datum)

GROUND WATER FLOW DIRECTION

NM NOT MEASURED

1607 GLENDA COURT

a

3 • C 3

I-

J 0

0 z

a

HOUSE

PRIVATE WELL

7cl

Fl I

F12 (*Z$

0 10 20 30 40

Scale (feet)

Fg may e)

F10 0.04(b

Figure 3

GROUND WATER TABLE ELEVATION MAP OCTOBER 2, 2003

Kaneb Pipe Line Company Andover, Kansas

Project No.

C001-031

Date

11/12/03

Prepared by

Reviewed by

Drawn by

JMA

Filenome

01031Q

REMONT NVIRONMENTAL

CAPITAL ROAD (1..inmurfac6sel)

GARAGE

PATIO

F2

F7 F3 •

:-...._ •

MW1 -'`' APPRORMAlE al • .---RELE.SE LOCATION

•

5261`.• T 1436 ....,

•c O4 •

• 0 1473256 SEC-

•......,.

G 15.1 -4:tL!•.z. 0 9.0

F4 •

Fl

235 1511 CAPITAL STREET 1 92.0 E 1.4 X 459 C 5.93 O 191

GRAVEL ORIVEMAK

F8q3 9 <0.5 T <0.5 E <0.5 X <0.5 G <0.5 • <0.5


SHED HOUSE

SECO-3 SECO-72' • • •

SECO-1 •

z

OPEN FIELD w/sorm loydown

3 I

3

I-X D 0 O

0 z J 0

• 1607 GLENDA COURT

B <0.5 T <0.5 E <0.5 X <0.5 G <0.5 D <0.5

BENZENE (ug/L) TOLUENE (ug/L) ETHYLBENZENE (ug/L) TOTAL XYLENES (ug/L) TPH-GRO (mg/L) TPH-DRO (mg/L)

HOUSE PRIVATE WELL B <o4' T <03 E <0.5 • <0.5 • <03 D <03

8 <0.5 T <0.5 • <0.5 • <0.5 • <0.5 D <0.5

F11 425

I 0 10 20 30 40

Scale (feet)

(0.5 T <0.5 E <0.5 x <0.5 C <0.5 O <0.5

HOUSE

GARAGE

HOUSE

.1) • 0

LEGEND

•




13 <0.5 T <0.5 E <0.5 x <05 C <0.5 D <0.5

ib F12

PROPERTY BOUNDARY

FENCE LINE

Figure 4 GROUND WATER ANALYTICAL MAP

OCTOBER 2, 2003

F9 8 <0.5 T <0.5 E <0.5 X <0.5 G <0.5 O <0.5

Project No.

C001 -031

Date

11/7/03


Prepared by

Drawn by

JMA REMONT

NVIRONMENTAL Reviewed by

Filename 01031Q

F10 B <0.5 T <0.5 E <0.5 x <0.5 • <0.5 D <0.5

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3

Figure 5

SOIL ANALYTICAL MAP APRIL 21-23 & AUGUST 5, 2003

HOUSE CD

PRIVATE WELL

0

3 0 U

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J

25 SAMPLE DEPTH (feet) BENZENE (ug/Kg) TPH—GRO (mg/Kg) TPH—DRO (mg/Kg)

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Project No. Prepared by Drawn by

C001 -031 JMA

Date Reviewed by Filename

10/29/03 01031Q

20 710

8 <2 G <0.5 D <10 REMONT

NVIRONMENTAL

APPENDIX A

FREMONT'S STANDARD SAMPLING METHODS AND PROCEDURES

METHODS AND PROCEDURES

Water Level Measurements

All ground water level measurements were obtained using an electric measuring device, which indicates

when a probe is in contact with ground water. Measurements were obtained by lowering the device into the

well until the water surface had been encountered, and by measuring the distance from the top of the inside

riser pipe to the probe. All of the measurements were recorded to the nearest 0.01'. To minimize cross-

contamination, the water level indicator was decontaminated with isopropyl alcohol and distilled water

between each well.

Monitoring Well Sampling

All monitoring wells were sampled from historically "cleanest" to "most contaminated" according to the

protocols listed below.

Field Protocol

Step 1 - Measure water level in each well.

Step 2 - Purge each monitoring well by evacuating a minimum of three well bore volumes using a

disposable polyethylene bailer.

Step 3 - Collect water samples using a disposable polyethylene bailer.

Step 4 - Cool samples to approximately 4°C for transportation.

Step 5 - Store water samples and transport to a specific laboratory, following all documentation and

chain-of-custody procedures.

Upon completion of ground water sampling, a chain-of-custody log was initiated. Chain-of-custody records

included the following information: project, project number, shipped by, shipped to, suspected hazard,

sampling point, location, field identification number, date collected, sample type, number of containers,

analysis required, and sampler's signature.

The chain-of-custody records were shipped with the samples to the laboratory. Upon arrival at the

laboratory the samples were checked in and signed by the appropriate laboratory personnel. Laboratory

identification numbers were noted on the chain-of-custody record. Upon completion of the laboratory

analysis, the completed chain-of-custody record was returned to the project manager.

Analytical Methods

The following list identifies the various chemical constituents and analytical methods which were used for

their quantification.

Chemical Parameter Method

TPH-GRO EPA Method 0A1, 8015B modified

TPH-DRO EPA Method 8015B

TEH 0A2

BTEX EPA Method 8021, 8260B

VOCs EPA Method 8260

APPENDIX B

LABORATORY REPORTS, QUALITY CONTROL DATA AND CHAIN-OF-CUSTODY DOCUMENTATION

TECHNOLOGY LABORATORY, INC.

CENTRE PROFESSIONAL OFFICE PARK 1012 CENTRE AVENUE

Fort Collins, Colorado 80526 (970) 490-1414

VOLATILE ORGANICS WATER ANALYSIS . REPORT

FREMONT ENVIRONMENTAL, INC 1530 Boise Avenue, Suite 205 Loveland, Colorado 80538

Date Benzene Toluene Ethylbenzene

Date Received: 10/03/03 Date Analyzed: 10/06/03 Project No.: CO01-031

Xylenes TPH-GRO TPH-DRO Lab ID Sample ID &Wed mg& 1.0/1 ilia ligil mg& mg/i.

5325-1 MW-1 10/02/03 5,261 1,436 258 1,473 15.1 9.0 5325-2 F-1 10/02/03 235 92.8 1.4 459 5.93 191 5325-3 F-2 10/02/03 358 14.8 44.8 1,130 244 86.2 5325-4 F-5 10/02/03 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 5325-5 F-8 10/02/03 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 5325-6 F-9 10/02/03 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 5325-7 F-10 10/02/03 <0.5 <0.5 <05 <0.5 <0.5 <0.5 5325-8 F-11 10/02/03 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 5325-9 F-12 0/02/03 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 5325-10 Duplica t 0/02/03 469 19.3 23.0 995 254 70.6 5325-11 Glenda 10/02/03 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 5325-12 Rector 10/02/03 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5

BTEX Method: EPA-8260B TPH-GRO Method: EPA-Modified 80158 TPH-DRO Method: EPA-8015B

TECHNOLOGY LABORATORY, INC

Page 1 of 3




VOLATILE ORGANICS WATER ANALYSIS REPORT

QA/QC SURROGATE RECOVERY

FREMONT ENVIRONMENTAL, INC. 1530 Boise Avenue, Suite 205 Loveland, Colorado 80538

LaI2112 Sample ID Dlbromoflouromethane

Lingsaa:1212%)

Date Received: 10/03/03 Date Analyzed: 10/06/03 Project No.: C001-031

(% Recovery)

1,2 Dichloroethane-d4 Toluene-d8 Limits (73-115%) ijmits (81-128%)

5325-1 MW-1 102 100 96 5325-2 F-1 99 93 95 5325-3 F-2 109 116 99 5325-4 F-5 102 95 94 5325-5 F-8 100 98 99 5325-6 F-9 101 98 99 5325-7 F-10 101 98 98 5325-8 F-11 103 99 99 5325-9 F-12 100 96 101 5325-10 Duplicate 104 113 98 5325-11 Glenda 100 95 101 5325-12 Rector 98 91 100


Page 2 of 3





QA/QC MATRIX SPIKE AND DUPLICATE RECOVERY


Date Received: Date Analyzed: Project No.:

10/03/03 10/06/03 ami-o31

Laboratory ID:

Sample ID:

5325-12

Rector

Spike Added

Latuggund Lira)

Sample Concentration

MS Concentration

(.161&)

MSD Concentration

1.141/1.1

MS MSD QC Percent Percent % Recovery

Scam Brom Limits

Benzene 100 <0.5 97 97 97 97 - 39-150 Toluene 100 <0.5 99 100 99 100--" 16-148 Ethylbenzene 100 <0.5 107 107 107 107 32-160 M,P-Xylene 200 <0.5 209 211 105 106 32-160 O-Xyiene 100 <0.5 103 104 103 104 32-160

MS = Matrix Spike MSD = Matrix Spike Duplicate


Page 3 of 3

TECHNOLOGY LABORATORY, INC. W.O. NUMBER 1012 CENTRE AVENUE CHAIN-OF—CUSTODY REPORT

FORT COLLINS, CO 80526 (970) 490-1414

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RELINQUISHED BY: ( x)i, (,..,-,/- -, DATE le: , 1:::,2 , " RECEIVED BY: , 7 df>.4

COMPANY: .7 TIME:

4: -_se'o COMPANY: (.04, 'VC COL,{re-'r- I 24 hr (100% Surcharge) RELINQUISHED BY:

''%;) i.t DATE: 1 0 / 3/a.t. RECEIVED BY:

(-) ) . 3-05 1,.. /AMC CB ._ orrhsarroal - - — - ,- - / f ..- . r •A,/ TIME: 1 , 1 r COMPANY: t---;-) 1 -

TECHNOLO e17 LABORATORY, INC.






Lab..E3 Sample ID Date Sampled

Benzene ug/1

Toluene paLL

Ethylbenzene us&

Date Received: 08/08/03 Date Analyzed: 08/12/03 Project No.: C001-031

Xylenes TPH-GRO ugLL mg/L.

TPH-DRO mg/L

5076-1 F-8 08/05/03 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 5076-2 F-9 08/06/03 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 5076-3 F-10 08/06/03 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 5076-4 F-11137f 08/06/03 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 5076-5 F-12 v 08/06/03 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 5076-6 Duplicate 08/06/03 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5

BTEX Method: EPA-8260B TPH-GRO Method: EPA-Modified 8015B TPH-DRO Method: EPA-8015B

Page 1 of 5






FREMONT ENVIRONMENTAL, INC. Date Received: 08/08/03 1530 Boise Avenue, Suite 205

Date Analyzed: 08/12/03

Loveland, Colorado 80538

Project No.: C001-031

Lab ID Sample ID Toluene-d8

Umits (80-113%)

(% Recovery)

4-Bromofluorobenzene Umits (80-121%)

Dibromoflouromethane Umits (87-113%)

5076-1 F-8 103 94 96 5076-2 F-9 103 95 95 5076-3 F-10 102 94 95 5076-4 F-11 102 96 96 5076-5 F-12 104 95 96 5076-6 Duplicate 104 94 97

RATORY, INC.

Page 2 of 5





QA/QC MATRIX SPIKE AND DUPLICATE RECOVERY

FREMONT ENVIRONMENTAL, INC. Date Received:

08/08/03 1530 Boise Avenue, Suite 205

Date Analyzed:

08/12/03 Loveland, Colorado 80538

Project No.:

CO01-031

Laboratory ID:

Sample ID:

Spike Added

5076-6

Duplicate

Sample Concentration

MS Concentration

MSD Concentration

MS Percent

MSD Percent

QC % Recovery

Comte WO_ fug/L) fug/L) (ug/L) Recovery Recovery Limits

Benzene 100 <0.5 104 105 104 105 39-150 Toluene 100 <0.5 105 107 105 106 46-148 Ethylbenzene 100 <0.5 111 112 111 112 32-160 M,P-Xylene 200 <0.5 220 223 110 112 32-160 O-Xylene 100 <0.5 110 112 110 112 32-160

MS = Matrix Spike MSD = Matrix Spike Duplicate

iea TECH NOLOG RATORY, INC.

Page 3 of 5


CENTRE PROFESSIONAL OFFICE PARK 1012 Centre Avenue


VOLATILE ORGANICS SOIL ANALYSIS REPORT





Date Benzene Toluene Ethylbenzene Xylenes TPH-GRO TPH-DRO Ls D Sample ID Sampled 119/1g kg Ka pg/Kq mg/Kg [gag<

5076-7 F-9 @ 20' 08/05/03 <2 <2 <2 5076-8 F-10 @ 20' 08/05/03 <2 <2 <2 5076-9 F-11 @ 20' 08/05/03 <2 <2 <2 5076-10 F-12 @ 20' 08/05/03 <2 <2 <2

<2 <0.5 <10 <2 <0.5 <10 <2 <0.5 <10 <2 <0.5 <10

BTEX Method: EPA-8260B TPH-GRO Method: EPA-Modified 8015B TPH-DRO Method: EPA-8015B

TECHNOLOGY LRIBORATORY, INC

Page 4 of 5




VOLATILE ORGANICS SOIL ANALYSIS REPORT






(% Recovery)

Toluene-d8 4-Bromofluorobenzene Dibromoflouromethane Lab ID Sample ID Umits (68-128%) Umits (88-111%1 Limits (77-117%1

5076-7 F-9 @ 20' 114 104 90 5076-8 F-10 @ 20' 97 103 91 5076-9 F-11 @ 20' 98 104 88 5076-10 F-12 © 20' 96 104 88

TECHNOLOG BORATORY, INC.

Page 5 of 5

TECHNOLOGY LABORATORY, INC. W.O. NUMBER -5-07,4

/r 1012 CENTRE AVENUE CHAIN-OF-CUSTODY REPORT FORT COLLINS, CO 80526

(970) 490-1414

COMPANY NAME

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1 F-8 515 vv 3 2( )e et- F-9 W3

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COMPANY: r;.t ._ COMPANY: Ekec114,e4. C--- -//1's

11 24 hr (100% Surcharge) RELINQUISHED BY: 9 c-,..,„4:, TIME: 61,7 DATE: 8P- 5/as RECEIVED BY: ..\1

' -g -(J- O 3 day (50% Surcharge) COMPANY: TIME: ; v (iS COMPANY: 71.1

Pace Analytical Services, Inc. 9608 Loiret Blvd.

Lenexa, KS 66219 Phone: 913.599.5665

Fax: 913.599.1759

May 06, 2003.

Mr. Paul Neneban

FREMONT ENVIRONMENTAL, INC.

1530 N. BOISE AVE.

SUITE 205

LOVELAND, CO 80538

RE: Lab Project Number: 6069815

Client Project ID: KANEB-Andover

Dear Mr. Neneban:

Enclosed are the analytical results for sample(s) received by the laboratory on April 24, 2003. Results reported

herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of

the report.

If you have any questions concerning this report please feel free to contact me.

Sincerely,

Adam Taylor

[email protected]

Project Manager

Kansas/NELAP Certification Number E-10116

Enclosures

REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc.

SAMPLE SUMMARY


Lenexa, KS 66219 Phone: 913.599.5665

Fax: 913.599.1759 www.pacelabs.com

Lab Project Number: 6069815


Project

Sample Number

Sample,

Number Client Sample ID Matrix Date Collected Date Received 6069815-001 606016822 F-1 30 Soil 04/21/03 15:10 04/24/03 07:30 6069815-002 606016830 F-2 25 Soil 04/21/03 17:30 04/24/03 07:30 6069815-003 606016848 F-3 20 Soil 04/22/03 09:45 04/24/03 07:30 6069815-004 606016855 F-4 24 Soil 04/22/03 11:20 04/24/03 07:30 6069815-005 606016863 F-5 24 Soil 04/22/03 13:40 04/24/03 07:30 6069815-006 606016871 F-6 24.5 Soil 04/22/03 15:00 04/24/03 07:30 6069815-007 606016889 F-7. 20 Soil 04/22/03 16:00 04/24/03 07:30 6069815-008 606016897 F-8 24 Soil 04/23/03 09:20 04/24/03 07:30 6069815-009 606016905 RECTOR WELL Water 04/23/03 08:30 04/24/03 07:30 6069815-010 606016913 DODSON WELL Water 04/23/03 08:45 04/24/03 07:30 6069815-011 606016921 LAYMON WELL Water 04/23/03 12:20 04/24/03 07:30 6069815-012 606016939 F-1 Water 04/23/03 09:15 04/24/03 07:30 6069815-013 606016947 F-2 Water 04/23/03 11:00 04/24/03 07:30 6069815-014 606016954 F-5 Water 04/23/03 09:00 04/24/03 07:30 6069815-015 606016962 F-8 Water 04/23/03 12:00 04/24/03 07:30 6069815-016 606016970 MW-1 Water 04/23/03 11:30 04/24/03 07:30 6069815-017 606016988 F-12 Water 04/23/03 10:30 04/24/03 07:30



ace Analytical® SAMPLE ANALYTE COUNT www.pacelabs.com


Lenexa, KS 66219 Phone: 913.599.5665

Fax: 913.599.1759



Project

Sample Number Sample NO Client Sample ID

Analysis

Code Analysis Description

Analytes

Reported

6069815-001 606016822 F-1 30 %MOISTURE Percent Moisture 1 °Al SL60 TPH Gas/BTEX

0A2 SL60 Total Extractable Hydrocarbons 9

6069815-002 606016830 F-2 25 %MOISTURE Percent Moisture 1 OA1 SL60 TPH Gas/BTEX 8








6069815-006 606016871 F-6 24.5 %MOISTURE Percent Moisture 1 OA1 SL60 TPH Gas/BTEX 8


6069815-007 606016889 F-7 20 %MOISTURE Percent Moisture 1 OA1 SL60 TPH Gas/BTEX


6069815-008 606016897 F-8 24 %MOISTURE Percent Moisture 1 OA1 SL60 TPH Gas/BTEX


6069815-009 606016905 RECTOR WELL OA1 WL60 TPH Gas/BTEX 8

0A2 WL60 Total Extractable Hydrocarbons 9

6069815-010 606016913 DODSON WELL OA1 WL60 TPH Gas/BTEX 8


6069815-011 606016921 LAYMON WELL OA1 WL60 TPH Gas/BTEX 8


6069815-012 606016939 F-1 OA1 WL60 TPH Gas/BTEX


6069815-013 606016947 F-2 OA1 WL60 TPH Gas/BTEX


6069815-014 606016954 F-5 OA1 WL60 TPH Gas/BTEX 8


6069815-015 606016962 F-8 OA1 WL60 TPH Gas/BTEX 8 0A2 WL60 Total Extractable Hydrocarbons 9

6069815-016 606016970 MW-1 OA1 WL60 TPH Gas/BTEX 8 0A2 WL60 Total Extractable Hydrocarbons 9




Lenexa, KS 66219 Phone: 913.599.5665

Fax: 913.599.1759



Project

Sample Number Sample No Client Sample ID

6069815-017 606016988 F-12

Analysis Analytes

Code Analysis Description Reported

OA1 WL60 TPH Gas/BTEX 8




www.pacelabs.com

Solid results are reported on a dty weight basis

Lab Sample No: 606016822 Project Sample Number: 6069815-001 Date Collected: 04/21/03 15:10 Client Sample ID: F-1 30

Parameters

Matrix: Soil Date Received: 04/24/03 07:30

Results Units Report Limit DF Analyzed By CAS No. Qual ReoLmt GC Semivolatiles Total Extractable Hydrocarbons Prep/Method: 0A2 / 0A2

Mineral Spirits

Jet Fuel

Kerosene

Diesel Fuel

Fuel Oil

Motor Oil

n-Tetracosane (5)

p-Terphenyl (5)

Date Extracted

ND

ND

ND

ND

ND

ND

84

86

04/28/03

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

%

%

13.

13.

13.

13.

13.

13.

1.2 04/28/03 22:56 MIN

1.2 04/28/03 22:56 MIN

1.2 04/28/03 22:56 MIN

1.2 04/28/03 22:56 MIN

1.2 04/28/03 22:56 MIN

1.2 04/28/03 22:56 MIN

1.0 04/28/03 22:56 MIN

1.0 04/28/03 22:56 MIN

04/28/03

68334-30-5

68334-30-5

646-31-1

92-94-4

Organics Prep Percent Moisture Method: SM 25406

Percent Moisture 20.1 1.0 04/28/03

GC Volatiles TPH Gas/BTEX Prep/Method: TPH GRO/BTEX / EPA 8021/0A1

Gasoline Range Hydrocarbons ND ug/kg 6300 1.2 04/28/03 21:50

Benzene ND ug/kg 63. 1.2 04/28/03 21:50 71-43-2 Toluene ND ug/kg 63. 1.2 04/28/03 21:50 108-88-3 Ethylbenzene ND ug/kg 63. 1.2 04/28/03 21:50 100-41-4 Xylene (Total) ND ug/kg 160 1.2 04/28/03 21:50 1330-20-7 Methyl-tert-butyl ether ND ug/kg 330 1.2 04/28/03 21:50 1634-04-4 a,a,a-Trifluorotoluene (S) 96 % 1.0 04/28/03 21:50 98-08-8 4-Bromofluorobenzene (S) 91 % 1.0 04/28/03 21:50 460-00-4

Date: 05/06/03 Page: 1 of 30




Lenexa, KS 66219 Phone: 913.599.5665

Lab Project Number: 6069815 Fax: 913.599.1759


ace Analytical® www.pacelabs.com

Lab Sample No: 606016830

Client Sample ID: F-2 25

Parameters

Project Sample Number: 6069815-002

Matrix: Soil

Results Units Report Limit OF Analyzed By

Date Collected: 04/21/03 17:30

Date Received: 04/24/03 07:30

CAS No. Qual ReaLmt

GC Semivolatiles Total Extractable Hydrocarbons Prep/Method: 0A2 / 0A2

Mineral Spirits ND mg/kg 11. 1.1 04/28/03 23:24 MIN

Jet Fuel ND mg/kg 11. 1.1 04/28/03 23:24 MIM

Kerosene ND mg/kg 11. 1.1 04/28/03 23:24 MIM

Diesel Fuel ND mg/kg 11. 1.1 04/28/03 23:24 MIM 68334-30-5

Fuel Oil ND mg/kg 11. 1.1 04/28/03 23:24 MIM 68334-30-5

Motor Oil ND mg/kg 11. 1.1 04/28/03 23:24 MIM

n-Tetracosane (5) 84 % 1.0 04/28/03 23:24 MIN 646-31-1

p-Terphenyl (5) 85 k 1.0 04/28/03 23:24 MIM 92-94-4

Date Extracted 04/28/03 04/28/03


Percent Moisture 11.3 k 1.0 04/28/03 MAM



Benzene ND ug/kg 56. 1.1 04/28/03 22:19 71-43-2

Toluene ND ug/kg 56. 1.1 04/28/03 22:19 108-88-3

Ethylbenzene ND ug/kg 56. 1.1 04/28/03 22:19 100-41-4

Xylene (Total) ND ug/kg 150 1.1 04/28/03 22:19 1330-20-7

Methyl-tert-butyl ether ND ug/kg 290 1.1 04/28/03 22:19 1634-04-4

a,a,a-Trifluorotoluene (S) 99 % 1.0 04/28/03 22:19 98-08-8

4-Bromofluorobenzene (5) 93 % 1.0 04/28/03 22:19 460-00-4


Lenexa, KS 66219 Phone: 913.599.5665



Date: 05/06/03 Page: 2 of 30



ti .,?;"-lettA2te, an*.


Lenexa, KS 66219 Phone: 913.599.5665



Parameters

GC Semi vol ati 1 es Total Extractable Hydrocarbons

Results

Units Report Limit DF Analyzed By CAS No. Dual Reamt

Prep/Method: 0A2 / 0A2


Project Sample Number: 6069815-003 Date Collected: 04/22/03 09:45


Matrix: Soil


Mineral Spirits

Jet Fuel

Kerosene

Diesel Fuel

Fuel Oil

Motor Oil

n-Tetracosane (S)

p-Terphenyl (5)

Date Extracted

Organics Prep Percent Moisture

Percent Moisture

GC Vol at i 1 es TPH Gas/BTEX

Gasoline Range Hydrocarbons

Benzene

Toluene

Ethylbenzene '

Xylene (Total)

Methyl-tert-butyl ether

a,a,a-Trifluorotoluene (5)

4-Bromofluorobenzene (5)

ND mg/kg 14.

ND mg/kg 14.

ND mg/kg 14.

370 mg/kg 14.

ND mg/kg 14.

ND mg/kg 14.

85

86

04/28/03

Method: SM 25406

26.3

Prep/Method: TPH GRO/BTEX / EPA 8021/0A1

360000 ug/kg 6700

1300 ug/kg 67.

4200 ug/kg 67.

3900 ug/kg 67.

18000 ug/kg 170

ND ug/kg 350

84 97

1.4

1.4

1.4

1.4

1.4

1.4

1.0

1.0

1.0

1.4

1.4

1.4

1.4

1.4

1.4

1.0

1.0

04/28/03

04/28/03

04/28/03

04/28/03

04/28/03

04/28/03

04/28/03

04/28/03

04/28/03

04/28/03

04/29/03

04/29/03

04/29/03

04/29/03

04/29/03

04/29/03

04/29/03

04/29/03

23:52 MIM

23:52 MIM

23:52 MIM

23:52 MIM

23:52 MIM

23:52 HIM

23:52 MIM

23:52 MIM

NAM

09:41

09:41

09:41

09:41

09:41

09:41

09:41

09:41

68334-30-5

68334-30-5

646-31-1

92-94-4

71-43-2

108-88-3

100-41-4

1330-20-7

1634-04-4

98-08-8

460-00-4

1

Daft: 05/06/03

Page: 3 of 30



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Lenexa, KS 66219 Phone: 913.599.5665

Fax. 913.599.1759 Lab Project Number: 6069815


Lab Sample No: 606016855 Project Sample Number: 6069815-004 Date Collected: 04/22/03 11:20


Parameters


Results Units Report Limit DF Analyzed BY CAS No. Qual RegLmt GC Semi vo 1 at i les Total Extractable Hydrocarbons Prep/Method: 0A2 / 0A2

Mineral Spirits ND mg/kg 12. 1.2 04/29/03 00:20 MIM

Jet Fuel ND mg/kg 12. 1.2 04/29/03 00:20 MIM

Kerosene ND mg/kg 12. 1.2 04/29/03 00:20 MIN


Fuel Oil ND mg/kg 12. 1.2 04/29/03 00:20 MIN 68334-30-5

Motor Oil ND mg/kg 12. 1.2 04/29/03 00:20 MIN

n-Tetracosane (S) 82 % 1.0 04/29/03 00:20 MIN 646-31-1

p-Terphenyl (S) 80 % 1.0 04/29/03 00:20 MIM 92-94-4



Percent Moisture 14.4 8 1.0 04/28/03 MAN

GC Vol at i 1 es TPH Gas/BTEX Prep/Method: TPH GRO/BTEX / EPA 8021/0A1


Benzene ND ug/kg 58. 1.2 04/29/03 11:34 71-43-2

Toluene ND ug/kg 58. 1.2 04/29/03 11:34 108-88-3

Ethyl benzene ND ug/kg 58. 1.2 04/29/03 11:34 100-41-4



a,a,a-Trifluorotoluene (5) 100 % 1.0 04/29/03 11:34 98-08-8

4-Bromofluorobenzene (S) 95 % 1.0 04/29/03 11:34 460-00-4

Date: 05/06/03 Page: 4 of 30




Lenexa, KS 66219 Phone: 913.599.5665





Parameters


Results Units Report Limit DF Analyzed By CAS No. Qual Reamt GC Semi vol ati les Total Extractable Hydrocarbons Prep/Method: 0A2 / 0A2

Mineral Spirits

Jet Fuel

Kerosene

Diesel Fuel

Fuel Oil

Motor Oil

n-Tetracosane (5)

p-Terphenyl (S)

Date Extracted

ND mg/kg 13.

ND mg/kg 13.

ND mg/kg 13.

ND mg/kg 13.

ND mg/kg 13.

ND mg/kg 13.

94 %

68 %

04/28/03

1.3

1.3

1.3

1.3

1.3

1.3

1.0

1.0

04/29/03

04/29/03

04/29/03

04/29/03

04/29/03

04/29/03

04/29/03

04/29/03

04/28/03

08:06 MIM

08:06 MIM

08:06 MIM

08:06 MIN

08:06 MIM

08:06 MIM

08:06 MIM

08:06 MIM

68334-30-5

68334-30-5

646-31-1

92-94-4


Percent Moisture 20.6 k 1.0 04/28/03 MAN

GC lfol avti 1 es TPH Gas/BTEX Prep/Method: TPH GRO/BTEX / EPA 8021/0A1


Benzene ND ug/kg 63. 1.2 04/29/03 12:03 71-43-2

Toluene ND ug/kg 63. 1.2 04/29/03 12:03 108-88-3




a,a,a-Trifluorotoluene (S) 100 % 1.0 04/29/03 12:03 98-08-8


Date: 05/06/03 Page: 5 of 30


without the written consent of Pace Analytical Services, Inc. 0

www.pacelabs.com


Lenexa, KS 66219 Phone: 913.599.5665

Fax: 913.599.1759 Lab Project Number: 6069815



Client Sample ID: F-6 24.5

Parameters



Results Units Report Limit DF Analyzed BY CAS No. Qual ReqLmt



Jet Fuel ND mg/kg 12. 1.2 04/29/03 08:34 MIN





n-Tetracosane (5) 90 % 1.0 04/29/03 08:34 MIM 646-31-1

p-Terphenyl (5) 67 % 1.0 04/29/03 08:34 MIM 92-94-4



Percent Moisture 19.9 k 1.0 04/28/03 MAN



Benzene ND ug/kg 62. 1.2 04/29/03 12:31 71-43-2

Toluene ND ug/kg 62. 1.2 04/29/03 12:31 108-88-3






Date: 05/06/03 Page: 6 of 30


without the written consent of Pace Analytical Services, Inc. AC Cpge

4.,?"

www.pacelabs.com



Parameters


Matrix: Soil

Results Units Report Limit DF Analyzed By



CAS No. Qual RegLmt

GC Semi vol ati les Total Extractable Hydrocarbons

Mineral Spirits

Jet Fuel

Kerosene

Diesel Fuel

Fuel Oil

Motor Oil

Total Petroleum Hydrocarbons

n-Tetracosane (5)

p-Terphenyl (S)

Date Extracted

Organics Prep Percent Moisture

Percent Moisture

GC Vol at i 1 es TPH Gas/BTEX

Gasoline Range Hydrocarbons

Benzene

Toluene

Ethylbenzene

Xylene (Total)

Methyl-tert-butyl ether

a,a,a-Trifluorotoluene (S)

4-Bromofluorobenzene (S)


ND mg/kg 11. 1.1

ND mg/kg 11. 1.1

ND mg/kg 11. 1.1

1000 mg/kg 11. 1.1

ND mg/kg 11. 1.1

ND mg/kg 11. 1.1

ND mg/kg 11. 1.1

87 % 1.0

81 % 1.0

04/28/03

Method: SM 25406

10.1 k 1.0

Prep/Method: TPH GRO/BTEX / EPA 8021/0A1

1300000 ug/kg 56000 11.1

1600 ug/kg 560 11.1

17000 ug/kg 560 11.1

13000 ug/kg 560 11.1

91000 ug/kg 1400 11.1

ND ug/kg 2900 11.1

90 % 1.0

94 % 1.0

04/29/03

04/29/03

04/29/03

04/29/03

04/29/03

04/29/03

04/29/03

04/29/03

04/29/03

04/28/03

04/28/03

04/29/03

04/29/03

04/29/03

04/29/03

04/29/03

04/29/03

04/29/03

04/29/03

09:02 MIN

09:02 MIN

09:02 MIN

09:02 MIN

09:02 MIN

09:02 MIN

09:02 MIN

09:02 MIN

09:02 MIN

MAN

12:59

12:59

12:59

12:59

12:59

12:59

12:59

12:59

68334-30-5

68334-30-5

646-31-1

92-94-4

71-43-2

108-88-3

100-41-4

1330-20-7

1634-04-4

98-08-8

460-00-4

2


Lenexa, KS 66219 Phone: 913.599.5665

Lab Project, Number: 6069815 Fax: 913.599.1759


Date: 05/06/03 Page: 7 of 30


without the written consent of Pace Analytical Services, Inc. !Sco,,,,

Af 0.

444a.


Lenexa, KS 66219 Phone: 913.599.5665

Lab Project Number: 6069815 Fax 913.599.1759




Parameters



Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt

GC Semivolatiles Total Extractable HYdrocarbons Prep/Method: 0A2 / 0A2


Jet Fuel ND mg/kg 12. 1.2 04/29/03 17:13 MIN





n-Tetracosane (S) 91 % 1.0 04/29/03 17:13 MIM 646-31-1

p-Terphenyl (5) 78 lc 1.0 04/29/03 17:13 MIM 92-94-4



Percent Moisture 16.6 k 1.0 04/28/03 NAM



Benzene ND ug/kg 60. 1.2 04/29/03 13:28 71-43-2

Toluene 75. ug/kg 60. 1.2 04/29/03 13:28 108-88-3


Xylene (Total) 300 ug/kg 160 1.2 04/29/03 13:28 1330-20-7




Date: 05/06/03 Page: 8 of 30





Client Sample ID: RECTOR WELL

Matrix: Water Date Received: 04/24/03 07:30

Parameters Results Units Report Limit DF Analyzed By CAS No. Oual ReoLmt

GC Semi vol ati 1 es Total Extractable Hydrocarbons Prep/Method: 0A2 / 0A2

Mineral Spirits ND mg/1 0.40 1.0 04/30/03 01:32 MIM

Jet Fuel ND mg/1 0.40 1.0 04/30/03 01:32 MIM

Kerosene ND mg/1 0.40 1.0 04/30/03 01:32 MIM

Diesel Fuel ND mg/1 0.40 1.0 04/30/03 01:32 MIN 68334-30-5

Fuel Oil ND mg/1 0.40 1.0 04/30/03 01:32 MIN 68334-30-5

Motor Oil ND mg/1 0.40 1.0 04/30/03 01:32 MIN

p-Terphenyl (S) 100 % 1.0 04/30/03 01:32 MIM 92-94-4



GC Vol ati 1 es TPH Gas/BTEX Method: EPA 8021/0A1

Gasoline Range Hydrocarbons ND ug/1 500. 1.0 05/01/03 21:55

Benzene ND ug/1 2.00 1.0 05/01/03 21:55 71-43-2

Toluene ND ug/1 2.00 1.0 05/01/03 21:55 108-88-3

Ethylbenzene ND ug/1 2.00 1.0 05/01/03 21:55 100-41-4

Xylene (Total) ND ug/1 5.00 1.0 05/01/03 21:55 1330-20-7

Methyl-tert-butyl ether ND ug/1 10.0 1.0 05/02/03 11:34 1634-04-4



Date: 05/06/03 Pave: 9 of 30




Lenexa, KS 66219 Phone: 913.599.5665



Parameters

GC Semi vol ati 1 es Total Extractable Hydrocarbons

Results

Units Report Limit DF Analyzed By CAS No. Qual RegLmt


(2` aceAnalytical®



Client Sample ID: DODSON WELL

Matrix: Water


www.pacelabs.com


Lenexa, KS 66219 Phone: 913.599.5665



Mineral Spirits ND mg/1 0.40 1.0 04/30/03 02:19 MIN

Jet Fuel ND mg/1 0.40 1.0 04/30/03 02:19 MIM

Kerosene ND mg/1 0.40 1.0 04/30/03 02:19 MIN

Diesel Fuel ND mg/1 0.40 1.0 04/30/03 02:19 MIM 68334-30-5

Fuel Oil ND mg/1 0.40 1.0 04/30/03 02:19 MIM 68334-30-5


p-Terphenyl (S) 105 % 1.0 04/30/03 02:19 MIM 92-94-4





Benzene ND ug/1 2.00 1.0 05/01/03 22:24 71-43-2

Toluene ND ug/1 2.00 1.0 05/01/03 22:24 108-88-3

Ethyl benzene ND ug/1 2.00 1.0 05/01/03 22:24 100-41-4



a,a,a-Trifluorotoluene (5) 100 1.0 05/01/03 22:24 98-08-8

4-Bromofluorobenzene (S) 95 1.0 05/01/03 22:24 460-00-4

Date: 05/06/03

Page: 10 of 30



441*.


Lenexa, KS 66219 Phone: 913.599.5665

Lab Project Number: 6069815 Fax: 913.5991759




Client Sample ID: LAYMON WELL

Matrix: Water


Parameters Results Units Report Limit OF

Analyzed By CAS No. Qual ReaLmt



Jet Fuel. ND mg/1 0.40 1.0 04/30/03 02:50 MIM


Diesel Fuel ND m9/1 0.40 1.0 04/30/03 02:50 MIN 68334-30-5

Fuel Oil ND mg/1 0.40 1.0 04/30/03 02:50 MIN 68334-30-5

Motor Oil ND mg/1 0.40 1.0 04/30/03 02:50 MIM

p-Terphenyl (S) 93 % 1.0 04/30/03 02:50 MIM 92-94-4



GC Volatiles TPH Gas/BTEX Method: EPA 8021/0A1


Benzene ND ug/1 2.00 1.0 05/01/03 22:52 71-43-2

Toluene ND ug/1 2.00 1.0 05/01/03 22:52 108-88-3

Ethyl benzene ND ug/1 2.00 1.0 05/01/03 22:52 100-41-4




4-BroMofluorobenzene (S) 94 1.0 05/01/03 22:52 460-00-4

Date: 05/06/03

Page: 11 of 30


without the written consent of Pace Analytical Services, Inc. ACC,.

ekliE

ace Analytical www.pacelabs.com



Client Sample ID: F-1

Matrix: Water


Parameters

GC Semi volati les Total Extractable Hydrocarbons

Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt



Jet Fuel ND mg/1 0.40 1.0 04/30/03 01:17 MIM

Kerosene ND mg/1 0.40 1.0 04/30/03 01:17 RIM

Diesel Fuel 11. mg/1 0.40 1.0 04/30/03 01:17 MIN 68334-30-5

Fuel Oil ND mg/1 0.40 1.0 04/30/03 01:17 MIM 68334-30-5


p-Terphenyl (5) 113 % 1.0 04/30/03 01:17 MIM 92-94-4

n-Tetracosane (5) 112 % 1.0 04/30/03 01:17 MIN 646-31-1



Gasoline Range Hydrocarbons 11000 ug/1 1250 2.5 05/02/03 12:03

Benzene 166. ug/1 5.00 2.5 05/02/03 12:03 71-43-2

Toluene 298. ug/1 5.00 2.5 05/02/03 12:03 108-88-3

Ethylbenzene 107. ug/1 5.00 2.5 05/02/03 12:03 100-41-4

Xylene (Total) 852. ug/1 12.5 2.5 05/02/03 12:03 1330-20-7

Methyl-tert-butyl ether 49.0 ug/1 25.0 2.5 05/02/03 12:03 1634-04-4



Date: 05/06/03

Page: 12 of 30

REPORT OF 1.111/(111111r(1111f ANALYSIS This report shall not be reproduced, except in full,


t;=7


Lenexa, KS 66219 Phone: 913.599.5665



ace Analytical® www.pacelabs.com

Pace Analytical Sonless, Inc. 9608 Loiret Blvd.

Lenexa, KS 66219 Phone: 913.599.5665





Parameters Results Units


Matrix: Water

Report Limit DF Analyzed By



CAS No. Qual, ReqLmt



Jet Fuel ND mg/1 0.40 1.0 04/30/03 02:04 MIM


Diesel Fuel 4.7 mg/1 0.40 1.0 04/30/03 02:04 MIN 68334-30-5

Fuel Oil ND mg/1 0.40 1.0 04/30/03 02:04 MIN 68334-30-5


p-Terphenyl (5) 114 % 1.0 04/30/03 02:04 HIM 92-94-4





Benzene 37.5 ug/1 10.0 5.0 05/02/03 12:32 71-43-2

Toluene 235. ug/1 10.0 5.0 05/02/03 12:32 108-88-3

Ethylbenzene 270. ug/1 10.0 5.0 05/02/03 12:32 100-41-4

Xylene (Total) 1280 ug/1 25.0 5.0 05/02/03 12:32 1330-20-7

Methyl-tert-butyl ether 52.7 ug/1 50.0 5.0 05/02/03 12:32 1634-04-4



Date: 05/06/03 Page: 13 of 30



"/


Lenexa, KS 66219 Phone: 913.599.5665



www.pacelabs.com

Lab Sample No: 606016954 Project Sample Number: 6069815-014 Date Collected: 04/23/03 09:00 Client Sample ID: F-5


Parameters Results Units Report Limit DF Analyzed By CAS No. Qual ReqLmt GC Semi vol ati 1 es Total Extractable Hydrocarbons Prep/Method: 0A2 / 0A2


Jet Fuel ND mg/1 0.40 1.0 04/30/03 03:53 MIM


Diesel Fuel ND mg/1 0.40 1.0 04/30/03 03:53 MIM 68334-30-5

Fuel Oil ND mg/1 0.40 1.0 04/30/03 03:53 MIM 68334-30-5


p-Terphenyl (S) 109 % 1.0 04/30/03 03:53 MIN 92-94-4

n-Tetracosane (5) 117 % 1.0 04/30/03 03:53 MIM 646-31-1




Benzene ND ug/1 2.00 1.0 05/02/03 01:46 71-43-2 Toluene ND ug/1 2.00 1.0 05/02/03 01:46 108-88-3

Ethylbenzene ND ug/1 2.00 1.0 05/02/03 01:46 100-41-4 Xylene (Total) ND ug/1 5.00 1.0 05/02/03 01:46 1330-20-7 Methyl-tert-butyl ether ND ug/1 10.0 1.0 05/02/03 01:46 1634-04-4 a,a,a-Trifluorotoluene (5) 100 % 1.0 05/02/03 01:46 98-08-8 4-Bromeluorobernzene (S) 98 % 1.0 05/02/03 01:46 460-00-4

Date: 05/06/03 Page: 14 of 30




Lenexa, KS 66219 Phone: 913.599.5665





Parameters Results Units


Matrix: Water

Report Limit DF Analyzed By



CAS No. Qual ReaLmt

GC Semi vol ati les Total Extractable Hydrocarbons Prep/Method: 0A2 / 0A2


Jet Fuel ND mg/1 0.40 1.0 04/30/03 01:48 MIN


Diesel Fuel ND mg/1 0.40 1.0 04/30/03 01:48 MIN 68334-30-5

Fuel Oil ND mg/1 0.40 1.0 04/30/03 01:48 MIN 68334-30-5


p-Terphenyl (5) 112 % 1.0 04/30/03 01:48 MIN 92-94-4



GC Vol &tiles TPH Gas/BTEX Method: EPA 8021/0A1


Benzene 18.9 ug/1 2.00 1.0 05/02/03 02:14 71-43-2

Toluene 9.20 ug/1 2.00 1.0 05/02/03 02:14 108-88-3

Ethylbenzene 2.03 ug/1 2.00 1.0 05/02/03 02:14 100-41-4

Xylene (Total) 11.8 ug/1 5.00 1.0 05/02/03 02:14 1330-20-7




Dato: 05/06/03 Paw 15 of 30



CR


Lenexa, KS 66219 Phone: 913.599.5665





Client Sample ID: MW-1

Matrix: Water


Parameters Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt GC Semivolatiles Total Extractable Hydrocarbons Prep/Method: 0A2 / 0A2


Jet Fuel ND mg/1 0.40 1.0 04/30/03 02:35 MIM


Diesel Fuel 21. mg/1 0.40 1.0 04/30/03 02:35 HIM 68334-30-5

Fuel Oil ND mg/1 0.40 1.0 04/30/03 02:35 MIM 68334-30-5


p-Terphenyl (5) 121 1.0 04/30/03 02:35 HIM 92-94-4

n-Tetracosane (S) 1 1.0 04/30/03 02:35 MIN 646-31-1 3




Benzene 3930 ug/1 50.0 25.0 05/02/03 13:01 71-43-2

Toluene 880. ug/1 50.0 25.0 05/02/03 13:01 108-88-3

Ethyl benzene 540. ug/1 50.0 25.0 05/02/03 13:01 100-41-4

Xylene (Total) 1000 ug/1 125. 25.0 05/02/03 13:01 1330-20-7

Methyl-tert-butyl ether ND ug/1 250. 25.0 05/02/03 13:01 1634-04-4


4-Bromofluorobenzene (5) 101 1.0 05/02/03 13:01 460-00-4

Date: 05/06/03

Page: 16 of 30




Lenexa, KS 66219 Phone: 913.599.5665

Fax: 913.599.1759





Parameters



Results Units Report Limit OF Analyzed By CAS No. Oual RegLmt GC Semi vol atiles Total Extractable Hydrocarbons Prep/Method: 0A2 / 0A2

Mineral Spirits ND mg/1 0.40 1.0 04/30/03 03:06 MIM Jet Fuel ND mg/1 0.40 1.0 04/30/03 03:06 MIM Kerosene ND mg/1 0.40 1.0 04/30/03 03:06 MIN Diesel Fuel 4.1 mg/1 0.40 1.0 04/30/03 03:06 MIM 68334-30-5 Fuel Oil ND mg/1 0.40 1.0 04/30/03 03:06 MIM 68334-30-5 Motor Oil ND mg/1 0.40 1.0 04/30/03 03:06 MIM p-Terphenyl (S) 105 t 1.0 04/30/03 03:06 MIM 92-94-4 n-Tetracosane (S) 111 % 1.0 04/30/03 03:06 MIN 646-31-1 Date Extracted 04/28/03 04/28/03


Gasoline Range Hydrocarbons 12400 ug/1 5000 10.0 05/01/03 17:58 Benzene 47.0 ug/1 20.0 10.0 05/01/03 17:58 71-43-2 Toluene 297. ug/1 20.0 10.0 05/01/03 17:58 108-88-3 Ethylbenzene 313. ug/1 20.0 10.0 05/01/03 17:58 100-41-4 Xylene (Total) 1620 ug/1 50.0 10.0 05/01/03 17:58 1330-20-7 Methyl-tert-butyl ether 101. ug/1 100. 10.0 05/01/03 17:58 1634-04-4 a,a,a-Trifluorotoluene (5) 106 t 1.0 05/01/03 17:58 98-08-8 4-Bromofluorobenzene (S) 94 t 1.0 05/01/03 17:58 460-00-4

Date: 05/06/03

Page: 17 of 30



• (1 ace AnaIicaI® www.pacelabs.com


Lenexa, KS 66219 Phone: 913.599.5665

Fax: 913.599.1759



PARAMETER FOOTNOTES

Dilution factor shown represents the factor applied to the reported result and reporting limit due to changes

in sample preparation, dilution of the extract, or moisture content

ND Not detected at or above adjusted reporting limit

NC Not Calculable

Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit

MDL Adjusted Method Detection Limit

(S) Surrogate

[1] The sample contains hydrocarbon mixture of diesel fuel and gasoline fractions. Quatitation was achieved

using diesel fuel as a reference standard.

[2] The sample contains hydrocarbon mixture of diesel fuel and gasoline fractions. Quatitation was achieved using

diesel fuel as a reference standard.

[3] The surrogate was below laboratory control limits, however the alternate surrogate was within limits.

Therefore, the data was accepted.

Date: 05/06/03 Page: le of 30



"iii246,t

QUALITY CONTROL DATA

Pace Analytical Services, inc. 9608 Loiret Blvd.

Lenexa, KS 66219 Phone: 913.599.5665

Fax: 913.599.1759



QC Batch: 143684 Analysis Method: 0A2

QC Batch Method: 0A2 Analysis Description: Total Extractable Hydrocarbons

Associated Lab Samples: 606016822 606016830 606016848 606016855 606016863

606016871 606016889 606016897

METHOD BLANK: 606021871

Associated Lab Samples: 606016822 606016830 606016848 606016855 606016863 606016871 606016889

606016897

Blank Reporting

Parameter Units Result Limit Footnotes

Mineral Spirits mg/kg ND 10.

Jet Fuel mg/kg ND 10.

Kerosene mg/kg ND 10.

Diesel Fuel mg/kg ND 10.

Fuel Oil mg/kg ND 10.

Motor Oil mg/kg ND 10.

n-Tetracosane (5) % 84

p-Terphenyl (S) % 86

LABORATORY CONTROL SAMPLE: 606021889

Spike LCS LCS % Rec

Parameter Units Conc. Result % Rec Limits Footnotes

Diesel Fuel mg/kg 500.00 455.7 91 62-130

n-Tetracosane (5) 87 58-143

p-Terphenyl (5) 86 38-146

MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 606021905 606021913

606015014 Spike MS MSD MS MSD % Rec Max

Parameter Units Result Conc. Result Result % Rec % Rec Limits RPD RPD Footnotes

Diesel Fuel mg/kg 0 490.20 461.4 469.8 94 96 53-145 2 20

n-Tetracosane (5) 85 89 58-143

p-Terphenyl (5) 85 86 38-146

Date: 05/06/03 Page: 19 of 30

REPORT OF LABORATORY ANALYSIS This report shall not be except in full,


ace Analytical® www.pacelabs.com QUALITY CONTROL DATA


Lenexa, KS 66219 Phone: 913.599.5665

Fax: 913.599.1759



QC Batch: 143736 Analysis Method: 0A2

QC Batch Method: 0A2 Analysis Description: Total Extractable Hydrocarbons


606016954 606016962 606016970 606016988


Associated Lab Samples: 606016905 606016913 606016921 606016939 606016947 606016954 606016962

606016970 606016988

Blank Reporting


Mineral Spirits mg/1 ND 0.40

Jet Fuel mg/1 ND 0.40

Kerosene mg/1 ND 0.40

Diesel Fuel mg/1 ND 0.40

Fuel Oil mg/1 ND 0.40

Motor Oil mg/1 ND 0.40

p-Terphenyl (S) t 122

n-Tetracosane (5) % 109


Spike LCS LCS % Rec


Diesel Fuel mg/1 12.50 10.35 83 59-131

p-Terphenyl (5) 113 44-138

n-Tetracosane (5) 102 56-131




Diesel Fuel mg/1 4.149 16.67 20.37 19.85

p-Terphenyl (S)

n-Tetracosane (5)

97

127

107

94

117

106

54-137

44-138

56-131

3 20

Date: 05/06/03 Page: 20 of 30



hAri,



Lenexa, KS 66219 Phone: 913.599.5665

Fax: 913.599.1759



QC Batch: 143707 Analysis Method: EPA 8021/0A1

QC Batch Method: TPH GRO/BTEX Analysis Description: TPH Gas/BTEX


606016871 606016889 606016897


Associated Lab Samples: 606016822

606016897

Parameter Units

Gasoline Range Hydrocarbons ug/kg

Benzene ug/kg

Toluene ug/kg

Ethylbenzene ug/kg

Xylene (Total) ug/kg

Methyl-tert-butyl ether ug/kg

a,a,a-Trifluorotoluene (S) k

4-Bromofluorobenzene (5) %


Parameter Units

Gasoline Range Hydrocarbons ug/kg

Benzene ug/kg

Toluene ug/kg

Ethylbenzene ug/kg

Xylene (Total) ug/kg



606016830 606016848 606016855

Blank Reporting

Result Limit Footnotes

606016863 606016871 606016889

ND 5000

ND 50.

ND 50.

ND 50.

ND 130

ND 260

94

94

Spike LCS LCS t Rec Conc. Result % Rec Limits Footnotes

100000 97520 98 79-122

1000.00 1162 116 82-121

1000.00 1101 110 82-116

1000.00 1076 108 85-116

3000.00 3285 110 87-119

103 73-112

94 79-122


606005932 Spike MS MSD MS MSD t Rec Max


Gasoline Range Hydrocarbons ug/kg 4456 133400 122900 127900 89 92 66-123 4 14

Benzene ug/kg 8.556 1334.00 1517 1505 113 112 63-128 1 16

Date: 05/06/03 Page: 21 of 30





Lenexa, KS 66219 Phone: 913.599.5665

Fax: 913.599.1759






Toluene ug/kg 26.91 1334.00 1410 1399 104 103 75-117 1 18

Ethylbenzene ug/kg 40.26 1334.00 1417 1410 103 103 78-119 1 14

Xylene (Total) ug/kg 175.7 4002.00 4302 4280 103 102 83-120 1 16

Methyl-tert-butyl ether ug/kg 27.12 1334.00 1320 1392 97 102 43-123 5 16

a,a,a-Trifluorotoluene (S) 102 101 73-112

4-Bromofluorobenzene (S) 88 92 79-122

Date: 05/06/03 Page: 22 of 30


without the written consent of Pace Analytical Services, Inc. Y. ^Cpp4o

aceAnalytical° Inincpacelabs.com QUALITY CONTROL DATA


Lenexa, KS 66219 Phone: 913.599.5665

Fax: 913.599.1759



QC Batch: 143995 Analysis Method: EPA 8021/0A1

QC Batch Method: EPA 5030 Analysis Description: TPH Gas/BTEX


606016954 606016962 606016970



606016970

Parameter Units

Gasoline Range Hydrocarbons ug/1

Benzene ug/1

Toluene ug/1

Ethylbenzene ug/1

Xylene (Total) ug/1

Methyl-tert-butyl ether ug/1

a,a,a-Trifluorotoluene (S) %

4-Bromofluorobenzene (S) %


Parameter Units


Benzene ug/1

Toluene ug/1

Ethylbenzene ug/1

Xylene (Total) ug/1


a,a,a-Trifluorotoluene (5)


606016913 606016921 606016939 606016947 606016954 606016962

Blank Reporting

Result Limit Footnotes

ND 500.

ND 2.00

ND 2.00

ND 2.00

ND 5.00

ND 10.0

102

92

Spike LCS LCS % Rec

Conc. Result % Rec Limits Footnotes

2000.00 2180 109 80-122

20.00 21.48 107 85-120

20.00 21.20 106 87-114

20.00 21.03 105 87-114

60.00 63.64 106 88-115

20.00 21.10 106 82-121

100 86-115

98 80-117


606015873 Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Result Result % Rec % Rec Limits RPD RPD Footnotes Benzene ug/1 0 20.00 24.70 21.87 124 109 82-121 12 16 1

Date: 05/06/03 Page: 23 of 30

REPORT OF LABORATORY ANALYSIS • This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.



Lenexa, KS 66219 Phone: 913.599.5665

Fax: 913.599.1759




Parameter 606015873 Spike MS MSD MS MSD % Rec Max

Units. Result Conc. Result Result % Rec % Rec Limits RPD RPD Footnotes 12 18 1

11 14

10 16

9 16

Toluene ug/1 0 20.00 23.35 20.81 117 104 85-112

Ethylbenzene ug/1 0.7186 20.00 22.32 19.92 108 96 84-114

Xylene (Total) ug/1 0 60.00 63.62 57.59 106 96 83-115

Methyl-tert-butyl ether ug/1 9.514 20.00 33.51 30.62 120 106 73-129


Date: 05/06/03 Page: 24 of 30





Lenexa, KS 66219 Phone: 913.599.5665

Fax: 913.599.1759



QC Batch: 144007

Analysis Method: EPA $021/0A1

QC Batch Method: EPA 5030

Analysis Description: TPH Gas/BTEX

Associated Lab Samples:

606016988



102

95

Spike LCS LCS % Rec


2000.00 1862 93 80-122

20.00 21.75 109 85-120

20.00 22.66 113 87-114

20.00 22.10 111 87-114

60.00 69.11 115 88-115

20.00 21.55 108 82-121

104 86-115

92 80-117

Blank Reporting


Gasoline Range Hydrocarbons ug/1 ND 500.

Benzene ug/1 ND 2.00

Toluene ug/1 ND 2.00

Ethylbenzene ug/1 ND 2.00

Xylene (Total) ug/1 ND 5.00

Methyl-tert-butyl ether ug/1 ND 10.0

a,a,a-Trifluorotoluene (5) %



Parameter Units


Benzene ug/1

Toluene ug/1

Ethylbenzene ug/1

Xylene (Total) ug/1








Benzene ug/1

Toluene ug/1

165.2 2000.00 2030

0 20.00 20.94 20.38

0 20.00 23.33 20.69

93 71-119

105 102 82-121 3 16

117 103 85-112 12 18 1

Date: 05/06/03 Page: 25 of 30



:71 rA



Lenexa, KS 66219 Phone: 913.599.5665







Ethylbenzene ug/1 0 20.00 22.11 20.35 111 102 84-114 8 14

Xylene (Total) ug/1 1.430 60.00 70.45 62.64 115 102 83-115 12 16

Methyl-tert-butyl ether ug/1 0 20.00 22.91 21.00 114 105 73-129 9 16


4-Bromofluorobenzene (5) 94 80-117

Date: 05/06/03 Page: 26 of 30


without the written consent of Pace Analytical Services, Inc. O

Sfketrol; 7,..


Lenexa, KS 66219 Phone: 913.599.5665

Fax: 913.599.1759

ace Analytical® Iveiv.pacelabs.com QUALITY CONTROL DATA



QC Batch: 143618 Analysis Method: SM 25406 QC Batch Method: SM 2540G Analysis Description: Percent Moisture Associated Lab Samples: 606016822 606016830 606016848 606016855 606016863

606016871 606016889 606016897

SAMPLE DUPLICATE: 606019057

606015709 DUP Parameter Units Result Result RPD RPD Footnotes Percent Moisture % 22.70 22.40 1

Date: 05/06/03 Page: 27 of 30


without the written consent of Pace Analytical Services, Inc. 0, AC C 01,„

.e..1.1111.0.141111t


Lenexa, KS 66219 Phone: 913.599.5665




QUALITY CONTROL DATA PARAMETER FOOTNOTES

Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate % Rec and RPD values.

LCS(D) Laboratory Control Sample (Duplicate)

MS(D) Matrix Spike (Duplicate)

DUP Sample Duplicate


NC Not Calculable

J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit


RPD Relative Percent Difference

(5) Surrogate

[1] The sample matrix affected the Matrix Spike and Matrix Spike Duplicate (MS/MSD) compound recovery. The

successful recovery of the Laboratory Control Sample (LCS) demonstrates the analytical system was in control

for this QA/QC sample group.

Date: 05/06/03 Page: 28 of 30




CROSS REFERENCE TABLE


Lenexa, KS 66219 Phone: 913.599.5665

Fax: 913.599.1759



Analytical

Lab Sample No Client Sample QC Batch QC Batch Analytical Batch

Identifier Identifier Method Identifier Method Identifier

606016322 , F-1 30 0A2 143684 0A2 143863

606016830 F-2 25 0A2 143684 0A2 143863 606016848 F-3 20 0A2 143684 0A2 143863

606016855 F-4 24 0A2 143684 0A2 143863

606016863 F-5 24 0A2 143684 0A2 143863

606016871 F-6 24.5 0A2 143684 0A2 143863

606016889 F-7 20 0A2 143684 0A2 143863

606016897 F-8 24 0A2 143684 0A2 143863

606016905 RECTOR WELL 0A2 143736 0A2 143950

606016913 DODSON WELL 0A2 143736 0A2 143950

606016921 LAYMON WELL 0A2 143736 0A2 143950

606016939 F-1 0A2 143736 0A2 143950

606016947 F-2 0A2 143736 0A2 143950

606016954 F-5 0A2 143736 0A2 143950

606016962 F-8 0A2 143736 0A2 143950

606016970 144-1 0A2 143736 0A2 143950

606016988 F-12 0A2 143736 0A2 143950

606016822 F-1 30 TPH 6RO/BTEX 143707 EPA 8021/OA1 143729



606016855 F-4 24 TPH 6RO/BTEX 143707 EPA 8021/0A1 143729

606016863 F-5 24 TPH 6RO/BTEX 143707 EPA 8021/0A1 143729

606016871 F-6 24.5 TPH 6RO/BTEX 143707 EPA 8021/OA1 143729

606016889 F-7 20 TPH 6RO/BTEX 143707 EPA 8021/0A1 143729

606016897 F-8 24 TPH 6RO/BTEX 143707 EPA 8021/0A1 143729

606016905 RECTOR WELL EPA 8021/OA1 143995

606016913 DODSON WELL EPA 8021/OA1 143995

606016921 LAYMON WELL EPA 8021/OA1 143995.

606016939 F-1 EPA 8021/0A1 143995

606016947 F-2 EPA 8021/0A1 143995

606016954 F-5 EPA 8021/0A1 143995

606016962 F-8 EPA 8021/0A1 143995

Date: 05/06/03

Page: 29 of 30



Lab Sample No Client Sample QC Batch QC Batch Analytical Identifier Identifier Method Identifier Method

606016970 MW-1 EPA 8021/0A1 143995

606016988 F-12 EPA 8021/0A1 144007

606016822 F-1 30 SM 25406 143618 606016830 F-2 25 SM 25406 143618 606016848 F-3 20 SM 25406 143618 606016855 F-4 24 SM 25406 143618 606016863 F-5 24 SM 25406 143618 606016871 F-6 24.5 SM 25406 143618 606016889 F-7 20 SM 25406 143618 606016897 F-8 24 SM 25406 143618

Date: 05/06/03

Page: 30 of 30


without the written consent of Pace Analytical Services, Inc. ,w *CCpg0


Lenexa, KS 66219 Phone: 913.599.5665

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Analytical Batch Identifier

ialaceArm4iftical® www.psestabs.com

CnAIN-u1=-CouSThu /•Analyucal mequest Document The ChaM-of-Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately.

Section B 735544 aired client Information: Section A

•

4^ • Required Client Information: Report To: Page: I of t

eallY To Be Completed by Pace Analytical and Client Section C Quote Reference: r/Le 4",_.11 CA VI...Am -la Cloject Manager:

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SAMPLE ID

min / dd / hh:mm alp Remarks / Lab ID .

Valid Moroi Codes 1-------__ IMMIX ; CODE WATER WT Lu SOIL SL 0

0 OIL cc o

One character per box. ARE

AR WP

(A—Z, 0-9 / .—) TISSUE TS Sample IDs MUST BE UNIQUE OTHER OT

0 o 6S2Z-

SHIPMENT METHOD

;f!' 11111 A.,:ot• - tit,i, -‘

,1 AIRBILL NO. SHIPPING DATE NO tL

IiHIBI P OF COOLERS RELINQUISHED BY / AFFILIATION [ DATE TIME 1 ACCEPTED BY I .'FF- 11 IATION DATE TIME

real;" IMACM2INE2A, AMPLE CONDITION SAMPLE NOTES

Temp in °C

Received on Ice SAMPLER NAME AND SIGNATURE

Sealed Cooler

Samples Intact Adltional Comments:

Client Information (Check quote/contract): Requested Due Date: *TAT:

606o/06

?3

hpf Off

OA OD /TY)

2,7 €0 DAT

naqueot uuuumei It The. Chain-of-Custody Si a LEGArboCUMENT. All iellavant fields must be completed securer. } $:1

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luired Client Information: Section A WanY

CAVierv.4%,---4•441

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Required Client Information:

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II Semple IDs MUST BE UNIQUE

SAMPLE ID One character per box.

8 mm / dd / hh:mm a/p (5 11 I I 1 8 Atrert,

2 iu

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F7' o 64.? 2,3 0 1 I F-704G32.30 A Nectnt /— 471 RINIusated All*gisl

Section D Required Client Information:

rer

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011501/11211BERNIREMISIIIIIM 191111111111111111111PEFIVAPII refillitiaMINABOIMINI111111101111111111 olz(5111111111111•111111111111116111 - ME IINIIIMINIE13/111311111.4 nisimmul z2.011111111111.11111131111 Mill

-ra 110111111111111111111EMLIIIIM111111101/5111111111111111111111111111113 5 E Fill11111111•11. .11%1111111111111 1111M11111111111111111119111111•111 n 6 MVICEIMII ' worm Anommosiss 69.. imummurzir nEWAn 7-8/1111111111111111111PME11111111 1112-4011111111111111111141111113111111111 811rE11111111611111.1111M1111111111111 111130111M11111111111111011111111111 a 111111111111111111111ERMIIIIIMILUIPO/030111111111111111111111211111111111111111

111111111111111111 MEIN IIIIIIIIIIIIIIBIII n IIMIN

11 111111 I I I IIIIIII F,

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/ AFFILIATION DATE TIME ACCEPTED BY 1 AFF ILIATION 1 DATE

Oging11/2221=Pa ra4611170M111FAV :74001MIIMITA

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PRINT N SAIIPLER:, Gy„..vir je,„ 41401€ ,4

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* Turn around times lees than 14 days subject to laboratory and contractual obligations and may resultin a Rush Turnaround Surcharge.

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Profile

Valid Matrix Codes MATRIX CODE WATER WT W SOIL SL 0

0 OIL OL 0 WIPE WP x AIR AR if TISSUE TS I--

OTHER OT

tion:

4 LA

TIME

SAMPLE CONDITION SAMPLE NOTES

ltddltIonal Comments:

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5 AI 4410,4"re.,

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691

ri

A

e_C) 3/


Lenexa, KS 66219 Phone: 913.599.5665

Far 913.599.1759

January 02, 2003

Mr. Paul Henehan FREMONT ENVIRONMENTAL, INC. 1530 N. BOISE AVE. SUITE 205 LOVELAND, CO 80538

RE: Lab Project Number: 6066068 Client Project ID: KANEB-ANDOVER

Dear Mr. Henehan:

Enclosed are the analytical results for sample(s) received by the laboratory on December 21, 2002. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report.

If you have any questions concerning this report please feel free to contact me.

Sincerely,

Adam Taylor [email protected] Project Manager

Kansas/NELAP Certification Number E-10116

Enclosures



ace Analytical www.pacelahs.com SAMPLE SUMMARY


Lenexa, KS 66219 Phone: 913.599.5665

Far 913.599.1759


Client Project ID: KANEB-ANDOVER

Project

Sample Number

Sample

Number Client Sample ID Matrix Date Collected Date Received

6066068-001 605701952 KANEB-ANDOVER_RECTOR WELL Water 12/18/02 17:30 12/21/02 10:00

6066068-002 605701960 KANEB-ANDOVER_MW-1 Water 12/18/02 17:45 12/21/02 10:00

6066068-003 605701978 KANEB-ANDOVER_LAYMON WELL Water 12/18/02 17:00 12/21/02 10:00



www.pacelabs.com SAMPLE ANALYTE COUNT ace Analytical®

6066068-002.

Paco Analytical Semites, Inc. 9608 Loiret Blvd.

Lenexa, KS 66219 Phone: 913.599.5665

Fax 913.599.1759



Analysis Analytes

Sample Nit. Client Sample ID Code Analysis Description Reported

605701951: KANEB-ANDOVER_RECTOR WELL 8260 WBTX BTEXMN by 8260 (OA1), Water 7

GAS WL60 TPH Gas 2


605701960 KANEB-ANDOVER_MW-1 8260 WBTX BTEXMN by 8260 (OA1), Water 7

GAS WL60 TPH Gas 2

605701978 KANEB-ANDOVER_LAYMON WELL 8260 WBTX BTEXMN by 8260 (OA1), Water 7

GAS WL60 TPH Gas 2


Project

Sample Number

6066068-001


without the written consent of Pace Analytical Services, Inc. ACCIN


Lenexa, KS 66219 Phone: 913.599.5665

Fax. 913.599.1759 Lab Project Number: 6066068



Client Sample ID: KANEB-ANDOVER RECTOR WELL Matrix: Water Date Received: 12/21/02 10:00

Parameters Results Units Report Limit DF Analyzed By CAS No. Qual ReqLmt

GC Semivolatiles Total Extractable HydrOcarbons Prep/Method: 0A2 / 0A2

Mineral Spirits . ND mg/1 0.40 1.0 12/27/02 03:07 SEC

Jet Fuel ND mg/1 0.40 1.0 12/27/02 03:07 SEC

Kerosene ND mg/1 0.40 1.0 12/27/02 03:07 SEC

Diesel Fuel ND mg/1 0.40 1.0 12/27/02 03:07 SEC 68334-30-5

Fuel Oil ND mg/1 0.40 1.0 12/27/02 03:07 SEC 68334-30-5

Motor Oil ND mg/1 0.40 1.0 12/27/02 03:07 SEC

p-Terphenyl (5) 99 % 1.0 12/27/02 03:07 SEC 92-94-4

n-Tetracosane (S) 94 % 1.0 12/27/02 03:07 SEC 646-31-1


GC Volatiles TPH Gas Method: EPA 8015 Modified

Gasoline Range Hydrocarbons ND mg/1 0.500 1.0 12/31/02 17:09 SEB

4-Bromofluorobenzene (5) 89 1.0 12/31/02 17:09 SEB 460-00-4

GC/MS Volatiles BTEXMN by 8260 (OA1), Water Method: EPA 8260

Benzene ND ug/1 2.0 1.0 01/01/03 04:02 JSR 71-43-2

Toluene ND ug/1 2.0 1.0 01/01/03 04:02 JSR 108-88-3

Ethyl benzene ND ug/1 2.0 1.0 01/01/03 04:02 JSR 100-41-4

Xylene (Total) ND ug/1 7.0 1.0 01/01/03 04:02 JSR 1330-20-7

Methyl-tert-butyl ether ND ug/1 10. 1.0 01/01/03 04:02 JSR 1634-04-4

Toluene-d8 (S) 96 1.0 01/01/03 04:02 JSR 2037-26-5

4-Bromofluorobenzene (S) 98 1.0 01/01/03 04:02 JSR 460-00-4

Date: 01/02/03

Page: 1 of 10




Lenexa, KS 66219 Phone: 913.599.5665

Far 913.599.1759 Lab Project Number: 6066068


Lab Sample No: 605701960 Project Sample Number: 6066068-002

Client Sample ID: KANEB-ANDOVER_MW -1 Matrix: Water

Parameters Results Units Report Limit DF Analyzed By



CAS No. Qual Reamt

GC Vol ati les TPH Gas Method: EPA 8015 Modified

Gasoline Range Hydrocarbons 29.0 mg/1 25.0 50.0 12/31/02 16:07 SEB

4-Bromofluorobenzene (S) 95 % 1.0 12/31/02 16:07 SEB 460-00-4 1


Benzene 69. ug/1 2.0 1.0 01/01/03 06:12 JSR 71-43-2

Toluene 12. ug/1 2.0 1.0 01/01/03 06:12 JSR 108-88-3

Ethylbenzene 4.9 ug/1 2.0 1.0 01/01/03 06:12 JSR 100-41-4

Xylene (Total) 8.7 ug/1 7.0 1.0 01/01/03 06:12 JSR 1330-20-7


Toluene-d8 (5) 92 % 1.0 01/01/03 06:12 JSR 2037-26-5

4-Bromofluorobenzene (S) 100 % 1.0 01/01/03 06:12 JSR 460-00-4

Date: 01/02/03 Page: 2 of 10



ace Analytical' www.pacelabs.com


Pace Analytical Swims, Inc. 9608 Lolret Blvd.

Lenexa, KS 66219 Phone: 913.599.5665

Far. 913.599.1759



Client Sample ID: KANEB-ANDOVER_LAYMON WELL Matrix: Water Date Received: 12/21/02 10:00

Parameters Results Units Report Limit DF Analyzed By CAS No. Qual ReciLmt ,


Mineral Spirits ND mg/1 0.40 1.0 12/27/02 03:35 SEC

Jet Fuel ND mg/1 0.40 1.0 12/27/02 03:35 SEC

Kerosene ND mg/1 0.40 1.0 12/27/02 03:35 SEC

Diesel Fuel ND mg/1 0.40 1.0 12/27/02 03:35 SEC 68334-30-5

Fuel Oil ND mg/1 0.40 1.0 12/27/02 03:35 SEC 68334-30-5

Motor Oil ND mg/1 0.40 1.0 12/27/02 03:35 SEC

p-Terphenyl (S) 99 % 1.0 12/27/02 03:35 SEC 92-94-4

n-Tetracosane (S) 92 % 1.0 12/27/02 03:35 SEC 646-31-1


GC Volatiles TPH Gas Method: EPA 8015 Modified

Gasoline Range Hydrocarbons ND mg/1 0.500 1.0 12/31/02 16:38 SEB

4-Bromofluorobenzene (5) 90 1.0 12/31/02 16:38 SEB 460-00-4


Benzene 17. ug/1 2.0 1.0 01/01/03 06:45 JSR 71-43-2

Toluene ND ug/1 2.0 1.0 01/01/03 06:45 JSR 108-88-3

Ethylbenzene 11. ug/1 2.0 1.0 01/01/03 06:45 JSR 100-41-4

Xylene (Total) ND ug/1 7.0 1.0 01/01/03 06:45 JSR 1330-20-7


Toluene-d8 (5) 96 % 1.0 01/01/03 06:45 JSR 2037-26-5

4-Bromofluorobenzene (S) 100 % 1.0 01/01/03 06:45 JSR 460-00-4

Date: 01/02/03 Page: 3 of 10


without the written consent of Pace Analytical Services, Inc. N 11000,0

Pace Analytical tlatvicas, inc. 9608 Loiret Blvd

Lenexa, KS 66219 Phone: 913.599.5665

Fax 913.599.1759 Lab Project Number: 6066068


PARAMETER FOOTNOTES

Dilution factor shown represents the factor applied to the reported result and reporting limit due to changes

in sample preparation, dilution of the extract, or moisture content


NC Not Calctiable

J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit MDL Adjusted Method Detection Limit

(S):., Surrogate

[U The sample was diluted due to the presence of high levels of the non-target analytes.

Date: 01/02/03 Page: 4 of 10




Pace Analytical Sonless, Inc. 9608 Lolret Blvd.

Lenexa, KS 66219 Phone: 913.599.5665

Fax 913.599.1759



QC Batch: 136229

Analysis Method: 0A2

QC Batch Method: 0A2

Analysis Description: Total Extractable Hydrocarbons

Associated Lab Samples:

605701952 605701978


Associated Lab Samples: 605701952 605701978

Blank Reporting


Mineral Spirits mg/1 ND 0.40

Jet Fuel mg/1 ND 0.40

Kerosene mg/1 ND 0.40

Diesel Fuel mg/1 ND 0.40

Fuel Oil mg/1 ND 0.40

Motor Oil mg/1 ND 0.40

p-Terphenyl (S) % 107

n-Tetracosane (S) % 106


Spike LCS LCS % Rec


Diesel Fuel mg/1 12.50 10.09 81 68-118

p-Terphenyl (S) 104 39-129

n-Tetracosane (S) 101 53-127




Diesel Fuel mg/1 0 16.67 14.99 12.92 90 78 58-123 15 19

p-Terphenyl (5) 109 93 39-129

n-Tetracosane (S) 103 90 53-127

Date: 01/02/03 Page: 5 of 10


without the written consent of Pace Analytical Services, Inc. ACC ,,,,,,,,

ace Analytical* oncpacelabs.com QUALITY CONTROL DATA

Pace Analytical Beniess, Ins. 9608 Lolret Blvd.

Lenexa, KS 66219 Phone: 913.599.5665

Fax 913.599.1759



QC Batch: 136488 Analysis Method: EPA 8015 Modified

QC Batch Method: EPA 8015 Modified Analysis Description: TPH Gas

Associated Lab Samples: 605701952 605701960 605701978



Blank Reporting

Parimeter Units Result Limit Footnotes

Gasoline Range Hydrocarbons mg/1 ND 0.500

4-Bromofluorobenzene (5) % 83


Spike LCS LCS % Rec


Gasoline Range Hydrocarbons mg/1 2.000 2.124 106 72-123

4-Bromofluorobenzene (S) 96 75-120




Gasoline Range Hydrocarbons mg/1 0.05453 2.000 2.195 1.997 107 97 64-123 9 20

4-Bromofluorobenzene (S) 100 99 75-120

Date: 01/02/03 Page: 6 of 10



ace Analytical® wimpacelament QUALITY CONTROL DATA


Lenexa, KS 66219 Phone: 913.599.5665

Fax 913.599.1759



QC Batch: 136381 Analysis Method: EPA 8260

QC Batch Method: EPA 8260 Analysis Description: BTEXMN by 8260 (OA1), Water




Parameter Units

Benzene ug/1

Toluene ug/1

Ethylbenzene ug/1

Xylene (Total) ug/1


Toluene-d8 (S) %



Parameter Units

Benzene ug/1

Toluene ug/1 Ethylbenzene ug/1

Xylene (Total) ug/1


Toluene-d8 (5)


605701960

Blank

Result

605701978

Reporting

Limit Footnotes

ND 2.0

ND 2.0

ND 2.0

ND 7.0

ND 10.

98

101

Spike LCS LCS % Rec


50.00 47.04 94 73-127

50.00 47.94 96 76-125

50.00 45.29 91 77-125

150.00 136.3 91 77-126

50.00 42.78 86 67-129

106 89-109

105 81-118




Benzene ug/1 0 50.00 41.76 46.66 84 93 74-134 11 18

Toluene ug/1 0 50.00 41.86 46.37 84 93 64-139 10 22

Ethylbenzene ug/1 0 50.00 38.28 40.08 77 80 65-131 5 18

Xylene (Total) ug/1 0 150.00 115.0 118.4 77 79 57-138 3 17

Methyl-tert-butyl ether ug/1 0 50.00 49.54 45.88 99 92 66-127 8 16

Date: 01/02/03 Page: 7 of 10




Lenexa, KS 66219 Phone: 913.599.5665

Far 913.599.1759 QUALITY CONTROL DATA siniparagabsaame





Units Result Conc. Result Result % Rec % Rec Limits RPD RPD Footnotes

104 106 89-109

101 105 81-118

Parameter

Toluene-d8 (5)


Date: 01/02/03 Page: 8 of 10


without the written consent of Pace Analytical Services, Inc. .e, %it ACC04141

ace Analytical' www.pacelabs.com

QUALITY CONTROL DATA PARAMETER FOOTNOTES

Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate % Rec and RPD values.

LCS(D) Laboratory Control Sample (Duplicate)

MS(D) Matrix Spike (Duplicate)

DUP Sample DUplicate


NC Not Calculable

J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit


RPD Relative Percent Difference

(S) Surrogate

Date: 01/02/03 Page: 9 of 10



Pace Analytical Services, Inc. 9608 Loiter Blvd.

Lenexa, KS 66219 Phone: 913.599.5665

Fax 913.599.1759 Lab Project Number: 6066068


KANEB-ANDOVER_RECTOR WELL

KANEB-ANDOVER_LAYMON WELL


KANEB-ANDOVER_MW-1


Lab Sample No Client Sample

Identifier Identifier


KANEB-ANDOVER_MW-1


605701952

605701978

605701952

605701960

605701978

605701952

605701960

605701978


Lenexa, KS 66219 Phone: 913.599.5665

Fax 913.599.1759 QUALITY CONTROL DATA wmpace►ebs.com

CROSS REFERENCE TABLE



Analytical

QC Batch QC Batch Analytical Batch

Method Identifier Method Identifier

0A2 136229 0A2 136370

0A2 136229 0A2 136370

EPA 8015 Modified 136488



EPA 8260 136381

EPA 8260 136381

EPA 8260 136381

Date: 01/02/03

Page: 10 of 10

REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full,


0 Bats,. 40, SG f 2'

Copy o:

Inyolce;44;./

P. •

F970i,k3 Zyoo

Pr9=2, fa: Profect Number:

00/..'01/

• Turn around times less than 14 clays subject to

Rush Tu Surcharge. ,

laboratory and . obligations:4nd May result In a:

' Turn'Around time (TAT) In calendar days

Project #:

Profile b:

648864 To Be Completed by Pace Analytical and Client Section C Quote Reference:

Project Manager. Client Infprma io RegUeeted rot

eck • uote/contract : ATP

Remarks / Lab ID

-/f5 " 0

(fr

SIG RE o SAMPLER: DATE Si ed: (MM / DD / YY)

24 i►

SAMPLER NAME AND SIGNATURE

Temp in °C

SAMPLE CONDITION

Received on Ice

Sealed Cooler

Samples Intact

Ye

Additional Comments:

SAMPLE NOTES

Required Client information: FNMA T044., '140.46

IAINI"vh0F404,0STVIOY 1.11Cal The Chain-of-Custody Is a LEGAL. DOCUMENT, An relevant fields must be completed accurately.

Section B

Rusfeted

/I,r-ACeAnalyticar wew.peratabemin

quired Client Information: Section A

nalysler.

Valid Matrix Codes 4- MATRIX • CODE WATER W--- w uj

SOIL

WIPE

SL 8 0 4 OIL OL , . WP ° X

al ' kv

One character per •box. AIA cr 0 Z

(A-Z, 0-9 / .-) TISSUE TS 5 i

0

MIN NIIEINSOMMENVIIMMIEMINCIIIIIII cammoni

Sample IDs MUST BE UNIQUE OTHER OT mm / dd / hh:mm alp 4u I Z z 2

ERAIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIMIRIEMIIIIIIUIIIIIIIIEIIICIIIIIIIIIIIIII

IMINIENSIBM11311:111M11 MIIIIIIIIIIIMICIIIIIII II 1:11111111111 4 1111111111111111111111111111111111111111111111 nun 11111E111111111111111

5671 11111 I 111 1111 1 I 1 11 an . 8 11111111111111111111111111111111111 1111111111111 111111111111111 111111111111111111111 9 111111111MMINIMENINIIIIIIIIIIIIII IIIIIIIIIIIIIIIIIIEIEIIMEIUMII ° MIMIEMM11011111111111111.11111 1111111111.111111111111111111111

112 111111 11111 1/111111111111 1111111Ni 11111111 REL INOIJISHED BY / AFFILIATION DATE TIME ACCEPTED BY / AFFILIAT

SHIPMENT r'ETHOD AIRBIL_L NO. I SHIPPING DATE

Section D Required Client Information

SAMPLE ID

Preservatives

111111111111111111E7M1 1111=5.21,N2E2111011r17111 Eala

PRINT rrie, of SAMPLER`

41,441e-4•• e /4. 6-#, 5

rrw-tn1 ram, nani






Sample ID: MW-1

Laboratory ID: 3884-1

Sampled: 12/18/02 Received: 12/23/02 Analyzed: 01/02/03


Compound Analyzed

Concentration Method

TPH-DRO

<0.5 mg/L EPA-8015 Modified


, TECHNOLOGY LABORATORY, INC. 1012 CENTRE AVENUE

W.O. NUMBER _MUM CHAIN-OF-CUSTODY REPORT

FORT COLLINS, CO 80526 (970) 490-1414

COMPANY NAME ..1.40.

SA

MP

LE

MAT

RIX

: S

OIL

(S

) A

IR (

A)

AQ

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S (

W)

OT

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0)

NU

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OF

CO

NTA

INE

RS

ANALYSIS REQUESTED OTHER

BTE

X, T

VP

H (G

RO

)

I39

1W

TE

PH

(D

RO

)

HV

d

TR

PH

(41

8.1)

OIL

& G

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AS

E

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260 TO

TAL

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CLP

IS

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C 8

270

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B / P

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NO

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O4, P

O4

--4}

LD

SA

MP

LE

PROJECT MA ER

PROJECT NUM

PROJECT LOCATION OR NAME

SAMPLERS SIGN . /C--)

LAB #

SAMPLE ID DATE/TIME SAMPLED

1 /1-1 (...r — / /741.02 /751 S A / k

I- I

PAGE / OF I COMMENTS LOGGED IN BY: Samples Pres. Y / N / NA

TURNAROUND TIME

ja‘RMAL(5-1 0 working days)

RELINQUISHED /e2 . I— DATE: t sA3/6 7_, RECEIVED BY:

COMPANY: TIME: 7 0 : 3 -4.) COMPANY: 4,

RECEIVED BY: iille 0 n 24 hr (100% Surcharge) RELINQUISHED BY: DATE: A) tifirg 44 IW n 3 day (50% Surcharge) COMPANY: TIME: COMPANY: "72__. 121z3/0 2_....

C o o i o 3 /





DELTA ENVIRONMENTAL CONSULTANTS, INC. Sampled: 10/11/01 11658 Huron St., Suite 102

Received: 11/14/01

Northglenn, Colorado 80234

Analyzed: 11/15/01

Sample ID: RECTOR SPIGOT Project No.: CO01-031


Compound Analyzed

Concentration (ug/L) Method

Benzene <0.5 EPA-8260 Toluene <0.5 EPA-8260 Ethylbenzene <0.5 EPA-8260 Total Xylenes <0.5 EPA-8260 TVPH (Purgeable) <0.5 mg/L EPA-8015 Modified

QA/QC SURROGATE RECOVERIES

Compound % Recovery % Rec. Limits

Chlorobenzene 99 75-125 Bromofluorobenzene 96 75-125






DELTA ENVIRONMENTAL CONSULTANTS, INC. Sampled: 10/11/01 11658 Huron St., Suite 102

Received: 11/14/01

Northglenn, Colorado 80234

Analyzed: 11/15/01

Sample ID: RECTOR MW Project No.: CO01-031


Compound Analyzed

Concentration (ug/L) Method

Benzene 1,305 EPA-8260 Toluene 154 EPA-8260 Ethylbenzene 384 EPA-8260 Total Xylenes 272 EPA-8260 TVPH (Purgeable) 8.11 mg/L EPA-8015 Modified

QA/QC SURROGATE RECOVERIES

Compound % Recovery % Rec. Limits

Chlorobenzene 99 75-125 Bromofluorobenzene 97 75-125


Deo lta CHAIN-OF-CUSTODY RECORD AA linvIrnmor :I

550 East Thornton Parkway, Suits 2245 Thornton, Colorado 00225

DELTA PROJECT NO.

0 a-C) 0 i - 3 I INVOICE CODE PAGE

i

OF i

SAM

PLE

MA

TRIX

: S

OIL

(S):

SD AIR

(A):

BU

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): A

GU

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0):

SLU

DG

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): O

TH

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)

p

V i-f-

ANALYSIS REQUESTED LAB NAME

PRINFCT MANAG .1.1.;NI

rAt-U L- TURN AROUND

)1....NoRmAL

0 RUSH

REQUESTED:

/ 20

1-1Z

. Zi

0 0 u.

r ti-nWA, ,7144 -.44-V, I-JA

1.;"-. ,:-

qtiti.' ;'," MOW

,,, j.r?,"*1 lEk'kt

!crN:n,4: /

:RjitE:g LOCATION )/ S-2, /6-FAX/PHONE RESULTS TO:

S MN

`'-- SAMPLE ID SAMPLE LOCATION/DESCRIPTION DATE/TIME SAMPLED

Rf_Csrog. SPl‘,o-r* VJA-1-f-12.__ We-LA..- SP( 4, oT to it k /0 (

Zs (—TO rt. NM./ 1?Ee-t-or_NS M Vn1 t ... /I I /0 I

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GENERAL COMMENTS:

SA4...r ,-€.. 12*-4-tara- Nov" 640,-) k sti*A4 4 oczoe - sA4-IPLE- 7) Ala v/tst git. 64-C. TOTAL NUMBER OF CONTAINERS

1 RELINQUISHED BY { Y (SIGNATURE) DATE 3 RELINdl . D BY R5)721 ( oa...... 1:11' yi 0 5 RELINQUISHED BY (SIGNATURE) 1 DATE

COMPANY TIME COMPANY I .. ....

e_ X ice )1, 1,-4E Co (4,:e_ TI4E

ill / COMPANY

.4, ,, _ . TIME

2 RECEIV Y (tTUR97.1 C

1/ DAT

3 -4 i 4 RECEIVED BY (SIGNATURE) 130D-AT LA :- e.:, _ ;,-,„ -, P:0 : DATE

COMPANY.FX4, c (.4 It (:,..‹... CO Vr. Cr.' In S COMPANY TIME COMPANY xi, a //// v/6/ TIME

Original - Return with Report • Yellow - Lab Copy • Pink - Sampler Copy

APPENDIX C

CROSS SECTIONS AND BORING LOGS

I-

0

z

--11 Iii

C 0 PRIVATE WELL

L ROAD 95 —

90 —

0 E. -

Li 85

'10

Drawn by

JMA

Filename

01031X

Prepared by

Reviewed by

REMONT ENVIRONMENTAL

A F

100 F12

F1

Fl 1 — — -4

:77 claystone.=====_" (silty)-

75 OPEN FIELD

0 20 40 60

Seale (feet)

70 —

B F5

100 -

95 —

z 4 , g so —

clay

80 —

— — - — - — — — — -

siltstan.ei Cic1X-e-Y

80 —

75 —

BO —

Figure 6

CROSS—SECTIONS


Drilling Equipment/Method CME45/HSA

Start/Finish Dote 4/21/03

Total Depth 31'

Boring/Wdl No. Fl

REMONT NVIRONMENTAL

Page 1 of 2

No El Well Installed?

Yes Casing ittr1.(Dia. PVC/2'

I I I (ft. above MSL) I 100.4 I 100.00

Project No./Name C001-031/Kaneb Andover

Drilling Contractor/Driller GSI/Corey

Geologist/Office MRG

Location


Approved By

Size/Type of Bit Sampling Method

Screen: Type Slotted IMtrI. PVC Length 10' I Dia. 2" I Slot Size 0.010"

devotion of: Ground Surface Top of Well Casing Top of Screen Bottom of Screen Ground Water Surface/Date Measured 22.64 4/23/03

Boring/Well Location Sketch Mop aa.o.raa. 1•00n0

rs e ... Ns

• F7

Wit.

O FS SE00-4o o

F4 • SECO-3

seta-2

SeCO- I

tb sa

BORING/WELL CONSTRUCTION LOG

DEPTH (feet)

WELL CONSTRUCTION

UTHOLOGY Penetration Rate

(Blows/ft.)

Sample No. and Interval

PID VALUES

(PPm) GRAPHIC

LOG VISUAL DESCRIPTION

Bentonite

A 2"

i

7 Clay with root fragments, dark brown

with iron oxide staining, stiff, moist

0

---=--_=--- = _ _ c =—=---=

';----:

=== -== --

=___= =cc

.....=._=_._=-

= =..----=_---.

----7.. =_ _ = _-== _-_ _ .

=_ _ _ .= _• .7 _= ._-. _ 2 === -. -_== _-_, _. - === -_—= _- _TE.

." == =_- = • = .-_ c = c == -=

= _ _

Weathered claystone, greyish brown, stiff, dense, hard

•

,

•

•

Blank

./.. #10-20

Sand

REMONT NVIRONMENTAL BORING/WELL

CONSTRUCTION LOG Page 2 of 2 I-1

F1 Location


Project No./Name

C001-031 /Kaneb Andover

DEPTH (feet)

WELL CONSTRUCTION


(Blows/ft.)


VALUES (PPrn)

GRAPHIC LOG

VISUAL DESCRIPTION

25

= = — =

— = — =

— — — = — _

==—=—==. =—==---=

— — — - ...------..,-- ---_--..._—,..- -- --- --- = ,-.-- — —.-- -- -= -,'"

Weathered claystone continued

Water level 22.64'

1

84

_

_ _ _ i--_—

2"

--

--_— — — _ _

—

Silty claystone, grey—olive brown,

fractures with sand, wet

— — — _ — — — _

_ _

— —

— — —_—

— _/---------

# 10-20... ...

slight odor

TD 31'

Silica Sand —

= =

= =

= _

— Screen

------

- ---- -

------

Drilling Equipment/Method

CME45/HSA

REMONT NVIRONMENTAL

Page 1 of 2 Total Depth Boring/Well No.

F2 31'

Size/Type of Bit Sampling Method Start/Finish Dote

4/21 -22/03 Well Installed?

Yes No q 12 Ground Woter Surface/Date Measured

22.81 4/23/03 Elevation of: Ground Surface Top of Well Casing Top of Screen Bottom of Screen

(ft. above MSL) 100.3 I 99.83

Project No./Nome

C001-031/Kaneb Andover Drilling Controctar/Driller

GSI/Corey Geologist/Office

MRG

Location


Approved By

Screen:

Type Slotted 'tart PVC !Length 10' I Dia. 2" I Slot Size 0.010" Casing kitr1.(Dia.

PVC/2'

Boring/Well Location Sketch Map en0J.11,11- 01"WD

mot - Fe. stm—s• n N4.

semo-3 sLto—i

F4 •


DEPTH (feet)

WELL CONSTRUCTION

LITHOLOGY Penetration Rate

(Blows/ft.)


PID VALUES

(DPm) GRAPHIC


15

Bentonite

A 2"

CH

Clay, dark brown with iron oxide staining, very moist, stiff, dense

0

0

n

F Blank

_

#10-20

__ _ _

_ — -- —_—

_—

_ — — — _

--- ___

Silty claystone, iron oxide staining and gypsum in veins, light brown

Silica Sand

2" — — Screen -------


CONSTRUCTION LOG Page 2 of 2 F-1

F2 Project No./Nome

C001 -031 /Kaneb Andover

Location


DEPTH (feet)

WELL CONSTRUCTION

GRAPHIC LOG

UTHOLOGY

VISUAL DESCRIPTION

Penetration Rate

(Blows/ft)


VALUES (PPrn)

Silty claystone continued

77 -

-77---3177- - Water level 22.81'

=

40 -----

45 -----

#10-20 Silica Sand

35 -----

-

- TD 31'

54

Start/Finish Date 4/22/03


CME45/HSA

REMONT NVIRONMENTAL

Page 1 of 2 Total Depth

30' Boring/Well No.

F3

Ground Water Surface/Date Measured Elevation of: Ground Surface Top of Well Casing Top of Screen Bottom of Screen

(ft. above MSL) I 99.9

Project No./Name C001-031/Kaneb Andover

Drilling Contractor/Driller GSI/Corey

Geotogist/Office

MRG

Location


Approved By


Wet Installed? Yes q No

Casing Mtrl./Dia. 'Length I Dia. ISlot Size

Screen: Type I art.

Boring/Well Location Sketch Map CAL...TAIL 00.6.10,

g • F.,

Fe

"4. '"`•

•

StE0-2


DEPTH (feet)

WELL CONSTRUCTION


(Blows/ft.)


PID VALUES

(PPm) GRAPHIC


Cloy, dark brown with iron oxide staining, moist, medium stiff

CH _

--=--.7.==-- Weatherd cloystone, brownish grey, ==== stiff, dense

10 ------ ----- -.. =- : : :-= = 0

= ==== =—=—

====

=-_—=-_-_—

=-.._=_--

....-.=.-==== - =_-. =-_-_

--=-__=--__ Weatherd cloystone, brownish grey with white (gypsum) mottling

—== -- --=

=_---_=—

= === == ----- ---- •-flt-t


CONSTRUCTION LOG Page 2 of 2 F - 1

F3 Location


Project No./Nome C001-031/Kaneb Andover

UTHOLOGY Penetration Sample DEPTH WELL GRAPHIC Rate No. and VALUES (feet) CONSTRUCTION LOG

VISUAL DESCRIPTION (Blows/fl) Interval (PPm)

=====..----.: Weathered claystone continued

========

-- -- :_—= ---= -:

25 ------ _ , . -•T- _ la -_=_- =- s ==== -_===,

t 210

' -. . . _--= _---

30 ------ - - ---==7-1- -TD 30' 18

35 ------ - _

_ _

------

Geologist/Office

MRG Approved By


CME45/HSA

REMONT NVIRONMENTAL

Totol Depth 24'

Boring/Well No. F4

-

ne. Ea

ot • Fe m

• SECO-4•

F* It C•-3 SII04

SECO-1

Fl

Start/Finish Dote

4/22/03


Ground Water Surface/Date Measured Elevation of: Ground Surface Top of Well Casing Top of Screen Bottom of Screen


Boring/Well Location Sketch Map aa*Ira/. 11110.0

Page 1 of 2

Project No./Name

C001-031/Kaneb Andover Drilling Contractor/Driller

GSI/Corey

Location


Well Installed?

Yes Ei No

Casing Mbd./Dia. Screen: Type I WI. I Length Dia. I Slot Size


DEPTH (feet)

WELL CONSTRUCTION


(Blows/ft.)


PID VALUES

(PPm) GRAPHIC


15 - -

CH

/

,,

Clay, dense, stiff, brown with iron oxide staining, hard, moist

I

0 I

0 Sandy claystone, weathered, with

gypsum and iron oxide staining

FREMONT NVIRONMENTAL BORING/WELL


F4 Location


Project No. Name

C001-031 /Kaneb Andover

DEPTH (feet)

WELL CONSTRUCTION


(Blows/ft)


VALUES (PPm)

GRAPHIC LOG

VISUAL DESCRIPTION

43

Weathered claystone continued

------

- ---- -

_ _

------

______

TD 24'

Boring/Well Location Sketch Mop

J

Project No./Nome


GSI/Corey

Location



CONSTRUCTION LOG Page 1 of 2 Boring/Well No. Total Depth

F5

31'

Geologist/Office

MRG Approved By

Size/Type of Bit

Sampling Method Drilling Equipment/Method

CME45/HSA Start/Finish Dote

4/22/03 Well Installed? Screen:

Type Slatted lutri. PVC 'Length 10' Imo. 2" Slot Size 0.010" Elevation of: Ground Surface Top of Well Casing Top of Screen Bottom of Screen Ground Water Surface/Dote Measured

(ft above MSL) I 100.3 I 99.83 I I I 22.81 4/23/03

No

Casing Mtrl./Dia.

PVC/2' Yes

DEPTH (feet)

WELL CONSTRUCTION


(Blows/ft.)


PID VALUES

(PPm) GRAPHIC


15

Bentonite

4 2"

Cloy, dark brown with iron oxide staining, very moist, stiff, dense

0

n

•

Blank

- ---

#10-20 40,

__ _ _

--- ___ ____ —___—

—

Siltstone, clayey, hard, dry Silica Sand



F5 Project No./Nome

C001-031/Kaneb Andover

Location


DEPTH (feet)

WELL CONSTRUCTION

GRAPHIC LOG

LITHOLOGY

VISUAL DESCRIPTION

Penetration Rate

(Blows/ft)


VALUES (PPrn)

Silty claystone 0

t 10-20 ilica

Sand

- 2" — Screen

— -7-

0

• Clayey siltstone, light brown, fractured

0

TD 31'

35 -----

40 -----

45 -----

d•Pilrad- 00460

• F7

mm lir SECO-4• "*.,.$4,

IF4 • ItCV .s• SEt0 -2

Boring/Well Location Sketch Map

REMONT NVIRONMENTAL

Page 1 of 2 Boring/Well No.

F6 Project No./Name



MRG


Location


Total Depth

24.5'

Approved By

Sampling Method

Top of Well Casing Ground Surface

99.3


CME45/HSA Well Installed?

Yes D No

Elevation of:

(ft. above MSL)

Size/Type of Bit

'Length Top of Screen Bottom of Screen

Start/Finish Date 4/22/03

'Slot Size Ground Water Surface/Date Measured

Casing Mtrl./Dio. Screen:

Type

DEPTH (feet)

WELL CONSTRUCTION


(131aws/fL)


PID VALUES

(PPm) GRAPHIC


_ _ _ _ _

— — —

CH

Clay, dark brown, stiff, dense, moist, iron oxide staining

0

0 ---=

— ---- _--

—_—

Siltstone with minor cloy, white/grey, hard, fractured

--=_=---_

== ---;:-- -- --- ----

Cloystone with white mottling



F6 Location



DEPTH (feet)

WELL CONSTRUCTION


(Blows/ft.)


VALUES (Pram)

GRAPHIC LOG

VISUAL DESCRIPTION

25

40

------

------

------

------

------

------

------

=======_-_---- Claystone

0

Siltstone, white

=====n,

__.==_-

" • .- . - -=== ==

Claystone, with gypsum in veins, brown, wet

,.'

. • :

TD 24.5'

Geologist/Office

MRG Approved By

REMONT NVIRONMENTAL

Page 1 of 2

Ground Water Surface/Dote Measured Devotion of: Ground Surface Top of Well Casing Top of Screen Bottom of Screen


Boring/Well No. Total Depth

F7 I 21' Project No./Name

C001-031 /Kaneb Andover Drilling Contractor/Duller

GSI/Corey

Location


Boring/Well Location Sketch Map CAPITAL Plellaig

MC0-40

MCO—]

• 0-

st.co,

Fe • re •


CME45/HSA Well Installed?

Yes No

Size/Type of Bit

Screen: Type I kltrl. I Length

Sampling Method

I Dia'

Start/Finish Date

4/22/03

I Slot Size

Casing Litr1./Dia.


DEPTH (feet)

WELL CONSTRUCTION


(Blows/ft.)


PID VALUES

(PPm) GRAPHIC


10 ------

'

7

Clay, dark brown with iron oxide staining, moist, very stiff and dense

0

58 - - - - - -t--_==_-===.---

___ ___-

f...-z-4f-_-=-7-2----2 ;

=--==--: 1---- - =1-1 -.=,.=...-.

JETL4-9EArg

=i3=E=Ef1=2

- —, -

--:-.7. ---= =--__a

=-14914. .: --= --= ----- =—==-:-- ; ---=----=-= -=-=-=-=,-=-=

Weathered claystone, dark brown with iron oxide staining, very stiff and dense

petroleum odor

- - - _

_ -

-

Siltstone, white, dry, hard



F7 Location



DEPTH (feet)

WELL CONSTRUCTION


(Blows/ft.)


VALUES (PPrn)

GRAPHIC LOG

VISUAL. DESCRIPTION

25 ---- -

—__--__ ___ _

Siltstone continued

TD 21'

------

------

------

------

______

Project No./Name

C001 —031 /Ka neb Andover Drilling Contractor/Driller


MRG Approved By

REMONT NVIRONMENTAL


31' Boring/Well No.

F8

No ID Well Installed?

Yes

Ground Water Surface/Dote Measured

23.15 4/23/03 Elevation of: Ground Surface Top of Well Casing Top of Screen Bottom of Screen

(ft. above MSL) 100.5 ) 100.28


CME45/HSA Casing Mtryttio. PVC/2'

Start/Finish Date

4/23/03

Slot Size 0.010"

Screen: Type Slotted !mut PVC Length 10' Dia. 2"

Location

Pipe Line Company Andover, Kansas


I -I

n ro

• n

MI I dr

F4 • Rao-.7-.7

.

FII •



DEPTH (feet)

WELL CONSTRUCTION


(Blows/fl)


PID VALUES

(PPrn) GRAPHIC


Bentonite

CH

4

Cloy, dark brown with iron oxide staining, stiff, dense, moist

0

0

0

2" = =-, _ =-1; =_- = r: =_- = = _

-_. a =_-.- = :: =-_ = ...,-.-- _ = == a= _-.-= = = ---=_-_---=-__=

------=---i = . — .. _ _ __, ___ ..

_=== _-_ .,' _-=-: _ .-. -_-_- 7 ,

=r- -- -T-. = =

=_=- = _-=_•= --_.= =_= a-_- a .-=-_ =_._.2 a:

= = =4.1

=-z. = == ==

-,__

Weatherd claystone, reddish brown, iron oxide staining, stiff, dense

.

, Blank

10-20 Silica Sand


CONSTRUCTION LOG pogo 2 of 2 F-1

F8 Location


Project No./Nome

C001-031/Kaneb Andover

DEPTH (feet)

WELL CONSTRUCTION


(Blows/ft.)


VALUES (PPrn)

GRAPHIC LOG

VISUAL DESCRIPTION

25

35

------

10-20

=

= —

_ =

=

= _

2

----- -=-----:

= ----=_—_—_

_ = --- . ==---__.=---

= : =. .- = 71.= _- ....._= -= . - .====.1

_.= _-- .. == .- _—= == 7= _- =-_ == =__=--__=-- = _=-: -----_-=m

== = === === LE

Claystone continued

Water level 23.15'

_. hard with white crystals in veins

.

0

0

0

ilica Sand

------

— =

=

= = —

_

— Screen

- -- - - --

Silty weathered claystone, moist-wet _ —

7--

------

------

- -- -- -

TD 31'

•


CME45/HSA Sampling Method Size/Type of Bit Start/Finish Date

8/5/03

FEMONT NVIRONMENTAL

Page 1 of 2 Boring/Well No.

F9 Total Depth

27'

Ground Water Surface/Dote Measured

Screen:

Type Slotted PVC !Length 10' IDia. 2" Isot Size 0.010" Elevation of: Ground Surface Top of Well Casing Top of Screen Bottom of Screen


Project No./Name


GSI/Steve Geologist/Office

PVH

Location


Approved By na •

(ft. above MSL)

No El Casing Mtr1.(Dia. PVC/2 .

Well Installed? Yes


DEPTH (feet)

WELL CONSTRUCTION


(Blows/ft.)


PID VALUES

(PPm) GRAPHIC


15

Bentonite

- — — —

10-20

::$

g:

)•..

X*:

:::

446

nX•

4•:.:.

:•:*:

:::

:::

:::::

":+::

X*: ..•

* ::

'4.4:4,

A& n:, .1".** V I nn•

:

••.

•

:•X

0: M

ON

'e:*

k:::: $::

';:O :

W

K.:4

•;+;

NV M

it .* 40:4 4

, kAo ke

N .

K.:. :$

'4* OM tl,

. .,,,+

i:I:i

k::::

0

2„

Blank

0:44;

Clay, dark brown, hard, no odor staining, moist, very stiff and dense

MIN

I Limestone, grey

CH

Cloy, dark brown, no odor

Silica Sand



F9 Location



DEPTH (feet)

WELL CONSTRUCTION


(Blows/ft.)


VALUES (PPm)

GRAPHIC LOG

VISUAL DESCRIPTION

25

30

40

10-20 Silica Sond

- - - - -

=

/ r' / C H /A ........ "4,

Clay. a/o

0

2,, --= _-_=____--

-- --- --- - -- --- ---

---- - — — - — —

- -

_

Weathered claystone, hard, no odor

Water level •-22'

-

TD 27'

Screen

-----

_ _

------

------

_ -

- - -- -

- - - - -

F

0n•n••••11. C.nn••••••n••••nn• F 1 2

REMONT NVIRONMENTAL

Page 1 of 2

Project No./Name


GSI/Steve GeologisVOffice

PVH


Location


Approved By


J

Boring/Well No. Total Depth

F10

27'


CME45/HSA Casing MtrI/Dia.

PVC/2'

Size/Type of Bit

Sampling Method

Screen:

Type Slotted )MW. PVC !Length 10' Iola. 2"

Start/Finish Dote

8/5/03

Slot Size 0.010" Well Installed?

Yes

No D

Devotion of: Ground Surface Top of Well Casing Top of Screen Bottom of Screen

(ft. above MSL)

Ground Water Surface/Dale Measured

DEPTH (feet)

WELL CONSTRUCTION


(Blows/ft.)


PID VALUES

(PPrn) GRAPHIC


15

B e n t o n i t e

P+:

n 1 XI 1 :•M

••n•n O.

tvt Nov 4:to oto

v.* mo• ••, :

t.::::

:•:

t o, t•:.:

n••n•• ;14 V W .c.,,:. *:: A. '4:.... :•:*: ::•:: .::::

4.1.

..: C.••• 0

,:.4

1:Iv

1:4o:

a

to,. o:.: koto

Itsts

*To

a

lex K.•4

'4.•04 VA 0 0: °0:••

0 C.: te.4 K.:4 ivi c::::

egg

:.

VA

ow

toto

a

Blank

''"/ "4P'. YV

A.,* '

'No -.n .'*n

'I'4. •

— N

:•:*:

Brown soil, no odor

r

n

Clay, brown, no odor

- — — —

10-20

Lumwommi Thin limestone layer, grey

F7

C ly

lf 4

Clay, brown, no odor

H

WA 1 1' — "1 Ca Thin limestone layer, grey

jClay, brown, no odor

/ staining, moist, very stiff and dense

Silica Sand



F10 Location


Project No_Mame C001 —031 /Kaneb Andover

DEPTH (feet)

WELL CONSTRUCTION


(Blows/ft.)


VALUES (PPril)

GRAPHIC LOG

VISUAL DESCRIPTION

25

#10-20 2''

------= - — — - -_--_z _ --- —______--

Weathered shale, no odor, rock fragments, some iron staining, light brown

Water level -22'

-

-

-

TD 27'

0

Silica Sand

- --- -

Screen

-

------

------

------

_ _____

— — —

- — — - — — - — — — --- — — —

- — — - — — - — — —

- — — -

•

ENVIRONMENTAL


25' Boring/Well No.

F- 11

Size/Type of Bit Sampling Method Start/Finish Date

8/5/03

Ground Water Surface/Dote Measured Elevation of: Ground Surface Top of Well Casing Top of Screen Bottom of Screen

(fL above MSL)

DEPTH (feet)

WELL CONSTRUCTION


(Blows/fL)


PID VALUES

(PPrn) GRAPHIC


15

_

Benton i t e

iii

0:

_ _ _ _

:::::

...... v..

.4•:

:•:•: .24. *: v. .........n

4v. t:*

:v: 44. 0:

t•*

...:* ::•:.:

tt, :::::

41:44

::::: .....,

::

444:

kV om w.

i* W ow ;: ♦ o:iv0 o; vv. v1, '444 ;::$ ;v•:

ett I I! Ki.

::$

•:,.N :•:, s.:.

1+: n•::::

g$ Mgt

ow M

k:$ 2"

Blank

C H

.4.

Cloy, brown, stiff, no odor

o

,

0

A

*:

i:v1 -, A -. .- ra -.2 Thin weathered limestone, no odor

C H

/

Cloy, brown, no odor

110-20

______ —

Weathered shale

Water level ~20'

Silica Sand



CME45/HSA

Boring/well Location Sketch Map

Project No./Name



PVH

Location


Approved By

Fin eyomas. dimata tameormasave

Casing 'AUL/Dia. PVC/2'

Screen:

Type Slotted [mtri. PVC Length 10' 'Dia. 2" I Slot Size 0. 0 1 d' No

Well Installed?

Yes Et



Fll Project No./Name C001-031/Kaneb Andover

Location


DEPTH (feet)

WELL CONSTRUCTION

GRAPHIC LOG

UTHOLOGY

VISUAL DESCRIPTION

Penetration Rate

(Blows/ft.)


VALUES (PPm)

25

i10-20 ilica

Sand

Weathered shale

wet at 22', rose to 20'

TD 25'

30 -----

35 -----

45 -----

40 -----


CME45/HSA

REMONT NVIRONMENTAL


27' Boring/Well No.

F12

Start/Finish Date

8/6/03


Well Installed?

Yes No D Ground Water Surface/Date Measured Elevation of: Ground Surface Top of Well Casing Top of Screen Bottom of Screen

(ft. above MSL) I


roject No./Name

C001-031/Kaneb Andover Drilling Contractor/Duller


PVH

Location


Approved By not

Screen:

Type Slotted I Mtrt. PVC I Length 10' I Dia. I Slot Size 0 .0 1 0" Casing MtryDia.

PVC/2'


DEPTH (feet)

WELL CONSTRUCTION


(Blows/ft.)


PID VALUES

(PPm) GRAPHIC


Bentonite

110-20

*:

:::::

*: 0 *: •••• 4:4 0

WO :1'441' MO

'4:4:• ':•:•:

O2 W

....t. A ri., '

'401. :•:•:

,.*:

tO 0 .40.

iii, :

M

0 tx

:,. 2"

::::$

M C4 0 041

o'.'v'4.4 441 0 00 0: VA 'AN

C.:.•!, A•:4

ev, 'AN

(:+: *:'

M.

v:: 0 M

a

:$

0

Blank

CL

'-,1 A'

* N 40-.4/

s*..- • '.‘ S,....VI%n :•• 1..0

Dark soil, no odor

0

n

V Cloy, no odor, iron staining and black flecks

/7"

Clay, softer, w/some weathered shale Silica Sand



F12 Location


Project No.7Nome C001 —031/Kaneb Andover

DEPTH (feet)

WELL CONSTRUCTION


(Blows/ft.)


VALUES (PPm)

GRAPHIC LOG

VISUAL DESCRIPTION

25

30

35

40

#10-20 2'

1

/''

Claspaleligt'firtagbrnroewnnt; softer, w/some

Weathered shale, no odor M 27'

Silica Sand

----- -

- — — — —

- — — — —

- — — — —

Screen

------

------

- _

_ _ _ _ _ _

Documents

Aam °cora ve IteAam (into ° °cora five Ite bLR SCANNED FEB 1 7 2012 Prepared by: Fremont Environmental Inc. 1530 North Boise Avenue, Suite 205 Loveland, Colorado 80538 (970) 663-2301