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A member of the Anglo American plc group
1
EVALUATION OF IRON ORE SINTERS AND PELLETS FOR BF AND DR USE
Presented by: MS Mashao
Kumba Iron Ore
A member of the Anglo American plc group
2
OVERVIEW
• List of most popular tests performed:– Tumble Strength (ISO 3271)– Crushing Strength (ISO 4700)– Swelling Index (ISO 4698)– Size range– Reducibility (ISO 4695)– Relative Reducibility (ISO 7215)– Reduction Disintegration (ISO 4695)– Reduction Disintegration and metallization
for DR feedstock (ISO 11257)
A member of the Anglo American plc group
3
OVERVIEW
• List of most popular tests performed:– Corex tests– REAS (Reduktion Erweichung und
Abschmelzung)– Drop tests
A member of the Anglo American plc group
4
PHYSICAL PROPERTIES
• Important properties– Size distribution– Strength– Degradation
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5
PHYSICAL PROPERTIES
Screening
Transport
Blast Furnace
Top
Middle Shaft 950 °C
Bosh 1100 °C
Bosh +1300 °C
Shaft 500 °C
A member of the Anglo American plc group
6
PHYSICAL PROPERTIES
• Tumble Strength– Percentage of + 6.3mm fraction gives TI– Percentage of – 0.5mm fraction in gives AI– Criterion of acceptance:
70% for TI Less than 5% for AI
A member of the Anglo American plc group
7
PHYSICAL PROPERTIES
• Compression Strength– Criterion of acceptance:
250 kg/pellet
A member of the Anglo American plc group
8
PHYSICAL PROPERTIES
• Characterize material susceptibility to:– Breakage– Degradation
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9
METALLURGICAL PROPERTIES
• Important properties– Reduction Disintegration– Reducibility– Swelling– Sticking– Softening and melting
A member of the Anglo American plc group
10
METALLURGICAL PROPERTIES
Screening
Transport
Blast Furnace
Top
Middle Shaft 950 °C
Bosh 1100 °C
Bosh +1300 °C
Shaft 500 °C
RDI
RI &RR
REAS & RUL
REAS
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11
REDUCTION DISINTEGRATION
• RDI for blast furnace• RDI for Midrex• RDI for Corex
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12
REDUCTION DISINTEGRATION
Blast Furnace
Direct Reduction
% - 3.15 mm < 40
% - 0.5 mm < 5
Acceptable Preferred
% -3.36 5 Max. 2
% Metallization 91 Min 93
A member of the Anglo American plc group
13
REDUCTION DISINTEGRATION
– Decrease in burden permeability– Poor gas distribution– Scaffolding– Increases fuel consumption– Lower productivity– Increased dust load in off gas– Material more susceptible between (400-
600)°C
A member of the Anglo American plc group
14
REDUCIBILITY
Screening
Transport
Blast Furnace
Top
Middle Shaft 950 °C
Bosh 1100 °C
Bosh +1300 °C
Shaft 500 °C
RI & RR
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15
REDUCIBILITY
• Reducibility Index• Relative Reducibility
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16
REDUCIBILITY
• Reducibility for sinters generally higher– Typical values for sinters (1.1 -1.4)%/min– Typical values for pellets (0.8 -1.4)%/min
• Final degree of reduction:– Typical value for sinters (60-70)%– Typical value for pellets (50-60)%
A member of the Anglo American plc group
17
REDUCIBILITY
• Productivity requires reducible feedstock
• Reducibility depends on:– Porosity– Surface area– Gas-solid contact
A member of the Anglo American plc group
18
FREE SWELLING INDEX
• General criterion for acceptance:– Swelling not be higher than (25-30)%– Noted that alkalis promote excessive
swelling
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19
FREE SWELLING INDEX
• Increase in volume which in turn decreases voids in charge
– Impedes gas flow – Pressure drop
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20
STICKING INDEX
• Impact on maximum bustle gas temperature
• Bustle temperature determines overall productivity
A member of the Anglo American plc group
21
METALLURGICAL PROPERTIES
Screening
Transport
Blast Furnace
Top
Middle Shaft 950 °C
Bosh 1100 °C
Bosh +1300 °C
Shaft 500 °C
REAS
REAS
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22
REAS
• Ideal BF conditions• Temperature profile increases from
ambient to 1600°C in 8hrs• Sample subjected to a fixed load
A member of the Anglo American plc group
23
REAS
– Softening temperature– Melting temperature– Dripping temperature– Differential pressure (dP)– Degree of reduction at time and
temperature– Compaction at time and temperature– Mass of dripping melt at time
A member of the Anglo American plc group
24
REAS
REAS TEST RESULTS F2040326 RMT2231B
0
200
400
600
800
1000
1200
1400
1600
1800
1 25 50 75 100 125 150 175 200 225 250 275 300 325 350 375 400 425 450 475
Time (min)
Tem
per
atu
re (
°C);
dP
(m
mH
2);
Dri
p
mas
s (g
); C
-sta
rt (
g/m
in)
0
20
40
60
80
100
120
Com
pac
tion
(%
); R
edu
ctio
n (
%)
F-Temp S-Temp dP Mass C-start Compaction Total reduction
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25
REAS
• General criterion for acceptance:– Cohesive zone should be small but at high
temperatures– Relative drip mass at least 70 per cent– Shape of dP curve
• Width• Height• Position of peak(s)
A member of the Anglo American plc group
26
PELLET vs. SISHEN 20mm
Pellet 20 mm ore
Size Range
9 x 16 mm 85 % - Min95% – Pref.
83.5 %
Fines 5 % Max< 3% Pref.
3.9 %
Tumble Strength
% + 6.3 mm 92 % 88
% - 0.5 mm 6 4.4
Hot Load
% Metallization 98 98
% Clustering 0 0
Linder
% Metallization 91 95
% < 3.36 5 2.4 (10)
Price $/tonne 240 205