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•-INM31A SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION HI
Project No.: CHEM Site: A440-S Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 80
Lab Sample ID:
0770306PD4RR
Group:
039578RR
Lab File ID: E1038.D
Date Received:
Date Analyzed:
GC Column: DB624 ID: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
. . . . Concentration Units:GAS No. Compound (ug/L or ug/Kg) ug/Kg
>
<1330-20-7 Xylenes(total) 50
•
3/8/95
3/17/95
1.0
Qu
,.
(uL)
Page2of2 FORM I VGA UUUU«J<* 3/90
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ————————•——
0770307D02Lab Name: CHEMTECH Contract: US EPA REGION Hi
Project No.: CHEM Site: A440-S Location: _________ Group: ___
Matrix: (soil/water) SOIL Lab Sample ID: O39579
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1039.D
Level: (low/med) LOW Date Received: 3/9/95
% Moisture: not dec. 18 Date Analyzed: 3/17/95
GC Column: DB624________ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _____(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChlorome thaneBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1,1-Dichloroethanel,2-Dichlorocthene(total)Chloroform1,2-Dichloroc thane2-Butanone1,1,1-Triculoroethane •Carbon TctrachlorideBromodichloromethanc1 ,2-Dichloropropane •cis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobcnzeneEthylbenzeneStyrene
1212 ,12121219121212121212121212121212121212121212121212121212121212
UUUUUBUUUU
- uUuuuuuuuuuuuuuuuuuuuuu <
Page 1 of 2 0FORMIVOA 00000.3 3/90
1A. . ._ VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION II
Project No.: CHEM Site: A440-S Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 18
Lab Sample ID:
SAMPLE NO.
0770307D02
Group:
O39579
Lab File ID: E1039.D
Date Received:
Date Analyzed:
GC Column: DB624 ED: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenes(total)
.
'
.
12
3/9/95
3/17/95
1.0
Q
U
(uL)
•
Page 2 of 2
°00064
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ————————
0770307D28Lab Name: CHEMTECH Contract: US EPA REGION H
Project No.: CHEM Site: A440-S Location: _________ Group: ___
Matrix: (soil/water) SOIL Lab Sample ID: 039580
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1028.D
Level: (low/med) LOW Date Received: 3/9/95
% Moisture: not dec. 57 Date Analyzed: 3/13/95
GC Column: DB624_____ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideCuloroethaneMethylene ChlorideAcetoneCarbon Bisulfide1 , 1-Dichloroethene1, 1-Dichloroe thane1 ,2-Dichloroethene( total)Chloroform1,2-Dichloroethane2-Butanone1, 1, 1-Trichloroe thaneCarbon TetrachlorideBromodiculoromethane1,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroethaneBenzenemns-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroetnene1, 1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
2323232323210572323232323232323232323232323232323232323232323232323
UUUuu
uuu
-. uuuuuuuuuuuuuuuuuuuuuuu
Page 1 of2
flft3l6i*75 MKMIVOA 000070 3/9°
LabNam
Project N
Matrix:
Sample u
Level:
% Moisti
GCColui
SoilExtr
* • "" -~" ~ 1AVOLATILE ORGANICS ANALYSIS DATA SHEET
e: CHEMTECH Contract: US EPA REGION II
o.: CHEM Site: A440-S Location:
(soil/water) SOIL
it/vol: 5.0 (g/mL) G
(low/med) LOW
ire: not dec. 57
Lab Sample ID:
SAMPLE NO.
0770307D28
Group:
O39580
Lab File ID: E1028.D
Date Received:
Date Analyzed:
ran: DB624 ID: 0.53 (mm) Dilution Factor:
act. Volume: (uL) Soil Aliquot Volume:
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg
. . __._ _ - - • • -1330-20-7 Xylencs(total)
*
•
23
*
3/9/95
3/13/95
1.0
QU
.
(uL)
Page2of2FORMIVOA. 000071 3/9°
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET —————————^~~
0770307D28RRLab Name: CHEMTECH Contract: US EPA REGION HI _____
Project No.: CHEM Site: A440-S Location: _________ Group: ___
Matrix: (soil/water) SOIL Lab Sample ID: O39580RR
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1040.D
Level: Gow/med) LOW Date Received: 3/9/95
% Moisture: not dec. 57 . Date Analyzed: 3/17/95
GC Column: DB624________ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: _________ (uL)
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-4 '75-00-375-09-267-64-175-15-075-35475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1, 1-Dichloroethanel,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1,1.2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1, 1,2,2-TetrachloroethaneTolueneChlorobenzeneEtbylbenzeneStyrene
232323232345742323232323232323232323232323232323232323232323232323
UUUUUB
- UUU
~ UUuuuuuuuuuuuuuuuuuuuuu
Page 1 of2FokMIVOA 000072 3/90
LabNam
Project Is
Matrix:
Sample u
Level:
% Moistt
GCColui
Soil Extr
. 1AVOLATILE ORGANICS ANALYSIS DATA SHEET
K CHEMTECH Contract: US EPA REGION ID
fo.: CHEM Site: A440-S Location:
(soil/water) SOIL
rt/vol: 5.0 (g/mL) G
(low/med) LOW
:ire: not dec. 57
Lab Sample ID:
SAMPLE NO.
0770307D28RR
Group:
O39580RR
Lab File ID: E1040.D: .
Date Received:
Date Analyzed:
inn: DB624 ID: 0.53 (mm) Dilution Factor:
act Volume: (uL) Soil Aliquot Volume:
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenes(total)
*
.
.
-
23
•
3/9/95
3/17/95
1.0
Q,U
(uL)
Page 2 of 2 .FORMIVOA n 3/9°
•;AR3 161*7.8 ....
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
0770307D29Lab Name: CHEMTECH Contract: US EPA REGION IE
Page 1 of 2
Project No.: CHEM Site: A440-S Location: '______ Group: ___
Matrix: (soil/water) SOIL Lab Sample ID: O39S81
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1041.D
Level: (low/med) LOW Date Received: 3/9/95
% Moisture: not dec. 68 Date Analyzed: 3/17/95
GC Column: DB624________ ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______._ (uL)
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-57M3-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-7100-4M100-42-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dichloroe thane1 ,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-Trichloroe thaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-TetrachlorocthaneTolueneChlorobenzcneEmylbenzeneStyrcne
313131313145723131313131313131313131313131313131313131313131313131
UUUuuB
UUU
. UUUUUuuuuuuuuuuuuuuuuuu
AR3i6t*79 KB*'™ 000082 3/9°
1A -VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION U
Project No.: CHEM Site: A440-S . Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 68
Lab Sample ID:
SAMPLE NO.
0770307D29
Group:
039581
Lab File ID: E1041.D
Date Received:
Date Analyzed:
GC Column: DB624" ED: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units;CASNo. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenes(total)
-
•
31
3/9/95
3/17/95
1,0
QU
-.,
'
(uL)
Page2of2 00008'}UUUUOOFORMIVOA 3/90
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
0770307D22Lab Name: CHEMTECH Contract: US EPA REGION IE
Project No.: CHEM Site: A440-S Location: _________ Group: ___
Matrix: (soil/water) SOIL Lab Sample ID: O39582
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1042.D
Level: (low/med) LOW Date Received: 3/9/95
% Moisture: not dec. 31 . Date Analyzed: 3/17/95
GC Column: DB624________ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4KXW2-5
DichlorodifluorometbaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1, 1-Dichloroethanel,2-Dichloroethene(total)Chloroform1,2-Dichloroe thane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroetuaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTerrachloroethene1,1,2,2-Tetrachloroe thaneTolueneChlorobenzeneEthylbenzeneStyrene
141414141422841414141414141414141414141414141414141414141414141414
UUUUUB
UUUUUUU
. U, UUUUUUUUUUUUUUuuuu
Page 1 of2
flR3l6i»8lFOWIV0*' 000089 3"°
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION EL
Project No.: CHEM Site: A440-S Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 31
Lab Sample ID:
SAMPLE NO.
0770307D22
Group:
O39582
Lab File ID: E1042.D, . - • f • • '
Date Received:
Date Analyzed:
GC Column: DB624 ED: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenes(total) 14
3/9/95
3/17/95
1.0
QU
(uL)
»
Page 2 of2FORMIVOA nnnnnn 3/9°000030
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ———————
0770307D34Lab Name: CHEMTECH Contract: US EPA REGION IE__________
Project No.: CHEM Site: A440-S Location: _________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: O39583
Sample wt/vol: 5.0 (g/mL) G , Lab File ID: E1031.D
Level: (low/med) LOW Date Received: 3/9/95
% Moisture: not dec. 37 Date Analyzed: 3/13/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-57W3-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromcthaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1, 1-Dichloroethane1 ,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1 , 1 , 1-TrichloroethaneCarbon TetrachlorideBromodicfaloromethane1,2-Dichloropropanecis-l,3-DichloropropencTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzencEthylbenzeneStyrcnc
161616161665461616161616161616161616161616161616161616161616161616
UUuuu
uuu
- uuuuuuuuuuuuuuuuuuuuuuu
Page 1 of 2AR316^83 FORMIVOA 000096 3/9°
LabNam
Project N
Matrix:
Sample u
Level:
% Moisti
GC Colm
Soil Ex tr
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
e: CHEMTECH Contract: US EPA REGION II
o.: CHEM Site: A440-S Location:
(soil/water) SOIL Lab Sample ID:
t/vol: 5.0 (g/mL) G
(low/med) LOW
ire: not dec. 37 ..... __._...._
SAMPLE NO.
0770307D34
Group:
039583
Lab File ID: E1031.D
Date Received:
Date Analyzed:
con: DB624 ED: 0.53 (mm) Dilution Factor
act Volume: (uL).
Soil Aliquot Volume:
3/9/95
3/13/95
1.0
(uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
1330-20-7 Xylenes(total)
•
16 U
Page 2 of 2 . --• SR3iC,.^'F°RMI™A. 000097 3/9°
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
0770308D05Lab Name: CHEMTECH' Contract: US EPA REGION EC
Project No.: CHEM . Site: A440-S Location: _________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: 039584
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1043.D
Level: (low/med) LOW Date Received: 3/9/95
% Moisture: not dec. 48 - Date Analyzed: 3/17/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-3
DichlorodiOuoromethaneChloromethane
74-83-9 Bromomethane75-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
Vinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dichloroc thanel,2-Dichloroethene(total)Chloroform1 ,2-Dichloroe thane2-Butanone1,1,1-Trichloroethane .Carbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEmylbenzeneStyrene
191919191928211919191919191919191919191919191919191919191919191919
UUUuuB
UUuuuuuuuuuuuuuuuuuuuuuuuu
Page 1 of 2
••;«R3I61*85 •' FORMIVOA 000103 3/9°
LabNain
Project N
Matrix:
Sample w
Level:
% Moisti
GCColiu
Soil Extr
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
e: CHEMTECH Contract: US EPA REGION II
o.: CHEM Site: A440-S Location:
(soil/water) SOIL
rt/vol: 5.0 (g/mL) G
(low/med) LOW•
ire: not dec. 48
Lab Sample ID:
SAMPLE NO.
0770308D05
Group:
039584
Lab File ED: E1043.Ds'
Date Received:
. Date Analyzed:
nn: DB624 ED: 0.53 (mm) Dilution Factor:
act Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound , (ug/L or ug/Kg) ug/Kg
• -- -1330-20-7 Xylenes(total)
.
•
,
— - -19
.
3/9/95
3/17/95
1.0
Q
U
.
»
(uL)
Page 2 of2At FORM I VGA nr\nin/! 3/9°AR3i6if86 000104.
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ——————————
0770308D03Lab Name: CHEMTECH Contract: US EPA REGION IE
Project No.: CHEM Site: A440-S Location: _________ Group: ___
Matrix: (soil/water) SOIL Lab Sample ID: 039679
Sample wt/vol: 5.0 (g/mL) G . Lab File ID: E1044.D
Level: '(low/med) LOW Date Received: 3/10/95W BWMH-l - | «————————^^MM
% Moisture: not dec. 56 Date Analyzed: 3/17/95
GC Column: DB624________ ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _____(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-57143-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-410042-5
DichlorodiQuoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disuifide1, 1-Dichloroethene1, 1-Dichloroethane1 ,2-Dichloroethene( total)Chloroform1,2-Dichloroc thane2-Butanone1,1,1-Trichloroethane 'Carbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromofonn4-Methyl-2-Pentanone2-HexanoneTetrachloroethcne1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
232323232338232323232323232323232323232323232323232323232323232323
UUUuuBU
- UUUUUUUuuuuuuuuuuuuuuuuuuu
Page 1 of2FORMIVOA 000110 2/90
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab.Name: CHEMTECH Contract: US EPA REGION ID
Project No.: CHEM Site: A440-S Location:
Matrix: (soil/water) SIOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) IX>W
% Moisture: not dec. 56
Lab Sample ID:
SAMPLE NO.
0770308D03
> Group:
O39679
Lab File ID: E1044.D
Date Received:
Date Analyzed:
GC Column: DB624 ED: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xyl«nes(total)
>
%
•
23
•
3/10/95
3/17/95
1.0
Q
U
••-
(uL)
Page 2 of2
AR3I6488 FORJiIVOA 000111 3/9°
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ———————
0770313D06Lab Name: CHEMTECH Contract: US EPA REGION II '
Project No.: CHEM Site; A440-S Location: _________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: O39815
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1045.D
Level: (low/med) LOW Date Received: 3/15/95
% Moisture: not dec. 75 Date Analyzed: 3/17/95
GC Column: DB624 EO; 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: _______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1 , 1-Dichloroethanel,2-Dichloroethene( total)Chloroform1 ,2-Dichloroe thane2-Butanone1 , 1 , 1 -TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-l,3-DicMoropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromofonn4-Metbyi-2-Pentanone2-HexanoneTetrachloroethene1, 1,2,2-TetrachloroethaneTolueneChlorobcnzencEthylbenzeneStyrene
40404040406917040404040404040404040.40404040404040404040404040404040
UUuuuB
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Page 1 of 2
000117
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION U
Project No.: CHEM • Site: A440-S Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 75
Lab Sample ID:
SAMPLE NO.
0770313D06
Group:
039815
Lab File ID: E1045.D
Date Received:
Date Analyzed:
GC Column: DB624 ED: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg
'.•
1330-20-7 Xylenes(total)
,
,
-
40
,
..-.
3/15/95
3/17/95
1.0
QU
(uL)
Page 2 of2FORMIVOA 000118 3/9°
1A _ SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
0770313D06RRLab Name: CHEMTECH Contract: US EPA REGION ID
Project No.: CHEM Site; A440-S Location: _________ Group: ___
Matrix: (soil/water) SOIL Lab Sample ED: 039815RR
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E10S3.D
Level: (low/med) LOW Date Received: 3/15/95
% Moisture: not dec. 75 Date Analyzed: 3/17/95
GC Column: DB624________ ED; 0.53 (mm) Dilution Factor; 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1, 1-Dichloroethanel,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethanc1, 1,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
404040404020021040404040404040404040404040404040404040404040100404040
UUUuu
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- uuuuuuuuuuuuuuuuuuuuuu
Page 1 of2AR3i6t*9i •FOkMIVOA 000119 3/9°
LabNam
Project N
Matrix:
Sample w
Level:
% Moisa
GCColui
Soil Extr
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
~ , * " - - ~ j , - - - - ' -
e: CHEMTECH Contract: US EPA REGION IE
o.: CHEM Site: A440-S Location:
(soil/water) SOIL
t/vol: 5.0 (g/mL) G
(low/med) LOW
ire: not dec. 75
Lab Sample ID:
SAMPLE NO.
07703 13D06RR
Group:
O39815RR
Lab File ID: E1053.D. . . S
Date Received:
Date Analyzed:
am: DB624 ED: 0.53 (mm) Dilution Factor:
net Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenes(total)
.
.. .. .
40
'
.
3/15/95
3/17/95
1.0
Q
U
(uL)
Page 2 of2 r FORMIVOA nnnion 3/9°AR3I6**92 . 0001,0
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ——————————
0770313D07Lab Name: CHEMTECH Contract: US EPA REGION II]
Page 1 of2 . .*•.•
CroRMtvOA 000130
Project No.: CHEM Site; A440-S Location: _________ Group: ___
Matrix: (soil/water) SOIL Lab Sample ED: O39818
Sample wt/vol: v 5.0 (g/mL) G . Lab File ID: E1056.D
Level: (low/med) LOW Date Received: 3/15/95
% Moisture: not dec. 32 Date Analyzed: 3/18/95
GC Column: DB624________ ED; 0.53 (mm) Dilution Factor: 1.0'
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-3 4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5 .
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideCbloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1 , 1-Dichloroethanel,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Butanone1,1,1-Trichloroe thaneCarbon TetrachlorideBromodichloromethane1,2-DichloroproDanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
1515151515591515151515151515151515151515151515151515151515261515
' 15 .
UUUUUBUUUUUUUUUUUuuuuuuuuuuuujfr-:-..uuu
o LabNam
Project N
Matrix:
Sample w
Level:
% Moistt
GCColui
Soil Extr
1A__ : VOLATILE ORGANICS ANALYSIS DATA SHEET
e: CHEMTECH Contract: US EPA REGION IT
o.: CHEM Site: A440-S Location:
(soil/water) SOIL
i/vol: 5.0 (g/mL), G
(low/med) LOW
ax: not dec. 32
Lab Sample ID:
SAMPLE NO.
0770313D07
Group:
039818
LabFileID:E1056.D
Date Received:
Date Analyzed:
on: DB624 ED: 0.53 (mm) Dilution Factor:
ict Volume: (uL) Soil Aliquot Volume:
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xyh!nes(total)
.
.... ___..
15
3/15/95
3/18/95
1.0
QU
•
(uL)
Page 2 of2FORMIVOA . .. 000131 3/9°
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
0770313D6DLab Name: CHEMTECH Contract: US EPA REGION HI _______
Project No.: CHEM Site: A440-S Location: _________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: O39819
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1057.D
Level: (low/med) LOW Date Received: 3/15/95
% Moisture: not dec. 25 Date Analyzed: 3/18/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3 .108-90-7100-41-410042-5
DichlorodifiuoromethaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1,1-Dichloroethanel,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Butanone1, 1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneCbloiobenzeneEthylbenzeneStyrcne
131313131355611313131313131313131313131313131313131313131325131313
UUUuuBBUUUUUUUUUUUUUUuuuuuuuuuuu
Page 1 of 2
000137 3/9°
. . . . . . .- - 1AVOLATILE ORGANIC
Lab Name: CHEMTECH
S ANALYSIS DATA SHEET
Contract: US EPA REGION II
Project No.: CHEM Site: A440-S Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 25
Lab Sample ID:
SAMPLE NO.
0770313D6D
Group:
O39819
Lab File ID: E1057.D
Date Received:
Date Analyzed:
GC Column: DB624 ED: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound . (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenes(total)
.
" ' ' •"" ' *
13
'
3/15/95
3/18/95
1.0
Qu
.
--
-
(uL)
Page 2 of2
>:'-.'"<Wfl3161.96-WVOA 000138" 3/9°
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ———————————
0770313D09Lab Name: CHEMTECH Contract: US EPA REGION II]
Project No.: CHEM Site: A440-S Location: _________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: O39820
Sample wt/vol: 5.0 (g/mL) G . Lab File ID: E10S8.D
Level: (low/med) LOW Date Received: 3/15/95
% Moisture: not dec. 47 Date Analyzed: 3/18/95
GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1,1-Dichloroethanel,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Butanone1, 1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropcneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
191919191975591919191919191919191919191919191919191919191931191919
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Page 1 of 2FORMIVOA rtrvAi AK 3/9°
000145
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION II
Project No.: CHEM Site: A440-S Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not .dec. 47
Lab Sample ID:
SAMPLE NO.
0770313D09
Group:
O39820
Lab File ID: E1058.D
Date Received:
Date Analyzed:
GC Column: DB624 ED: 0.53 (mm) Dilution Factor:i
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg
f - -"
1330-20-7 Xylcnesl total)
'
- •
,^
19
3/15/95
3/18/95
1.0
QU
(uL)
Page 2 of2FORMIVOA 000146 3/9°
lA _ SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
0770313D13Lab Name: CHEMTECH Contract: US EPA REGION EC
Project No.: CHEM Site: A440-S Location: _________ Group: ___
Matrix: (soil/water) SOIL Lab Sample ID: 039823
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1070.D
Level: (low/med) LOW Date Received: 3/15/95
% Moisture: not dec. 67 Date Analyzed: 3/18/95
GC Column: DB624________ ED; 0.53 (mm) Dilution Factor; 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01475-00-3 .75-09-267-64-175-15-075-35475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-710041-4100-42-5
DichlorodiSuoromethaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1,1-Dichloroc thanel,2-Dichloroethene(total) .Chloroform1,2-Dichloroethane2-Butanone1 , 1 , 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromofonn4-MethyI-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TerrachloroethaneTolueneChlorobenzeneEthylbenzcneStyrene
30303030308237030303030303098303030303030303030303030303030380303030
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Page 1 of2
000168 3/9°
TAVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION II
Project No.: CHEM Site: A440-S Location:.
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 67
•Lab Sample ID:
SAMPLE NO.
0770313D13
Group:
039823
LabFHeID:E1070.D>.'
Date Received:
Date Analyzed:
GC Column: DB624 ED: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenes(total)
. - .
.
. *
30
3/15/95
3/18/95
1.0
QU
(uL)
Page 2 of 2 0001 £Quuuib* 3/90
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
0770313D14Lab Name: CHEMTECH Contract: US EPA REGION IE
Project No.: CHEM Site: A440-S Location: _________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: .O39822
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1060.D
Level: (low/med) LOW Date Received: 3/15/95
% Moisture: not dec. 26 Date Analyzed: 3/18/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ________(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-3 .75-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-57143-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4KXW2-5
DichlorodifuioromethaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1 , 1-Dichloroe thanel,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromofbrm4-Methyl-2-Pentanone2-HexanoneTerrachloroethene1, 1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStymie
141414141448141414141414141414141414141414141414141414141414141414
UUUuuBUUUUUUUuuuuuuuuuuuuuuuuuuu
Page Iof2•AR3I650I FORMIVOA 000161 3/9°
IAVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION U
Project No.: CHEM Site: A440-S Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (Eow/med) LOW
% Moisture: not dec. 26
Lab Sample ID:
SAMPLE NO.
0770313D14
Group:
039822
.Lab File ID: E1060.D
Date Received:
Date Analyzed:
GC Column: DB624 ED: 0.53 (mm) Dilution Factor
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:GAS No. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenes(total)
- --
-14
•
3/15/95
3/18/95
1.0
QU
(uL)
Page2of2FORMIVOA 3/9°000162
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
0770313D16Lab Name: CHEMTECH ___ Contract: US EPA REGION IE ________
Project No.: CHEM Site: A440-S Location: _________ Group: ___
Matrix: (soil/water) SOIL Lab Sample ED: O39821
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1069.D
Level: (low/med) LOW Date Received: 3/15/95
% Moisture: not dec. SO Date Analyzed: 3/18/95
GC Column: DB624________ ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CASNo. Compound . (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100414100-42-5
DichlorodiQuoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dichloroe thanel,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1 , 1 , 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
2020202020719320202020202020202020202020202020
, 20202020202012202020
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Page 1 of 2 ... ...AR3J6503 FORMIVOA 000153 3/9°
LabNam
Project N
Matrix:
Sample u
Level:
% Moisti
GCColui
Soil Extr
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
e: CHEMTECH Contract: US EPA REGION EC
o.: CHEM . Site: A440-S Location:
(soil/water) SOIL
l7vol: 5.0 (g/mL) G
(low/med) LOW• - i
ire: not dec. 50
Lab Sample ID:
SAMPLE NO.
0770313D16
Group:
O39821
Lab File ID: E1069.D
Date Received:
Date Analyzed:
mil: DB624 ED: 0.53 (mm) Dilution Factor:
act Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 XylenesUotal)
- '
, i
•
...
..— .
20
~•
• -- -«-.
3/15/95
3/18/95
LO
QU
-•-
'
(uL)
Page 2 of 2FORMTVOA 3/9°
•AR3-I650U-
IA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
0770313PD3Lab Name: CHEMTECH Contract: US EPA REGION U
Project No.: A446-S Site: _____ Location: _________ Group: ___
Matrix: (soil/water) SOIL Lab Sample ID: O39824
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1071.D
Level: (low/med) LOW Date Received: 3/15/95
% Moisture: not dec. 38 Date Analyzed: 3/18/95
GC Column: DB624________ ED; 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-57143-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-414100-42-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1, 1-Dichloroethanel,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Butanone1, 1, 1-TrichloroethaneCarbon TettachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-MethyI-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachIoroethaneTolueneChlorobenzeneEthylbenzeneStyrene
16161616163816161616161616161616161616161616161616161616169.1161616
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Page 1 of2
;'J;"«'R3I6505 'roRMIVOA 000017
1AVOLATILE ORGANIC
Lab Name: CHEMTECH
S ANALYSIS DATA SHEET
Contract: US EPA REGION EC
Project No.: A446-S Site: Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 38
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
GC Column: DB624 ID: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
Page 2 of
1330-20-7 Xylenesdotal) 16
T
SAMPLE NO.
0770313PD3
Group:
O39824
E1071.D
3/15/95
3/18/95
1.0
Qu
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(uL)
3/90
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
0770313D33Lab Name: CHEMTECH Contract: US EPA REGION II
Project No.: A446-S Site: _____ Location: _________ Group: ___
Matrix: (soil/water) SOIL Lab Sample ID: O3982S
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1063.D
Level: (low/med) LOW Date Received: 3/15/95
% Moisture: not dec. 33 Date Analyzed: 3/18/95
GC Column: DB624________ ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (iiL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q.
75-71-874-87-374-83-975-01475-00-375-09-267-64-175-15-075-3575-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-6124-48-179-00-57143-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfidc1 , 1-Dichloroethene1 , 1-Dichloroc thane1 ,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1 , 1 , 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethanc1 , 1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
151515151556
•• 5115151515151515151515151515151515151515151515281515IS
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Page 1 of2
fiR3l6507FORMIVOA 000095 3"°
LabNam
Project N
Matrix:
Sample u
Level:
% Moisti
GCColui
Soil Extr
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
e: CHEMTECH Contract: US EPA REGION IE
fo.: A446-S Site: Location:
(soil/water) SOIL
rt/vol: 5.0 (g/mL) G
(low/med) LOW
ire: not dec. 33
Lab Sample ID:
Lab File ID:. : . •- - .,,.' • •
Date Received:
Date Analyzed:
mn: DB624 ED: 0.53 (mm) Dilution Factor:
act Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenes(total)
t
15
•
-
SAMPLE NO.
0770313D33
Group:
039825
E1063.D
3/15/95
3/18/95
1.0
Qu
.
(uL)
Page 2 of 2 ,3/9°
AR3I6508
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET —————————
0770314PD5Lab Name: CHEMTECH Contract: US EPA REGION IE ____'
Project No.: A446-S Site: _____ Location: ___________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: 039963
Sample wt/vol: 5.0 (g/mL) G Lab File ID:E106S.D
Level: (low/med) LOW Date Received: 3/16/95
% Moisture: not dec. 77 . Date Analyzed: 3/18/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0
Pagelof2 ,. 00004?
'
Soil Extract Volume: ______(uL) Soil Aliquot Volume: _______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10*1591-78-6127-18-479-34-5108-88-3108-90-710041-4100-42-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dichloroethanc1 ,2-Dichloroethene( total)Chloroform1 ,2-Dichloroe thane2-Butanone1,1, 1-TricbloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-l,3-DichloropropencTrichloroetheneDibromochlorometnane1 , 1,2-TrichloroethaneBenzenetrans- 1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzene • .Styrene ~ -.
43684343432601200434343364343180434343434343434343434343434343
24004343
~ 43
U
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1A__ VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract US EPA REGION tt
Project No,: A446-S Site: Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not.dec. 77
Lab Sample ID:
SAMPLE NO.
0770314PD5•
Group:
O39963
Lab File ID: E1065.D
Date Received:
Date Analyzed:
GC Column: DB624 ED: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenes(total)
,
43
3/16/95
3/18/95
1.0
QU
-
(uL)
Page 2 of2FORMiyOA 000043 3/9°
A R 3 I 6 5 1 0
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
0770314PD5DLLab Name: CHEMTECH Contract: US EPA REGION EC
Project No.: A446-S Site: _____ Location: _________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: O39963DL
Sample wt/vol: 4.0 (g/mL) G Lab File ID: E1103.D
Level: (low/med) MED Date Received: 3/16/95
% Moisture: not dec. 77 Date Analyzed: 3/24/95
GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: 10000 (uL) Soil Aliquot Volume: ____100 (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18 *79-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dichloroethanel,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Butanone1,1,1-TricbloroethaneCarbon TetracblorideBromodichloromethane1,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-Trichloroe thaneBenzenetrans-l ,3-DichloropropeneBromofonn4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
5200520052005200520052004700520052005200520052005200520052005200520052005200520052005200520052005200520052005200520015300520052005200
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Page 1 of 2
flR3l65H ^^ °°00-4
. .. . - 1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION EC
Project No.: A446-S Site: Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 4.0 (g/mL) G
Level: (low/med) MED
% Moisture: not dec. 77
Lab Sample ID:
SAMPLE NO,
0770314PD5DL
Group:
O39963DL,
LabFileID:E1103.Ds
Date Received:
Date Analyzed:
GC Column: DB624 ID: 0.53 (mm) Dilution Factor:
Soil Extract Volume; 10000 (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenss(total) 5200
,
•
•
,
3/16/95
3/24/95
1.0
100
QU
(uL)
Page2of2FORMIVOA t\nr\f\AK 3/9°
•AR3I6SI2 ' 000045
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ———————
0770314PD6Lab Name: CHEMTECH Contract: US EPA REGION IE _____
Project No.: A446-S Site: _____ Location: _________ Group: ___
Matrix: (soil/water) SOIL Lab Sample ID: 039962
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1064.D
Level: (low/med) LOW Date Received: 3/16/95
% Moisture: not dec. 56 Date Analyzed: 3/18/95
GC Column: DB624________ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-2778-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
DicnlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dicbloroethane1 ,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Butanone1 , 1 , 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzene. * _. . -trans-i,j-LMcnioropropeneBromoform4-Memyl-2-Pentanone2-HexanoneTetrachloroethene1, 1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzene
• Styrene
232323232310011023232323232323232323232323232323
. 23232323132346232323
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Page 1 of2A'R3165 i 3FORM1VOA 000033 3/9°
O
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION Et
Project No.: A446-S Site: Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 56
Lab Sample ID:
SAMPLE NO.
0770314PD6
Group:
O39962 •
Lab File ID: E1064.D
Date Received:
. Date Analyzed:
GC Column: DB624 ED: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenes(total)
f
.
23
3/16/95
3/18/95
1.0
QU
~.
(uL)
Page 2 of 2 , ;s .-i «««««*' FORMIVOA 000034 3/90
AR3I65U
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ————————
0770314D35Lab Name: CHEMTECH Contract: US EPA REGION IE ____'
Project No.: A446-S . Site: _____ Location: ___________ Group:
Matrix': (soil/water) SOIL Lab Sample ID: O39964
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1074.D
Level: (low/med) LOW Date Received: 3/16/95
% Moisture: not dec. 31 Date Analyzed: 3/18/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-7KXM1-4100-42-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethane 'Methylene ChlorideAcetoneCarbon Disulfidc1,1-Dichloroethene1, l-Dichloroethane1 ,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1,1,1 -TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobcnzcncEmylbenzeneStyrene
141414141437151414141414141414141414141414141414141414141414141414
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Pagelof2 0000 7FORMIVOA VUUUo ( 3/90AR3I65I5
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION IT
Project No.: A446-S Site: Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 31
Lab Sample ID:
SAMPLE NO.
0770314D35
Group:
O39964
LabFiIeID':E1074.D'• ' ' s'
Date Received:
Date Analyzed:
GC Column: DB624 ED: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
•
1330-20-7 Xylenes(total)
~~
i
14
3/16/93
3/18/95
1.0
QU
(uL)
Page 2 of 2 nnAnc;QFORM IVOA U U U U J O 3/90
AR3I65I6
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
0770315D08Lab Name: CHEMTECH Contract: US EPA REGION III'
Project No.: A446-S Site: _______ Location: __________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: O39965
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1075.D
Level: (low/med) LOW Date Received: 3/16/95
% Moisture: not dec. 24 Date Analyzed: 3/18/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: _______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-710CM1-4HXW2-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1,1-Dichloroethanel,2-Dichloroethene( total)Chloroform1 ,2-Dichloroe thane2-Butanone1, 1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
131313131344131313131313131313131313131313131313131313131313131313
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Page 1 of 2FORMIVOA OOOOR4 3/9°Anoirr"!-* wvv/uj*±RJ I 65 i 7
VOLATILE ORGANICS .ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION H
Project No.: A446-S Site: Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)' G
Level: (low/med) LOW
% Moisture: not dec. 24
Lab Sample ID:
OT70315D08'•
Group:
039965
Lab File ID: E1075.D
Date Received:
Date Analyzed:
GC Column: DB624 ED: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
•
1330-20-7 Xylenes(total)
'
-
13
3/16/95
3/18/95
1.0
Qu
(uL)
Page 2 of 2 , " _ " r\r\r\r\r"FORMIVOA OUUUbO 3/90
A R 3 I 6 5 I 8
1A SAMPLE NO..VOLATILE ORGANICS ANALYSIS DATA SHEET ~
0770316D10Lab Name: CHEMTECH Contract: US EPA REGION H ______"
Project No.: A446-S Site: _____ Location: ___________ Group: ___
Matrix: (soil/water) SOIL Lab Sample ID: O40047
Sample wt/vol: 5.0 (g/mL) G ' Lab File ID:E1081.D
Level: (low/med) LOW Date Received: 3/17/95
% Moisture: not dec. 43 Date Analyzed: 3/18/95.
GC Column: DB624_________ ED; 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) , Soil Aliquot Volume: ______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-lOrl
591-78-6127-18479-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChloromedianeBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichloroethane1 ,2-Dichloroethene( total)Chloroform1,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene ~ _
18181818185238181818181818181818181818181818181818181818189.1181818
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Pagelof2 OOOJ11FORM IVOA v u u J. I i 3/90
AR3I65I9
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VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION El
Project No.: A446-S Site: Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 43
Lab Sample ID:
SAMPLE NO.
0770316D10
Group:
O40047
Lab File ID: E1081.D
Date Received:
Date Analyzed:
GC Column: DB624 ID: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
3/17/95
3/18/95
1.0
(uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xyleiies(totaJ) 18
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Page2of2 00011?FORM IVOA U U U 11'- 3/90
AR316520
1A ' SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ———————
077031SD12Lab Name: CHEMTECH Contract: US EPA REGION III ________"
Page 1 of 2FORMIVOA
AR3I652I
Project No.: A446-S Site: _____ Location: _________ Group: ___
Matrix: (soil/water) SOIL Lab Sample ID: O39966
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1085.D
Level: (low/med) LOW Date Received: 3/16/95 •
% Moisture: not dec. 59 Date Analyzed: 3/22/95
GC Column: DB624_________ ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: _______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01475-00-375-09-267-64-175-15-075-35-475-34540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,1-Dichloroe thane1 ,2-Dichloroethenc( total)Chloroform1 ,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetracnloroemene1, 1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
2424242424242902424242424248424242424242424242424242424242420242424
UUUUUJB
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. ..• - - - - - - • .-. 1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION II
Project No.: A446-S Site: Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. .59
Lab Sample ID:
SAMPLE NO.
0770315D12"
Group:
039966
Lab File ID: E1085.D
Date Received:
Date Analyzed:
GC Column: DB624 ED: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenes(total)
.
.
24
*
•
3/16/95
3/22/95
1.0
QU
"
„
(uL)
Page 2 of 2 .FORMIVOA 00007P 3/9°
AR316522
1A • SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ———————-
0770316D23Lab Name: CHEMTECH Contract: US EPA REGION II '_____
Project No.: A446-S Site: _____ Location: _________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: 040045
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1079.D
Level: (low/med) LOW Date Received: 3/17/95
% Moisture: not dec. 48 Date Analyzed: 3/18/95
GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: _______ (uL)u
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg • Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-2778-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-lOrl
591-78-6127-18-479-34-5108-88-3108-90-7100-41-410CM2-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMetbylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1, 1-Dichloroethanel,2-Dichloroethenc{ total)Chloroform1 ,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromediane1,2-Dichloropropanccis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachlorocthene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
1919
,_ 19191948551919191919191919191919191919191919191919191919191919
UUUuuB
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000095SR3I6523 3/9°
<l
IAVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION II
Project No.: A446-S Site: Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 48
Lab Sample ID:
SAMPLE NO.
0770316D23
Group:
O40045
Lab File ID: E1079.D. . . ' *
Date Received:
Date Analyzed:
GC Column: DB624 ID: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylencs(total)
• - - - - .
19
3/17/95
3/18/95
1.0
QU
(uL)
Page2of2 000096FORMIVOA vv/vu
A"R3 165214
1A __SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
0770316D24Lab Name: CHEMTECH Contract: US EPA REGION EC
Page 1 of2
Project No.: A446-S Site: _____ Location: _________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: 040046
Sample wt/vol: 5.0 (g/mL) G Lab File ED: E1086.D
Level: (low/med) LOW Date Received: 3/17/95
% Moisture: not dec. 58 Date Analyzed: 3/22/95
GC Column: DB624________ ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01475-00-375-09-267-64-175-15-075-35475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichlorocrnene1,1-Dichloroethancl,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Mernyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
2424242424211102424242424242424242424242424242424242424242419242424
UUUUUJB
UUUUUUUUUUUUUuuuuuuuuuJuuu
FORMIVOA 000103 3/90AR3I6525
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION II
Project No.: A446-S Site: Location:
Matrix: (soil/water) SOIL
Sample wr/vol: 5.0 (g/mL) G
Level:/
(low/med) LOW
% Moisture: not dec. 58
Lab Sample ID:
SAMPLE NO.
0770316D24"
Group:
O40046
LabFileID:E1086.D
Date Received:
Date Analyzed:
GC Column: DB624 ED: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
i Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
•
1330-20-7 Xytenes(total) 24
3/17/95
3/22/95
1.0
QU
-., .
(uL)
30010
Page 2 of2FORM IVOA 3/90
AR3I6526
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ——————————
0770316D27Lab Name: CHEMTECH Contract: US EPA REGION IE
Project No.: A446-S . Site: _____ Location: _________ Group: ___
Matrix: (soil/water) SOIL Lab Sample ID: O40048
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1087.D
Level: (low/med) LOW Date Received: 3/17/95
% Moisture: not dec. 31 Date Analyzed: 3/22/95
GC Column: DB624________ ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01475-00-375-09-267-64-175-15-075-35-475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-1879-34-5108-88-3108-90-7100-41-410042-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dichloroe thane1 ,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1, 1. 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DicnloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetnms-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetracnloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
141414141414451414141414141414141414141414141414141414141412141414
UUUuuJB
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- UuuuuuuuuuuuuuuuuuuJuuu
Page 1 of 2 0001 1 9K FORM I VGA U U U 1 - 3/9Q
AR3I6527
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION II
Project No.: A446-S Site: Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) 1LOW
% Moisture: not dec. 31
Lab Sample ID:
SAMPLE NO.
0770316D27
Group:
O40048
Lab File ID: E1087.D
Date Received:
Date Analyzed:
GC Column: DB624 ED: 0.53 (mm) Dilution Factor
Soil Extract Volume: (uL) Soil Aliquot Volume:
—- Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenes(total)
.
.* - . - - -
14
3/17/95
3/22/95
1.0
QU
„
(uL)
0001;Page 2 of 2 ; . ' •
FORMIVOA 3/90
AR3I6528
1A SAMPLE NO.VOLATILE pRGANICS ANALYSIS DATA SHEET
0770316D31Lab Name: CHEMTECH Contract: US EPA REGION IE
Project No.: A446-S Site: _____ Location: _________ Group: ___
Matrix: (soil/water) SOIL Lab Sample ID: 040043
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1077.D
Level: (low/med) LOW Date Received: 3/17/95
% Moisture: not dec. 52 Date Analyzed: 3/18/95
GC Column: DB624____•_____ ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: _______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-57143-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethyiene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1, 1-Dichloroethane1 ,2-Dichloroethene(total)Chloroform1 ,2-Dichloroe thane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichlorocthaneBenzenetnns-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-Tetrachloroe thaneTolueneChlorobenzeneEthylbenzeneStyrene
212121212161212121212121212121212121212121212121212121212111212121
UUUuuBUUUUUUuuuuuuuuuuuuuuuuuJuuu
Pagelof2 000030FORMIVOA 3/90
'AR3I6529
• - . • ... .'"-;- IAVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION II
Project No.: A446-S Site: Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (Jow/med) LOW
% Moisture: not dec. 52
Lab Sample ID:
SAMPLE NO.
0770316D31
Group:
O40043
Lab File ID: E1077.D
Date Received:
Date Analyzed:
GC Column: DB624 ED: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenes(total)
i
21
,
3/17/95
3/18/95
LO
QU
(uL)
Page 2 of2FORMIVOA 000081 3/90
-AR3I6S3D
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
0770316D32Lab Name: CHEMTECH Contract: US EPA REGION EC
Project No.: A446-S Site: _____ Location: _________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: O40044
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1078.D
Level: (low/med) LOW Date Received: 3/17/95
% Moisture: not dec, 37 Date Analyzed: 3/18/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMernylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroediene1, 1-Dichloroc thanel,2-Dichloroethene(total)Chloroform1 ,2-Dichloroc thane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromcthanc1,1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromofonn4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1, 1,2,2-TetrachloroethaneTolueneChlorobcnzencEthylbenzeneStyrcne
16161616164216161616161616161616161616161616161616161616169161616
UUUuuBUUUU
, UUUUuuuuuuuuuuuuu
L_ uuJuuu
Page 1 of 2
«R3I653I
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
o LabNam
Project N
Matrix:
Sample u
Level:
% Moisti
GCColui
SoilExtr
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
e: CHEMTECH Contract: US EPA REGION IE
To.: A446-S Site: Location:
(soil/water) SOIL
rt/vol: 5.0 (g/mL) G
(low/med) LOW
as: not dec. 37
Lab Sample ID:
SAMPLE NO.
0770316D32
Group:
0400-44
Lab File ID: E1078.D
Date Received:
Date Analyzed:
am: DB624 ID: 0.53 (mm) Dilution Factor-
act Volume: (uL) Soil Aliquot Volume:' . - - , . • - - - - - : - •• ---T- -— r --••-•
• Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
•
1330-20-7 Xylenes(total) 16
,
•
3/17/95
3/18/95
1.0
Q
. U
*
(uL)
Page 2 of2nnnnoo 3/90
°88
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET —————————
0770320D15Lab Name: CHEMTECH__ Contract: US EPA REGION II
Project No.: A446-S Site: _____ Location: _________ Group: ___
Matrix: (soil/water) SOIL Lab Sample ID: 040093
Sample wt/vol: 5.0 (g/mL) G Lab File ED: E1088.D
Level: (low/med) LOW Date Received: 3/21/95
% Moisture: not dec. 46 Date Analyzed: 3/22/95
GC Column: DB624________ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ________(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6 '124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-1879-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChloromethaneBromomedianeVinyl ChlorideChloroedianeMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dichloroethanel,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TricbloroetbaneBenzenetnms-l,3-DichloropropeneBromofonn4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1, 1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrcne
1919191919191001919191919191919191919191919191919191919191918191919
UUUuuB
UUUUU
•• UuuuuuuuuuuuuuuuuJuuu
000177
Page 1 of2FORM I VGA 3/90
'••..-":.-.-±.J. 1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET '—————
r " - 0770320D18Lab Name: CHEMTECH Contract: US EPA REGION IE
Project No.: A446-S Site: _____ Location: , Group:
Matrix: (soil/water) SOIL Lab Sample ID: 040095 _
Sample wt/vol: 5.0 (g/mL) G Lab File ID: E1090.D
Leyel: (low/med) LOW Date Received: 3/21/95
% Moisture: not dec. 65__ Date Analyzed: 3/23/95
GC Column: DB624________ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _____._(uL) . . Soil Aliquot Volume: _____ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-710041-410042-5
DicliilorodifluoromeuianeChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,1-Dichloroethane1 ,2-Dichloroethene( total)Chloroform1 ,2-Dichloroethane2-Butanonc1 , 1 , 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeaeTricliloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-l,3-DichloropropcneBromoform4-Mcthyl-2-Pentanone2-HexanoneTetntchloroethene1, 1,2,2-TetracnloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
292929292920
1700292929292929590292929292929292929292929292929
7800292929
UUUuuIBEUUuuuuEUuuuuuuuuuuuuuuEuuu
Page I of 2 ___FDRMIVOA 000144 3/9°
AR3 1653*4
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION II)
Project No.: A446-S Site: Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture; not dec. 65
Lab Sample ID:
SAMPLE NO.
0770320D18
Group:
O40095
Lab File ID: E1090.D
Date Received:
Date Analyzed:
GC Column: DB624 ED: 0.53 (mm) Dilution Factor:
Soil Extract Volume: 1 (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenes(total)
'
29
3/21/95
3/23/95
1.0
I
QU
-
(uL)
Page2of2 QQn 1 4 <r
SR3I6535
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
0770320D18DLLab Name: CHEMTECH Contract: US EPA REGION IE
Project No.: A446-S Site: ^ ^ Location: _________ Group:
Matrix: (soil/water) _SOIL Lab Sample ID: 040095DL
Sample wt/vol: 4.0__(g/mL) G ' Lab File ID: EU02.D
Level: (low/med) MED_ Date Received: 3/21/95
% Moisture: not dec. 65 Date Analyzed: 3/24/95
GC Column: DB624_________ ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: JiOQQO (uL) Soil Aliquot Volume: ____100 (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-61244S-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-4 •79-34-5108-88-3108-90-710041-410042-5
DichlorodifluoromethaneChloromethaneBromomethancVinyl ChlorideChlotoethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1,1-Dichloroethanel,2-Dichloroethene(totai)Chloroform1,2-Dichloroethane2-Butanone1, 1, 1-Trichloroe thaneCarbon TetrachlorideBromodichloromediane1 ,2-Dichloropropanecis-l,3-DichloropropeneTricMoroetheneDibromochloromethane. 1 , 1 ,2-TrichlorpethaneBenzenetrans-l,3-DichloropropeneBromoform4-Melhyl-2-Pentanone2-HexanoneTetrac:hloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrerc
3400340034003400340034003000340034003400340034003400340034003400340034003400340034003400340034003400340034003400340010200340034003400
UUuuuuJuuuuuuuuuuuuuuuuuuuuuu
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Page 1 of2
1-6536 FORMIVOA °°°H6
LabNam
Project N
Matrix: (
Sample w
Level:
% Moisti
GCColui
SoilExtn
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
s: CHEMTECH Contract: US EPA REGION II
o.: A446-S Site: Location:
soil/water) SOIL
t/vol: 4.0 (g/mL) G
(low/med) MED
ire: not dec. 65
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
nn: DB624 ED: 0.53 (mm) Dilution Factor:
ict Volume: 10000 (uL) Soil Aliquot Volume:
Concentration Units:'CAS No. Compound (ug/L or ug/Kg) ug/Kg
-i
1330-20-7 Xylenes(total) 3400
SAMPLE NO.
0770320D18DL
Group:
O40095DL
E1102.D
3/21/95
3/24/95
1.0
100
Qu
-.
*
'
(uL)
Page2of2FORMIVOA 3/90
AR3I6537
1A . SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET '——————, : 0770320D2i
Lab Name: CHEMTECH Contract: US EPA REGION II
Project No.: A446-S Site: _____ Location: _________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: O40094 _
Sample wt/vol: j.0 (g/mL) G Lab File ID: E1089.D_
Level: . (low/med) LOW Date Received: 3/21/95_
% Moisture: not dec. 66 Date Analyzed: 3/22/95_
GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ____(uL) Soil Aliquot Volume: __ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
75-71-874-87-374-83-975-01475-00-3 '75-09-267-64-175-15-075-35475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-612448-179-00-57143-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-710041-410042-5
DichlorodifluoromedianeChloromcthaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1 , 1-Dichloroethane1 ,2-Dichloroethene(total)Chloroform1 ,2 -Dichloroediane2-Butanone1, IJ-TrichloroethaneCarbon TetrachlorideBromodichloromethaue1,2-Dichloropropane .cis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetiachloroethene1; 1,2,2-TetrachloroethaneTolueneChlorobenzeneEtfaylbenzeneStyrene
2929292929266402929292929292402929292929292929292929292929
- 29110292929
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, UUu
uuuuuuuuuuuuuuu
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Page 1 of 2FORMIVOA J 3/90
AR3I6538
Lab Nam
Project N
Matrix:
Sample w
Level:
% Moisa
GCColui
Soil Extn
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
e: CHEMTECH Contract: US EPA REGION II
o.: A446-S Site: Location:
'soil/water) SOIL
t/vol: 5.0 (g/mL) G
(low/med) LOW
ire: not dec. 66
Lab Sample ID:
SAMPLE NO.
0770320D21
Group:
O40094
Lab File ID: E1089.D
Date Received:
Date Analyzed:
nn: DB624 ID: 0.53 (mm) Dilution Factor:
ict Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenes(total) 29
*
3/21/95
3/22/95
1.0
QU
-
(uL)
Page 2 of 2 HOH1 QC'FORMIVOA UUIUJO 3/90
AR3I6539"
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
0770320D36Lab Name: CHEMTECH Contract: US EPA REGION IE
Project No.: A446-S Site: _______ Location: -_________ Group: ___
Matrix: (soil/water) _SOIL Lab Sample ID: O40096
Sample wt/vol: 5.0 (g/mL) G . Lab File ED:E1100.D
Level: (low/med) _LOW Date Received: 3/21/95
% Moisture: not dec. __29__ Date Analyzed: 3/24/95 _
GC Column: DB624________ ED: 0.53 (mm) Dilution Factor: 1.0 _
Soil Extract Volume: ______(uL) Soil Aliquot Volume: _____' (uL)
Concentration Units:CAS No. Com|X>und (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01475-00-375-09-2 .67-64-175-15-075-354 -75-34-4540-59-067 6-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-7100-41-4100-42-5
DicMorodifiuoromethaneChloiromethaneBronaiomethaneVinyl ChlorideChloiroethaneMethylene ChlorideAcetoneCarbon Disulfide .1,1-Dichloroethene1,1-Dichloroethane1 ,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Buianone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzene .tnns-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HejtanoneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylltenzeneStyreiie
141414141411171414141414141414141414141414141414141414141414141414
UUUuuJB
UUUuuuuuuuuuuuuuuuuuuuuuuu
Pagelof2 0001^8' FORMIVOA vvvx.o 3/90
~AR3"l 651*0
r^h Nam
Project N
Matrix: (
Sample w
Level:
% Moisti
GCColui
SoilExtn
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
e: CHEMTECH Contract: US EPA REGION III
o.: A446-S ' Site: Location:
soil/water) SOIL
t/vol: 5.0 (g/mL) G
(low/med) LOW
ire: not dec. 29
Lab Sample ID:
SAMPLE NO.
0770320D36
Group:
O40096
LabFileID:E1100.D
Date Received:
Date Analyzed:
nn: DB624 ID: 0.53 (mm) Dilution Factor:
ict Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenes(total)
--
14
3/21/95
3/24/95
1.0
QU
.
(uL)
Page 2 of 2FORM IVOA ^ 3/9°
AR3l65t*l •
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ————
0770320D37Lab Name: CHEMTECH Contract: US EPA REGION II
Project No.: A446-S Site: _____ Location: _________ Group: ___
Matrix: (soil/water) _SOIL Lab Sample ID: O40097
Sample wt/vol: 5.0__(g/mL) G Lab File ID: E1092.D
Level: (low/med) LOW Date Received: 3/21/95
% Moisture: not dec. 30 Date Analyzed: 3/23/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
75-71-874-87-374-83-975-01475-00-375-09-267-64-175-15-075-354 •75-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18479-34-5108-88-3108-90-710041-410042-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoineCarbon Disulfide1,1-Dichloroethene1,1-Dichloroethanel,2-Dichloroethene(total)Chloroform1,2-Dichloroethane2-Butanone1 , 1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-9. ,3-DichloropropeneBromoform4-Mediyl-2-Pentanone2-HeximoneTetrachloroethene1, 1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrcn;
1414141414132214141414141414141414141414141414.14141414141440141414
UUUuuJB
U-UUU
~ uuuuuuuuuuuuuuuuuuuuu
Page 1 of 2x FORMIVOA 000166 3/9°
A.R3I65H2
Lab Nam
Project N
Matrix:
Sample w
Level:
% Moisti
GCColui
Soil Extn
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
e: CHEMTECH Contract: US EPA REGION II
o.: A446-S Site: Location:
[soil/water) SOIL
t/vol: 5.0 (g/mL) G
(low/med) LOW
ire: not dec. 30
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
nn: DB624 ID: 0.53 (mm) Dilution Factor:
act Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
*•
1330-20-7 Xylenes(total)
*
14
SAMPLE NO.
0770320D37
Group:
O40097
E1092.D
3/21/95
3/23/95
1.0
Qu
———— £
(uL)
001*'
Page 2 of 2
flR3l65»,3 roSMIV°A
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
077IJ320D37BLab Name: CHEMTECH Contract: US EPA REGION II'
Project No.: A446-S Site: _____ Location: __________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: O40100
Sample wt/vol: 5.0 (g/mL) G Lab File ID; E1095.D
Level: (low/med) LOW Date Received: 3/21/95
% Moisture: not dec. 51__ Date Analyzed: 3/23/95
GC Column: DB624_________ ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _\.____(uL) , . Soil Aliquot Volume: ___ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-612448-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-410042-5
DiclilorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethyiene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,1-Dichloroethanel,2-Dichloroethene(total)Chloroform1 ,2-Dichloroethane2-Butanone1 , 1 , 1-TrichloroethaneCarixm TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-Ii ,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBemienetranii-1 ,3-DichloropropeneBrornoform4-Methyl-2-Pentanone2-Hftxanone .Tetr,ichloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
2020202020191902020202020202020202020202020202020202020202047202020
UUuuuJB
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000175
Page 1 of2FORMIVOA 3/90
AR3I65U
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION IE
Project No.: A446-S Site: Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 51
Lab Sample ID:
SAMPLE NO.
0770320D37B
Group:
O40100
Lab File ID: E1095.D
Date Received:
Date Analyzed:
GC Column: DB624 ED: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
1330-20-7 Xylenes(tptal) 20
3/21/95
3/23/95
1.0
QU
_
(uL)
ooorPage 2 of2
FORMIVOA . 3/90
Appendix DReviewed and Corrected
Tentatively Identified Compounds
-AR3I651*'6
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770306PW1
Lab Name: CHEMTECH_________________ Contract: US EPA REGION III
Project No. A43S Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: O39493
Sample wt/vol: 25.0 (g/mL) ML - LabFileID:L1145.D
Level: (low/med) _______ Date Received: 3/8/95
% Moisture: not dec. _________ Date Analyzed: 3/9/95
GC Column: DB624______ ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:Number TICs found: 1___ (ug/L or ug/Kg) ug/L
CAS Number1. 110-54-3 ———2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Namei L\f A &Uw
•
.
RTf f*\-*••>*•
-
Est. Cone.———— 7—
-
Q—— J-
IRMI VOA-TIC 000041 3/90
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770306PW2
Lab Name: CHEMTECH _______________ Contract: US EPA REGION EQ
Project No. A43S Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: 039494
Sample wt/vol: 25.0 (g/mL) ML ,-• Lab File ID: LI 146.D
Level: (low/med) _______ Date Received: 3/8/95
% Moisture: not dec. _______ Date Analyzed: 3/9/95
GC Column: DB624 ^ ^ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: _____ (uL)* > - , - ' . . - ' . . ^ - - . , . . . - - . . .
Concentration Units:Number TICs found: __ 1 ._.,_. _ _ . ' (ug/L or ug/Kg) ug/L
CAS Numljer, 1. 110-54-3 ——2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound NameHexane —————————————
1
,
RT—— 5rS3-
Est Cone.—— 6rfi—
'- _.
Q— j_
. "„. ; FORMI VOA-TIC 000049 3/9°A f^ I /* r- t *» *' • - • , ' >;, \* ** \*r \j £ \j
AR3 165^8
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS Q770306PW4
Lab Name: CHEMTECH__________________. Contract: US EPA REGION in
Project No. A435 Site: _____ Location: __________ Group:
Matrix: (soil/water) WATER Lab Sample ED: O39495
Sample wt/vol: 25.0 (g/mL) ML -' Lab File ED: LI 147.D
Level: (low/med) _______ Date Received: 3/8/95
% Moisture: not dec. _______ Date Analyzed: 3/9/95
GC Column: DB624 ED; 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found: 1___ (ug/L or ug/Kg) ug/L
CAS Number1. 110-54-3 ———2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound NameHexaae ———————————
1
i
RT5M
EstConc.—— fc?—
*•
Qw"
flf?3l65I»9 FORMIVOA-11C °0005S
4 IE SAMPLENO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS U770306W17
Lab Name: CHEMTECH_________________ Contract: US EPA REGION III
Project No. A435 Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: 039490
Sample wt/vol: 25.0 (g/mL) ML - Lab File ID: LI 142.D
Level: (low/med) "___ Date Received: 3/8/95
% Moisture: not dec. ______ Date Analyzed: 3/9/95
GC Column: DB624 __ ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: __ __ (uL)
"Concentration Units:Number TICs found: 1 (ug/L or ug/Kg) ug/L
CAS Number1. 110-54-3 ———2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound NameHexanc —————————————
t
i
RT- «j -yt
Est. Cone.——— 5rt—
' -
Q— t—
- FORMI VOA-TIC 000019 3/90
AR3J6550
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS Q770306W19
Lab Name: CHEMTECH_____________,______ Contract: US EPA REGION Ed
Project No. A435 Site: ______ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ED: O39491
Sample wt/vol: 25.0 (g/mL) ML - Lab File ID:L1143.D
Level: (low/med) ________ Date Received: 3/8/95
% Moisture: not dec. _______ Date Analyzed: 3/9/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ________(uL) Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found: 1 . (ug/L or ug/Kg) ug/L
CAS Number1. 110*540 ———2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name[lexane —————————————
I
RTf etj*JnJt*
EstConc.. i . . ^ £J.J
-
QJ
TORMI VOA-TIC 0000 6
;- .-:•.-"-. ' IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770306W20
Lab Name: CHEMTECH________________ Contract: US EPA REGION III
Project No. A43S Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: O39492
Sample wt/vol: 25.0 (g/mL) ML -- Lab FileID:L1144.D
Level: (low/med) ____' ' Date Received: 3/8/95
56 Moisture: not dec. Date Analyzed: 3/9/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor __U{__
Soil Extract Volume: _;______^uL) Soil Aliquot Volume: ___ __ (uL)
Concentration Units:Number TICs found: 1____ (ug/L or ug/Kg) ug/L
CAS Number1. 110-M-3 ———2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound NameHexane ————————————
'
RT—— 5-53-
Est. Cone.—— 6r6—
• -
Q— j_
AR3I6552- FORMIVOA-TIC 000033 3/90
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770307TB1
Lab Name: CHEMTECH__________________ Contract: US EPA REGION ffl
Project No. A435 Site: _______ Location: _________ Group:
Matrix: (soil/water) WATER . Lab Sample ED: 039496
Sample wt/vol: 25.0 (g/mL) ML „•• Lab File ID:L1148.D
Level: (low/med) ________ Date Received: 3/8/95
% Moisture: not dec. _________ Date Analyzed: 3/9/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:Number TTCs found: 2 (ug/L or ug/Kg) ug/L
CAS Number1.2. 110-54-33.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound NameUnknownHexane
•
*
RT3.635.52
EstConc.2.213
1 ^.
QJJ
000065 3/9°
; IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770307W02
Lab Name: CHEMTECH _________ Contract: US EPA REGION in
Project No. A435 Site: . Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: O39585
Sample wt/vol: _ 25.0 (g/mL) ML --• Lab File ID:L1157.D
Level: (low/med) . • Date Received: 3/9/9.5
% Moisture; not dec. _______ Date Analyzed: 3/11/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ________(uL) Soil Aliquot Volume: ___ (uL)i ' , . . . . . . - - - -
, Concentration Units:Number TICs found: ___ 0___ (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name RT Est. Cone.
.
Q
FOR^I VOA-TIC 000073 3/90
A R3T65:§iT'"'"''.'
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770307W22
Lab Name: CHEMTECH____________________ Contract: US EPA REGION III
Project No. A435 Site: _____ Location: __________ Group:
Matrix: (soil/water) WATER Lab Sample ED: O39588
Sample wt/vol: 25.0 (g/mL) ML - Lab FileID:L1163.D
Level: (low/med) _______ Date Received: 3/9/95
% Moisture: not dec. ________ Date Analyzed: 3/12/95
GC Column: DB624______ ED: ,0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
\
RT Est. Cone.
•-.
Q
AR3J6555F°RMIVOA~11C 000093 3/9°
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770307W28
Lab Name: CHEMTECH__________________ Contract: US EPA REGION III
Project No. A435 Site: _____ Location: __________ Group:
Matrix: (.soil/water) WATER Lab Sample ID: 039586
Sample wt/vol: 25.0 (g/mL) ML ,- Lab File ID: LU58.D
Level: (low/med) _______ . , Date Received: 3/9/95
% Moisture: not dec. _^_____ Date Analyzed: 3/11/95
GC Column: DB624 ____ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ________(uL) Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found: ___ 0___ (ug/L or ug/Kg) ug/L
CAS Number1.2.3.
. 4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
v
•
RT
,
Est. Cone. Q
"A'R3|fiC:qc FORM I VOA-TIC 000080 3/90
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770307W29
Lab Name: CHEMTECH___________________ Contract: US EPA REGION ETC
Project No. A435 Site: ______ Location: __________ Group:
Matrix: (soil/water) WATER Lab Sample ID: 039587
Sample wt/vol: 25.0 (g/mL) ML - Lab FileID:L1162.D
Level: (low/med) _______ Date Received: 3/9/95
% Moisture: not dec. _________ Date Analyzed: 3/12/95
GC Column: DB624______ ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _________(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
•
*
.
RT Est. Cone.
,
Q
A R 3 16557 FC*M I VOA~TIC 000086 3/90
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770307W34
Lab Name: CHEMTECH_____________• Contract: US EPA REGION EH
Project No. A43S Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: O39589
Sample wt/vol: __25.0 (g/mL) ML -' Lab File ID: LI 164. D
Level: (low/med) _______ Date Received: _3/9/95_
% Moisture: not dec. . ...... - Date Analyzed: 3/12/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found: _0____ (ug/L or ug/Kg) ug/L
9
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
'
RT Est. Cone. Q
flnol6558 FORMI VOA-TIC 000100 3/9°
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770308TB1
Lab Name: CHEMTECH___________________ Contract: US EPA REGION ffl
Project No. A43S Site: ______ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: O39S90
Sample wt/vol: 25.0 (g/mL) ML -• Lab Hie ED: LI 165.D
Level: (low/med) _______ Date Received: 3/9/95
% Moisture: not dec. ________ Date Analyzed: 3/12/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
-
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165 FORMIVOA-TIC 000107 3/9°
_; . "-,'"": ,1E SAMPLEJSTO, VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS 0770308W03
Lab Name: CHEMTECH _________________ Contract: US EPA REGION EQ
Project No. A435 Site: _____ Location: __________ Group:
Matrix: (soil/water) WATER Lab Sample ID: O39677
Sample wt/vol: 25.0 (g/mL) ML -- Lab File ID; L1174.D
Level: (low/med) _ ______ Date Received: 3/10/95
% Moisture: not dec. _______ Date Analyzed: J3/12/95
GC Column: DB624____' .ED; 0.53 (mm) Dilution Factor __1.0__
Soil Extract Volume: ____ (uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:Number TICs found: 0 • (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
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FORMI VOA-TIC «««-«-• 3/9°flR3l6560 000135
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770308W05
Lab Name: CHEMTECH___________________ Contract: US EPA REGION Ed
Project No. A435 Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER - LabSgmpleED: O39S93
Sample wt/vol: 25.0 (g/mL) ML -' Lab FileID:L1168.D
Level: (low/med) _________ Date Received: 3/9/95
% Moisture: not dec. _______ Date Analyzed: 3/12/95
GC Column: DB624______ ED; 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
•
RT Est. Cone.
-
Q
AR3/656/ FORM I VOA-TIC 000128 3/90
" - - IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 077030829B
Lab Name: CHEMTECH . Contract: US EPA REGION Ed
Project No. A435 Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER ' Lab Sample ED: 039591
Sample wt/vol: 2S.O___(g/mL) ML - Lab File ED:L1166.D
Level: (low/imed) _______ Date Received: 3/9/95
% Moisture: not dec. ' . . : . , , , . . Date Analyzed: 3/12/95
GC Column: DB624 ____ ED: 0.53 (mm) Dilution Factor; 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: _____ (uL)
, Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/L
CAS NumberI.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
•
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RT Est. Cone.
• _
Q
.-- FORMIVOA-TIC OOQ114 3/9°AR3I6562
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 077030829C
Lab Name: CHEMTECH___________________ Contract: US EPA REGION IE
Project No. A43S Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: O39S92
Sample wt/vol: 25.0 (g/mL) ML - Lab File ID:L1167.D
Level: (low/med) _______ Date Received: 3/9/95
% Moisture: not dec. Date Analyzed: 3/12/95
GC Column: DB624 ED; 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found: 0___ (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
•
RT Est. Cone. Q
AR3I6563 w""*0 ™' 000121 3/90
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS
II
IDI770309TB1
Lab Name: CHEMTECH _______________ Contract: US EPA REGION in
Project No. A435 Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: 039678_
Sample wt/vol: 25.0 (g/mL) ML -' Lab File ID: L117S.D
Level: (low/med) _______ Date Received: 3/10/95; ' •, ,. • . . •;•<.• r- : . - • - . ' ' ' -
% Moisture: not dec. __._____ Date Analyzed: 3/12/95• ; 2'__ ~ ' ' , - . ' - ' ' ! . ' ' ' ' - - ' "
GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: ___ __ (uL)
Concentration Units:Number TICs found: ___ 1___ (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound NameUnknown
•
RT3.72
Est Cone.2.6
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QJ
FORM I VOA-TIC 000142 3/90AR3I656U
IE ^AMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770313W06
Lab Name: CHEMTECH_________________ Contract: US EPA REGION IE
Project No. A435 Site: • Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: 039811
Sample wt/vol: 25.0 (g/mL) ML - Lab FileID:L___80_D
Level: (low/med) _______ Date Received: 3/15/95
% Moisture: not dec. _______ , Date Analyzed: 3/16/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor 1.0
Soil Extract Volume: __________(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
•
RT Est. Cone.
-
Q
AR3 I 6565 FORMI VOA-TIC 000149 3/9°
ME SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770313W07
Lab Name: CHEMTECH________________ Contract: US EPA REGION III
Project No. A435 Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: 039814
Sample wt/vol: 25.0 (g/mL) ML -•' LabFileID:L118LD
Level: (low/med) ' ___ Date Received: _3/15V95_
% Moisture: not dec. __ __' Date Analyzed: 3/16/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: (uL) Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found: 0___ . . .' . (ug/L or ug/Kg) ug/L
CAS Numtier1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
.
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RT Est. Cone. Q
FORM I VOA-TIC n A n i r- * ' 3/90a -. ~ ruKM j; YUA-UU A n n •> i- r»SR3J6566 OOOloB
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770313W6D
Lab Name: CHEMTECH_____________;____ Contract: US EPA REGION ffl
Project No. A447 Site: _____ Location: ___________ Group:
Matrix: (soil/water) WATER Lab Sample ID: O39826
Sample wt/vol: 25.0 (g/mL) ML -' Lab File ID:L1189.D
Level: (low/med) _________ Date Received: 3/15/95
% Moisture: not dec. _________ Date Analyzed: 3/19/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: _______ (uL)
Concentration Units:Number TICs found: 0___ (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
i
RT EstConc.
• -
Q
AR3i6567RMIVOA-Tlc 000015 3/90
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS CI770313W09
Lab Name: CHEMTECH_________________ Contract: US EPA REGION EP
Project No. A447 Site: ______ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: 039827
Sample wt/vol: 25.0 (g/mL) ML ,- Lab FileED:L1190.D
Level: (low/med) __\_______ Date Received: 3/15/95
% Moisture; not dec. .___ . Date Analyzed: 3/19/95
GC Column: DB624 EO: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: __________(uL) Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/L
<l
CAS Number1.2.3.
. 4.5.6.7.8.
* 9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
i
RT Est Cone. Q
•!_ FORM I VOA-TIC 000022 3/90AR3I6568
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770313W16
Lab Name: CHEMTECH____________________ Contract: US EPA REGION III
Project No. A447 Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER • Lab Sample ID: O39828
Sample wt/vol: 25.0 (g/mL) ML -• LabFileID:L1191.D
Level: (low/med) _______ Date Received: 3/15/95
% Moisture: not dec. ________ Date Analyzed: 3/19/95
GC Column: DB624______ ED; 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:Number TTCs found: 0____ (ug/L or ug/Kg) ug/L
CAS NumberI.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
•
RT Est, Cone.
--
Q
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AR3 16569 FORMIVOA-TIC 000029 3/90
, r , ; IE .'. SAMPLE NO..... VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS 0770313W14
Lab Name: CHEMTECH________________ Contract: US EPA REGION III
Project No. A447 Site: • Location: _____________ Group:
Matrix: (soil/water) WATER Lab Sample ID: 039829
Sample wt/vol; 25,0 (g/mL) ML -- LabFileID:L1192.D
Level: (low/med) _______ Date Received: 3/15/95_
% Moisture: not dec. _______ Date Analyzed: 3/19/95_
GC Column: DB624______ EP; 0.53 (mm) Dilution Factor: 1.0 _
Soil Extract Volume: _______(uL) Soil Aliquot Volume: _____ (uL)
; - Concentration Units:Number TICs found: ___ 0 (ug/L ot ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
•
RT Est. Cone.
• ,.
Q
FORM I VOA-TIC 000035 3/90AR316570
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770313W13
Lab Name: CHEMTECH__________________ Contract: US EPA REGION EQ
Project No. A447 Site: _______ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: 039830
Sample wt/vol: 25.0 (g/mL) ML - LabFileID:L1193.D
Level: (low/med) _______ Date Received: 3/15/95
% Moisture: not dec. _______ Date Analyzed: 3/19/95
GC Column: DB624___________ ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _________(uL) Soil Aliquot Volume: ________ (uL)
Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name RT Est. Cone.
^
Q
AR31657! FORM I VOA-TIC 000042 3/9°
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770313PW3
Lab Name: CHEMTECH_________________ Contract: US EPA REGION EQ
Project No. A447 Site: _____ Location: _______' Group:
Matrix: (soil/water) WATER Lab Sample ED: 039831
Sample wt/vol: 25.0 (g/mL) ML ',- Lab FileID:L1194.D
Level: (low/med) . . ' . . . . . . Date Received: 3/15/95
% Moisture: not dec. _______ Date Analyzed: _3/19/_95_
GC Column: DB624 ED: ,0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ___ (uL) Soil Aliquot Volume: _ (uL)
, -Concentration Units:Number TTCs found: ___ 0___ (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
i
RT EstConc.
•i
Q
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FORM I VOA-TIC 000048 3/90
•AR3I6572
IE - SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770313PW33
Lab Name: CHEMTECH_________________ Contract: US EPA REGION ETC
Project No. A447 Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: O39832
Sample wt/vol: 25.0 (g/mL) ML - Lab File ID: LI 195.D
Level: (low/med) ________ Date Received: 3/15/95
% Moisture: not dec. _______ Date Analyzed: 3/19/95
GC Column: DB624______ ED; 0.53 (mm) Dilution Factor; 1.0
Soil Extract Volume: _______(uL)' Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
t
RT Est. Cone.
• .
Q
m
AR3I6573 FORM I VOA-TIC 000056 3/9°
rr ilE SAMPLE NO.: VOLATILE ORGANICS ANALYSIS DATA SHEET
TENfAtrVELY IDENTIFIED COMPOUNDS 0770314TB1
Lab Name: CHEMTECH ______;_______ Contract: US EPA REGION ffl
Project No. A447 Site: . Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: 039833
Sample wt/vol: 25.0 (g/mL) ML „, Lab File ID:U196.D
Level: (low/med) __ _ _ _ _ _ Date Received: 3/15/95
% Moisture: not dec. . • Date Analyzed: 3/19/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: (uL) Soil Aliquot Volume: _____ (uL)
. : Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name RT Est. Cone.
"
Q
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FORMI VOA-TIC 3/9°
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770314PW6
Lab Name: CHEMTECH___________________ Contract: US EPA REGION EH
Project No. A447 Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ED: 039967
Sample wt/vol: 25.0 (g/mL) ML ,. LabFileEO:L1197.D
Level: (low/med) _______ Date Received: 3/16/95
% Moisture: not dec. _______ Date Analyzed: 3/19/95
GC Column: DB624 ED; 0.53 (mm) Dilution Factor. 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found: 0___ (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
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RT Est Cone.
•-
Q
AR3I6575 FORM I VOA-TIC 000072 3/90
^ -IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770314PW5
Lab Name: CHEMTECH_________________ Contract: US EPA REGION m
Project No. A447 Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ED:. O39968
Sample wt/vol: 25.0 (g/mL) ML - Lab FileID:L1198.D
Level: (k»w/med) _______ Date Received: _3/16/95_
% Moisture: not dec. . . •__ Date Analyzed: 3/19/9!)_
GC Column: DB624______ ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: '_____(uL) Soil Aliquot Volume: ______ (uL)
1 Concentration Units:Number TICs found: 1___. . (ug/L or ug/Kg) ug/L
CAS Number
2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
•
l
RT (Est. Cone."5 £1 1 IT
• „
Q_!__
^316576 FORMIVOAJnc 000081 3/90
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770314W35
Lab Name: CHEMTECH_________________ Contract: US EPA REGION EH
Project No. A447 Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER , Lab Sample ID: O39969
Sample wt/vol: 25.0 (g/mL) ML - Lab File ID: LI 199.D
Level: (low/med) _____' Date Received: 3/16/95
% Moisture: not dec. _______ Date Analyzed: 3/19/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor 1.0
Soil Extract Volume: __________(uL) Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found: 0 ___ (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
i
RT Est. Cone.
• — .
Q
,
SR3I6577 FORM I VOA-TIC 000089 3/90
IE SAMPLE NO.VOLATELE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770315TB1
Lab Name: CHEMTECH__________________ Contract: US EPA REGION III
Project No. A447 Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: 039970
Sample wt/vol: 25.0 (g/mL) ML „- Lab FileID:L1200.D
Level: (low/med) _______ Date Received: j/16/95_
% Moisture: not dec. ________ Date Analyzed: _3/19/95_
GC Column: DB624________ ED: '0.53 (mm) Dilution Factor: __U)__
Soil Extract Volume: _______(uL) Soil Aliquot Volume: ___ __ (uL)
; Concentration Units:Number TICs found: Q .... (ug/L or ug/Kg) ug/L
41
CAS Number. 1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29. .30.
Compound Name
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RT Est. Cone.
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Q
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FORM I VOA-TIC n n n A n r 3/90AR3(6578 """•""""• 0.00096
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770315W08
Lab Name: CHEMTECH_________________ Contract: US EPA REGION EQ
Project No. A447 Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: O39971
Sample wt/vol: 25.0 (g/mL) ML - Lab File ED; L1203.D
Level: (low/med) _______ ' Date Received: 3/16/95
% Moisture: not dec. _________ Date Analyzed: 3/19/95
GC Column: DB624______ ED; 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found: 1 (ug/L or ug/Kg) ug/L
CAS Number•4, ————————2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound NameWafcaewa —————————————
I
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AR3I6579 FORMIVOA-TIC Q00103 3/9°
v llE ' SAMP1LENO.VOLATILE ORGANICS ANALYSIS DATA SHEETtfiNTATEVELY IDENTIFIED COMPOUNDS 077031SW12
Lab Name: CHEMTECH______' Contract: US EPA REGION III
Project No. A447___ Site: Location: ___________ Group:
Matrix: (soil/water) WATCR Lab Sample ED: 039972
Sample wt/vol: __25.0 (g/mL) ML -' Lab File ID: L1202.D
Level: (low/med) _______ Date Received: 3/16/95
% Moisture: not dec. _______ Date Analyzed; 3/19/95 _GC Column: DB624 ED; 0.53 (mm) Dilution Factor __1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found: ___0___ (ug/L or ug/Kg) ug/L
CAS NumberI.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name RT Est Cone.
-
Q
;AR3!658G
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770316W31
Lab Name: CHEMTECH_________________ Contract: US EPA REGION EQ
Project No. A447 Site: _____ Location: __________ Group:
Matrix: (soil/water) WATER Lab Sample ID: O40051
Sample wt/vol: 25.0 (g/mL) ML -' Lab File ID: L1207.D
Level: (low/med) _______ Date Received: 3/17/95
% Moisture: not dec. _______ Date Analyzed: 3/20/95GC Column: DB624_______ ED; 0.53 (nun) Dilution Factor 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: ^ ^ (uL)
Concentration Units:Number TICs found: 1 (ug/L or ug/Kg) ug/L
CAS Number_L, ————————2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound NameyaknewH ————————————
RT——— Zr6rf-
Est. Cone.—— i-fi— .
" -
Q—— f ——
FORM I VOA-TIC ^ 3/90000119
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770316W32
Lab Name: CHEMTECH__________________ Contract: US EPA REGION EQ
Project No. A447 • Site: _____ Location: _________ Group:
Matrix: (soU/water) WATER Lab Sample ID: O400S2
Sample wt/vol: 25.0 (g/mL) ML - Lab File ED; L1208.D
Level: (low/med) ________ Date Received: 3/17/95
% Moisture: not dec. _____' Date Analyzed: 3/20/95_
GC Column: DB624______ ED; 0.53 (mm) Dilution Factor: __L£ _
Soil Extract Volume: ' ____(uL) Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found: ___0___ (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name RT Est Cone.
• ~.
Q
•
AR3I658-2 K"*"™-™ 000127
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS Q770316W23
Lab Name: CHEMTECH_________________ Contract: US EPA REGION in
Project No. A447 Site: _____ Location: ____________ Group:
Matrix: (soil/water) WATER Lab Sample ED: O40053
Sample wt/vol: 25.0 (g/mL) ML - Lab File ED: L1209.D
Level: (low/med) ___________ Date Received: 3/17/95
% Moisture: not dec. Date Analyzed: 3/20/95
GC Column: DB624 ______ ED: 0.53 (mm) Dilution Factor; 1.0
Soil Extract Volume: _______ (uL) Soil Aliquot Volume; (uL)
Concentration Units:Number TICs found: 1 ___ (ug/L or ug/Kg) ug/L
CAS Number— fc ————— , ——2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound NameUnkaawB — : ——————————
RT—— 3 46-
Est, Cone.| ——— S—-
Q—— J ——
•
AR3 { 6583 FORMI VOA-TIC 000135 3/90
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770316W24
Lab Name: CHEMTECH________________ Contract: US EPA REGION ffl
Project No. A447___ Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: O40054
Sample wt/vol: __25.0__(g/mL) ML -' LabFileID:L1210.D
Level: (low/med) _______ Date Received: 3/17/95
% Moisture:: not dec. ________ Date Analyzed: 3/20/9S
GC Column: DB624 ED; 0.53 (mm) Dilution Factor 1.0
Soil Extract Volume: __ (uL) Soil Aliquot Volume: __ _ (uL)
Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.IS.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name.
i
RT (Est Cone. Q
FORMI VOA-TIC - 3/900 0 0 1 4 -
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770316W10
Lab Name: CHEMTECH_________________ Contract: US EPA REGION Ed
Project No. A447 Site: ________ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: 040055
Sample wt/vol: 25.0 (g/mL) ML ,- LabFileID:L1211.D
Level: (low/med) ________ Date Received: 3/17/95
% Moisture: not dec. _______ Date Analyzed: 3/20/95
GC Column: DB624 EO: 0.53 (mm) Dilution Factor 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: _____._ (uL)
Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Namei
i -
RT (Est. Cone.
•
1
Q
lk>RMIVOA-'nc °00143
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770316W27
Lab Name: CHEMTECH ____________ Contract: US EPA REGION ffl
Project No. A447 Site: _____ Location: ____________ Group:
Matrix: (soil/water) WATER Lab Sample ID:. O40056
Sample wt/vol: 25.0 (g/mL) ML -• Lab File ID: L1212.D
Level: (low/med) _______ Date Received: 3/17/95
% Moisture: not dec. _______ Date Analyzed: _3/20/95_
GC Column: DB624____, ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: (uL) Soil Aliquot Volume: __ (uL)
Concentration Units:Number TICs found: 0_____ (ug/L or ug/Kg) ug/L
CAS NumberI.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
i
•
RT Est. Cone.
• -
Q
«
FORM * VOA-TIC 000155 3/90
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770316TB1
Lab Name: CHEMTECH_______________ __ Contract: US EPA REGION III
Project No. A4S5 Site: ______ Location: _______• Group:
Matrix: (soil/water) WATER Lab Sample ID: O400S9
Sample wt/vol: 25.0 (g/mL) ML -• Lab File ID: L1232.D
Level: (low/med) _______ Date Received: 3/17/95
% Moisture: not dec. • Date Analyzed: . 3/25/95
GC Column: DB624_________ ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found: 1___ (ug/L or ug/Kg) ug/L
CAS Number
2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound NameUnit-own ————————————
RT—— SrW-
Est Cone.——— £9—
• -
Q1 j —
A R 3 / 6 5 £ 7 FORMl VOA"TIC
IE • SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770320TB1
Lab Name: CHEMTECH_____________-_____ Contract: US EPA REGION III
Project No. A45S Site: _____ Location: _______'• Group:
Matrix: (soil/water) WATER Lab Sample ID: O40110
Sample wt/vol: 25.0 (g/mL) ML - Lab File ID: L1243.D
Level: (low/med) ________ Date Received: 3/21/95
% Moisture: not dec. _______ Date Analyzed: 3/25/95
GC Column: DB624 __' ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ___ (uL) Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found; 0 (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name RT Est. Cone.
' -
Q
FORMI VOA-TIC 000 71 3/90
AR3I6588
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770320W15
Lab Name: CHEMTECH_________________ Contract: US EPA REGION III
Project No. A4S5 Site: _____ Location: ___________ Group:
Matrix: (soil/water) WATER Lab Sample ID: O40101
Sample wt/vol: 25.0 (g/mL) ML ' Lab File ID: L1233.D
Level: (low/med) _______ Date Received: 3/21/95
% Moisture: not dec. _______ Date Analyzed: 3/25/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ________(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/L
:AS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name RT Est Cone.
~
Q
A R 3 I 6 5 fi Q VOA'TIC ftflrt 37fd£"
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS .0770320W18
Lab Name: CHEMTECH_____________• Contract: US EPA REGION III
Project No. A45S Site: _____ Location: __________ Group:
Matrix: (soil/water) WATER Lab Sample ID: O40103
Sample wt/vol: 25.0 (g/mL) ML - Lab File ID: LI235.D
Level: (low/med) _______ Date Received: 3/21/95
% Moisture: not dec. _______ Date Analyzed: 3/25/95
GC Column: DB624 ______ ED: 0.53 (mm) Dilution Factor: 1.0
Soil Exiract Volume: ________(uL) Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found: 1 (ug/L or ug/Kg) ug/L
CAS Number-4, ———————2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound NameC _T— I IJJL j-y •. _m
,
RT—— 3*69-
Est Cone.—— 24-
• -
Q— , ——
000 35FORM I VOA-TIC 3/90
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 0770320W21
Lab Name: CHEMTECH__________________ Contract: US EPA REGION III
Project No. A455 Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: 040102
Sample wt/vol: 25.0 (g/mL) ML ' Lab File ID: L1234.D
Level: (low/med) _______ Date Received: 3/21/95
% Moisture: not dec. ________ Date Analyzed: 3/25/95
GC Column: DB624 ED: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: __________(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name RT Est. Cone.
-
Q
FORMI VOA-TIC 3/90
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH_______ Contract: US EPA REGION III
Project No. A446-S____ Site: _____ Location: _____ Group: _______
Instrument ID: VOA1__________ Calibration Date: 3/18/95 Time: 0956
Lab File ID: E1067.D_____;____ Init Calib. Date(s): 2/24/95 2/24/95
Heated Purge: (Y/N) Y Init Calib. Times: 0918 T256
GC Column: DB624 EO; 0.53 (mm)
COMPOUND
i
•
Toluene-d8Bromofluorobenzene1 ,2-Dichlorocthane-d4
RRF
1.0160.6941.413
RRF50
0.9860.6561.931
MINRRF
0.0100.2000.010
%D
3.05.5-36.7
MAX%D
100.0|25.0100.0
All other compounds must meet a minimum RRF of 0.010.;
Page 2 of 2 , .AR3 i 6592FORM VOA 3/9°
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH_______ Contract: US EPA REGION III
Project No. A446-S_____ Site: _____ , Location: ______ Group:
Lab File ID: E1067.D Init Calib. Date(s): 2/24/95 2/24/95
Heated Purge: (Y/N) Y Init Calib. Times: 0918 1256
GC Column: DB624 ED; 0.53 (mm)
COMPOUNDDichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroetnaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1.1-Dichloroethanetrans-1 ,2-Dichloroethenecis-l,2-DichloroetheneChloroform1,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochlorometbane1 , 1 ,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroediene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrcnem+p-Xyleneso-xylene
RRF0.5170.6170.4020.6610.2921.7190.4342.9591.9232.7282.0791.4372.9361.8230.1660.5400.5350.7020.4330.5550.3930.6410.3690.9120.3950.4960.4890.3280.5560.7041.2240.9771.4840.8770.5441.133
RRF500.3370.5680.4790.6300.4432.7260.4443.9342.3273.2232.4331.4013.4631.8730.1010.6050.4710.7680.3600.6140.3750.5370.2871.0300.4160.3940.2700.1590.4500.4371.2040.7301.4510.8080.5271.114
MINRRF
0.1000.100
0.1000.200
0.2000.100
0.1000.1000.200
0.2000.3000.1000.1000.5000.1000.100
0.2000.5000.4000.5000.1000.3000.3000.300
%D34.& >7.9-19.24.7
< 51.7< 58.6 >
-2.3< 3.QJ-21.0-18.1-17.02.5-17.9-2.7
f"39.2_H.T -12.0
12.0-9.416.9-10.64.616.222.2-12.9-5.320.6
C5L5_>19.1
C37.g1.6
CT25.32.27.93.01.7
MAX%D100.0100.025.025.0100.0100.0100.0100.025.025.0100.0100.0•25.025.0'100.025.025.025.0100.025.025.025.025.025.025.025.0100.0100.025.025.025.025.025.025.025.025.0
Instrument ID: VOA1 Calibration Date: 3/18/95 Time: 0956
All other compounds must meet a minimum RRF of 0.010. 000205
Pagei0f2 AR3I6593
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH_____' Contract: US EPA REGION III
Project No. A446-S_____ Site: _____ Location: ______ Group:
Instrument ID: VOA1 Calibration Date: 3/17/95 Time: 2132
Lab File ID: E1051.D______\_____"Init Calib. Date(s): 2/24/95 2/24/95
Heated Purge: (Y/N) . Y Init. Calib. Times: 0918 (256
GC Column: DB624 ED: 0.53 (mm)
COMPOUND
Toluene-d8Bromofluorobenzenel,2-Dichloroetliane-d4
RRF
1.0160.6941:413
RRF50
0.9870.6462.014
MINRRF
0.0100.2000.010
%D
2.96.9-42.5
MAX%D
100.025.0100.0
All other compounds must meet a minimum RRF of 0.010.000204Page2of2 •
FORM VH VGA flR3|659U •-.*»
7A •VOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH_______ Contract: US EPA REGION III
Project No. A446-S____ Site: ____ Location: ________ Group:
Lab File ID: E1051.D_____________ l. Calib. Date(s): 2/24/95 2/24/95
Heated Purge: (Y/N) Y Init Calib. Times: 0918 1256
GC Column: DB624 ED: 0.53 (mm)
COMPOUNDDichlorodifluoromethaneChloromediancBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroemene1 , 1-Dichloroethanetrans- 1 ,2-Dichloroethenecis-1 ,2-DichloroetheneChloroform1 ,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-1, 3-DichloropropcncBromofbrm4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrencm+p-Xyleneso-xylene
RRF0.5170.6170.4020.6610.2921.7190.4342.9591.9232.7282.0791.4372.9361.8230.1660.5400.5350.7020.4330.5550.3930.6410.3690.9120.3950.4%0.4890.3280.5560.7041.2240.9771.4840.8770.5441.133
RRF500.3850.6220.4800.7470.4112.5400.4454.1992.6303.3382.5931.6843.6282.0080.1010.6270.5280.8200.3940.6360.4090.5870.3091.0340.4230.3970.3080.1740.4630.4531.1830.7491.4370.8450.5271.091
MENRRF
I
0.1000.100
0.1000.200
0.2000.100
0.1000.1000.200
0.2000.3000.1000.1000.5000.1000.100
1
0.2000.5000.4000.5000.1000.3000.3000.300
%D*75.5 >-0.8-19.4-13.0Q0.8
-2.5C31.9CSeTsJ?-22.4-24.7-17.2-23.6-10.1CJ2-W-16.11.3-16.89.0-14.6-4.18.416.3-13.4-7.120.0
1137.0-T371C?16.7
C.3SJ*?3.323.33.23.63.03.7
MAX%D100.0100.025.025.0100.0100.0100.0100.025.025.0100.0100.025.025.0100.025.025.025.0100.025.025.025.025.025.025.025.0100.0100.025.025.025.025.025.025.025.025.0
Instrument ID: VOA1 Calibration Date: 3/17/95 Time: 2132
All other compounds must meet a minimum RRF of 0.010.000203
Pagelof2 AR3I6595
6A . ^ r .. N ,,VOLATILE ORGANICS INITIAL CALIBRATION DATA " ~" " "
Lab Name: CHEMTECH________ Contract: US EPA REGION III
Lab Code: CHEM_____ Case No.: A446-S SAS No.: ' SDG No.: _______
Instrument ID: VOA1_____ Calibration Date(s): 2/24/95 2/24/95Heated Purge: (Y/N) _Y_ Calibration Times: 0918 1256
GC Column DB624 _____ EOT 0.53 (mm)
Lab File ID: RRF10 = E1002.D RRF20 = E1004.DRRF50 = E1001.D RRFlOO = E1005.D RRF200 = E1003.D
COMPOUNDChloromethaneDichlorodifiuoromethaneBromomethane *Vinyl Chloride *ChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichlorocthene *1,1-Dichloroethane *trans- 1 ,2-Dichloroethenecis-l,2,-DichloroetheneChloroform *1,2-Dichloroethane *2-Butanone1,1,1-Trichloroethane *Zarbon Tetrachloride *Bromodichloromethane *1 ,2-Dichloropropanecis-1, 3-Dichloropropene *Frichloroethene *Dibromochloroinethane *1,1,2-TrichlQroethane *Benzene *trans-l,3-Dichloropropene *Bromoform *4-Methyl-2-Pentanone2-Hexanoneretrachloroetheae *1 , 1 ,2,2-Tetrachloroethane *Toluene *Chlorobenzene *Ethylbenzene *Styrene *n+p-Xylenes *o-xylene ;Foluene-dSBromofluorobenzene *1 ,2-Dichloroethane-d4
RRF100.5730.4420.4340.5510.3651.6910.5482.5361.6232.2631.6891.1652.4441.4610.1490.4760.4530.6180.3770.4800.3420.5920.3330.7910.3420.4720.4690.2830.5240.8031.1500.9021.3740.7670.4891.0490.9650.6911.195
RRF200.6560.5260.4170.7010.2731.9010.7553.0362.0412.9732.2751.5633.2452.2000.3190.6070.5980.7940.4990.6580.4490.7800.4921.0390.4870.6810.8410.5980.6540.6681.4011.1261.6520.9710.5971.2331.2080.7861.736
RRF500.7020.6310.4610.7530.3241.8160.2923.3442.0842.9512.2541.5613.1641.847.0.1140.5710.5870.7320.4460.5620.4260.6470.3540.9490.3950.4640.3660.2330.6040.7011.3091.0301.5950.9420.6041.2521.0340.7041.382
RRFlOO0.5650.4530.3420.6480.2511.6410.3342.8131.9732.7792.1511.4662.9731.9030.1520.5290.5250.7100.4340.5480.3800.6070.3510.9110.3920.4450.4550.3150.4880.7521.1320.8951.3930.8570.5041.0790.9840.6781.494
RRF2000.5900.5310.3590.6490.2461.5440.2403.0661.8932.6742.0261.4312.8561.7040.0990.5150.5110.6550.4080.5250.3690.5780.3170.8710.3610.4190.3140.2110.5130.5981.1260.9351.4080.8460.5241.0510.8890.6121.257
RRF0.6170.5170.4020.6610.2921.7190.4342.9591.9232.7282.0791.4372.9361.8230.166 <0.54010.5350.7020.4330.5550.3930.6410.3690.9120.3950.4960,489 (0.328 t0.5560.7041.2240.9771.4840.8770.5441.1331.0160.6941.413
%RSD9.614.712.611.317.68.22E&10.29.510.511.511.410.714.92.£9.4ll.l9.810.511.911.112.819.010.1
L___l21.3JiHr=_L__'12.511.110.210.18.79.39.88.911.79.015.2
000185
* Compounds .with required minimum RRF and maximum %RSD values.All other compounds must meet a minimum RRF of 0.010. A ft 3 j 6 S Q £
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH________ Contract: US EPA REGION ffl
Project No. CHEM_____ Site: A440-S Location: _____ Group:
Instrument ID: VOA1 Calibration Date: 3/18/95 Tune: 0956
Lab File ED: E1067.D__________ Init. Calib. Date(s): 2/24/95 2/24/95
Heated Purge: (Y/N) ____ Init Calib. Times: 0918 1256
GC Column: DB624 ED; 0.53 (mm)
COMPOUND
Toluene-d8Bromofluorobenzene1 ,2-Dichloroethane-d4
RRF
1.0160.6941.413
RRF50
0.9860.6561.931
MENRRF
0.0100.2000.010
%D
••-.
•
3.05.5-36.7
MAX%D
100.025.0100.0
All other compounds must meet a minimum RRF of 0.010.
Page2of2 - Q „ . - _ . ^AR3I6597 FORMVHVOA - uuu-^u^ 3/9Q
7A 'VOLATILE CONTINUING CALIBRATION CHECK ,
Lab Name: CHEMTECH ____ Contract: US EPA REGION III
Project No. CHEM_____ Site: A440-S Location: _____ Group:
Instrument ED1: VOA1 Calibration Date: 3/18/95 Time: 0956
Lab File ID: E1067.D____. Init Calib. Date(s): 2/24/95 2/24/95
Heated Purge: (Y/N) ____ Init. Calib. Times: 0918 1256
GC Column: DB624 ED: 0.53 (mm)
COMPOUNDDichlorodifluoromethaneChloromcdianeBromomethaneVinyl ChloriiieChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,1-Dichloroetnanetrans-1 ,2-Dichloroethenecis-1, 2-DichloroetfaeneChloroform «1 ,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1, 3-DichloropropeneTrichloroethcneDibromochloromethane1, 1,2-TrichloroethaneBenzenetrans-l,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-Hexanone
' Tetrachloroeihene1,1,2,2-TetrsichloroethaneTolueneChlorobenzeiieEfhylbenzeneStyrenem+p-Xyleneso-xylene
RRF0.5170.6170.4020.6610.2921.7190.4342.9591.9232.7282.0791.4372.9361.8230.1660.5400.5350.7020.4330.5550.3930.6410.3690.9120.3950.4960.4890.3280.5560.7041.2240.9771.4840.8770.5441.133
RRF500.3370.5680.4790.6300.4432.7260.4443.9342.3273.2232.4331.4013.4631.8730.1010.6050.4710.7680.3600.6140.3750.5370.2871.0300.4160.3940.2700.1590.4500.4371.2040.7301.4510.8080.5271.114
MENRRF
0.1000.100
<
(0.1000.200
0.2000.100
i0.1000.1000.200
0.2000.3000.1000.1000.5000.1000.100
0.2000.5000.4000.500 i0.1000.3000.3000.300
%DC_J4,8 >
7.9-19.24.7
T-51.7J5CT-58.6
-2.31-33.0-21.0-18.1-17.02.5-17.9-2.7
L 39.2 2-12.012.0-9.416.9-10.64.616.222.2-12.9-5.320.6
(_44.8 _C51.5 >
19.137.9-21.6
, 25.32.27.93.01.7
MAX%D100.0100.025.025.0100.0100.0100.0100.025.025.0100.0100.025.025.0100.025.025.025.0100.025.025.025.025.025.025.025.0
> 100.0Lioo.o25.025.025.025.025.025.025.025.0
077 3 BOlb
Pan. 1 nf t
All other compounds must meet a minimum RRF of 0.010.
AR3I6598 000201
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH_________ Contract: US EPA REGION lEt
Project No. CHEM Site: A440-S Location: _______ Group:
Instrument ED: VOA1 Calibration Date: 3/17/95 Tune: 2132
Lab File ID: E1051.D____________ Mt Calib. Date(s): 2/24/95 2/24/95
Heated Purge: (Y/N) _.___ Init Calib. Times: 0918 1256
GC Column: DB624 ED: 0.53 (mm)
COMPOUND
Toluene-d8Bromofluorobenzene1 ,2-Dichloroethane-d4
RRF
i
1.0160.6941.413
RRF50
0.9870.6462.014
MINRRF
0.0100.2000.010
%D
-
2.96.9-42.5
MAX56D
100.025.0100.0
All other compounds must meet a minimmn RRF of 0.010.
Page2of2 fl P J C q Q n 000200"* H n O f O O y \m
.. - - - •- , • . . - : , 7A
VOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH Contract: US EPA REGION ETC
Project No. CHEM Site: A440-S Location: _____ Group:
Instrument ID: VOAl Calibration Date: 3/17/95 Time: 2132
Lab File ID: E1051.D_______ Init. Calib. Date(s): 2/24/95 2/24/95
Heated Purge: (Y/N) ___ Init Calib. Tunes: 0918 1256
GC Column: DB624 ED: 0.53 (mm)
COMPOUNDDichlorodifluoromethaneChloromethane •BromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1 , 1-Dichloroethanecis-l,2-Dichloroethenetrans-1 ,2-DichloroetheneChloroform1 ,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetracMorideBromodichloromethane1 ,2-Dichloropropanecis-1, 3-Dichlo:ropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrenem+p-Xyleneso-xylene
RRF0.5170.6170.4020.6610.2921.7190.4342.9591.9232.7282.0791.4372.9361.8230.1660.5400.5350.7020.4330.5550.3930.6410.3690.9120.3950.4960.489
. 0.3280.5560.7041.2240.9771.4840.8770.5441.133
RRF500.3850.6220.4800.7470.4112.5400.4454.1992.6303.3382.5931.6843.6282.0080.1010.6270.5280.8200.3940.6360.4090.5870.3091.0340.4230.3970.3080.1740.4630.4531.1830.7491.4370.8450.5271.091
M1NRRF
0.1000.100
0.1000.200
0.2000.100
0.1000.1000.200
0.2000.3000.1000.1000.5000.1000.100
(0.2000.5000.4000.5000.1000.3000.3000.300
%DT 25.5 J
-0.8-19.4-13.0
I -40.8(~3fl&
-2.5""-41-JLx1-36.8 -22.4-24.7-17.2-23.6-10.1
_ 39.2I>>-16.11.3-16.89.0-14.6-4.18.416.3-13.4-7.120.0
C37.0L2"47.0316.7
-~35.7 :>3.323.33.23.63.03.7
MAX%D100.0100.05.025.0100.0100.0™'100.0100.025.025.0100.0100.025.025.0100.05.025.025.0100.025.025.025.025.025.025.025.0100.0100.0""25.025.025.025.025.025.025.025.0
I
cdtcc
T»_— i -.e
All other compounds must meet a minimum RRF of 0.010.
AR3I6600 °001"
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH_______ Contract: US EPA REGION III
Project No. CHEM_____ Site: A440-S Location: _____ Group:
Instrument ED: VOA1___________ Calibration Date: 3/17/95 Tune: 0926
Lab File ED: E1035.D__________ Init Calib. Date(s): 2/24/95 2/24/95
Heated Purge: (Y/N) ___ Init Calib. Times; 0918 1256
GC Column: DB624 ED; 0.53 (mm)
COMPOUND
Toluene-d8Bromofluorobenzene1 ,2-Dichloroethane-d4
RRF
1.0160.6941.413
RRF50
0.7300.5031.637
MINRRF
0.0100.2000.010
%D
••--
28.127.5 \-15.9
MAX%D
100.0;>25.0100.0
All other compounds must meet a minimum RRF of 0.010.
Page2of2 AR3I660I FORMVII>OA 000198 3/90
-— — 7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH Contract: US EPA REGION III
Project No. CHEM____ Site: A440-S Location: _____ Group:
Instrument ED; VOA1________ Calibration Date: 3/17/95 Time: 0926
Lab File ID: E1035.D_____ '. Init Calib. Date(s): 2/24/95 2/24/95
Heated Purge: (Y/N) ___ Init Calib. Times: 0918 1256
GC Column: k DB624 ED: 0.53 (nan)
COMPOUNDDichlorodifluoromethaneChlorometharic
. BromomethaceVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroefflene1 , 1-Dichloroethanetrans-1 ,2-Dicliloroethenecis-l,2-DichloroetheneChloroform1 ,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheioeDibromochloromethane1 , 1,2-TrichloiroethaneBenzenetrans-1 ,3-DicliloropropeneBromoform4-Methyl-2-Pcntanone2-HexanoneTetrachloroediene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrenem+p-Xyleneso-xylene
RRF0.5170.6170.4020.6610.2921.7190.4342.9591.9232.7282.0791.4372.936
. 1.8230.1660.5400.5350.7020.4330.5550.3930.6410.3690.9120.3950.4960.4890.3280.5560.7041.2240.9771.4840.8770.5441.133
RRF500.2950.5130.4440.6260.3272.3840.5014.0242.2583.3822.5731.5043.7372.1470.1360.6590.5000.8700.3740.6760.3760.5830.3191.1060.4690.4330.3290.2080.4210.5431.1970.7%1.5140.8460.5541.173
MENRRF
0.1000.100
0.1000.200
0.2000.100
0.1000.1000.200
0.2000.3000.1000.1000.5000.1000.100
0.2000.5000.4000.5000.1000.300
. 0.3000.300
%D£~42JD
16.9-10.45.3
-12.038'.7I>-15.4
(-36.0-17.4-24.0-23.8-4.6
T -274-2-17.818. I-22.06.5
-23.913.6-21.84.39.013.6-21.3-18.712.7
C32.7 >^ 36.6 >24.322.92.218.5-2.03.5-1.8-3.6
MAX%D100.0100.025.025.0100.0100.0100.0100.025.025.0100.0100.025.025.0100.025.025.025.0100.025.025.025.025.0
\2S.6.25.025.0100.0100.025.025.025.025.025.025.025.025.0
All other compounds must meet a minimum RRF of 0.010.000197
Pare 1 of 2
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH_______ Contract: US EPA REGION HI
Project No. CHEM Site: A440-S Location: _____ Group:
.Instrument ID: VOA1 Calibration Date: 3/13/95 Tune: 0937
Lab File ID: E1019.D__________ Init Calib. Date(s): 2/24/95 2/24/95
Heated Purge: (Y/N) ___ Init. Calib. Times: 0918 ' 1256
GC Column: DB624 ED: 0.53 (mm)
COMPOUND
Toluene-d8Bromofluorobenzene1 ,2-Dichloroethane-d4
RRF
1.0160.6941.413
RRF50
0.7800.5191.706
MINRRF
0.0100.2000.010
%D
••-
22_2_25.2 '"~3X}?I "
MAX%D
100.0}25.0100.0
All other compounds must meet a minimum RRF of 0.010.
Page2of2 fl D Q I fi c n ~ -- 000198& n 3 ] 6603 FORM VTT VOA 3/90
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH Contract: US EPA REGION in
Project No. CHEM____ Site: A440-S Location: _____ Group:
Instrument ID: VOA1 Calibration Date: 3/13/95 Time: 0937
Lab File ID: E1019.D Init Calib. Date(s): 2/24/95 2/24/95
Heated Purge: (Y/N) ___ Init. Calib. Tunes: 0918 1256
GC Column: DB624 ED; 0.53 (mm) '\l&(-\<0 I
COMPOUN1DDichlorodifluoromethaneChloromedianeBromomethaneVinyl ChlorideChloroethancMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1 , 1-Dichloroedianetrans-1, 2-Dii:hloroethenecisl,2-DichloroetheneChloroform1 ,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1. 3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-Trichloroethane
I Benzenei trans-1, 3-Dicbloropropene! Bromoform
4-Methyl-2-]Pentanone2-HexanoneTetrachloroethene1 * 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene ,m+p-Xyleas(total)o-xylene
RRF0.5170.6170.4020.6610.2921.7190.4342.959 .1.9232.7282.0791.4372.9361.8230.1660.5400.5350,7020.4330.5550.3930.6410.3690.9120.3950.4960.4890.3280.5560.7041.2240.9771.4840.8770.5441.133
RRF500.4320.6290.4430.7150.3352.3400.6214.2752.2723.3642.5542.3083.6912.1630.1400.6400.5020.8400.3940.6450.3800.5800.3231.0770.4580.4260.3640.2300.4390.5381.2150.7591.4910.8590.5711.172
MINRRF
0.1000.100
0.1000.200
(0.2000.100
0.1000.1000.200
0.2000.3000.1000.1000.5000.1000.100
0.2000.5000.4000.5000.1000.3000.3000.300
%D16.4-1.9-10.2-8.2-14.736. 0
C-44 >-18.1-23.3-22.8r so-25.7-18.715:7-.-18.56.2-19.79.0-16.23.39.512.5-18.1-15.914.1
C3335C29.9_>21.023.60.722.3-0.52.1-5.0-3.5
MAX%D100.0100.025.025.0100.0100.0100.0100.025.025.0100.0100.025.025.0100.025.025.025.0100.025.025.025.025.025.025.025.0100.0100025.025.025.025.025.025.025.025.0
All other compounds must meet a minimum RRF of 0.010. •'.. ' ... „. >' U"-/J •
ppt.
6AVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: CHEMTECH _____ Contract: US EPA REGION EQ
Lab Code: CHEM_____ Case No.; A440-S SASNo.: _____ SDGNo.:
Instrument ID: VOA1 Calibration Date(s): 2/24/95 2/24/95
Heated Purge: (Y/N) _Y_ CaUbration Times: 0918 1256
GC Column DB624 ED: 0.53 (mm)
Lab File ID: RRF10 = E1002.D RRF20 = E1004.DRRF50 = E1001.D RRFlOO = E1005.D RRF200 - E1003.D
COMPOUNDChloromethaneDichlorodifluoromethaneBromomethane *Vinyl Chloride *ChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene *1 , 1 -Dichloroethane *trans-1, 2-Dichloroethcnecis-1 ,2,-DichloroetheneChloroform *1,2-Dichloroethane *2-Butanone1,1,1-Trichloroethane *Carbon Tetrachloride *Bromodichloromethane *1 ,2-Dichloropropanecis-1, 3-Dichloropropene *rrichloroethene *Dibromochloromethane *1,1,2-Trichloroethane - *Benzene *trans-l,3-Dichloropropene *Bromoform *4-Methyl-2-Pentanone2-Hexanoneretrachloroethene *1,1,2,2-Tetrachloroethane *roluene *Chlorobenzene *Ethylbenzene *Styrene *m+p-Xylcnes *o-xyleneroluene-48Bromofluorobenzene *1 ,2-Dichloroethane-d4
RRF100.5730.4420.4340.5510.3651.6910.5482.5361.6232.2631.6891.1652.4441.4610.1490.4760.4530.6180.3770.4800.3420.5920.3330.7910.3420.4720.4690.2830.5240.8031.1500.9021.3740.7670.4891.0490.9650.6911.195
RRF200.6560.5260.4170.7010.2731.9010.7553.0362.0412.9732.2751.5633.2452.2000.3190.6070.5980.7940.4990.6580.4490.7800.4921.0390.4870.6810.8410.5980.6540.6681.4011.1261.6520.9710.5971.2331.2080.7861.736
RRF500.7020.6310.4610.7530.3241.8160.2923.3442.0842.9512.2541.5613.1641.8470.1140.5710.5870.7320.4460.5620.4260.6470.3540.9490.3950.4640.3660.2330.6040.7011.3091.0301.5950.9420.6041.2521.0340.7041.382
RRFlOO0.5650.4530.3420.6480.2511.6410.3342.8131.9732.7792.1511.4662.9731.9030.1520.5290.5250.7100.4340.5480.3800.6070.3510.9110.3920.4450.4550.3150.4880.7521.1320.8951.3930.8570.5041.0790.9840.6781.494
RRF2000.5900.5310.3590.6490.2461.5440.2403.0661.8932.6742.0261.4312.8561.7040.0990.5150.5110.6550.4080.5250.3690.5780.3170.8710.3610.4190.3140.2110.5130.5981.1260.9351.4080.8460.5241.0510.8890.6121.257
RRF0.6170.5170.4020.6610.2921.7190.434 <2.9591.9232.7282.0791.4372.9361.8230.166 <0.5400.5350.7020.4330.5550.3930.6410.3690.9120.3950.4960.489 i0.328 <0.5560.7041.2240.9771.4840.8770.5441.1331.0160.6941.413
%RSD9.614.712.611.317.68.242dL10.29.510.511.511.410.714.9-52.99.411.19.810.511.911.112.819.010.114.121.342.3£LL.12.511.110.210.18.79.39.88.911.79.015.2
* Compounds with required minimum RRF and marin tm %RSD values. 0 0 O 1.„,,_,.,~:-:»t>n~,nn,« ^^^ j ^^^
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH _______ Contract: US EPA REGION III
Project No. A455-S Site: _____ Location: ______ Gromp:
Instrument ID: VOA1 Calibration Date: 3/25/95 Tune: 0940
Lab File ID: L1238.D Init. Calib. Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) ____ Init Calib. Times: 1022 . 1314
GC Column: DB624 ED: 0.53 (mm)
COMPOUND2-Hexanone1, 1,2,2-Tetrachloroethane1 ,3-Dichlorobenzene1 ,4-Dichlorobenzene1 ,2-Dichlorobenzene1 ,2-Dibromo-3-chloropropane
X
.
1 .4-Bromofluorobenzene
RRF0.1310.3370.8840.8790.7500.062
0.521
RRF50.1130.3500.8290.8470.7360.066
0.548
MINRRF
0.5000.6000.5000.400
%D13.7-3.96.23.61.9-6.5
'--• -
-5.2
MAX%D
30.030.030.030.0
M other compoiinds must meet a minimum RRF of 0.010. - '-:'-;
Page2of2 ' - , • • • • fi D Q 1 C C n C 000110urwvr vn vn* ft ft J J 0 u U D 7/Qn
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH_________ Contract: US EPA REGION III
Project No. A455-S____ Site: _____ Location: _______ Group:
Instrument ED: VOA1 Calibration Date: 3/25/95 Time: 0940
Lab File ED: L1238.D__________ Init. Calib. Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) ___ Init. Calib. Times: 1022 1314
GC Column: DB624 ED: 0.53 (mm)
COMPOUNDDichlorodifluoromcthaneChloromethaneVinyl ChlorideBromomethaneChloroethane1 , 1-DichloroetheneMethylene ChlorideAcetoneCarbon Disulfidetrahs- 1 ,2-Dichloroemene1 , 1-Dichloroe thanecis-l,2-DichloroetheneBromochloromethaneChloroform2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBenzene1 ,2-DichloroethaneTrichloroethene1 ,2-Dichloropropanc1 ,2-DibromoethaneBromodichloromethanecis-1, 3-DichloropropeneToluenetrans-1 ,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzene *Ethylbenzenem&p-xyleneso-xyleneStyreneBromoform4-Methyl-2-pentanone
RRF0.3300.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.8620.2640.185
RRF50.1830.2180.2330.0950.1080.4250.259(G.Q49}0.8160.4170.5480.4690.3950.6010.1260.6860.6271.1040.2770.4460.4450.3320.6180.5271.2480.3770.2470.5220.4570.8771.5021.0871.0940.8170.3120.163
MENRRF
0.1000.100
0.100
0.200
0.1000.200
0.1000.1000.5000.1000.300
0.1000.2000.2000.4000.1000.1000.2000.1000.5000.1000.3000.3000.3000.100
%DC44.5>
17.413.423.415.611.3f W*35.5 14.411.811.612.716.014.611.3-9.3-1.37.82.83.011.013.17.65.44.84.14.32.8-1.17.25.54.86.15.2
-18.211.9
MAX%D
30.030.0
30.0
30.0
30.030.0
30.030.030.030.030.0
30.030.030.030.030.030.030.030.030.030.030.030.030.030.0
*J&+*~r'"-3
\/6l-H.o2.OjfOjZPST-A0f-f.o310l*A0Ho*3.<*<* &Off.o3**ralS&**** **-***•
%
•All other compounds must meet a minimiim RRF of 0.010.
Pagelof2 fiDQICCm 000109FORM vn VOA A R J I b b u 7 3/90
. ' -, ., . ...., ...-:_-. .... • .: . ~ '..it. 'VOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH ______ Contract: US EPA REGION III
Project No. A455-S____ Site: _____ Location: _____ Group:
Instrument ID: VOA1 Calibration Date: 3/24/95 . Time: 1742
Lab File ID: L1222.D___________ Init. Calib. Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) ___ Init. Calib. Times: 1022 1314
GC Column: DB624 ID: 0.53 (mm)
COMPOUND2-Hexanone1, 1,2,2-Tetirachloroe thane1 ,3-Dichlorobenzene1 ,4-Dichlorobenzene1 ,2-Dichlorobenzene1 ,2-Dibromo-3-chloropropane
4-Bromofluoirobenzene
RRF0.1310.3370.8840.8790.7500.062
.
0.521
RRF50.0840.2820.8670.8470.7320.060
0.441
MINRRF
0.5000.6000.5000.400
%D .(35V)16.31.93.62.43.2
"
15.4
MAX%D
30.030.030.030..0
--
All other compounds must meet a minimum RRF of 0.010.
/90
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH ______ Contract: US EPA REGION III
Project No. A4S5-S____ Site: ______ Location: ______ Group:
Instrument ID: VOA1 Calibration Date: 3/24/95 Time: 1742
Lab File ID: L1222.D Init. Calib. Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) ___ Init. Calib. Times: 1022 1314
GC Column: DB624 ID: 0.53 (mm)
All other compounds must meet a minimum RRF of 0.010.
Pagelof2 ' flp~ , rrnn 0001^7FORM vn VGA H n o i o o u y
COMPOUNDDichlorodifluoromethaneChloromethaneVinyl ChlorideBromomethaneChloroe thane1,1-DichIoroemeneMethylene ChlorideAcetoneCarbon Disulfidetrans-1 ,2-Dichloroethene1,1-Dichloroethanecis-1 ,2-DichloroetheneBromochloromethaneChloroform2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBenzene1 ,2-DichloroethaneTrichloroemene1 ,2-Dichloropropane1 ,2-DibromoethaneBromodichloromethanecis-1 ,3-DichloropropeneToluenetrans-l,3-Dichloropropene1 , 1 ,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneEthylbenzenem&p-xyleneso-xyleneStyreneBromoform4-Methyl-2-pentanone
RRF0.3300.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.8620.2640.185
RRF50.2950.2310.2540.1270.1480.4590.4845.0400.9130.4500.5960.4730.364.0.6270.0950.6950.6471.0510.2480.4720.3920.2940.5640.4601.2150.3260.2150.5890.4090.8661.4481.1001.0610.8060.2760.118
MINRRF
0.1000.100
0.100
0.200
0.1000.200
0.1000.1000.5000.1000.300
0.1000.2000.2000.4000.1000.1000.2000.1000.5000.1000.3000.3000.3000.100
%D10.612.55.6-2.4-15.64.26.2
C47.4J4.24.9
• 3.911.922.610.9C33.D8.1-4.5'12.313.0-2.621.623.015.717.47.317.016.7-9.79.58.48.93.78.96.5-4.5f36.2)
MAX%D
30.030.0
30.0
30.0
30.030.0
30.030.030.030.030.0
30.030.030.030.030.030.030.030.030.030.030.030.030.030.0
fLt~V*&~J
VIMK»Io??o*tyr*i0WOH°*"*ofT-osio"-*-1e,?7o3*o »"*O-fl-03*- ° "3~J
•
i
^VOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: CHEMTECH________ Contract: US EPA REGION III
Project No.: A455-S_____ Site: _____ Location: _____ Group:
Instrument ID: VOA1_____ Calibration Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) _ Calibration Tunes: 1Q22 1314
GC Column DB-624 ED: 0.53 (mm)Lab File DD: . , RRF1 =L1011.D . RRF2 = L1007.DRRF5 = L1008.D RRF10 = L1010.D RRF25 = L1009.D
COMPOUND2-Hexanone1,1,2,2-Tetrachloroethane *1,3-Dichlorobenzene *1,4-Dichlorobenzene *1,2-Dichlorobenzene *1 ,2-Dibromo-3-chloropropane
4-Bromofluorobenzene
RRF10.1710.3851.1421.1020.9660.062
0.595
RRF20.1250.3381.0051.0180.8500.072
0.711
RRF50.1230.3290.9170.9110.7820.067
0.512
RRF100.1270.3430.7930.8010.6740.064
0.428
RRF250.1070.2930.5640.5650.4760.047
0.360
RRF0.1310.3370.8840.8790.7500.062
—~
0.521
%RSD18.39.824.923.824.815.2
26.5
* Compounds with required minimum RRF and maximum 9&RSD values.All other compounds must meet a minimum RRF of 0.010.
Page2of2
, A R 3 I 6 6 I O ' FORMVIVC)A
6AVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: CHEMTECH Contract: US EPA REGION HI
Project No.: A455-S_____ Site: _______ Location: _____ Group:
Instrument ID: VOA1_____ Calibration Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) _ Calibration Tunes: 1022 1314
GC Column DB-624 _____ ED: 0.53 (mm)
Lab File ID: RRF1 , = L1011.D RRF2 = L1007.DRRF5 = L1008.D RRF10 - L1010.D RRF25 = L1009.D
COMPOUNDChloromethaneVinyl Chloride *Bromomethane *Chloroe thane1 , 1-Dichloroethene *VIeth'ylene ChlorideAcetoneCarbon Disulfidetrans- 1 ,2-Dichloroethene1 , 1-Dichloroethane *:is-l,2-DichloroetheneBromochloromethane *Chloroform *2-Butanone1,1,1-Trichloroethane *Carbon Tetrachloride *Benzene *1,2-Dichloroethane *rrichloroethene *1 ,2-Dichloropropane1,2-Dibromoethanc *Bromodichloromethane *cis-l,3-Dichloropropene *Toluene *trans-l,3-Dichloropropene *1,1,2-Trichloroethane *Fetrachloroediene *Dibromochloromethane *Chlorobenzene *Ediylbenzene *m&p-xylenes *o-xylene *Styrene *Bromoform *4-Methyl-2-pentanone
RRF10.2900.2800.1410.1890.5340.7070.1361.0550.5280.7070.6240.6020.9170.2050.8680.6741.4320.3380.5350.5930.5170.7860.6671.2720.4850.3440.7010.5771.2752.0821.4071.5021.0870.3020.264
RRF20.2920.2%0.162
L 0.1870.5100.7700.0751.0410.5050.6780.5620.4940.7570.1360.7790.6291.2230.2830.4600.5160.3620.6670.5381.5890.3810.2480.5280.4370.9231.5801.1821.2010.8490.2950.177
RRF50.2760.2860.1330.1290.5030.4690.0660.9940.4760.6270.5450.4600.6820.1300.7700.6361.1870.2850.4700.4880.3630.6810.5521.3760.3840.2450.5260.4380.9051.5421.1521.1570.8480.2800.170
RRF100.2380.2490.1030.0750.4530.3660.0530.8920.4610.5940.5080.4230.6200.1270.7400.6261.1670.2760.4490.4850.3590.6520.5531.2710.3830.2450.5090.4330.8751.4861.0671.0670.8210.2570.170
RRF250.2220.2340.0800.0610.3950.2670.0490.7840.3930.4950.4480.3730.5450.1120.6210.5320.9800.2420.3860.4200.3100.5590.4761.0500.3330.2070.4240.3770.7501.2610.9030.8990.7040.1860.145
RRF0.2640.2690.1240.128 i0.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.8620.2640.185
%RSD12.29.826.0"46.911.5"32.0,r46.4 ,12.010.913.312.218.420.225.511.88.513.412.111.512.520.512.112.414.914.219.918.816.420.719.016.119.016.217.724.8
41 Compounds with required minimum RRF and maximum XRSD values.All other compounds must meet a minimum RRF of 0.010. .
Page 1 of 2 , ^ .....FORM VI VOA nnn «-_• 3/90
6AVOLATILE ORGANICS INmAL CALIBRATION DATA
Lab Name: CHEMTECH________ Contract: US EPA REGION in
Project No.: A455-S_____ Site: _____ Location: _____ Group:
Instrument ID: VOA1 ___ Calibration Date(s): 1/30/95 1/30/95
Heated. Purge: (Y/N) _ CalibrationTim.es: 1628 2013
GC Column DB-624 ED: 0.53 (mm) --
Lab File ID: RRF1 =L1002.D RRF2 = L1004.DRRF5 == L1001.D RRF10 = L1005.D RRF25 = L1003.D
COMPOUNDDichlorodifluoromethane
. - •
• - - -----
RRF10.253
(
;
RRF20,458
RRF50.334
RRF100.294
.
RRF250.310
RRF"0.330
-
""•
•
%RSD23.4
\
* Compounds with required minimum RRF and maximum 56RSD values.All other compounds muiit meet a minimum RRF of 0.010.
Pagelof2 000 1FORM VI VOA l/ •
AR3I66I2
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH_________ Contract: US EPA REGION Ed
Project No. A447-S____ Site: ____ • Location: _____ Group:
Instrument ID: VOA1 Calibration Date: 3/20/95 Time: 1025
Lab File ED: L1205.D_____________ Init Calib. Date(s): 1/31/95 1/31/95s
Heated Purge: (Y/N) ___ Init. Calib. Times: 1022 1314
GC Column: DB624 ED: 0.53 (mm)
COMPOUND2-Hexanone1 , 1 ,2,2-Tetrachloroethane1 ,3-Dichlorobenzene1 ,4-Dichlorobenzene1 ,2-Dichlorobenzene1 ,2-Dibromo-3-chloropropane
4-Bromofluorobenzene
RRF0.1310.3370.8840.8790.7500.062
0.521
RRF50.1090.3400.9370.9370.8110.062
0.582
MINRRF
f
0.5000.6000.5000.400
%D16.8-0.9-6.0-6.6-8.10.0
-
-11.6
MAX%D
30.030.030.030.0
All other compounds must meet a minimum RRF of 0.010.
Pag'2of2 4R3I66I3 FORM vn VGA 000195 3rao
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH_______ Contract: US EPA REGION EQ
Project No. A447-S____ . Site: ___ Location: ' Group:
Instrument ID: VOA1 Calibration Date: 3/20/95 Tune: 1025
Lab File ED: L120S.D Init Calib. Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) ___ Init Calib. Times; 1022 1314
GC Column: DB624 ED; 0.53 (mm)'
•fe»
COMPOUNDDichlorodifluoromethaneChloromethani;Vinyl ChlorideBromomethanciChloroethane1,1-DichloroeiheneMethylene ChlorideAcetoneCarbon Disul£idetrans-1 ,2-Dichloroethene1 , 1-Dichloroethanecis-l,2-DichloroetheneBromochloromethaneChloroform2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBenzene1 ,2-DichloroeihaneTrichloroe there1 ,2-Dichloropropane1 ,2-DibromoeithaneBromodichloromethanecis-l,3-DichloropropeneToluenetnns-l,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroctheneDibromochloromethaneChlorobenzeneEthylbenzenem&p-xyleneso-xyleneStyreneBromoform4-Methyl-2-pentanone
RRF0.3300.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.142
, 0.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.590
- 1.1421.1650.8620.2640.185
RRF50.2530.2570.2640.1280.1660.5230.374(0.048 \1.0350.4990.6670.5520.4520.6770.1170.8140.7271.2030.2840.5570.4590.3620.6720.5431.4310.3980.2550.6490.5130.9851.5891.1571.161 ,0.8550.3260.149
MENRRF
0.1000.100
0.100
0.200
0.1000.200
0.1000.1000.5000.1000.300
0.1000.2000.2000.4000.1000.1000.200
' 0.1000.5000.1000.3000.3000.3000.100
%D23.32.71.9-3.2-29.7-9.227.5
C36.8)-8.6-5.5-7.6-2.83.83.817.6 --7.7-17.4-0.40.4-21.18.25.2-0.42.5-9.2-1.31.2
-20.9-13.5-4.20.1-1.30.40.8-23.519.5
MAX%D
30.030.0
30.0
30.0
30.030.0
30.030.030.030.030.0
30.030.0
130.030.030.030.030.030.030.030.030.030.030.030.0
.•C't~~S&-A
V&LKoZOtlollbwZld 7703/4 K32.0??03/£v^307703/c' V/-i*7077^31$ W/DQllfZiyv/JlLc*ShAtAJL «l«*
V
All other compounds must meet a minimum RRF of 0.010.
Page 1 of2FORM VH VOA wvi.^-* 3/9Q
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH_______ Contract: US EPA REGION III
Project No. A447-S____ Site: ____ Location: _____ Group:
Instrument ID: VOA1 Calibration Date: 3/19/95 Tune: 1229
Lab File ID: L1187.D__________ Init Calib. Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) ___ Init Calib. Tunes: 1022 1314
GC Column: DB624 ED: 0.53 (mm)
COMPOUND2-Hexanone1, 1,2,2-Tetrachloroethane1 ,3-Dichloro benzene1 ,4-Dichlorobenzene1,2-Dichlorobenzene1 ,2-Dibromo-3-chloropropane
4-Bromofluorobenzene
RRF0.1310.3370.8840.8790.7500.062
0.521
RRF50.1070.3330.9921.0150.8400.064
0.455
MINRRF
0.5000.6000.5000.400
'
%D18.31.2-12.2-15.5-12.0-3.2
"--•
12.7
MAXS6D
30.030.030.030.0
AU other compounds must meet a minimum RRF of 0.010.
Page2of2 . -»* 000193- « n J l o 6 l 5 FORM vn VOA 3/90
'• --" ---- r. . . , . . . . • 7A
VOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH Contract: US EPA REGION EQ
Project No. A447-S Site: ____ Location: _____ Group:
Instrument ED: VOA1____^_____ Calibration Date: 3/19/95 Time: 1229
Lab File EO: L1187.D__________ Init. Calib. Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) ____ Init. Calib. Times: 1022 1314
GC Column: DB624 ED: 0.53 (mm)
COMPOUNDDichlorodifiuoromethaneChloromethaneVinyl ChlorideBromomethaneChloroethanj1,1-DichloroetheneMethylene ChlorideAcetoneCarbon Bisulfidetrans-1 ,2-Dichloroethene1,1-Dichloroethanecis-1 ,2-DichloroetheneBromochloromethaneChloroform2-Butanone1, 1,1-TrichloroethaneCarbon TetrachlorideBenzene1 ,2-DichloroethaneTrichloroethene1 ,2-Dichloropropane1,2-Dibromoe thaneBromodichloromethanecis*l ,3-DichloropropeneToluenetrans-1 ,3-Dichloropropene1,1 ,2-TrichloroedianeTetrachloroetheneDibromochloromethaneChlorobenzeneEthylbenzenem&p-xyleneso-xyleneStyreneBromoform4-Methyl-2-]jentanone
RRF0.3300.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.8620.2640.185
RRF50.2260.2540.2580.1250.1660.5080.310.049")1.0670.4860.6030.5650.4370.7300.1160.8580.7521.2350.2910.5540.4760.3610.7150.5631.4430.3980.2600.6760.5111.0181.6981.2211.2440.9210.3320.148
MINRRF
0.1000.100
0.100
0.200
0.1000.200
0.1000.1000.5000.1000.300
0.1000.2000.2000.4000.1000.1000.2000.1000.5000.1000.3000.3000.3000.100
%D01.50
4.1-0.8-29.7-6.1
C39.9 )( 35.5 J-12.0-2.72.7-5.27.0-3.718.3 --13.5-21.5-3.1-2.1 .-20.44.85.5-6.9-1.1-10.1-1.3-0.8-25.9-13.1-7.7-6.8-6.9-6.7-6.8-25.820.0
MAXXD
30.030.0
30.0
t
30.0
30.030.0
30.030.030.030.0
L30.0
30.030.030.030.030.030.030.030.030.030.030.030.030.030.0
V&i-Kot°77o3/sw££3?*£>3)3 v/ey.C ft 3 3 '-A W/aO77O3I3 V/'tf077$ 3/3 v/ 13&$ T'.O'/J pyvvO 7Q3i 3pW S'
/o?yo3)yf>w£>6"7-?62H->t>\?/G&7*&3!iib/3g<3<z?_>3f5T"J3/7?n3tz»s 2Of f 0? 5 / -OJJ03 5 0%
All other compounds must meet a minimum RRF of 0.010.
Pa*,of* ,„„_ 000192A R 3 I 6 6 I 6 FORM w VOA 3/9°
6AVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: CHEMTECH________ Contract: US EPA REGION EQ
Project No.: A447-S_____ Site: ______ Location: _____ Group:Instrument ED: VOA1 Calibration Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) _ Calibration Tunes: 1022 1314GC Column DB-624 ED: 0.53 (mm)
Lab File ED: RRF1 =L1011.D RRF2 = L1007.DRRF5 « L1008.D RRF10 « L1010.D RRF25 = L1009.D .
COMPOUND2-Hexanone1,1,2,2-Tetrachlorocthane *1,3-Dichlorobenzene *1,4-Dichlorobenzene *1,2-Dichlorobenzene *1 ,2-Dibromo-3-chloropropane
*
*
4-Bromofluorobenzene
RRF10.1710.3851.1421.1020.9660.062
O.S95
RRF20.1250.3381.0051.0180.8500.072
•
0.711
RRF50.1230.3290.9170.9110.7820.067
0.512
RRF100.1270.3430.7930.8010.6740.064
0.428
RRF250.1070.2930.5640.5650.4760.047
0.360
RRF0.1310.3370.8840.8790.7500.062
~ -
0.521
%RSD18.39.824.923.824.815.2
26.5* Compounds with required minimum RRF and maximum %RSD values.All other compounds must meet a minimum RRF of 0.010.
Page2of2 nnm CO
6AVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: CHEMTECH Contract: US EPA REGION Ed
Project No.: A447-S_____ Site: _____ Location: _____ Group:
Instrument ID: VQA1 _____ Calibration Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) _ Calibration Times: 1022 1314
GC Column DB-624 ED: 0.53 (mm) ; --
Lab File ID: RRF1 =L1011.D RRF2 = L1007.DRRF5 = L1008.D RRF10 = L1010.D RRF25 - L1009.D
COMPOUNDChloromethanejVinyl Chloride *JBromomethane *jChloroethane|l,l-Dichlorctethene *JMethylene Chloride[AcetoneCarbon Disulfidetrans-l,2-Dichloroethene1,1-Dichloroethane *cis-l,2-DichtoroetheneBromochloromethane *Chloroform *2-Butanone1,1,1-Trichloroethane *Carbon Tetrachloride *[Benzene *|l,2-Dichloroethane *jrrichloroethcne *1 ,2-Dichl oropropane1,2-Dibromoethane *[Bromodichloromethane *bis-l,3-Dichloropropene *[Toluene *[trans-1, 3-Dichloropropene *1 , 1 ,2-Trichloroethane *retrachloroethene *Dibromochloromethane *Chlorobenzene *Ethylbenzene *n&p-xylenes *o-xylene *Styrene • *Bromofonn *4-Methyl-2-pentanone
RRF10.2900.2800.1410.1890.5340.7070.1361.0550.5280.7070.6240.6020.9170.2050.8680.6741.4320.3380.5350.5930.5170.7860.6671.2720.4850.3440.7010.5771.2752.0821.4071.5021.0870.3020.264
RRF20.2920.2960.1620.1870.5100.7700.0751.0410.5050.6780.5620.4940.7570.1360.7790.6291.2230.2830.4600.5160.3620.6670.5381.5890.3810.2480.5280.4370.9231.5801.1821.2010.8490.2950.177
RRF50.2760.2860.1330.1290.5030.4690.0660.9940.4760.6270.5450.4600.6820.1300.7700.6361.187 .0.2850.4700.4880.3630.6810.5521.3760.3840.2450.5260.4380.9051.5421.1521.1570.8480.2800.170
RRF100.2380.2490.1030.0750.4530.3660.0530.8920.4610.5940.5080.4230.6200.1270.7400.6261.1670.2760.4490.4850.3590.6520.5531.2710.3830.2450.5090.4330;8751.4861.0671.0670.8210.2570.170
RRF250.2220.2340.0800.0610.3950.2670.0490.7840.3930.4950.4480.3730.5450.1120.6210.5320.9800,2420.3860.4200.3100.5590.4761.0500.3330.2070.4240.3770.7501.2610.9030.8990.7040.1860.145
RRF0.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.8620.2640.185
%RSD12.29.826.06.911.5T21T;'46.412.010.913.312.218.420.225.511.88.513.412.111.512.520.512.112.4Li4,-914,219.918.816.420.719.016,119.016.217.724.8
* Compounds; with required minimum RRF and maximum %RSD values.All other compounds must meet a minimum RRF of 0.010.
Page 1 o f 2 , . . ' . .. FORM VI VOA 3/90
Aft3l66l8 ' 000162
6AVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: CHEMTECH _____ Contract: US EPA REGION III
Project No.: A447-S_____ Site: _____ Location: _____ Group:
Instrument ED: VOA1________ Calibration Date(s): 1/30/95 1/30/95Heated Purge: (Y/N) _ Calibration Times: 1628 2013
GC Column DB-624 ED: 0.53 (mm)
Lab File ID: RRF1 =L1002.D RRF2 « L1004.DRRF5 - L1001.D RRF10 = L1005.D RRF25 - L1003.D
COMPOUNDDichlorodifluoromediane
RRF10.253
RRF20.458
•
•
RRF50.334
RRF100.294
RRF250.310
RRF0.330
"•*•-
%RSD23.4
* Compounds with required minimum RRF and maiimum 56RSD values.All other compounds must meet a minimum RRF of 0.010.
Page 1 of2FORM VI VOA 3/90
AR3I66I9 000161
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH Contract: US EPA REGION HI
Project No. A435-S Site; Location:_____ Group:
Instrument ED: VOA1 __ Calibration Date: 3/16/95 Tune: 0822
Lab File ID: L1178.D Init Calib. Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) ___ Init Calib. Tunes; 1025 1314
GC Column: DB624 ED: 0.53 (mm)
COMPOUND2-Hexanone1 , 1 ,2,2-Tetrachloroethanel,3-Dichlorol>enzene1 ,4-Dichlorobenzene1 ,2-Dichlorobenzene1 ,2-DibromO"3-chloropropane
.
.1
4-Bromofluorobenzene
RRF0.1310.3370.8840.8790.7500.062
0.521
RRF500.1210.3510.9060.9130.7890.079
0.548
MINRRF
0.5000.6000.5000.400
%D7.6-4.2-2.5-3.9-5.2-27.4
-5.1
MAX%D
30.030.030.030.0
All other compounds must meet a minimum RRF of 0.010.
Page2of2 Afni£C9n 000200Hn.iiKi.vn. FORMvnvOA uv 3/90
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH_________ Contract: US EPA REGION Etl
Project No. A43S-S____ Site: _____ Location: _____ Group:
Instrument ED: VOA1 Calibration Date: 3/16/95 Time: 0822
Lab File ED: L1178.D_____________ Init Calib. Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) ___ Init Calib. Times; 1025 1314
GC Column: DB624 ED: 0.53 (mm)
COMPOUNDDichlorodifluoromethaneChloromethaneVinyl ChlorideBromomethaneChloroethane1 , 1-DichloroetheneMethylene ChlorideAcetoneCarbon Disulfidetrails- 1 ,2-Dichloroethene1 , 1-Dichloroe thanecis-1 ,2-DichloroetheneBromochloromethaneChloroform2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBenzene1 ,2-DichloroethaneTrichloroethene1 ,2-Dichloropropane1 ,2-DibromoethaneBromodichloromethanecis-l,3-DichloropropeneToluenetrans-1 ,3-Dichloropropene1 , 1,2-TrichloroethaneTetrachloroethcneDibromochloromethane
. ChlorobenzeneEthylbenzenem&p-xyleneso-xylcneStyreneBromoform4-Metbyl-2-pentanone
RRF0.3300.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.8620.264
• 0.185
RRF500.2620.2470.2630.1250.1490.5060.5180.0511.0030.4870.5800.5510.4310.7110.1220.8710.7631.2300.2950.5430.4820.3560.7150.5861.4700.4270.2620.6070.5220.9721.6841.2361.2620.9050.3300.164
MENRRF
0.1000.100
0.100
0.200
0.1000.200
0.1000.1000.5000.1000.300
0.1000.2000.2000.4000.1000.1000.2000.1000.5000.1000.3000.3000.3000.100
%D20.46.42.2-0.8-16.4-5.6-0.4
O2.9J-5.2-3.06.5-2.68.3-1.014.1--15.2-23.3-2.7-3.5-18.03.66.8-6.9-5.2-12.1-8.7-1.6-13.0-15.5-2.9-5.9-8.2 .-8.3-5.0-25.011.4
MAX%D
30:030.0
30.0
30.0
30.030.0
30.030.030.030.030.0
30.030.030.030.030.030.030.030.030.030.030.030.030.030.0
AjjeCiaW'Scales
VSTD050VBLK04)770313W06)770313W07STORAGE BLALCS
-
4
1All other compounds must meet a minimum RRF of 0.010.
P*elof2 1R3I662; FOKMVDVOA 000199 3/90
7AVOLATILE CONTINUING CALIBRATION.CHECK
Lab Name: CHEMTECH_______ Contract: US EPA REGION III
Project No. A43S-S____ Site: _____ Location: _____ Group:
Instrument ED: VOA1 Calibration Date: 3/12/95 Time: 0932
Lab File ED: L1160.D __________ Init Calib. Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) ___ Init Calib. Times: • 1025 1314
GC Column: DB624 ED; 0.53 (mm)
COMPOUND2-Hexanone1,1,2,2-Teaachloroethane1 ,3-Dichlorobenzenc1 ,4-Dichlorobenzcnc1 ,2-Dichlorobenzcnel,2-Dibromo-3-chloropropane
•
4-Bromofluorobenzene
RRF0.1310.3370.8840.8790.7500.062
,
I
0.521
RRF500.0910.2970.9670.9540.8230.055
0.469
MENRRF
0.5000.6000.5000.400
%DC30.5)11.9-9.4-8.5-9.711.3
-•-..
10.0
MAX96D
30.030.030.030.0
*
All other compounds must meet a minimum RRF of 0.010. •
' 000198$ R3 i 66 22 FORM VH VOA 3/90
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH_____• Contract: US EPA REGION Efl
Project No. A435-S____ Site: _____ Location: _____ Group:
Instrument ID: VOA1 Calibration Date: 3/12/95 Time: 0932
Lab File ED: L1160.D__________ Init Calib. Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) ___ Init Calib. Times: 1025 1314
GC Column: DB624 ED: 0.53 (mm)
COMPOUNDDichlorodifiuoromedianeChloromethaneVinyl ChlorideBromomethaneChloroethane1,1-DichIoroetheneMethylene ChlorideAcetoneCarbon Disulfidetrans-1 ,2-Dichloroethene1 , 1-Dichloroethanecis-1 ,2-DichloroetheneBromochloromethaneChloroform2-Butanone1, 1, 1-TrichloroethaneCarbon TetrachlorideBenzene1,2-DichloroethaneTrichloroethene1 ,2-Dichloropropane1 ,2-DibromoethaneBromodichloromethanecis-1 ,3-DichloropropeneToluenetrans-1, 3-Dichloropropcne1 , 1 ,2-TrichloroethaneTetrachloroethene
. Dibromochloromethane
. ChlorobenzeneEthylbenzenem&p-xyleneso-xyleneStyreneBromoform4-Methyl-2-pentanone
RRF1 0.3300.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.8620.2640.185
RRF500.2400.2580.2730.1430.1700.5180.326C0.042)1.0330.5060.6510.5540.4210.6850.1000.8590.7451.1950.2710.5360.4590.3360.6570.5541.3570.3810.2390.6560.4790.9741.6421.2291.1890.8880.3030.130
MINRRF
0.1000.100
0.100
0.200
0.1000.200
0.1000.1000.5000.1000.300
0.1000.2000.2000.4000.1000.1000.2000.1000.5000.1000.3000.3000.3000.100
%D27.32.3-1.5
-15.3C-32.83
-8.1G6.O(44.7)-8.4-7.0-5.0-3.210.42.729.6--13.6-20.40.34.9
-16.58.212.01.80.5-3.53.17.4-22.2-6.0-3.1-3.3-7.6-2.1-3.0-14.829.7
MAX%D
30.030.0
30.0
30.0
30.030.0,30.030.030.0.30.030.0
30.030.030.030.030.030.030.030.030.030.030.030.030.030.0
Assoti*rt*'Sa le;
VSTD050VBLK03)770307W293770307W22)770307W340770308TB1)77030829B377030829C0770308W05 '3770308WGr||3770309TB. V
4All other compounds must meet t minimum, RRF of 0.010. n • • • •
Pa*Iof2 AR3I6623 FORMIVOA 000197 3/90
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH Contract: US EPA REGION Efl
Project No, A43S-S Site: _____ Location: _______ Group:
Instrument ID: VOA1 Calibration Date: 3/11/95 Tune: 0929
Lab File ED: L1150.D___________ Init. Calib. Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) Init Calib. Times: 1025 1314
GC Column: DB624 ED: 0.53 (mm)
COMPOUND2-Hexanone1, 1,2,2-Tetrachloroethane1 ,3-Dichlorobenzene1,4-Dichlorobenzene1 ,2-Dichlorobenzene1 ,2-Dibromo-3-chloropropaiie
'
.
4-Bromofluorobenzene
RRF0.1310.3370.8840.8790.7500.062
I
0.521
RRF50.1180.3711.0251.0020.8950.069
0.488
MENRRF
0.5000.6000.5000.400
%D9.9
-10.1-16.0-14.0-19.3-11.3
~--.
6.3
MAX%D
30.030.030.030.0
All other compounds must meet a rninimum RRF of 0.010.
Page2of2 A fi^i fi £ 9 i, 000136v:rHHO I D0_:l4 BAim vn VOA lion
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH________ Contract: US EPA REGION Efl
Project No. A435-S____ Site: ____ Location: _____ Group:
Instrument ID: VOA1 Calibration Date: 3/11/95 Time: 0929
Lab File ID: L11SO.D__________ Init. Calib. Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) ___ Init Calib. Times: 1025 1314
GC Column: DB624 CO: 0.53 (mm)
COMPOUNDDichlorodifluoromethaneChloromethaneVinyl ChlorideBromomethaneChloroethane1,1-DichloroetheneMethylene ChlorideAcetoneCarbon Disulfidetrans-l,2-Dichloroethene1 , 1-Dichloroethanecis-l,2-DichloroetheneBromochloromethaneChloroform2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBenzene1 ,2-DichloroedianeTrichloroethene1 ,2-Dichloropropane1,2-DibromoethaneBromodichloromethanecis-l,3-DichloropropeneToluenetrans-1 ,3-Dichloropropene1,1,2-TrichloroethaneTetnchloroetheneDibromochloromethane
. ChlorobenzeneEthylbenzenem&p-xyleneso-xyleneStyreneBromoform4-Methyl-2-pentanone
RRF0.3300.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.862
> 0.2640.185
RRF50.3480.2910.3080.1610.1810.5830.3640.0551.1550.5480.7420.6250.4780.7760.1280.9350.8131.2730.3270.5650.4930.3950.7570.6071.4280.4240.2790.6920.5571.0521.7461.3201.2740.9790.3630.164
MINRRF
0.1000.100
0.100
0.200
0.1000.200
0.1000.1000.5000.1000.300
0.1000.2000.2000.4000.1000.1000.2000.1000.5000.1000.3000.3000.3000.100
%D-5.5-10.2-14.5-29.8G41.4}-21.729.527.6-21.2-15.9-19.7-16.4-1.7-10.29.9--23.731.33-6.3-14.7-22.81.4-3.4-13.2-9.0-8.9-7.9-8.1-28.9-23.2-11.3-9.8-15.6-9.4-13.607.5}11.4
.MAX%D
30.030.0
30.0
30.0
30.030.0
30.030.030.030.030.0
30.030.030.030.030.030.030.030.030.030.030.030.030.030.0
Associate*S«*flt*
VSTD050VBLK02)770307W023770307W28
-
•
iAll other compounds must meet a minim im, RRF of 0.010.
AR3I6625 K*MvnvoA 000195
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH _____ Contract: US EPA REGION ffl
Project No. A435-S____ Site: _____ Location: _____ Group:
Instrument ID: VOA1 Calibration Date: 3/9/95 Time: 1033
Lab File ED: L1137.D__________ Init Calib. Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) ___ InitCalib.Tim.es: 1025 1314
GC Column: DB624___ ED: 0.53 (mm)
O
COMPOUND2-Hexanone1, 1,2,2-Tetraichloroethane1 ,3-Dichlorobenzene1 ,4-Dichlorobenzene1 ,2-Dichlorobenzene1 ,2-Dibromo-3-chloropropane
.
4-Bromofluorobenzene
RRF0.1310.3370.8840.8790.7500.062
0.521
RRF50.0700.2410.7950.7910.6750.050
0.568
MENRRF
0.5000.6000.5000.400
*
%DO6.6}28.510.110.010.019.4
•-
-9.0
MAX56D
30.030.030.030.0
-
All other compounds must meet a minimum RRF of 0.010. ••••-• ,.;:.... j.
AR3I6626 FORM w VOA 000194 3/90
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH___________ Contract: US EPA REGION EQ
Project No. A435-S____ Site: _____ Location: ________ Group:
Instrument ED: VOA1 Calibration Date: 3/9/95 Time: 1033
LabFileID:L1137.D Init Calib. Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) ___ Init Calib. Tunes: 1025 1314
GC Column: DB624 ED: 0.53 (mm)
COMPOUNDDichlorodifluoromethaneChloromethaneVinyl ChlorideBromometbaneChloroethane1,1-DichloroetheneMethylene ChlorideAcetoneCarbon Disulfidetrans-1, 2-Dichloroediene1 , 1-Dichloroethanecis-1 ,2-DichloroctheneBromochloromethaneChloroform2-Butanone.1 , 1 , 1-TrichloroethaneCarbon TetrachlorideBenzene1 ,2-DichloroethaneTrichloroethene1 ,2-Dichloropropane1,2-DibromoethaheBromodichloromethanecis-1 ,3-DichloropropeneToluenetrans-1 ,3-Dichloropropene1, 1,2-TrichloroethaneTetrachloroetheneDibromochloromethane
. ChlorobenzeneEthylbenzenem&p-xyleneso-xyleneStyreneBrouioform4-Methyl-2-pentanone
RRF0.3300.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.382
. 0.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.8620.2640.185
RRF50.2380.2190.2230.1210.1340.4210.660r 6.035 J0.8550.4080.5510.4540.3400.5880.0790.6860.6070.9640.2290.4380.3650.2700.5280.4241.1300.3040.1930.5310.3880.7691.2750.9700.9240.6930.2670.100
MINRRF
0.1000.100
0.100
0.200
0.1000.200
0.1000.1000.5000.1000.300
0.1000.2000.2000.4000.1000.1000.2000.1000.5000.1000.3000.3000.3000.100
%D27.917.017.12.44.112.1-27.9O3.9J10.313.711.115.527.716.544.439.31.919.519.64.827.029.321.123.913.822.625.21.114.218.619.815.120.719.6-1.1
G5.91
MAX%D
30.030.0
30.0
30.0
30.030.0
30.030.030.030.030.0
30.030.030.030.030.030.030.030.030.030.030.030.030.030.0
Associw**5a»v»lt?
VSTDOSOVBLK01)770306W17)770306W193770306W203770306PW1)770306PW2)770306PW4)770307TB1
4
IAll other compounds must meet t minimum RRF of 0.010.
SR3I6627 mRMvnvo» 000193
6AVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: CHEMTECH _______ Contract: US EPA REGION HIProject No.: A43S-S Site:, _____ Location: _____ Group:
Instrument ED: VOA1 CalibrationDate(s): 1/31/95 1/31/95Heated Purge: (Y/N) _ Calibration Times: 1022 1314
GC Column DB-624 ED: 0.53 (mm)Lab File ED: RRF1 =L1011.D RRF2 - L1007.DRRF5 - L1008.D RRFIO - L1010.D RRF25 - L1009.D
COMPOUND2-Hexanone1,1,2,2-Tetrachloroethane *1,3-Dichlorobenzene *1,4-Dichlorobenzene *1,2-DichloroIjenzene *1 ,2-Dibromo-3-chloropropane
,
"
4-Bromofluorobenzeoe
RRF10.1710.3851.1421.1020.9660.062
0.595
RRF20.1250.3381.0051.0180.8500.072
l
1
0.711
RRF50.1230.3290.9170.9110.7820.067
0.512
RRFIO0.1270.3430.7930.8010.6740.064
.
0.428
RRF250.1070.2930.5640.5650.4760.047
0.360
RRF0.1310.3370.8840.8790.7500.062
0.521
%RSD18,39,,824,923.824,815.2
26.5
* Compounds with required minimum RRF and maximum XRSD values.All other compounds must meet a minimum RRF of 0.010.
Page2of2 ' JFORM VI VOA 000164 3/9°R31552g
6AVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: CHEMTECH _____ Contract: US EPA REGION EQ
Project No.: A435-S_______ Site: _____ Location: _____ Group:
Instrument ED: VOA1_____ Calibration Date(s): 1/31/95 1/31/95
Heated Purge: (Y/N) _ Calibration Tunes: 1022 1314
GC Column DB-624 ED: 0.53 (mm)
Lab File ED: RRF1 =L1011.D RRF2 - L1007.DRRF5 - L1008.D RRFIO - L1010.D RRF25 = L1009.D
COMPOUNDChloromethaneVinyl Chloride *Bromomethane *Chloroethane1,1-Dichloroethene *Methylene Chloride[AcetoneCarbon Disulfidetrans-1 ,2-Dichloroethene1,1-Dichloroethane *:is-l,2-DichloroetheneBromochloromethane *Chloroform ' *2-Butanone1,1,1-Trichloroediane *Carbon Tetrachloride *Benzene *1,2-Dichloroethane *rrichloroethene *1 ,2-Dichloropropane1,2-Dibromoethane *[Bromodichloromethane *cis-1, 3-Dichloropropene *Toluene *trans-l,3-DichIoropropene *1 , 1 ,2-Trichloroethane *retrachloroethene *Dibromochloromedume *Chlorobenzene *Emylbenzene *n&p-xylenes • *o-xylene *Btyrene *Bromofonn *|4-Methyl-2-pentanone
RRF10.2900.2800.1410.1890.5340.7070.1361.0550.5280.7070.6240.6020.9170.2050.8680.6741.4320.3380.5350.5930.5170.7860.6671.2720.4850.3440.7010.5771.2752.0821.4071.5021.0870.3020.264
RRF20,2920.2960.1620.1870.5100.7700.0751.0410.5050.6780.5620.4940.7570.1360.7790.6291.2230.2830.4600.5160.3620.6670.5381.5890.3810.2480.5280.4370.923• 1.5801.1821.2010.8490.2950.177
RRF50.2760.2860.1330.1290.5030.4690.0660.9940.4760.6270.5450.4600.6820.1300.7700.6361.1870.2850.4700.4880.3630.6810.5521.3760.3840.2450.5260.4380.9051.5421.1521.1570.8480.2800.170
RRFIO0.2380.2490.1030.0750.4530.3660.0530.8920.4610.5940.5080.4230.6200.1270.7400.6261.1670.2760.4490.4850.3590.6520.5531.2710.3830.2450.5090.4330.8751.4861.0671.0670.8210.2570.170
RRF250.2220.2340.0800.0610.3950.2670.0490.7840.3930.4950.4480.3730.5450.1120.6210.5320.9800.2420.3860.4200.3100.5590.4761.0500.3330.2070.4240.3770.7501.2610.9030.8990.7040.1860.145
RRF0.2640.2690.1240.1280.4790.5160.0760.9530.4730.6200.5370.4700.7040.1420.7560.6191.1980.2850.4600.5000.3820.6690.5571.3110.3930.2580.5370.4520.9451.5901.1421.1650.8620.2640.185
%RSD12.29.826.0:46.£>11.5?-P6.4:12.010.913.312.218.420.225.511.88.513.412.111.512.520.512.112.414.914.219.918.816.420.719.016.119.016.217.724.8
* Compounds with required minimum RRF and marimnm XRSD values.All other compounds must meet a minimum RRF of 0.010.
Page 1 of 2 . ' . " ; . 'FORM VI VOA 3/90
AR3I6629 : °°0]G3
6AVOLATILE ORGANICS. INITIAL CALIBRATION DATA
Lab Name: CHEMTECH Contract: US EPA REGION Ed
Project No.: A435-S_____ Site: . Location: _____ Group:
Instrument LD: VOA1 Calibration Date(s): 1/30/95 1/30/95
Heated Purge: (Y/N) _ Calibration Tunes: 1628 2013
GC Column DB-624_______ ED: 0.53 (mm)
Lab File ED: . . , . RRF1 =L1002.D , RRF2 = L1004.DRRF5 = LlOOl.D RRFIO = L1005.D RRF25 = L1003.D
COMPOUNDDichlorodifluoromethane
•
•
•* ' "*
--
RRF10.253
RRF2a.458
RRF50.334
RRFIO0.294
RRF250.310
RRF0.330
%RSD?3.4
* Compounds with required minimum RRF and maTimum 56RSD values.All other compounds must meet a minimum RRF of 0.010.
Page 1 of 2 7 ""•FORM VI VOA 3/9°
flR3l6630
Page 8 of 8
DEFINITION OF CODES USED IN TABLE I(Loir Concentration)
I = %RSD exceeded 30% in the volatile initial calibration.Positive results are qualified HJ". When the %RSD exceeded50*, guantitation limits are qualified "UJ11.
C — %D exceeded 30% in the volatile continuing calibrationPositive results are qualified "J". When the %D exceeded50%, quantitation limits are qualified "UJ".
F = RF less than 0.05 in the calibration. All quantitationlimits are qualified "R" and positive results are qualified"L".
+ = The "B" qualifier, denoting blank contamination, supersedesthe qualifier issued in this table.
R = The "R" qualifier, denoting unusable results, supersedes thequalifier issued in this table.
AR31663