53 PELA ————

- - - - 53PELA ————

TECHNICAL MEMORANDUM NO. 3

FOR REMEDIAL INVESTIGATION/FEASIBILITY STUDY

CITY DISPOSAL CORPORATION LANDFILL

(DUNN LANDFILL)

9 (PELA Reference No. 495201)

Appendix B.

Results of Analyses of Soil Samples and

Ground-Water Samples - Summary Package B

CA1379-CA1381, CA1383

CA1393-CA1387

CA2136-CA2143, CA2149-CA2151

February, 1990

P. E. LaMoreaux & Associates, Inc. _

Summary Package

for

CITY DISPOSAL CORPORATION LANDFILL

Ctotin or CwtfOtfy D»t» *#qu//ttf fw ETC O*ta Management Summary foporttWASTE MANAGEMENT, INC 405O1379-CA13BI ,CAI383,

CA1393-CA1397CA2136-CA2U3.CA2U9-CA21S)ETC Jimp/t Na Company Samp/* Point Oaf* TVm* Hour*

Swep T. Davis

Thi« Tvcfviical is trt 1NSITE* by LOOeSTPfi" D«ti

ETC

CASE NARRATIVE

This technical report submitted by ETC Corporation contains theanalytical results and required deliverables for Waste Management,Inc. site 405 samples as identified below:

w

ETC IDCA1379CA1380CA1381CA1383CA1893CA1895CA1896CA1897CA2136

CLIENT ID1GWB14RR1GWB16RRDUP03TB1GWP3A1GWP4A1GWP4C1GWP4B1GWP6RR

ETC IDCA2137CA2138CA2139CA2140CA2141CA2142CA2143CA2150CA2151

CLIENT ID1GWP2B1GWP1B1GWP1B1GWP1C1GWP3C1GWP6A1GWP7ADUP03FB

^

During the preparation and analysis of these samples, the followingwas observed:

VQLATTTiRSifQV70076l t Samples CA1380 and CA1381 required dilution whichresulted in elevated method detection limits (MDLs).

ACID /BASE /NEUTRAL:fOC7QQ87^ : The surrogate recoveries for sample CA2139 were outsideof QC limits which may be attributed to the sample matrix. Theresults have been confirmed by a replicate analysis and this datahas been included in the report.

Sample CA2150 was extracted outside of extraction hold time.

fOG70030l!Primary Analysis: Instrument JA: 6'x4 mm ID l.S%SP2250/i.95%SP240iConfirmation Analysis: Instrument KB: 6'x2 mm ID 3% SP2100

The confirmation analysis was performed outside of analysis holdtime . However , quantitation was performed from the primaryanalysis only.

File I 000017

ETC

fOG7QQ44l:Primary Analysis: Instrument HA: 6'x4 mm ID l.5%SP2250/i.95%SP240lConfirmation Analysis: Not requiredDOT in Evaluation Standard Mixes A, B, and C did not meet percentrelative standard deviation criteria. A calibration curve for4,4'-DDD, 4,4'-DDE, and 4,4'-DDT was plotted.

The analytical sequence was completed outside of the 72 hourcriteria. This did not appear to affect the retention timedeterminations because the surrogate retention time did not shiftoutside of QC limits for Individual Standard Mixes A and B at theend of the sequence.

Individual Standard Mixes A and B did not meet percent differencecriteria at the end of the sequence. However, samples of interesthad been run prior to these standards.

Low Matrix Spike and Matrix Spike Duplicate recoveries may beattributed to matrix interference.

Primary Analysis: Instrument HA: 6'x4 mm ID 1.5%SP2250/l.95%SP240lConfirmation Analysis: Not required

Gamma-BHC did not meet percent difference criteria in theIndividual Standard Mix A at the end of the sequence. However, allsamples of interest had been analyzed prior to that standard.

The Matrix Spike and Matrix Spike Duplicate recoveries were outsideof QC limits. However, these are advisory limits only.

fOG70Q481:Primary Analysis: Instrument JA: 6'x4 mm ID 1.5%SP2250/1.95%SP2401Confirmation Analysis: Instrument KB: 6'x2 ramID 3% SP2100

The surrogate recoveries for all samples in the primary analysisexceeded QC criteria. However, the surrogate criteria is advisoryonly.The confirmation analysis was performed outside of analysis holdtime. However, quantitation was performed from the primaryanalysis only.

File I 000017

ETC

fOG7QQ501 :Primary Analysis: Instrument HA: 6'x4 mm ID 1.5%SP2250/1.95%SP2401Confirmation Analysis: Instrument KB: 6'x2 mmID 3% SP2100

The surrogate recoveries for sample CA2142 exceeded QC criteria.However, the surrogate criteria is advisory only.

The confirmation analysis was performed outside of analysis holdtime. However, quantitation was performed from the primaryanalysis only.

Primary Analysis: Instrument HA: 6'x4 mm ID 1.5%SP2250/1.95%SP2401Confirmation Analysis: Instrument KB: 6'x2 mm ID 3% SP2100

Sample CA2150 was extracted outside of extraction hold time.

Surrogate recoveries for sample CA2150 exceeded QC criteria.However, the surrogate criteria is advisory only.

The confirmation analysis was performed outside of analysis holdtime . However , quantitation was performed from the primaryanalysis.

Release of the data contained in this hardcopy data package hasbeen authorized by the following signature.

ebelPresident of Operations

Date/

File I 000017

' 1AVOLATILE ORGANiCS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: ETC Corp.

Lab Code: Case No.:

Matrix: (soil/water) UATER

Sample wt/vol: 5.0 (g/mL) ML

Level: (low/mad) LOW

% Moisture: not dec.

Column: (pack/cap) PACK

Cant rac t:

SAS No.: SDG No.:

Lab Sample ID: CA1379U

Lab File ID: >C7269

Date Received: 09/29/89

Date Analyzed: 10/05/89

Dilut ion Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UG/L

74-87-3---------Chloromethane___________74-83-9---------Bromomethane____________75-01-4————————Uinyl Chloride__________75-00-3 —————— — Ch loroe thane____________75-09-2———— ——— Methylene Chloride______67-64-1---------Acetone__________75-15-0— ——— - — Carbon Disulf ide____.75-35-4-————--1,1-Dichloroethene______75 — 34 3 — — — •* ———»— 1-j 1—Di oh. I'D r Ool hah"e'540-59-0——• ———— 1,2'-B-tchlorettr*h"e"' (total),67-66-3 ———————— Ch torofornr " ' ' ~~107-06-2———————1 .2--B-rchtoroethane78-93-3 ———— -- — 2-Butanone______________71-55-6————-—-1,1,1-Trichloroethane___56-23-5---------Carbon Tetrachlor ide____108-05-4---————Uinyl Acetate___________75-27-4---------Bromodichloromethane78-87-5—————-1,2-0ichloropropane_____10061-01-5—————cis-l,3-Dichloropropene__79-01-6---------Trichloroethene_________124-48-l--------Dibromochloromethane____79-00-5————————1,1,2-Trich loroe thane____71-43-2—-—•———Benzene_________________10061-02-4*-———trana-l,3-Dichloropropene.75-25-2——;————Bromoform_______________108-10-1—-^———4-Methyl-2-Pentanone____591-78-6—•—————2-H«xanone______________127-18-4———————Tet rach loroe thene_______79-34-5————————1,1,2,2-Tet rach loroe thane.108-88-3———————Toluene_________________108-90-7———————Chlorobenzene______,_____100-41-4—————--Ethyl benzene____________100-42-5-———-Styrene_________________1330-20-7——————Xylene (total)_________

I.110.110.110.11012.1615.1515.15.15.15.110.1515.11015.15.15.15.15.1515.1515,110.110.151515,15.15.1515

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VOLATILE ORGANICS ANALYSIS DATA SHEET'

Lab Name: ETC Corp.

ERA SAMPLE NO.

Lab Code: Case No.:

Matrix: <soi1/water) UATER

Sample wt/vol: 5.0 <g/mL> ML

Level: (low/med) LOW

H Moisture: not dec.


Cont ract:

SAS No,: SDG No.:


Lab File ID: >C7270



Dilution Factor: 1


74-87-3-- — ———— Chlorome thane______________I 1074-83-9-------- -Bromome thane_______________I 1075-01-4————————vinyl Chloride_____________11075-00-3 ———————— Chlo roe thane_______________11075-09-2— — ———— Methyl one Chloride_________1267-64-1 ———————— Acetone___________________122075-15-0 ——————— Carbon Disu If ide___;______1575-35-4———— ——— 1,1-Di chioroe thane_________1575-34-3 ——————— 1,1-0 i chlo roe thane540-59-0 —————— V,2-Dichlorethene (total)__1567-66-3————————Chloroform_________________15107-06-2- — -- —— 1,2-Dichloroe thane_________1578-93-3 ——————— -2-Butanone_________________122071-55-6 — ——— —— 1,1,1-Trichloroe thane______1556-23-5- — ————— Carbon Tet rach lor ide_______15108-05-4———————vinyl Acetate______________11075-27-4------ — -Bromod ichloromethane_______1578-87-5———————1,2-0 ichloropropane________1510061-01-5————cis«l,3-Dichloropropene____1579-01-6 ——————— Trichloroethene___________15124-48-1—————•—Dibromochlorome thane_______1579-00-5 ———————— 1,1,2-Trichloroe thane______1571-43-2——'—-——Benxene___________________1210061-02-6*—----trana-1,3-Dichloropropane__1575-25-2————"———Bromoform________________15108-10-1-^--————4-M«thyl-2-Pentanone_______123591-78-6——————2-H«xanone_______________110127-18-4———————Tetrachloroethene__________1579-34-5————————1,1,2,2-Tet rach loroe thane__15108-88-3 ——————— Toluene___________________I 160108-90-7———————Chlorpbeniene______________15100-41-4——————Ethylbenzene_____________113100-42-5 ——————— Styrene___________________151330-20-7——————Xylene (total)____________I_________________________________________I

<37>

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VOLATILE 0»CA*1CS A/UUSI* OAIAT«T>TIVILY XDwrxrxtt COMPOUNDS

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COMCOttUTXOIIor uf/Xf)Numbar TIC» founds

1/17

1AVOLATILE ORGAN ICS ANALYSIS DATA SHEET

Lab Name: ETC Corp.

SAMPLE NO.

Lab Code: Case No.:

Ma t r i x: (soil/we tar) WATER

Sample wt/vol: .0* Cg/mL) ML


\ Moisture: not dec.


Cont ract!

SAS No.: SDG Np.:


Lab F i l e ID: >C72792-1

Date Received: 09/J4/89


D i l u t i o n Factor: *«1


74-87-3 ——————— Chlorome thane____________11000 IU74-83-9————————Bromomethane_______________I 1000 IU75-01-4————————Uinyl Chloride_____________11000 IU75-00-3———————Chloroe thane_________ 11000 ig75-09-2———————Methylene Chloride________1520 I67-64-1————————Acetone___________________11000 IU75-15-0———————Cerbon Disulf ide__________1500 IU75-35-4————————1,1-Dichloroethene_________1500 IU75-34-3———————1,1-Dichloroe thane________1500 IU540-59-0——————1,2-Oichlorethene (total)__1500 IU67-66-3————————Chloroform_________________1500 IU107-06-2 —————— 1,2-Di chloroe thane________1500 IU78-93-3 ———————— 2-Butanone_________________11000 IU71-55-6———————1,1,1-Trichloroe thane______1500 IU56-23-5———————Carbon Tet rach lor ide______1500 IU108-05-4———————Uinyl Acetate______________11000 IU75-27-4———————Bromodichlorome thane______1500 IU78-87-5 ——————— 1,2-Dichloropropane_______1500 IU10061-01-5—————ci»-l,3-Dichloropropene____1500 IU79-01-6———-———Tricnloroethene___________1500 IU124-48-1—--———Dibromochlorome thane______1500 IU79-00-5———————1,1,2-Trichloroe thane______1500 IU71-43-2————+•'•——Benzene_________________1500 IU10061-02-6——-—-tr«n»-l,3-0ichloropropene__1500 IU75-25-2————————Bromoform_________________1500 IU108-10-1——————4-Methyl-2-Pentanone______11000 IU591-78-6———————2-Hexanone_________________I 1000 IU127-18-4———————Tet rach loroethene__________1500 IU79-34-5———————1,1,2,2-Tetrachloroethane__1500 tU108-88-3——————Toluene_________________1240 IJ108-90-7——————Chlorobenzene____________1500 IU100-41-4——————Ethylbenaeene_____________1500 IU100-42-5——————Styrene_________________1500 IU1330-20-7——————Xylene (total)____________1500 IU_________________________________________I_____________I_____

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IEVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

Lab Name:ETC Corp

Lab Code:

Labui

Case No.:

Ma t r i x: t so i1/we t e r)WATER

Contract:

SAS No.:

Sample wt/vol:

Leve 1 : C low/mod > LOW


Column: (pack/cap)

^Cg/mDML

SDG No.:


Lab File ID: >C7279

Date Received: Q9/J-9V99


Dilut ion Factor: •& I

Number TICa found:CONCENTRATION UNITS:(ug/L or ug/Kg)UG/L

CAS NUMBER

——

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COMPOUND NAME

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Lab Name: ETC Corp.

SAMPLE NO.

Lab Code: Case No.:

Matrix: (soil/water) WATER

Sample wt/vol: 5.0 Cg/mL) ML

Leve1: C1ow/med) LOUI

S Moisture: not dec.


Contract:

SAS No.: SDG No.:


Lab File ID: >C7280

Date Received: 09 tT/8


Dilution Factor: l

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

74-87-3————————Chlo rome thane___________74-83-9-- — -----Sromome thane___________75-01-4———————Uinyl Chloride_________75-00-3———————Chlopoe thane_________•75-09-2————————Methylene Chloride______67-64-1————————Acetone_________________75-15-0———— —— Capbon Disulf ide_^______75-35-4———————1,1-0ichloroethene______75-34-3 ——————— 1,1-Di chlo roe thane____-540-59-0——————1,2-Dichlopethene (total).67-66-3————————Chlopoform______________107-06-2 —————— 1,2-D i chlo roe thene______78-93-3———————2-Butanone_____________71-55-6———————1,1,1-Tpichlopoe thane___56-23-5———————Capbon Tat rechloride____108-05-4———————Uinyl Acetate___________75-27-4———————BromoxJich lorome thane____78-87-5———————1,2-Dichloropropane,____10Q61-01-5--*---ci»-l,3-Dichloropropene__79-01-6-—-fM^jp—Trichlopoe thene________124-48- l--iSjS2^--Dibpemoch lorome thene____79-00-5—-*JgSe^l,i^2-Tpichlopoethane___71-43-2—-t p'i -BenMne10061-02-6*-*-—-tPane-1,3-Dichloropropene,75-25-2——————— Bpomofopm_____________108-10-1 —————— 4-Methyl-2-Pentanone____591-78-6——————2-Hexanone_____________127-18-4——————Tet rachJ opoe thene_______79-34-5———————1,1,2,2-Tetrechloroethene.108-88-3——————Toluene_______________108-90-7——————Chlopobenzene__________100-41-4———————Ethylbenzene____________100-42-5———————Stypene_________________1330-20-7—————Xylene (total)________

110110(1011014.110.15151$151515.110151511015151515151515.15.15110110151515.151515.15

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1Atourtu CMWIIG* AJULTIIItM tANVU NO

109-99-9 Tat rahydrofuran

14


EPA SAMPLE NO.

Lab Name:ETC Corp. ] Laboratory

Lab Code: Case No.:

Matrix: (soil/water)WATER

Sample vt/vol: 5.0 (g/mL)ML



Contract:

SAS No.: SDG No.:

Lab Sample ID: CA1383V

Lab File ID: >C7280

Date Received: 09/ 0/89ey


Column: (pack/cap) *-i.

CONCEITNumber TICs found: O fuq/L <

CAS NUMBER

————— ... .... _ ————

COMPOUND NAME

"TZo c /=>*-*,,•

... _ ... ___ . - ____ —————————

Dilution Factor : f

PRATION UNITS:sr ug/Kg)UG/L

RT EST. CONC

——————————————————————

———————————

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FORM I VOA-TICT5 1/87 Rev


ERA SAMPLE NO.

Lab Name: ETC Corp.

Lab Code: Case No.:



Level : C lou/med) LOLJ



Contract:

SAS No.: SDG No.:

Lab Sample 10: CA1893U

Lab File ID: >C7331

Date Received:


D i l u t i o n Factor: 1


74-87-3 —————74-83-9 —————75-01-4 —————75-00-3 ————75-09-2 ————67-64-1--^ ——75-15-0 ————75-35-4 ————75-34-3 —————540-59-0 ————67-66-3 —————107-06-2 ————78-93-3 —————71-55-6 —————56-23-5 —————108-05-4 ————75-27-4 —————78-87-5 ————10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5 —— ' ——71-43-2 —————10061-02-6 ——75-25-2 —————10Q-10-1 ————591-78-6 ————127-18-4 ————79-34-5 —————108-88-3 ————108-90-7 ————100-41-4 ————100-42-5 ————1330-20-7 ———

---Chlorome thane---Bramome thane— -Uiny 1 Ch lor ide—— Chloroethane---Mathylene Chloride---Acetone amm—— Carbon Disu 1 f ide_...M_.---l;l-Dich lo roe thane—— 1 r 1-Dich lo roe thane— -1,2-Dichlorethene (total ) __---Ch loroform---1.2-Dich 1 area than a---2-But anone—— 1.1 . 1-Tr ichlo roe thane---Carbon Tat rach lor i da—— Uinyl Acetate---Bromod ich lor ome thane,---1 r 2-D ichlo rop ropane---c i»-l , 3-D ichlo rop ropene ____- — Tr ich lo roe thane—— Dibromoch lor ome thane—— 1P1 .2-Tr ich loroe thane---Banzana— -t ranm-1 , 3-0 ichlo rop ropene __---Bromof orm---4-Mathyl-2-Pentanone „ ,,,„— -2-Haxanone _ _, „—— Tat rach lorae thane--- 1, 1, 2, 2-Tet rach loroe thane __---Toluene---Ch lorobanzana ,_,„„---Ethy lhanzane r ,._---Styrena ,——— Xyl«na (total)

1110110110110131101515151515151101515110151515151515151515110110151515151515151

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IE,VOLATILE ORGANIC* ANALYSIS DATA SHEETTENTATIVELY IDENTITIED COMPOUNDS

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EPA SAMP*.c HO.

Casa He.: SDC No.:

Matrix: (•oil/vatafi

Saopla vt/vol:Laval: (lev/mad)% Moitturas not dae.Coluan: (pack/cap)

Nunbar Tics round:

(q/mLl

Lab SaaplaLab fila ID:Data Xacaivad:

Data Analyzad:Dilution Factor:

CONCEKT1UTION UNITS;,,(ug/t or ug/Kq)

CAS NUMBER

1.3.3.4.5.«.7.1.9.

10.11.12.13.14.15.1«.17.IS.19.20.21.22.23.24.25.2«.27.'as.29.30.

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Lab Name: ETC Corp.

ERA SAMPLE NO

Lab Code: Case No.:

Matrix: (soil/water) LJATER


Level : ( low/med) LOUI

Column

Contract:

SAS No.: SOG No.:


Lab File ID: >C7330

Date Received:

sture: not dec. Date Analyzed: 10/11/89

n: (pack/cap) PACK Dilution Factop: 1

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L OP ug/Kg) UG/L Q

174-87-3 —————74-83-9 ——————75-01-4 ——————75-00-3 ——————75-09-2 ——————67-64-1 ——————75-15-0 ——————79-39-4----.--75-34-3 ——— ——54Q.59-0------6"7-66-3 ——————107-06-2 —————78-93-3 ——————71-55-6 ——————56-23-5 ——————108-05-4 —————75-27-4 ——————78-87-5 ——————10061-01-5 ———79-01-6 ——————124-48-1 —————79-00-5 ——————71-43-2 ——————10061-02-6' ———75-25-2 ——————108-10-1 ————591-78-6 —————127-18-4 —————79-34-5 ——————108-88-3 ————108-90-7 ————100-41-4 —————100-42-5 —————1330-20-7 —— --

--Ch 1 aroma thane--Bpo mo me thane--Uinyl Chloride--Ch loroethane ,--Me thy lene Chlor iden_— Acetone--Carbon Diaulf ida— 1 1 1-D ich lo roet hene--1 . 1-D ich loroethane— 1,2-Dichlorethene CtotaJ > __--Ch lopof orm „„„._--1.2-Dich lopoe thane--2-Butanone--1 .1 .1-Trieh lo roe thane--Carbon Tet rachlor ide— Uinul Acetate— Bromod ich 1 aroma thane--1 .2-Dich lopooropane--c is- 1,3-0 ich loropropene ____— Tpichlopaathene--Dibromochlopoma thane— 1.1 . 2-Tr i eh lo roe thane--Banzana__— trans-1 .3-Dich lorooropene— Bromoform--4-Methul-2-Pentanona— 2-Haxanona.--Tet rach loroa thane— 1 ,1 ,2 ,2-Tatrach loroethane __--Toluene „_— Chin robe nzene |<B n,__— Ethylbenzana--Styr«ne_ iiira--Xvlena (total) „„.„

1110110110110131101515.151515151101515110151515151515151515110110151515151515151

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EPA L! HO

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Matrix: (aoil/vatar)

Saapla vt/vol:L«val: (low/mad)I Moisturat not dac.Column: (pack/cap)

Nuabar TIC» found:

D*t* Analysed: /<>//// 89Dilution Factor: /

CONCENTRATION UNITS://,(ug/t or uq/Ka) t/f/A____ v '

CAS NUMBER

1.2.3.4.5.ft.7.1.9.

10.11.12.13.14.IS.1«.17.IS.19.20.21.22.23.24.25.2«.27. '2S.29.30.

COMPOUND NAME

i/ti%M»"l , -n-j-

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EPA SAMPLE NO

Lab Name: ETC Corp.

Lab Code: Case No.:

Matrix: Csoi1/water) WATER


Level: Clow/mod) LOU



Cont rac t

SAS No. SOG No . :

Lab Sample ID: CA1895v

Lab File ID: >C7334

Date Received:


Di lut ion Factor: 1


74-87-3————————Chlorome thane______________I 1074-83-9 ——————Bromome thane_____________I1075-01-4————————"Jinyl Chloride_____________11075-00-3————————Chlo roe thane_______________11075-09-2———————Methylene Chloride________1567-64-1———————Acetone__________________UO-75-15-0———————Carbon Disulf ide_______ 1575-35-4———————1,1-Dichloroethene________1575-34-3———————1,1-0 ichloroe thane________15540-59-0——————1,2-Dichlorethene (total)__1567-66-3 ——————— Chloroform_______________15107-06-2 —————— 1,2-Oichloroe thane________1578-93-3 ———————— 2-Butanone_________________11071-55-6 ——————— 1,1,1-Tr ichloroe thane______1556-23-5———————Carbon Tet rachlor ide______15108-05-4——————Uinyl Acetate____________11075-27-4-- — - —— -Bromod ichloromethane______1578-87-5———————1,2-Dichloropropane_______1510061-01-5—————ci*-l,3-0ichloropropene____1579-01-6———————Tr ich loroethene___________15124-48-1--.—-——Dibromochlorome thane______1579-00-5——'————1,1,2-Trichloroethane______1571-43-2————————Benzene___________________1510061-02-6————trane-l,3-Dichloropropene__1575-25-2———————Bromoform_______„________15108-10-1——————4-Methyl-2-Pentanone______110591-78-6——————2-Hexanone_______________I10127-18-4——————Tetrach loroethene_________1579-34-5———————1,1,2,2-Tetrachloroethane__15108-88-3 —————— Toluene_________________15108-90-7——————Chlorobenzene____________15100-41-4——————Ethylbenzene_____________15100-42-5——————Styrene_________________151330-20-7—————Xylene <total)___________15

IIUIUIUtuIBIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

22FORM I UQA 1/87 Rev

uYOLKRL* OMMXCS MUtYSZS •» SANK* NO,

109-99-9 Tetrahydrofuran,

1/17 R«v.

23

IIVOLATILE OUGANICS ANALYSIS DATA SHEET


E?A SAMPLZ MO

Lab Nama:Lab Coda: Cast He.

Matrix: <»oil/vatar)Saapla vt/veliLaval: (low/mad)\ Moiatura: not dae.Coluan: (pack/cap)

Contract:SAS NO.: SOG No.:

Lab Saapla ID:Lab Tilt ID:Data Racaivad:Data Analyzad:Dilution factor:

CONCENTRATION UNITS:

/

Nuabar TIC» found: ^ (uo/L or ua/Ka) 1/3 /^-| ——— ——————————————————— — ————————— —— ———————1 CAS NUMBER

1.2.3.4.S.«.7.• .*.

10.11.12.13.14.15.1C.17.!«.'1$.20.'21.22.23.24.25.2«.27.21.29.30.

COMPOUND HAW

TvrJfayd/Mft{/rttfrfff tvrt

W

'/$f/-zl

1ST. CONC.

_ ?<?«>/*

n

——

——

x vox-tie 24 1/17 R«v


Lab Name: ETC Corp.

ERA SAMPLE NO

Lab Code: Case No.:

Matrix: (soiI/water) UATER


Level: (lowXmaci) LOUt



Contract:

SAS No.: SDG No.:

Lab Sample 10: CA1896U

Lab File ID: >C7336

Date Received: /0/Mfi f

Date Analyzed: 10x12/89


CAS NO. COMPOUNDCONCENTRATION UNITS:(ugxL or ugXKg) UGXL

74-87-3————————Chlorome thane______________11074-83-9 —— ————— Bromome thane_______________1 1075-t)l-4————————Uinyl Chloride_____________11075-00-3 ——————— Chlo roe thane_____________HO75-09-2———————Methylene Chloride________1367-64-1————————Acetone___________________11675-15-0———————Carbon Disulf ide__________1575-35.4———————1,1-Dichloroethene________1575-34-3 ——————— 1,1-Dichloroe thane________(5540-59-0 —————— 1,2-Dichlorethene (total)__1267-66-3————————Chloroform_________________15107-06-2 —————— 1,2-Dichlo roe thane________(578-93-3 ——— - ——— 2-Butanone_________________I 1071-55-6————————1,1,1-Trichloroethane______1556-23-5———————Carbon Tet rach lor ide______15108-05-4——————Uinyl Acetate____________1475-27-4———————Bromodi chlorome thane______1578-87-5————————1,2-Dichloropropane________1510061-01-5————cim-l,3-Dichloropropene____1579-01-6— ———— --Tr icHloroe thane____________15124-48-1———————Dibromochlorome thane_______1579-00-5——*————1,1,2-Trichloroe thane______1571-43-2———————Benzene_________________1310061-02-6—————tran»-l,3-Dichloropropene__1575-25-2———————Bromoform________________15108-10-li———————4-Methyl-2-Pentanone_______110591-78-6——————2-Hexanone_______________110127-18-4——————Tet rach loroethene_________1579-34-5———————1,1,2,2-Tetrachloroethane__15108-88-3 —————— Toluene_________________\3&108-90-7— ———— Chlorobenzene____________15100-41-4——————Ethylbenzene_____________141100-42-5 ——————— Styrene___________________151330-20-7—————Xylene (total)

25

IUtu!UtuIBIIUIUIUIJIUIUIUIUIUIJIUIUIUIUIUIUIJIUIUtuIUIUIUIIUIIU

FORM I UOA 1/87 Rev

ml 6-66-60T

OM IKm VAvxve mnw OZIIVMO

Tt

,VC*LAT:UE OPGANICS ANALYSIS DATA SHEITTENTATIVELY IDENTIflED COMPOUNDS

EPA t HO.

Lab Nama:lab coda i Cata Ho

Contract:SA5 NO.: 506 No.:

Matrix: (aoil/vatar)Sampla vt/vol:

Laval: (low/sad)% Moitturtt not dae.Coluan: (pack/cap)

Numbar TICs found:

>Lab Saapla 10:Lab Fiia ID:Data lacaivad:Data Analytad: /Dilution Factor: /

!/

COMCINTJUTIOM WITS(ug/t or

rom x VOA-TIC 271/17

EPA SAMPLE NO.VOLATILE ORGAN ICS ANALYSIS DATA SHEET

Lab Name: ETC Corp.

Lab Code: Case No.:

Ma t P i x: C so i1/wa t e r) WATER


Level: (lou/med) LOW



Contract:

SAS No.: SDG No.:


Lab File ID: >C7335

Date Received:


Dilut ion Factor: 1


74-87-3 ——————— Chloromethane____________110 IU74-83-9—————-—Bromomethane_______________110 IU75--01-4———————Vinyl Chloride____________I44W £#£ I75-00-3 ———————— Chloroethane_______________I 10 IU75-09-2 ——————— Methylene Chloride________12 IB67-64-1 ——————— Acetone__________________lAgOSO "2*70 \75-15-0————————Carbon Disulfide___________15 IU75-35-4———————1,1-Dichloroethene________15 IU75-34-3———————1,1-Dichlo roe thane________15 - IU540-59-0 —————— 1,2-Oichlorethene (total)__1*3**77? I67-66-3————————Chloroform_________________15 IU107-06-2 —————— 1,2-Di Chloroethane________15 .IU78-93-3 ——————— 2-Butanone_______________110 IU71-55-6 ——————— 1,1,1-Trichloroe thane______15 IU56-23-5————————Carbon Tet rachlor ide_______15 IU108-05-4——————vinyl Acetate____________110 IU75-27-4—- — ----Bromodich lorome thane______15 IU78-87-5 ——————— 1,2-Dichloropropane_______15 IU10061-01-5--——cis-1,3-Dichloropropene____15 IU79-01-6 ———————— Trichloroethene____________16 I124-48-1——————Dibromoch lorome thane______15 IU79-00-5——•————1,1,2-Trichloroe thane______15 IU71-43-2———————Benzene_________________12 IJ10061-02-6————tran»-l,3-Dichloropropene__15 IU75-25-2————————Bromofortn__________________15 IU108-10-1——————4-MethyI-2-Pentanone______168 I591-78-6———————2-Hexanone_________________110 IU127-18-4——————Tetrachloroethene_________15 IU79-34-5 ——————— 1,1,2,2-Tetrachloroethane__15 IU108-88-3——————Toluene_________________\^^Jtft \108-90-7——————Chlorobenzene____________15 IU100-41-4——————Ethylbenzene_____________126 I100-42-5——————Styrene_________________15 IU1330-20-7—————Xylene (total)___________155 I______________________________________I____________I_____

28FORM I VOA 1/87 Rev

1AVOUhfXtt OMMTCCi AKALTSXt MXfc

t»A SANKJ NO,


29

IE •VOIATIU ORCANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUKDS

EPA SAMPLE HO.

Lab Naaa: &Z*T *h rnHA*

. ttspr*«* No. 1

Contract:

SAS NO.: , , . , , . S

Matrix: (aoil/watar)Saapla vt/vol:

Laval: (lov/aad)% Moisturai not d«c.Coluan: (pack/cap)

(*/»U

II

SOG No.:

Lab Saapla ID:

Lab Fila ID:Data Xacaivad:Data Analyzad: / P / f l f f ?Dilution Factor: /

CONCXKTXATION WXJJJ/X-Nuabar Ties foun«

1 ———————CAS NUMBKX

1.2.3.4.S.«.7.• .9.

10.11.12,13.14.15.1C.17.IS.19.20.21.22.23.24.23.2«.27.* ——————————2t.29.30.

It .? fua/L <

COMPOUND NAMX

l/flfitSwfGS/%*?£//W/tfJ>(/tftfncwn

>r uq/Xg)^

XT•••*••••/•^y/:f"3Z/:0k

j^r1ST. CONC.

•••••**«*a»««£/•z-/^ztr~

Q•••*«

—

=

———

fOJW I VOfc-TIC 30 1/17 Rtv

\

1AUOLATILE ORGAN ICS ANALYSIS DATA SHEET

EHA SAMPLE NO.

Lab Name: ETC Corp.

Lab Code: Case No.:






Cont ract:

SAS No.: SDG No . :


Lab F i l e ID: >C7352

Date Received:


Dilution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L OP ug/Kg) UG/L

74-87-3 — ————— Chlopome thane____________11074-83-9—-—————Bpomome thane_______________11075-01-4———————Uinyl Chlopide____________11075-00-3 — ————— Chlopoa thane_____________11075-09-2———————Methyl one Chlopide________1367-64-1———————Acetone_____________ IIP75-15-0———————Carbon Disulfide__________1575-35-4———————X,l-0ichlopoethane_______15-75-34-3———————1,1-Dichlopoe thane________15540-59-0——————1,2-0ichlopethene (total)__1567-66-3 ———————— Chlopofopm_________________15107-06-2———— — 1,2-Dichlopoe thane________1578-93-3———— ——— 2-Butanone_______________11071-55-6———————1,1,1-Tpichlopoe thane______1356-23-5———————Capbon Tet pachlop ide______15108-05-4——————Uinyl Acetate____________11075-27-4-- — -———BPO mod ichlorome thane______1578-87-5 ———————— 1,2-DichloPoppopane________1510061-01-5————ci»-1,3-Dichlopoppopene____1579-01-6———————Trichlopoe thene___________116124-48-1——————Dibromochloromethane_^____1579-00-5——'————1,1,2-Tr iehloro* thane______1571-43-2———————Benzene__________________1510061-02-6— — --t pana-1,3-DichlopopPOpene^_l575-25-2———————Bpomofopm______ 15108-10-1——————4-Mathyl-2-Pentanona______110591-78-6——————2-Haxanone_______________110127-18-4——————Tetpachlopoa thane_________1579-34-5———————1,1,2,2-TetpachloPoethane__15108-88-3 —————— Toluene_________________15108-90-7——————Chlopobenzene____________15100-41-4——————Ethylbenzena_____________15100-42-5——————Stypana_________________151330-20-7—————Xylane (total)___________15

FORM I UOA31

1IUIUIUIUIBIUIUIUIUIUIUIUIUIJIUIUIUIUIU1IUIUIUIUIUIUIUIUIUIUIUIUIUIU

1/87 Rev

s

i

38

sI

_ •» •• *•• i: iM I i!

I

^3

*J! I'ihi1!i I 3 s S

I I - 1 -2 8 2 : 2 2 1J 3!! 1! 1

n ITIT CM

\M

I

IIVOLATIU ORCANICS ANALYSIS DATA SHEET


£?A

UbUbCoda: CM. HO.:

Matrix: (aoil/vatar)

Sanpla vt/voliUval: (lov/«ad)

% Moisturat not dac.column: (pack/cap)

Number TIC» found:

Contract:S A S N O . : ____ SDC No.:

Ub Stapla ID:

Ub Fila ID:Data Racaivad:Data Analyzad:Dilution Factor:

CONCENTRATION UNITS(ug/t or ug/Kg) "*

1t CAS NUMBER

1.2.3.4.5.ft.7.S.9.

10,11.12.13.14 . "IS.1«.17.IS.1», ""20.21.22.23.24.23.2ft,27. " —————————2S.2t,30.

COMPOUND NAMI

7k<4j&>t tSswctil/fl /£-rteusrt

. . _._

-

*T EST. CONC.

pom i VOA-TXC 33 1/17

\


EPA SAMPLE NO.

Lab Name: ETC Corp.

Lab Code: Case No.:






CAS NO. COMPOUND

Cont ract

SAS No. : SDG No . :


Lab File ID: >C7353

Date Received :


Dilution Factor: 1

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

74-87-3 —————74-83-9 —————75--01-4 —————75-00-3 ————75-09-2 ————67-64-1 —— ----75-15-0 —————75-35-4 —————75-34-3 ————540-59-0 ————67-66-3 —————107-06-2 ————78-93-3 ————71-55-6 —————56-23-5 ————108-05-4 ————75-27-4 —————78-87-5 —————

1- — Ch loromethane ,„ 1---Bromomethane _ _, 1— -Uinvl Chloride 1—— Ch 1 o roe thane I---Methvlene Chloride 1---Acetone „ , " ~ 1—— Carbon DiaulffHe 1—— 1 r 1-Dichl QPO* thane " 1- — 1 . 1-Dichloroethane " 1—— 1,2-Oichlorethene (total) __ 1---Chloroform „_ 1—— Ir2-Dichloroathane 1---2-Butanone . 1—— 1 .1 .1-Triehloroethana 1—— Carbon Tat rach lor ide 1—— Uinyl Acetate 1—— Bromodich lorome thane 1

10061-01-5 ———— ci*-l,3-0ichloropropene ____ 179-01-6---------Triehlnraethene 1124-48-1 ————79-00-5 —— ' ——71-43-2 —————10061-02-6 ——75-25-2 —————108-10-1 ————591-78-6 ————127-18-4 ————79-34-5 —————108-88-3 ————108-90-7 ————100-41-4 ————100-42-5 ————1330-20-7 ———

—— Dibromoch lorome thane 1• — -1 .1 .2-Tr iehloroe thane 1- — Benzene M I I I 1—— t ran»-l ,3-Oich loropropene __ 1---Bromef arm , 1—— A-Methyl-2-Pentenone .,„_,._„.,.„.. 1— -2-Hexenane _,, ,.„„ 1—— Tetrechloraethene , 1—— 1,1,2,2-Tetrechloroethene __ 1---Toluene, BIIII 1—— Chlorabenzene 1—— Ethyl benzene , . 1—— Styrene „ _, . 1——— Xylene (tatel) 1

1

1010101021055 "559510551055555555510105555555

1IUIUIUIUIBIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1


uVOIARU OMMXCS AJULYfX*


35

ItVOLATILE ORGAXICS ANALYSIS DATA SHEET


EPA SAMP*.! NO

Lab Coda: _____m Casa No.:

Matrix: (aoil/watar)Saapla vt/vel:

Laval: (low/mad)% Moisturat not dac.Coluan: (pacX/cap)

Numbar TIC» found:

Contract:SAS NO.:

I

SDG No.:

IDtUbLab rii« ID:Data Mcaiv«d:Data Analyzad:Dilution Factor:

CONCtNTRATXON UNITS t/.(ug/L or uoyKqi /g /

/

FORM I 36 1/17


ERA SAMPLE NO,

Lab Name: ETC Corp.

Lab Cods: Case No.:

Matr ix : (so 11/water) U1ATER

Sample wt/vol! 5.0 (g/mL) ML

Level: ( low/mod) LOLJ .



Cont ract:

SAS No.: SOG No . :


Lab File ID: >C7354

Date Received:


Di lut ion Factor


I74-87-3———————Chloroma thane____________11074-83-9—-————Bromome thane_____________11075-01-4———————Uinyl Chloride____________11075-00-3———————Chloroe thane_____________11075-09-2———————Methylene Chloride________1267-64-1 ——————— Acetone_________________11075-15-0———————Carbon Disulf ide__________I5~75-35-4—————-1,1-Dichloroethene________1575-34-3 ——————— l,l-Drchloroethane_r_______15540-59-0 —————— 1,2-0ichlorethene (total)__1567-66-3————————Chloroform_________________15107-06-2 —————— 1,2-Dichloroethane________1578-93-3 ——————— 2-Butanone_______________11071-55-6 ——————— 1,1,1-Trichloroethane______1556-23-5———————Carbon Tetrachloride______15108-05-4——————"Jinyl Acetate____________11075-27-4— — -----Bromod ich lorome thene______1578-87-5———————1,2-Dichloropropane_______1510061-01-5————ci»-l,3-Dichloropropene____1579-01-6—————.—Trichloroa thene___________187124-48-1——————Dibromoch lorome thane______1579-00-5——'—————Ir1.2-Triehloroe thane 1571-43-2———————Benzene_________________1510061-02-6———--tran»-l,3-Dichloropropene__1575-25-2———————8romoform________________15108-10-1——————4-Methyl-2-Pentanone______110591-78-6——————2-Hex«none_______________110127-18-4——————Tetrachloroethene_________1579.34-5 ——————— 1,1,2,2-Tetrachloroethane__15108-88-3 —————— Toluene_________________15108-90-7——————Chlorobenzene.____m______15100-41-4——————Ethylbenzene_____________15100-42-5 —————— Styrene_________________151330-20-7—————Xylene (total)___________15

.__ ..._____________ I __

tuIUIUIUIBIUIUIUIUIUIUIUIUIJIUIUtuIUIUItuIUIUIUIUIUIUIUIUIUIUIUIUIU


1AVOUTHJ OfiOMXCi MUU.TSX* MS*

CM ftAJOU NO.

109-99-9 T«trahydrofuran

1/iT

38

IEVOLATILE CRCAJUCS ANALYSIS DATA SHEET


CPA SAMPLI NO

S*mpl* wt/vol:I*v«l : ( low/m«d)% Moisturtt not d>e.Coluan: (pack/cap)

Numb«r TIC« found i &

Dilution Factor!

CONCOTXATION(ug/L or

rent x VO»-KC 39 1/17

\


EPf> SAMPLE NU

Lab Name: ETC Corp.

Lab Code: Case No.:

Cont ract

SAS No.

Ma t r i x: (soil/wa ten) UATER

Sample wt/vol: 5.0

Leve1: C1ow/med) LOW

Sf Moisture: not dec.


(g/mL) ML

SDG No.:

Lab Sample ID: CA214D'.1

Lab File ID: >C7375

Date Received: lo/oo/**!




40

•-4

74-87-3 —————74-83-9 —————75-01-4 —————75-00-3 —————75-09-2 —————67-64-1 —————75-15-0 —————75-35-4 —————75-34-3 —————54Q-59-0 ————67-66-3 —————107-06-2 ————78-93-3 —————71-55-6 —————56-23-5 —————108-05-4 ————75-27-4 —————78-87-5 —————10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5 —————71-43-2- ————10061-02-6 ——75-25-2 —————108-10-1 ————591-78-6 ————127-18-4 ————79-34-5 —————108-88-3 ————108-90-7 ————100-41-4 ————100-42-5 ————1330-20-7 ———

1---Ch loromethane „ 1---Bromomethane .. _ 1—— Um-jl Chloride 1---Ch loroethane ,„ I---Methylene Chloride 1---Acetone . , 1---Carbon Disulfide , 1---1 rl-Dich lo methane 1---1,1-Dich loroethane 1—— 1,2-Dichlorethene (total ) __ 1---Chloroform 1---1 ,2-Dich loroethane 1---2-Butanone ,.,„„ ,, 1---1.1.1-Triehloroethana 1---Carbon Tetrachloride 1---Uinyl Acetate t---Bromod ich loromethane 1---1 P2-Dich laroprapane 1---c is-1 ,3-0 ich loropropene ____ 1— -Tr ieh In roe thane 1— -Dihrnmoch I a r ante th ana 1——— 1.1 f 2- Tri eh la roe thane 1— -Benzene „ 1—— t rans-1 , 3-D ich loropropene __ 1---Sromoform , 1——— 4-M«thyl-2-Pantanona 1---2-Hexanone inra . . . 1__-Tat raeh In roe thane 1- — 1, 1,2 ,2-Tet rach lo roe thane __ 1---Toluane , 1---Ch larobenzane _ 1— -Ethyl benzene , 1---Styrene, ._. 1——— Xyl.n. (totall t

1

10101011111055~1155510451055515552551010120555555

I !IUIUIUI1IU tIU 1tU :1 1IU !IU 1IU •tU 11 J !IU 1tU :IU 1IU :tU 11 !IU 1!UIJ 1IU iIU 1!U !IU 11 IIU 1IU !IU 1IU :IU 1!U !1 1

FORM I UOA 1/87 Rev

VOUffXUm urn* NO.

s.o r«/»u ML^^

109-99-9 T«tr«hydrofuran,

XOl CAiiUO V

OUMiM

» in/oi /^qt io/t3/gq

1 A

1/17 ««v

41

IEVOLATILE ORGAN ICS ANALYSIS DATA SHEET


ERA SAMPLE NO.

Lab Name:ETC Corp. I Laboratory

Lab Code: Case No.:

Matr ix: Csoi1/water)WATER

Sample wt/vol: 5.0 Cg/mDML

LeveI: Clow/med) LOW

S Moisture: not dec._____

Column: (pack/cap)

Number TIC* found:

Cont ract:

SAS No.: SDG No.:

Lab Sample ID*. CA214QU

Lab File ID: >C7375

Date Received: (<Yo<*/*ei


Dilution Factor: I

CONCENTRATION UNITS:Cug/L or ug/Kg)UG/L

CAS NUMBER

01.02.03.

"rtU.

COMPOUND NAME

CARBON DIOXIDEUNKNOWNUNKNOWNUHKHOUJM

RT

1.531.303.73

10.103.35

EST. CONC

140045161U(jQ

42

Q

BJaa•j"— •

FORM I UQA-TIC 1/87 Rev


ERA SAMPLE NO.

Lab Name: ETC Corp.

Lab Code: Case No . :

M a t r i x : (soil 'water) WATER

Sample wt/vol : 5.0 Cg/mL) ML

Level: ( low/mod) LOU1



Con t rac t:

SAS No.: SDG No.:


Lab File ID: >D8Q38




CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UG/L Q

74-87-3 —— ——74-33-9 —————75-01-4 -----75-00-3 — — —75-09-2 ------67-64-1 —— ——75-15-0 -----75-35-4 ------75-34-3 ------540-59-0-----67-66-3 ------107-06-2 -----78-93-3 ----- -71-55-6 —————56-23-5 — — —108-05-4 ————75-27-4 -----78-87-5 —————10061-01-5 ——79-01-6 —————124-48-1 -----79-00-5 —————71-43-2 —————10061-02-6 ——75-25-2 ------108-10-1 -----591-78-6 —— —127-18-4 -----79-34-5 —— ——108-38-3 -----108-90-7 -----100-41-4 -----100-42-5 -----1330-20-7 —— -

1---Chloro me thane 1---Bro mo me thane 1---UinulChloride 1---Chloroethane 1---Me thvlene Chloride 1---Ace t one 1---Carbon Disulfide 1—— 1.1-Dichloroethane I---1.1-Dichloroethane 1- — 1,2-Dichlorethene (total ) __ 1---Ch loro f arm I---1.2-Dichlarae thane 1---2-Butanone 1---1.1.1-Trichloroethane 1---Carbon Tet rach lor ide 1— -Yinul Acetate 1---Bromod ich loro me thane I- — 1 r2-Dieh loropropana 1---c is-1 , 3-D ich loroprooene 1---Trichloroethene „ 1---Dibromoch loroma thane t— -1.1.2-Trichioroathan* 1---Benzene „ 1---trans-l,3-Dich loropropene __ 1---Bro mo form 1---4-Me thol-2-Pent anone 1---2-Hexanone 1---Tet rach lor o« thane 1---1,1,2,2-Tetrachloroethane 1---To luene _ , 1---Ch lorobanzane, 1

---Storane .,,„ 1---Xylmnm (total ) .„, , I

I

1010101027

55555105

10555555555101055555

5

1IUIUIUIU1 JIJIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

1 T.

FORM I I'd A 1/37 Re'

uOfcftMRCS MULT*** MC*

KM ftAJOU NO,

44

IEUOLAULE ORGAN ICS ANALYSIS DATA SHEET

TENTATIUELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

Lab Name-.ETC Corp.

Lab Code: Case No.:

Matrix: (so iI/water)WATER

Sample wt/vol: 5.0 (g/mDML

Level : < low/med) LOUI

% Moisture: not dec ,______

Column: (pack/cap) fa *•.(£.

Number TICs found: O

Con t rac t:

SAS No.: SDG No.i


Lab File ID: >D8039



Dilution Factor: (

CONCENTRATION UNITS:(ug/L or ug/Kg)UG/L

CAS NUMBER COMPOUND NAME RT EST. CONC

FORM I UOA-TIC 1/87 Rev

45


ERA SAMPLE NO.

Lab Name: ETC Corp.

Lab Code: Case No.:

Met P ix : Cao i 1 --'water ) HATER

Sample ut/vol: 5.0 (g/mL) ML

Level: Uow/med) LOW



CAS NO. COMPOUND

Cont ract:

SAS No.: SDG No.:


Lab File ID: >D3039


Date Analyzed: 10/17-'89

Dilut ion Factor: 1


74-87-3- ——— ——— Ch lorome thane______________I 107-4-83-9-- — -- — -Bromomethane_______________I 1075-01-4————————vinyl Chloride_____________11075-00-3 — - — —— -Chloroe thane_______________I 1075-09-2 ———————— Methylene Chloride_________1467-64-1 ———————— Acetone___________________I 1275-15-0 ———————— Carbon Disulf ide___________1575-35-4---------1,1-Oichloroethene_________1575-34-3- ——————— 1,1-Dichlopoe thane_________15540-59-0———————1,2-Dichlorethene (total )__1567-66-3------ —— Chloroform_________________15107-06-2———————1 ,2-Dichloroethane_________1578-93-3 — — ———— 2-Butanone_________________I 1071-55-6 — ---———1,1,1-TrichloPoe thane______1556-23-5 ———————— Capbon Tetrach lopide_______15108-05-4———————Uinyl Acetate______________I 1075-27-4---- -----Bromod ich lo pome thane_______1573-87-5 ———————— 1,2-Di chio pop popane_________1510061-01-5—————c is-1,3-Dichiopoppopene____1579-01-6 ——————— -Tpichlopoethene____________15124-48-1- —— ———Dibpomochlopome thane_______1579-00-5 ———————— 1,1,2-Trichlopoe thane______1571-43-2 ——————— Benzene_________________1510061-02-6-———tpans-1,3-Dichlopopropene__1575-25-2 ——————— -Bpomof orm_________________15108-10-1———————4-Methyl-2-Pentanone_______110591-78-6 ——————— 2-Hexanone________________1 10127-18-4 —————— Tetpachlopoethene_________1579.34-5————————1,1,2,2-TetPachlopoethane__15103-88-3- —— ----Toluene___________________15108-90-7-- —— - — Chlopobenzene______________15100-41-4- ——— ---Ethyl benzene_______________15100-42-5--------Stypene___________________151330-20-7——————Xylene (total )____________15

Q

A S46

IUIUIUIUIJ1IUIUIUIUIUIUIUIUIUIUIUIUIUIUI U 'IUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I UQA 1/87 Rev.

A»« it/1

o« ruvvt vomo *x§nm nurmo



EPA SAMPLE NO.

Lab Name:ETC Corp.

Lab Code: Case No.:

Mat r ix : CSQ i 1/"water )WATER

Sample wt/ôl: 5.0 <g/mL>ML

Laêl: (low/med) LOW

S M o i s t u r e : not dec.

Con tract:

SAS No.: SDG No.:


Lab F i l e ID: >D8039



o lumn : ( pack/ca

Number TICs foun

CAS NUMBER

3) <#fc/<:

CONCEN1li O , (uaxL

COMPOUND NAME

'ftn^ fst-^J .

Di lut ion Factor: '

FRATION UNITS:sr ug/Kg)UG/L

RT EST. CQNC Q

FORM I VJQA-TIC 48 1/87 Rev

UOLATILE ORGAN ICS1AANALYSIS DATA SHEET

ERA SAMPLE NO

Lab Name: ETC Corp.

Lab Code: Case No.:






Con t rac t:

SAS No.: SDG No . :


Lab File ID: >D8040





74-87-3 ———————— Chlorome thane___________74-83-9---------Bromomethane____________75-01-4————————Uinyl Chloride__________75-00-3- — -- —— -Ch1 oroethane____________75-09-2 ——————— -Methylone Chloride______67-64-1 —————— --acetone_________________75-15-0- ——————— Carbon Disul fide________75-35-4—————-1,1-Oichloroethene______75-34-3 — -- — —— 1,1-Dichloroe thane______54Q-59-0———————1,2-Oichlorethene (total),67-66-3---—-—-Chloroform______________10 7- 06-2 — ————— 1,2-Dichloroethane______78-93-3----———2-Butanone______________71 -55-6-- — ———— 1,1,1-Trichloroethane___56-23-5---------Ca'rbon Tet rach lor ide____108-05-4———————Uinyl Acetate___________75-27-4---------Bromodichloromethane____78-87-5---------1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene_79-01-6 —— — —•—Tr ichloroethene_________124-48-1----—--Dibromochloromethane____79-00-5————————1,1,2-Tr ichlo roe thane___71-43-2 ———————— Benzene_________________10061-02-6—————trans-l,3-Dichloropropene.75-25-2---——-—Bromoform_______________108-10-1--—————4-Methyl-2-Pentanone_____591-78-6 ——————— 2-Hexanone______________127-18-4——— ——— Tet rach loroethene_______79-34-5——————-1,1,2,2-Tetrachloroethane.108-88-3 — ————— Toluene_________________108-90-7——— — --Chlorobenzene___________100-41-4--- — - — Ethyl benzene____________10 0-42-5-- ————— Styrane _______________1330-20-7——————Xylene t total )_________

110110110110.14161515151515151101515110.15151515151515151511011015151515151515

Q

IUIUIUIUIJIJIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

49FORM I UQA 1/37 Rev,

OS

. IEVOLATILE ORGAN ICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

Lab Name:ETC Corp.

Lab Code: Case No.:

Matr ix: (soiI/water)WATER

Sample wt/ôl: 5.0 Cg/mL)ML

Lev«l: Clow/med) LOU


Column: t pack/cap)

Number TICs found:

Cont ract:

SAS No.: SDG No.:


Lab File ID: >D8040



Dilution Factor: I. ..



FORM I UOA-TIC51

1/37 Rev


Lab Name: ETC Corp.

EPA SAMPLE NO.

Lab Code: Case No.:



Level : ' low/med) LOU



CAS NO. COMPOUND

Lon t rac t:

SAS No.: SOG No.:


Lab File ID: >D8041



Dilution Factor: 1

CONCENTRATION UNITS:Cug/L or ug/Kg) UG/L

74-87-3---—————Ch lorome thane___________74-83-9---------Bromomethane____________75-01-4————————Uinyl Chloride__________75-00-3- — -- ——— Chloroe thane____________75-09-2 — — ———— Methylene Chloride______67-64-1---------Ace tone_________________75-15-0- —— — ——Carbon Disulf ide________75-35-4———————-1,1-0 i chio roe thene______75-34-3 ——————— -1,1-Dichloroe thane______540-59-0 ———— — 1,2-Dichlorethene (total).67-66-3 —— — ——— Chloroform______________107-06-2 — ————— 1,2-Dich lo roe thane______78-93-3 — - — —— -2-Butanone______________71-55-6 —— --- ——1,1 ,1-Trichloroethane___56-23-5 — —— ——— Carbon Tet rachlor ide____108-05-4———————Uinyl Acetate___________75-27-4---------Bromodichloromethane79-87-5————————1,2-Dichloropropane_____10061-01-5—————cis-l,3-Dichloropropene__79-01-6 —————— — Tr ich lo roe thene_________124-48-l--------Dibromoehloromethane____79-00-5 ———————— 1,1,2-Tr ich loroe thane____71-43-2-- — ———— Benzene_________________10061-02-6—————trans-1,3-Dichloropropene.75-25-2---- ———— Bromoform_______________108-10-1 ——————— 4-Methyl-2-Pentanone____591-78-6———————2-Hexanone______________127-18-4— ——— — Tetrach loroe thene_______79-34-5——————-1,1,2,2-Tetrachloroethane.103-38-3 ——— ——— Toluene_______________108-90-7——--—-Chlorobenzene___________100-41-4———————Ethyl benzene____________100-42-5---—-—Styrene_________________1330-20-7——————Xylene (total)_________

110.11011011012I 1015.1515151515110.151511015151515151515151511011015151515151515

Q

IDIUIUIUI JIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I UOA 1/87 Rev



EPA SAMPLE Nb.

Lab Name: ETC Corp.

Lab Code: Case No. :

Mat P ix : (soi I/water ) WATER

Sample wt/vol: 5.0 <g/mL)ML

Level: flou/med) LOW

S Moisture: not dec. _____

Column: (pack/cap)

Con tract:

SAS No.: SDG No.:

Lab Sample ID: Cft215flU

Lab File ID: >D3Q41



Dilution Factor: I

Number TICs found:CONCENTRATION UNITS:(ug/L or ug/Kg)UG/L


I UOA-TIC 1/87 Rev

53

UJ9U NO.OMAinCS MUU.TSZS

54

1AVOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: ETC Corp.

Lab Code: Case No.:


Sample wt/vol: 5.0 (9/nL) ML




Contract:

SAS No.:: SDG No.:

Lab Sample ID: CA2150V

Lab File ID: >I8248



Dilution Factor: l


74-87-3——————Chloromethane__________74-83-9——-—-—Bromonethane____________75-01-4——————Vinyl Chloride_________75-00-3-—————Chloroethane75-09-2——————Methylene Chloride67-64-1———————Acetone_____________75-15-0——————Carbon Disulfide75-35-4——————1,1-Dichloroethene______75-34-3——————1, l-Dichloroethane______540-59-0—————i, 2-Dichlorethene (total)_67-66-3-—————Chloroform____________107-06-2—————1,2-Dichloroethane______78-93-3———————2-Butanone_____________71-55-6——————l, l, 1-Trichloroethane____56-23-5-—-———Carbon Tetrachloride_____108-05-4——————Vinyl Acetate___________75-27-4-—•-—-—Bromodi chloromethane_____78-87-5-——-——1,2-Dichloropropane______10061-01-5————cis-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48 -1————-Dibromochloromethane_____79-00-5——————l, l, 2-Trichloroethane____71-43-2—-———Benzene ___________10061-02-6———trans-l.3-Dichloropropene75-25-2——————Bromoform_____________108-10-1—————4-Methyl-2-Pentanone_____591-78-6——————2-Hexanone_____________127-18-4 —————Tetr achloroethene_______79-34-5——————l ,1,2,2-Tetrachloroethane_108-88-3—————Toluene______________108-90-7—————Chlorobanzene__________100-41-4—————Ethylbenzene___________100-42-5—————styrene______________1330-20-7—————Xylene (total)________

i_____________________________________.——.— l

101010109101055510510551055555555510105555555

ruuuuuuuuuuu

uYOURXJ OMMICS AlULtflXi


I/it

56

VOUkTIU OMAJUCS 'ANALYSIS DATA SHUTTENTATIVELY IDENTIFIED COMPOUNDS

SAhP-Z .10.

Contract:SA5 No.: SDC No.:

Matrix: (soil/vatar)

Saapla vt/vol:

Laval: (low/Bad)

% Noiaturai notColuan: (pack/cap)

Muabar TICa found: _£

Lab Saapla ID:

Lab Fila ID:Data Xacaivad:

Data Analyxad:Dilution Factor: I

COMCXHT1UTXOII WITS:or

roim x 57


Lab Name: ETC Corp.

EPA SAMPLE NO.

Lab Code: Case No.:

Mat r ix: (soi1/water) WATER

Samp 1 e wt ••'vo 1 : 5.0 Cg/mL) ML

Lew*l: (low/med) LOLJ



CAS NO. COMPOUND

Lont rac t:

SAS No.: SDG No.:


Lab File ID: >D3042

Date Received: 10/10/8*


Dilution Factor: 1

CONCENTRATION UNITS:Cug/L or ug/Kg) UG/L Q

74-87-3 ------74-83-9 - — ——75-01-4 ......75-QQ-3 ------75-09-2 ------67-64-1 — — —75-19-0 ------75-35-4 —————75-34-3 —————540-59-0 -----67-66-3 — — —107-06-2 ——— -78-93-3 -----71-55-6 —— ——56-23-5 ------108-05-4 ————75-27-4 —————78-37-5 ------10061-01-5 ——79-01-6 ----- -124-48-1 -----79-00*5 —————71-43-2 —————10061-02-6 ——75-25-2 —————108-10-1 ————591-78-6 -----127-18-4 —— —79-34-5 ------108-88-3 ————108-90-7 -----100-41-4 -----100-42-5 -----1330-20-7 ———

---Chlopo me thane---Brn ma me thane---Uin-jl Chloride---Ch lo roe thane---Methulena Chloride---Ace tone---Carbon Diaulfide---1 ,1-Dichloroethena---1 ,1-Dichloroethane---1,2-Dichlorethene t total ) __---Ch lorof orm—— 1.2-Dichloroethane---2-Butanone---1.1.1-Trichloroethane---Carbon Tet rach lor ide---Uinyl AcBtate_---Bromod ich lorome thane—— 1 .2-Dichloroorooarte—— cis-1, 3-D ichloropropene ____---Trichloroathena---Dibromoch lorome thane— -1.1 .2-Tri eh loroa thane---Benzene..,— --trans-l,3-Dich loropropene---Bromof orm— -4-Methyl-2-Pentanona ,.„„,.,„,---2-Hexanona---Tat rach loroa thane---l,l,2>2-""etrach loroe thane __---Tnluana---Ch lorobanzana---Fthy Ibanzana ,.,_., „ n ni---St yrene—— -Vylana ( total ) in ,

11101101 1011019181515151515151101515110151515151515151515110110151515151515151

1IDIUIUIU'1UIUIUI I J -IUIU

' IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

r n '

FORM I UQA 1/87 Re-

oaownes AJULTSII

59

IEVOLATILE ORGANICS ANALYSIS DATA SHEET


ERA SAMPLE NO.

Lab Name:ETC Corp.

Lab Code: Case No.:

Matr ix: (so iI/water)WATER

Sample wt/vol: 5.0 Cg/mL>ML

Level: (low/mod) LOU

\ Moisture: not dec._____

Column: (pack/cap)

Number TICs found:

Cont ract:

SAS No.: SDG No.:


Lab File ID: >D8042

Date Received: 10/10/'89


Dilution Factor: '____


CAS NUMBER COMPOUND NAME RT EST. CQNC


60

ISSEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET

EFA SMMPLE NO.

Lab Name: ETCNJ

Lab Code:

Cont ract:

Case No.:

Matrix: (soi1/watar) UATER

Sample wt/vol: 920.0 Cg/mL> ML

Level: (low/mod) LQLJ

S Moisture: not dec. dec.

Extraction: (SepF/Cont/Sonc> CONT

GPC Cleanup: (Y/N) N pH:

CAS NO. COMPOUND

SAS No.: SDG No.:

Lab Sample ID: CA1379C

Lab File ID: >G9015


Date Extracted: 10/04/89




108-95-2 ——————— Phenol________________111-44-4———————bis<2-Chloroethyl )ether95-57-8————————2-Chlorophenol________541-73-1———————1,3-Dichlorobenzena.106-46-7——————1,4-Dichlorobenzene.100-51-6——————Benzyl alcohol____

I111111111111111111111111

95-50-1—————— — 1,2-DichIorobenzene_____95-48-7————————2-Methyl phenol__________108-60-1———————bia(2-Ch loroisop ropy l)ether_ 111106-44-5 ——————— 4-Methylphenol_____________111621-64-7------—N-Nitroao-di-n-propylamine 111

111.111111,111111,154

•bis(2-Chloroethoxy)methane_111•2 ,4-Oichlorophenol_________I 11

120-82-1—--———1,2,4-Trichlorobenzene_____11191-20-3———————Naphthalene______________111106-47-8———————4-Chloro«nilin«____________11187-68-3—*---

67-72-1---- — ---Hexachloroethane._98-95-3 ———————— Nitrobenzene_____78-59-1---------Isophorone_______88-75-5————————2-Nitrophenol____105-67-9 ——————— 2,4-Di methyl phenol,65-85-0———————Benzole acid_____111-91-1————120-83-2————

——— -MaxachLorobutad lane_____59-50-7———•--——4-Chloro-3-mathylphenol_91-57-6————"———2-Mathylnaphtha lane_____77-47-4——..:———Hcxachlorocyclopantadiana,88-06-2———————2,4,6-Trichlorophenol___95-95-4———•————2,4,5-Tr ichlorophenol____91-58-7———————2-Chloronaphthalene_____88-74-4———————2-Nitroani 1 ine_________131-11-3 —————— Dimethylphthalata_______208-96-8- ————— Acenaphthylena_________606-20-2———————2,6-Dini tro toluene.

FORM I SO -1

111111111111111154111154111111111I__

61

iuIDIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

1/87 Rev

. 1CSEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO,

Lab Name: ETCNJ

Lab Code: Case No.:



Leve1: Clow/mod) LOW


Ex t r ac t i on: C SepF/Con t/Sonc) CQNT

GPC Cleanup: CY/N) N pH:

Contract:

SAS No . : SDG No . :


Lab File ID: >G9Q15

Date Received: 09/29x89



Di lut ion Factor : 1


I 99-09-2 ———————— 3-Ni t roan i line_____________15483-32-9- —— - ——— Acenaphthene_______________11151-28-5 ———————— 2,4-Dinitrophenol__________1541-00-02-7———————4-Nitrophenol______________154132-64-9 ——————— Dibenzofuran_______________111121-14-2———————2,4-Dinitrotoluene_________I 1184-66-2———•———Diethylphthalate__________1117005-72-3— ———— 4-Chloropheny1-phenylet her_11186-73-7————————Fluorene__________________I 11100-01-6——————4-Ni t roan i line____________154534-52-1 ——————— 4,6-Dinitro-2-methylphenol_15486-30-6————————N-Ni trosod iphenylamine (1)_111101-55-3 ——————— 4-Bromopheny 1-pheny let her__I 11118-74-1 ——————— Hexachlorobenzene__________11187-86-5———————Pentachlorophenol_________15485-01-8————————Phenanthrene_______________111120-12-7——————Anthracene_______________11184-74-2———————Di-n-butylphthalate_______111206-44-0———————-Fluoranthene_______________111129-00-0———————Pyrene____________________11185-68-7———————Butylbenzylphthalate______11191-94-1———————3,3'-Dichlorobenzidine_____12256-55-3—-—-——Benzo(a)anthracene________111218-01-9——————Chryaene_________________111117-81-7———————bim(2-Ethylh«xyl >phth«late__I 11117-84-0———'———Di-n-octylphthal«te________111205-99-2 —— - ——— B«nzo(b)f luo ran thane______111207-08-9——————Benzo(k)f luoranthene______11150-32-8———•-----BenzoCa)pyrene____________111193-39-5——————Indano(l,2,3-cd)pyrene_____11153-70-3———————OibenzC«,h) anthracene______111191-24-2———————8enzoCg,h, i )perylene_______111________________________________________I .

CD - Cannot be separated from Diphenylamine

IUIUIUIU.IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I SU -2 621/87 Rev

IFSEMIUQLATLLE ORGAN ICS ANALYSIS DATA SHEET


EPA SAMPLE NO

Lab Name:ETCNJ

Lab Code: Case No.:

ha t r i x: (soil/wa t e r)WATER

Sample wt /vo l : 920 .0 Cg/mDML

Level: ( low/med) LOLJ

\ Moisture: not dec._____ dec.___

Ex t r ac t i on: C SepF/Con t/Sonc) CONT

GPC Cleanup: <Y/N> N pH:___

Number TICs found: £"

Cont ract:

SAS No.: SOG No.:


Lab File ID: >G9015


Date Extracted:10/04/89


Dilution Factor: /___


CAS NUMBER

01. 141-78-602.03.04.05.

.

COMPOUND NAME

Acetic acid, ethyl eater .UNKNOWNTr ich loro-propene isomerUNKNOUINUNKNOWN

RT

5.246.509.146.807.90

EST. CONC

60079332121

' Q

JBJBJBJBJB

FORM I SU-TIC 63 1/87 Rev,

ISSEM1OOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO,

Lab Name: ETCNJ Cont ract:

Lab Code: Case No.: SAS No.: SDG No.:

Matrix: Csoi1/water) WATER Lab Sample ID: CA1380C

Sample ut/vol: 920.0 (g/mL) ML Lab File ID: >G9016

Level: (low/med) LOW Date Received: 09/29/89

Moisture: not dec. dec.

Extraction: CSepF/Cont/Sonc ) CONT

GPC Cleanup: <Y/N> N pH:



Dilution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L Q

108-95-2 —111-44-4—95-57-8 ——541-73-1 —106-46-7—100-51-6 —95-50-1 ——95-48-7 ——108-60-1 —106-44-5 —621-64-7--67-72-1 ——98-95-3 ——78-59-1 ——88-75-5 ——105-67-9 —65-85-0 ——111-91-1 —120-83-2 —1 On_R9_l__

91-20-3 ——106-47-8—87-68-3 ——59-50-7 ——91-57-6 ——77-47-4 ——

95-95-4 ——91-58-7 ——88-74-4 ——131-11-3 —208-96-8 —606-20-2—

1———— -Phenol 1————— bis(2-Chloroethyl ) ether ____ 1----"2-Chloraphenal 1———— -1 r3-Dichlorobenzene I—— -— 1 .4-Dich lorobenzene 1__ — --Benzyl alcohol 1_--_ — 1 .2-Dichlorohenzene I------2-Methylphenol 1————— bi»(2-Chloroisopropyl ) ether 1————— 4-Methylphenol_ ,„._. 1___.___N-Ni t roso-d i-n-propy lamine _ 1------Hexach lo roe thane 1------Nitrobenzene 1------ laophorone 1__-.___2-Ni t rophano 1 1————— 2 ;4-Di methyl phenol I--..---Banzo ic acid , iimii MII 1------bi»(2-Chloroethoxy)me thane __ 1————— 2 , 4-Dich lorapheno L _ .. _ 1————— Ir2 .4-Trich lorobenzene 1————— Naphtha lane 1— - —— 4-Chloroani 1 ina 1————— Haxachlarohutadiena 1————— 4-Ch loro-3-fliethylpheno 1 ____ 1— ——— 2-M«thylnaphthalena . ._., _. 1

————— 2 ,4,6-Tr iehlnroph«nal_, .. _l—— ---2 j.4r5-Tr iehloropheno 1 1————— 2-Chloronaphthal«n« 1__--_-2-Ni t roan i 1 ina mi 1_-_---Dim«thy Iphtha late wiin_ MII_ _l————— Acanaphthulana 1__ — — 2 T6-Dini t roto luene .__ ,._ 1

1

1111111111111111112111111211115411111111111111111111541154111111

1IDIU 'IDIUIUIUIUIUIUIJIUIU 1IU 1IJIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

64


• 1CSEMIUOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:



Level : < low/mod) LQUI

K Moisture: not dec. dec.

Extraction: (SepF/Cont/Sonc> CONT


Cont ract:

SAS No.: SDG No.:

Lab Sample ID: CA13.80C

Lab File ID: >G9Q16

Date Received: 09x29/89





99-09-2 -------83-32-9 — — ——51-28-5 ——————100-02-7 —————132-64-9 —————121-14-2 ————84-66-2 ——————7005-72-3 ————86-73-7 ——————100-01-6 —————534-52-1 —————86-30-6 ——————101-55-3 —————118-74-1 —————87-86-5 ——————85-01-8 ——————120-12-7 —————84-74-2 ——————206-44-0 —————129-00-0 —————85-68-7 ——————91-94-1 ——————56-55-3 —————218-01-9 —————117-81-7 —————117-84-0 ——— '--205-99-2 —— ---ofi7_no_o______50-32-8 —————193-39-5 —————53-70-3 ——————191-24-2 —————

--3-Ni t roan i 1 ine--Acenaphthene--2 . 4-Dini t roohenol--4-Ni t ropheno 1--Dibenzof uran--2 ,4-Dini t rota luene ,,. _— Dieth-jlohtha late--4-Ch lorophenyl-phenylether _--Fluorene „„_- - 4- N i t r o a n i 1 i n e ,„ , „--4,6-Dinit ro -2 -me thy Ipheno 1 _--N-Nitrosodiphenylamina Cl ) _--4-Bromophenyl-pheny let her __--Hexach Lorohenzane ,M_--Pant aehlarophano 1 mi ,.,_._,_, .--Phenanthrene ,,,._.--Anthracene— Di-n-hut«jlphthalate--Fluoranthene _..--Pyrena,. ,,.„„„.., ,—— Butylbenzylphthalate _— 3.3 '-Diehlorobenzidine—— BenzaCalanthraeene— Chrysane— bis(2-Ethylhaxyl )ph thai ate _— Di-n-octy Iphtha 1 a ta--Banzo tb) f luaranthana—— 9«nrn(k)f luaranthena--Banso Ca Ipyrana _,„-- IndanoCl .2 .3-cd )o«jpena--Dihanz (a .h ) anthracene--Ban*Qtqrhri Iparvlana

5411545411111111115454111111541111111111112211111111111111111111

IIU 1IUIU 'IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

(1) - Cannot be separated from Diphanylamine

FORM I SU -2 65 1/87 Rev

IFSEMIUQLATJLE ORGAN ICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

Lab Name:ETCNJ . Contract:

Lab Code: Case No.: SAS No.:

Ma t r i x: (soil/wa t e r)WATER

Sample wt/vol: 920.Q Cg/mDML

Level: ( low/med) LOU1

N Moisture: not dec._____ dec.____

Extract ion: (SepF/Cont/Sonc) CQNT

GPC Cleanup: CY/N) N pH:___

SDG No.:

Lab Sample 10: CA1380C

Lab File ID: >G9016




Dilution Factor: /

Number TICs found:CONCENTRATION UNITS:(ug/L or ug/Kg)UG/L

CAS

01.02.03.04.05.06.07.08.09.10.11.12.13.14.15.16.

NUMBER

141-78-6108-93-0108-88-3

116-02-9873-94-9

4536-23-6100-41-4

29943-42-8

,

11 COMPOUND NAME

lAcetic acid, ethyl esterICyc lohexeno 1IBenzene, methyl-t UNKNOWN1 Cyc lohexano I , 3 ,3 ,5-t r imethy1 Cyc lohexanone , 3,3,5-trimeth1 UNKNOUN1 UNKNOLJNIDi methyl-benzene isomer1 UNKNOWN!Tr ich loropropene isomer1 UNKNOWNIHexanoic acid, 2-methyl-1 Benzene, ethyl-1 UNKNOUN1 4H-Pyr«n-4-one , tet rahydro-111111 "1 '111ItIII

RT

5.327.684.436.5411.7311.407.9913.527.156.819.153.809.666.958.297.38

EST. CQNC

58036091564339312920201816109aa

iI' Q

usuuIJBuIJIJBIJIJ1 JIJB 1

1 JIJ1 J1 J1 J111111111 ...111111

FORM I SU-TIC 66

IBSEtl I VOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Coda: Case No.:

Ma t P i x: (soil/wa ten) WATER


Lave 1: C low/mod ) LQUI


Extraction: (SepF/Cont/Sonc) CONT


Cont ract:

SAS No.: SDG No.:


Lab File ID: >G9017



Deta Analyzed: 11/13/89



I108-95-2———————Phenol____________________I 11111-44-4———————bis(2-Chloroethyl )ether____11195-57-8————————2-Chlorophenol_____________111541-73-1———————1,3-Dichlorobenzene________111106-46-7——————1,4-Dichlorobenzene_______111100-51-6 ——————— Benzyl alcohol_____________11195-50-1 ——————— l,2-Dichlorob«nzena_______11195-48-7————————2-Methyl phenol_____________111108-60-1 ——————— bis(2-Chloroisopropyl)ether_lll106-44-5 ——————— 4-Methyl phenol_____________12621-64-7———————N-Ni troso-di-n-propy lamine_11167-72-1 —————— --Hexachlo roe thane___________I 1198-95-3————————Nitrobenzene_______________I 1178-59-1————————Isophorone_________________1288-75-5———————2-Nitrophenol____________111105-67-9——————2,4-Di methyl phenol________11165-85-0———————Benzoic acid_____________154111-91-1 ——————— bis(2-Chloroethoxy)me thane_I 11120-83-2 ——————— 2,4-Dichlorophenol_________I 11120-82-1———————1,2,4-Trichlorobenzene_____11191-20-3———————Naphthalene______________111106-47-8——————4-Chloroaniline___________11187-68-3————*——Hexachlorobutadiene________I 1159-50-7————————4-Chloro-3-methylphenol____11191-57-6————'———2-M*thylnaphthalene________I 1177-47-4———- ——Hexachlo roc yc lopentadiene__11188-06-2———————2,4,6-Trichlorophanol______11195-95-4——————2,4,5-Tr ich lorophanol______15491-58-7———————2-Chloronaphthalene_______11188-74-4————————2-Ni t roan i line_____________154131-11-3——————Dimethylphthalate_________111208-96-8———————Acenaphthylene_____________111606-20-2 ——— - —— 2,6-0 in itro toluene________111__ __ __ __ ____________________I

Q

IIUIUIUIUIUIUIUIUIUI 3IUIUIUUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

"67FORM 1 SU -1 1/87 Rev

' 1CSEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Leb Name: ETCNJ

Lab Code: Case No.:



Level: C low/mod) LQLJ

H Moisture: not dec. dec.

Extraction: CSepF/Cont/Sonc) CONT


Contract:

SAS No.: SDG No.:


Lab File ID: >G9017




Dilut ion Factor : 1


99-09-2——-----3-Nitroaniline.83-32-9 ————— ---Acenaphthene,_

______154______111______154______154______111______111______111

7005-72-3—————-4-Chlorophenyl-phenylether_I 1186-73-7————————Fluorene__________________I 11100-01-6 ——————— 4-Nitroani line_____________154534-52-1——- ——— 4,6-Oinitro-2-methylphenol_15486-30-6————————N-Nitrosodiphenylamine (1)_111101-55-3--------4-Bromopheny1-phenylet her__I 11118-74-1 —— ———— Hexach lorobenzene__________11187-86-5 ——————— Pent ach lorophenol_________15485-01-8- —— ————Phenanthrene____________120-12-7——— ——— Anthracene______________

51-28-5 ———————— 2,4-Dinitrophenol_VOO-02-7———————4-Nitrophenol____132-64-9 ——— ——Dibenzofuren_____121-14-2——————2,4-Dinitrotoluene.84-66-2 ——————— -D i e thy Iph thai ate__

__111__111__til__111__111__111__122__111__111

117-81-7——————bis(2-Ethylh«xyl)phthalate_111117-84-0———"———Oi-n-octylphthalate________111205-99-2——-———BenzoCb)f luoranthene_______I 11207-08-9——————BenzoCk)f I uo ran thane______11150-32-8———————BenzoCa)pyr«ne_____________,111193-39-5——————Indeno(l,2,3-cd)pyrene___53-70-3---------Dibenz(a,h)anthracene____

84-74-2————————Di-n-butylphthalate206-44-0———————Fluorenthene______129-00-0————85-68-7—————91-94-1—————56-55-3—————21B-01-9————

•Pyrene_______________•Butylbenzylphthalate_•3,3'-Dichlorobenz id in a,•Benzo(a)anthracene___•Chrysene_____________

191-24-2--------Benzo(g,h,i)perylane.

111111

(1) - Cannot be separated from Diphenylamine

FORM I SU -2

IUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUI

68 1/87 Rev

IFSEMI VOLATILE ORG^NICS ANALYSIS DATA SHEET

'TENTATIVELY IDENTIFIED COMPOUNDSEPA SAMPLE NO.



Matrix: (soi I/water ) WATER

Sample wt/vol: 920.0 (g/mL)ML

Level: (low/mad) LOUI

S Moisture: not dec. _____ dec. ____

Extract ion: (SepF/Cont/Sonc ) CONT

GPC Cleanup: (Y/N) N pH: ___

SDG No, :


Lab File ID: >G9017




Dilution Factor: J______

Number TICa found:CONCENTRATION UNITS:Cug/L or ug/Kg)UG/L

CAS NUMBER

01. 141-78-602. 108-93-003. 928-94-904. 108-89-305.06. 873-94-907. 116-02-908.09.10.11.12.13.lii. 1220? 11"11*. 29943-42-8'V

11 COMPOUND NAME

(Acetic acid, ethyl ester1 Cyc lohexano 112-Hexen-l-ol, (Z>-1 Benzene , methyl-l UNKNOUN1 Cyc lo hex an one, 3,3,5-trimethICyc lohexano 1, 3,3,5-trimethy1 UNKNOUN1 Dimethyl-benzene isomer1 Trichloropropene isomer1 UNKNOUN1 UNKNOUNI UNKNOUNireiiuuene, 1 (1 ..hyaVmry- thy 11 4H-Pyran-4-one , tet rahydro-l111111 *1 "11111111

RT

5.277.677.754.426.5511.3911.747.987.169.163.796.8213.47

7.39

EST. CONC

5602801701108535332521171714151 An8

• Q

JJJJBJJJBJJBJJJ-3— <rrJ


' IBaEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO.

Lab Name: ETC Corp.

Lab Code: Case No.:

Hat r ix : (so i 1 ''water ) WATER


Level: <low/mad) LOW

\ Moisture: not dec. dec.

Extract ion: tSepF/Cont/Sonc) SERF


Cont ract:

SAS No.: SDG No.:


Lab File ID: >G8656

Date Received: ^0/i/^

Date Extracted: 10x06/89




108-95-2 ——————— Phenol____________________110111-44-4——————bi»(2-Chloroethyl)ether____11095-57-8 ———————— 2-Chlorophenol_____________110541-73-1- ——— ---1 ;3-Dichlorobenzene________I 10106-46-7———— — -1,4-Dich lorobenzene-_-1______110100-51-6- —— — --Benzyl alcohol_____________I 1095-50-1 ——— — — -1,2-Dichlorobenzene_______11095-48-7————————2-Methylphenol_____________I 10108-60-1 — - ———— bis(2-Chloroisopropyl )ether_UO106-44-5 ————— --4-Methylphenol_____________I 10621-64-7--------N-Nitroso-d i-n-propylam me_I 1067-72- l---------Hexachlo roe thane__________11098-95-3- —— -- —— Nitrobenzene_______________I 1078-59-1- — ------Isophorone_________________I 1088-75-5 ———————— 2-Nitrophenol______________110105-67-9-——————2,4-Di methyl phenol_________11065-85-0 ——————— Benzoic acid_____________151111-91-1-———-—bis<2-Chloroethoxy)methane_t10120-83-2———————2,4-Dichlopophenol_________I 10120-82-1 ——— -——1,2,4-Tr ichlorobenzene_____I 1091-20-3————————Naphthalene________________I 10106-47-8-——————4-Chlopoani i me____________11087-68-3--—————Haxachlorobutadiene_______11059-50-7——————4-Chloro-3-mathyl phenol____11091-57-6———————2-Mathyl naphthalene_______11077-47-4—- ——— — Hexachlorocyc lopentadiene__I 1088-06-2--- ————— 2,4,6-Tpichlorophenol______11095-95-4- — ————— 2,4,5-Trichlorophenol______15191-58-7———— ——— 2-Chloronaphthalene_______11088-74-4————————2-Ni troani 1 ine_____________15113l-ll-3--------Oimethylphth«late I 10208-96-8--- — —— Acenaphthylene____________110606-20-2 — ---- — 2,6-Dinitrotoluene_________I 10

IUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU


1L3EMIUOLATILE ORGANICS ANALYSIS DATA SHEET

iruc. rsu,

Lab Name: ETC Corp. .

Lab Code: Case No.:

Matrix: (soiiXwater) WATER




Extract ion: (SepF/Cont/Sonc> SERF


Contract:

SAS No.: SDG No.:


Lab File ID: >G8656

Date Received:





99-09-2 ———————— 3-Nitroanil me_____________15183-32-9- ——— ——— Acenaphthene,_____________I 1051-28-5 ———————— 2,4-Dinitrophenol__________151100-02-7- —————— 4-Nitropheno 1______________151132-64-9 — — - —— Dibenzofuran_______________110121-14-2 ——————— 2 .4-Dinitrotoluene ______I 1084-66-2 — - ————— Diethylphthalate___________1107005-72-3- — -- — 4-Chlorophenyl-phenylether_I 1086-73-7————————Fluorene_______________ 110100-01-6 ——————— 4-Nitroani 1 ine_____________151534-52-1 ——————— 4,6-Dinitro-2-methylphenol_15186-30-6- — ————— N-Nitrosodiphenylamine (1)_110101-55-3--------4-BromophenyI-pheny1 ether__110118-74-1---- —— -Hexachlorobenzene__________1 1087-86-5- ——— — — Pentach loropheno 1__________15185-01-8 ———— —— Phenanthrene_____________110120-12-7———————Anthracene_________________11084-74-2- — ———— Di-n-butylphthalate_______110206-44-0———————F luoranthene_______________I 10129-00-0———————Pyrene____________________I 1085-68-7————————Butylbenzylphthalate_______I 1091-94-1————————3,3 '-Dichlorobenzidine_____12056-55-3-- ————— B»nzo(a>*nthracene________110218-01-9-—————Chryaene_________________110117-81-7———————bi»(2-Ethylhexyl)ph thai ate_110117-84-0——————Oi-n-octylphthalate_______110205-99-2——————Benzo(b)f luoranthene______110207-08-9 ——— ——— BenzoCk)fluoranthene_______I 1050-32-8-- ———— -BenzoCa)pyrene___________110193-39-5———————Indeno(l,2,3-cd)pyrene_____11053-70-3 — — ———— DibenzCa ,h>anthracene______110191-24-2- — -----Benzo(g,h , i )perylene______110

IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIU


FORM I SO -2 1/87 Rev

IFSEMI VOLATILE ORGANICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

Lab Name:ETC Corp,

Lab Code: Case No.:

Ma t r i x: (soil/wa t e r1 WATER


Level: Clow/med) LOW

S Moisture: not dec. _ dec.___

Extraction: CSepF/Cont/Sonc) SEPF


Number TICa found: 7

Cont ract:

SAS No.: SDG No.:


Lab File ID: >G8656

Date Received:



Dilution Factor: _/


CAS NUMBER

01. 872-50-402.03. 149-57-504. 108-88-3

COMPOUND NAME

2-Pyrro I id inone , 1-methyl- CUNKNOWN , •Hexanoic acid, 2-ethyl- C8CIBenzene , methyl- C9CI )

RT

10.245.24

12.363.14

EST. CONC

110100198

Q

JJBJJB

FORM I SU-TIC 1/87 Rev

72

' ISSEMIVOLATILE ORGANIC^ ANALYSIS DATA SHEET

SAMPLE NO

Lab Name: ETC Corp.

Lab Code: Case No.:



Level: (low/med) LOU


Extract ion: (SepF/Cont/Sonc) SERF

GPC Cleanup: rY/N> N pH:

Cont ract:

SAS No.: SDG No.:


Lab Fi Le ID: >GS657

Date Received: '&***!


Date Analyzed: 10713/89


CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg> UG/L

108-95-2 —————— Phenol__________________110111-44-4———————bis(2-Chloroethyl Jet her____11095-57-8- — - ———— 2-Ch lorophenol_____________I 10541-73-1———————1,3-Dich lorobenzene________110106-46-7——— —— -l,4-Dichlorobenzene_^______I 10100-51-6--- ———— Benzyl alcohol____________11095-50-1 — - — ----1,2-0ich lorobenzene________I 1095-49-7————————2-Methyl phenol_____________110108-60-1-—-———bisC2-Chloroisopropyl)ether_l10106-44-5 ——————— 4-Methyl phenol_____________I 10621-64-7- — ————N-Ni troso-di-n-propy lamine_I 1067-72-1 ————— - — Hexachlo roe thane___________I 1098-95-3 ——— -- —— Nitrobenzene_____________11078-59-1---------Isophorone_________________I 1088-75-5 ———————— 2-Nitrophenol______________110105-67-9 —— ———— 2,4-Di methyl phenol_________11065-85-0- —— - — — Benzoic acid_____________152111-91-1———-——bisC2-Chloroethoxy)methane_110120-83-2 ——————— 2,4-D ich lorophenol_________110120-82-1———————1,2,4-Tr ich lorobenzene_____I 1091-20-3———————Naphthalene______________110106-47-8-——————4-Chloroani 1 ine____________I 1087-68-3—-—----H«xachIorebut adiana_______11059-50-7——•'—————4-Chloro-3-me thy! phenol____11091-57-6———————2-hethylnaphthalene_______11077-47-4- —————— Hexachlorocyelopentadiene__11088-06-2 ———————— 2,4,6-Tr ich lorophenol______11095-95-4————————2,4,5-Tr ich lorophenol______15291-58-7———————2-Chloronaphthal«ne_______11088-74-4————————2-Nitroini 1 ine_____________152131-11-3 —————— Dimethylphtha late_________110208-96-8--- — - — Acenaph thy lane_____________1 10606-20-2 —————— 2,6-Dinitro toluene________110

iuIUIUIUIUIUIUIUIUIUIUIUIUIUIU1UIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI_

FORM I SY -1 1/97 Rev.

1CSEMIUQLATILE ORGAN ICS ANrtLVSIS DATA SHEET

SAMPLE NO

Lab Name: ETC Corp. •

Lab Coda: Case No.:

Matrix: tsoiI/water) WATER

Sample wt/vol: 960.0 (g/mL> ML



Extraction: (SepF/Cont/Sonc) SERF

GPC Cleanup: (Y/N) N PH:

Cont ract:

SAS No.: SDG No.:


Lab File ID: >G8657

Date Received:





(1) - Cannot be separated from Diphenylamina

FORM I SU -2

Q

11 99-09-2 -----83-32-9 ————51-28-5 — ——100-02-7 ———132-64-9 —— -121-14-2 ———84-66-2 -----7005-72-3 ——36-73-7 ———— •100-01-6 - ——534-52-1 ——— -86-30-6 ————1 m -<55-?----.118-74-1 ——— •87-86-5 ———— -85-01-8 ———— •120-12-7 ——— -84-74-2 ———— •206-44-0 ——— -129-00-0 ——— -85-68-7 ———— •.91-94-1 ———— -56-55-3--; —— •218-01-9 ——— •117-81-7 ——— •117-84-0 ——— -205-99-2 ——— -207-08-9 ——— -50-32-8 ———— -193-39-5 ——— -53-70-3 ———— -191-24-2 ——— -

----S-Nvtraani 1 me----Acanaphthene----2,4-Dinitrophenol.. I----4-Nitrophenol 1----Dihenzofurann |----2 t4-Dini t rato luene • 1——— Disthylphtha 1 a t a _, . _ 1____4-Ch loropheny 1-pheny let her _ 1----Fluorene 1,___4_Ni t roan i 1 ine , ,,_,,. ,,.,., 1----4,6-Dini tro-2-methylpheno 1 _ 1----N-Ni t rosodipheny lamine C 1) _ 1----4-Bromophenyl-pheny lether____l----Hexachlorobenzene 1.---Pentach loropheno 1 1----Phenanthrene 1----Anthracene^ ,, _MII 1——— Di-n-butylphthalate., ..,_ , ,,BI 1----Flunranthena _ „ t----Pyrane ,„,, 1——— But ulhanzvjlphtha late I----3P3'-Oiehlarobenzidina 1——— BanTo(a)anthracene 1— — ChrV*en*._, .,._ I——— bis(2-Ethylhexyl )phthalate _ 1• ---Di-n-oct-jlphtha late 1----Benio(h ) f Luoranthena 1----SenTQ Ck ) f 1 uo ran thane I.- — Banzo (« )pyrene „ .., ._in 1.---Indanofl r2r3-cd ip-jrane 1._ — Dibanzfa .hlanthraeena 1.,__BenzQtgrh . i iparulena 1

5210525210101010105252101010521010101010102110101010101010101010

1IUIUIUIUIUIUIUIU 'IUIUIUIUIUIUIUIUIUIUIUIUIUIUIU .IUIUIUIUIUIUIUIUIU1

741/87 Rev

IFSEMIUOLATILE ORGAN ICS ANALYSIS DATA SHE.ET

TENTATIUELY IDENTIFIED COMPOUND*

EPA SAMPLE NO.

Lab Name:ETC Corp.

Lab Code: Case No.:

Matrix: CsoiI/water)WATER


Level: < low/med) LOUI

S Moisture: not dec._____ dec.___

Extract ton: (SepF/Cont/Sonc> SEPF

GPC Cleanup: (Y/N) N pH:___

Cont ract:

SAS No.: SDG No.:


Lab File ID: >G8657

Date Received: S0/3frf



Dilution Factor: '

Number TICs found:CONCENTRATION UNITS:Cug/L or ug/Kg)UG/L

CAS NUMBER

01.02. 108-88-3

,

COMPOUND NAME

UNKNOUINBenzene , methyl- C9CI )

RT

5.273.13

EST. CONC

9110 . -

Q

JBJB

FORM I SU-TIC75

1/97 Rev

IBSEMIY0LATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NQ

Lab Name: ETCNJ

Lab Code: Case No.:


Sample wt/vcl: 970.0 Cg/mL) ML

Level: (low/med) LOUJ

S *1o i s t u r e : not dec. dec.

Extraction: tSepF/Cont/Sonc) SERF

GP!.: Cleanup: (Y/N) N pH:

Contract: I___

SAS No.: SDG No.:

Lab Sample ID:

Lab File ID: >GS836

Date Received: lO/OV."*!1*


Date Analyzed: 10/28/S'?


CAS NO. COMPOUNDCONCENTRATION UNITS:tug/L or ug/Kg) UG/L

1Q8-95-2 ——————— Phenol____________________111-44-4———————bis(2-Chloroethyl >ether____95-57-8 ———————— 2-Chlorophenol_____________54l-73-l--------l,3-Dichlorobenzene________106-46-7--------l,4-Dichlorobenzene_______100-51-6---- ——— Benzyl alcohol_____________95-50-1 ——————— 1,2-Dich lorobenzene_______95-48-7————————2-Methyl phenol_____________108-60-l--------bia(2-Chloroisop ropy 1)ether_106-44-5 ——————— 4-Methyl phenol_____________621-64-7--------N-Nitroso-di-n-propylam me__67_72-l---------Hexachloroethane98-95-3 — —— ——— Nitrobenzene_______________78-59-1---------Isophorone88-75-5————————2-Nitrophenol______________105-67-9 —— ————2,4-Di methyl phenol_________65-85-0——--- — -Benzo ic ac id_______________111-91-1———————b is C2-Chloroethoxy)methane_120-83-2—-—-—2,4-Dichlorophenol_________120-82-1——————1,2,4-Tnch lorobenzene_____91-20-3————————Naphthalene_______________106-47-8———————4-Chloroani 1 ine____________67-68-3------ — -Hexachlorobutad iene________59-50-7— ————— -4-Ch loro-3-methyl phenol____91-57-6 ———————— 2-Methyl naphtha lane________77-47-4---------Hexachlorocyclopentad iene_88-06-2 ——— ———— 2,4,6-Trich lorophenol______95-95-4————————2,4,5-Trichlorophenol______91-5Q-7-—————2-Chloronaphthalene________88-74-4- — -- —— -2-Nitroani1 me_____________131-11-3 — — ——— Dimethylphthalate__________208-96-8 ——— — — Acenaph thy Iene_____________6 06-2 0-2--—————2,6-Dmitro toluene_________

101010101010101010101010101010105210101010101010101010521052101010

Q

IUIUIUIUIUIUIUIU!UIUIUIUtuIUIUIUIUIUIUIUIUIUiUIUIUIU:UIUIUIUIUIUIUI

76FORM I SU -1 1/87

N

1CSEMIUQLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Cont ract:

SAS No.:

fla t P i x : (soil /wa t e r ) UATER


Level: ( low/med) LOLJ

J not dec. dec.

Extraction: (SepF/Cont/Sonc > SERF

GRi: Cleanup: (Y/N) N pH:

SDG No.:

Lab Sample ID: CA189P-',

Lab File ID: >G3336

Date Received: 10/05 'b"*



Dilution Factor: 1


99-09-2 ———————— 3-Nitroani 1 ine_____________15283-32-9 —— - — - — Acenaph thane_______________I 1051-28-5 ———————— 2,4-Dinitrophenol__________152100-02-7--- —— — 4-Ni trophenol______________152132-64-9---- ——— Dibenzofuran_______________I 10121-14-2 ——— - —— 2,4-Dinitro toluene_________I 1084-66-2 ———— - —— Die thy Ipht ha late___________I 107005-72-3 —————— 4-Ch lorophenyl-phenylether_I 1086-73-7————————Fluorene__________________I 10100-01-6--- ——— ~4-Nitroani 1 me_____________152534-52-1--——-—4J6-Dinitro-2-melhylphenol_15286-30-6 — -------N-Nitrosodiphenylamine CD_I 10101-55-3--------4-Bromophony1-phenylether__I 10118-74-1 —————— -Hexach lorobenzene__________I 1087-86-5- ———— — -Pentach lorophcnol__________15285-01-8--————— -Phenanthrene_______________110120-12-7- —————— Anthracene________________I 1084-74-2 ——— — ——Di-n-butylphthalate________I 10206-44-0 ——————— Fluoranthene_______________I 10129-00-0 ——————— Pyrene____________________11085-68-7————————Butylbanzylph thai ate_______I 1091-94-1 ———————— 3,3 '-Dichlorobenzidme_____12156-55-3 ———————— Benzo(«)anthracene_________1 10218-01-9———————Chryaene__________________I 10117-81-7———————bia(2-Ethylhexyl Jphtha.late_1 10117-84-0 — — ——— Di-n-octylphthe late________I 10205-99-2 —————— BenzoCbJf luoranthene______HO207-08-9 — --———BenzoCk)f luoranthene_______HO50-32-8- ——————— 8enzoCa)pyrene_____________110193-39-5———————Indeno(l,2,3-cd)pyrene_____I 1053-70-3- —————— -OibenzCa ,h )anthracene______I 10191-24-2 — -- ——— Benzo(g,h,i Jperylene_______I 10

tuIUIUIUIUIUIUIUIUIUIUIUIUIU:UIU!UIUIUIU!UIUIUIUIUIUIUIUIUIUiUIU

(1 ' - Cannot be separated from Diphenylamine

FORM I SU -2 77 1.--37 Re

IFSEMIUDLATILE ORGAN ICS ANALYSIS DATA SHEET


ERA SAMPLE NO.'


Lab Code: Caae No.: SAS No.:

Matr ix: Caoi1/water)WATER

Sample wt/vol: 970.0 (g/mDML

Level : C low/mod) LOU)

\ Moiature: not dec._____ dec.___



Number TICa found: *

SDG No.:


Lab File ID: >G8836y

Date Received: 1G/09V89

Date Extracted: 10x07''S


Dilution Factor: i


CAS NUMBER

01.

COMPOUND NAME

UNKNOWN

RT

7.52

EST. CONC

44

Q 1

JB 1

1

1

1

1

1

1

1:1;1

!

1

1

1

!

1

FORM I SU-TIC 7B ,..,

IBSEMIUGLATILE ORGANICS ANALYSIS DATA SHEET

ERA SAMPLE NO,

Lab Name: ETCNO

Lab Code: Case No.:

Ma t rix: (soil/wa t e r) WATER


Level: Clow/mod) LQU

S f"lo iature: not dec. dec.

Extraction: (SepF/Cont/Sonc) SEPF

GPV.: Cleanup: (Y/N) N pH:

Cont pact:

SAS No.: SDG No.:


Lab File ID: >G8837

Date Received: lO/QJ^vS'-1




*ra


79

Q

108-95-2-111-44-4-95-57-8 —541-73-1-106-46-7-100-51-6-95-50-1 —95-48-7--108-60-1-106-44-5-621-64-7-67-72-1 —98-95-3--73-S9-1--88-75-5--105-67-9-65-85-0 —111-91-1-120-83-2-120-82-1-91-20-3—106-47-8-87-68-3—59-50-7--91-57-6 —77-47-4--88-06-2--95-95-4--91-58-7--8S-74-4--131-11-3-208-96-8-606-20-2-

— ——— -Pheno 1— —— --bis(2-Chloroethyl Jet her _____-__-__2-Ch loropheno 1-------1 .3-Dich lorobenzene_-__.__! .4-Dichlorobanzene_.__-__ Benzyl alcohol--- —— -1 .2-Dich lorobenzene_._ — — 2-Methvlphenol-------bis(2-Chloro i sop ropy 1 )ether__._____4_|-|ethy Ipheno 1------- N-Nitroso-d i-n-propy lamine_ __ _ _ _ _ _ _ Hexach loroe thane_ _ _ _ _ _ _ N i treabanzene------- laophorone------ -2 -N i t ropheno 1-------2 ,4-Dimethylphenol-- — ---Banzoic acid,

—————— 2 r4-Dichloroph«nol--- — --1 .2.4-Trich lorobenzene—————— Naphtha lane__iiini-- —— —4-Chloroan i 1 me——— ---Haxach lorobutadiene------- 4- Ch loro-3-methylpheno 1_._ — --2 -Methyl naphtha lane-------Hexach lorocyc lopentad lene___- — -2 .4r6-Trich lo ropheno 1-_--_-_2 .4.5-Trich loropheno 1-------2-Ch Inronaphtha lane—— ——— 2-Nitroaniline——— ———— dimathylphthalate, , ,_., , „ ,„__--_-_ Acenaph thy lene„__„__. 7 jA-Dini t roto lu«n«M.Bii ,_., , . „

11111111111111111141111111111115711111111111111111111571157111111

1 tIU :IU 1!U -t !IU 1!UIU 1!U :IU . 11U !IJ 1!UIU 1IU iIU 1!UIU 1!U :IU 1IU :IU 1IUIU 1IU :IU 1:UIU 1IU :IU 1IUIU 1tuIU 1!U i1 1

FORM I SU -1 1/87 Re

1CSEN I VOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.t



Level: Clow/med) LOU

S l"!o isture: not dec. dec.

Extraction: (SepF/Cont/Sonc> SERF


Contract:

SAS No.: SDG No.:

Lab Sample ID: CA1896::

Lab File ID: >G3837

Date Received: 10/09V39




NO. COMPOUNDCONCENTRATION UNITS:<ug/L or ug/Kg) UG/L

99-09-2 ————83-32-9 ————51-28-5 ———— -100-02-7 ———132-64-9 ——— -121-14-2 ——— -84-66-2 ————7005-72-3 —— -86-73-7 ————100-01-6 ——— -534-52-1 ——— -86-30-6 —— — -101-55-3 ——— -118-74-1 ——— -87-86-5 ———— -35-01-8 ———— -120-12-7 ——— -34-74-2 ———— -206-44-0 ——— •129-00-0 ——— -85-68-7 ———— -91-94-1 ———— -56-55-3 ———— -218-01-9 ——— -117-81-7 ——— •117-84-Q ——— -205-99-2 ——— -207-08-9 ——— -50-32-8 ———— -193-39-5 ———53-70-3 ———— -191-24-2 ——— -

1----3-Nitroanilina 1----Acenaphthene 1----2 ,4-Din 1 1 ropheno 1 1.---4-N! t ropheno 1 1----Dibenzofuran t--— 2.4-Dinitrotoluana 1——— Diethylphthalate^ . 1----4-Ch lorophenyl -ph any let her _ 1----Fluorene. ,„ 1- — -4-Ni t roan i 1 ina 1-- — 4,6-Dinitro-2-methylpheno 1 _ 1-— -N-Nitrosodiphenylamine (1 ) _ J- — -4-8romopheny 1-pheny let her __ 1-- — Hexachlorabenzena 1-— -Pentach lo ropheno 1 1----Phenanthrena 1----Anthracene,.,,. ,. 1. ——— Di-n-hutylphtha late 1...-Fluor an thane 1. — .Pyrane ,„_ ,„ 1- — -Butyl hanzwlph thai ate 1——— 3 r3 '-Dichlorohanzidina t--.-8anzn(a)«nthr*cana_ immm . . ,1• -— Chrysene 1—— -bi»<2-Ethylhexyl)phtha late _ 1. ——— Di-n-octylphthalata 1-- — Banzafb IflLjoranthana 1----BenzoCk)fluar*nthane I.---Banzei (a )pyrana , ,._ r , .. I----IndanoCl .2 r3-ed ) pur en* 1- — -Dibenz ta .h )anthracene 1- — -Ben ro Co .h . i )p«r«jlane 1

1

5711575711111111115757111111571111111111112311111111111111111111

1iUIUIU .IU *iUIUtuIUIUIUIUIU;uIU!U1U:UIU!UIUIUIUiUIUIUIUIUIU

IUtuIU1

ClJ - Ca-->not be separated from Oiphenylamine

FORM I SU -2 1 -'37 Re'

IFSEMIUOLATILE ORGANICS ANALYSIS DATA SHEET


EPA SAMPLE NO.


La>> Code: Case No.: SAS No.:

Matr ix: Cso iI/water)WATER

Sample wt/vol: 870.0 Cg/mL)ML


S -oiature: not dec,_____ dec.____


GP:_ Cleanup: CY/N) N pH:____

Number TICs found: If

SDG No.:

Lab Sample ID: CA189;1::

Lab File ID: >G8837

Date Rece i ved : 10/Q5*/'-''J


Date Analysed: 10/28-''L-"J

Dilution Factor: I..


CAS NUMBER

01. 116-02-902. 108-88-303. 873-94-904.05.136 .07. 100-41-4OS. 49S-81-709. 20324-32-710.11.

COMPOUND NAME

Cyc lohexano 1, 3,3,5-trimethyBenzene, methyl- C9CI)Cyc lohexano no, 3,3,9-trimethDimethyl-benzene isomerDimethyl-benzene isomerUNKNOWNBenzene, ethyl- C9CI9CI)Cyc lohexanemethanol, .alpha.2-Propanol , 1- (2-me thoxy- 1-mUNKNOWNUNKNOWN

RT

12.895.5312.588.318.927.548. 0914.9211.6711.774.65

EST. CQNC

2602602501207569502113119

1|. Q

1 JIJ1 J1 J1 Juei juuuuiiiiiitiiiiiiiiiiiii

FORM I SU-TIC 0 I i/a?Rev.

IB EPA SAMPLE NO,SEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET

tab Name: ETCNJ

Lab Coda: Case No.:

Matrix: CsoiI/water) WATER

Sar.iple wt/vol: 910.0 (g/mL) ML


S MO i s t u r e : not dec. dec.



CAS NO. COMPOUND

Cont ract:

SAS No.: SOG No.:

Lab Sample ID: CA189T1::

Lab File ID: >G3838

.JDate Received: 10/05VS?

Date Extracted: 10/07/39 "

Date Analyzed: li3/23/Sv

Dilution Factor: 1


108-95-2 - ——111-44-4 ————95-57-8 ————541-73-1 ———106-46-7 ———100-51-6 ———95-50-1 ————9*5-48-7 ————108-60-1 ———106-44-5 ———621-64-7 ———67-72-1 ————98-95-3 ————78-59-1 ————88-75-5 ————105-67-9 ———65-85-0 ————111-91-1 ———120-83-2 ———120-82-1 ———91-20-3 ————106-47-9 ———87-68-3 ————59_Sn_7__,.__91-57-6 ————77-47-4 ————

95-95-4 ————Q i EQ -y _ _

83-74-4 ————131-11-3 ———208-96-8 ———606-20-2 ———

----Phonal——— bis(2-Chloroethyl ) ether ________2-Chlarophanal ,.----1 .3-Dichlorobenzone_-__! r4-Oieh lorabenzene----Benzyl alcohol. ,.----1 f 2-Dieh lorobenzena. ——— 2-MBthylpheno 1——— bi»(2-Chloro iaopropyl )ether__-__4-Met hy Ipheno 1 , , ,„----N-Nitroso-di-n-propylam ine___---- He xachloroe thane--__Ni t robanzena „----Isophorona----2-Nit rnphano 1——— 2 r 4-D i ma thyl phenol----Benzoie acid----bi*C2-Chloroethoxy ) me thane _ .——— 2,4-Oieh lorophano 1——— 1 .2 r4-Tr ich lorobenzene— --Naphthalene_- — 4-Ch loroan i 1 ina----Havaehlornhutadiana ,_, _--__4-Ch loro-3-methylpheno 1 ____——— 2-M«thyl naphthalene----Hexach lorocyc lopantad lane __----2f4j.6-Trieh loropheno 1----2.4;5-Trieh lornpheno 1_--_9-rh loronaph thai ana- ——— 2-Nitrnaniline,----Dimwthylphthalate----Ae^naphthy lane _ nn . , „———— O^-Dinitrntoluana

11111111111111111221111111111111111111111111111111111551155111111

1 1U :IU 1IU " :IU 1IU itu iiu ;IU tIU '•\ \IUIU 1IU '•IU 1IU :IU 1! J :IU 1IU :IU 1IU iIU 1IUIU 1!UIU 1:U :IU 1!U 'IU 1'U 'IU - IIU1 1

82FORM I SU -1 •S? R*

- 1CSEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:



Level: Clow/mad) LOW

Cont ract:

SAS No.: SDG No.:


Lab File ID: >G8338*J

Date Received:

9J i"io i sture : not dec. dec.

Extraction: ( SepF/Cont /Sonc ) SEPF

Qpr Cleanup: (Y/N) N pH:

CAS NO. COMPOUND



Dilution Factor: 1


99-09-2 ———————— 3-Nitroani 1 me_____________15583-32-9- ——— -- — Acenaphthene_______________I 1151-28-5 — --- ——— 2,4-D;ni trophenol__________155100-02-7- ——— —— 4-Ni trophenol______________155132-64-9 — — ———Dibenzofuran_______________I 11121-14-2 ——————— 2,4-Dinitrotoluene_________I 1184-66-2 — -- ———— Qiethylphthalate___________I 117005-72-3——-——4-Chlorophenyl-phenylether_t1196-73-7- ——————— Fluorene__________________I 11100-01-6 ——————— 4-Nitroani 1 me_____________155534-52-1 —— -- —— 4,6-Dmitro-2-methylphenol_15586-30-6- — — -- — N-Nitrosodiphenylamme (1)_111101-55-3 — - ———— 4-Bromophenyl-phenylether__I 11118 -74-1 ------ --He xach lorobenzene__________i 1187-86-5- —————— -Pentachloropheno 1__________1558*5 -01-3 — —— - — -Phenan throne_______________111120-12-7——————Anthracene________________I 1184-74-2 — ———— — Di-n-butylph thai ate________I 112 06-44-0———————Fluoranthene_______________t 11129-00-0———————Pyrene____________________11185-68-7————————Sutylbeniylphthalate_______I 1191-94-1 ——————— 3,V-Dichlorobenzidine_____12256-55-3————————Benzo(a)anthracen«_________t 11218-01-9———————Chrysene__________________I 11117-81-7——————-bia(2-Ethylhexyl )phthalate_I 11117-84-0 ——— ——Di-n-octylphth«late_______111205-99-2 ——————— BenzoCb)f luoranthane_______I 11207-08-9 ————— —BenzoCk)f luoranthene_______I 1150-32-8---------8enzo(a )pyrene____________I 11193-39-5———————Indeno(l,2,3-cd)pyrene_____I 1153-70-3 —— —— —— Dibenz(a,h) anthracene_____I 11191-24-2 ——————— Benzo(g,h, i )perylene_______I 11

(1) - Cannot be separated from Diphenylamme

FORM I SU -2

IUIDIDIUIUIU!UIU"UIUIUIU!UIUIUIU'UIUIUIU!UIU:UIUtUIU!UIU!UIUIUIU

83 I-'37 P*

IFSEMIUOLATILE QRGANICS ANALYSIS DATA SHEET


ERA SAMPLE NO.

Lab Name:ETCNJ

Lab Code: Case No.:


Savple wt/vol: 910.0 (g/mDML

Level : t loui/med) LOW

S *io i sture! not dec. __ dec . ____

Extract ion: CSepF/Cont/Sonc) SEPF

GF:": Cle.mup: (Y/N) N pH:___

TICa found: />

Cont ract:

SAS No.: SDG No.:

Lab Sample ID: CA189?:::

Lab File ID: >G3838

Date Received: 10/Q*/:-:v


Date Analyzed: 10/28/':'J

Dilution Factor: ..._/____


CAS

01.02.03.04.05.06.

It?13.'I*.1-

NUMBER

928-94-9108-88-3116-02-9

873-94-998-99-5

108-10-1626-93-710C-41-4109-52-4

COMPOUND NAME

2-Hexen-l-ol , CZ)- (8CI9CI)Benzene, methyl- (9CI)Cyc lohexanol, 3,3,5-trimethyUNKNOWNCyc lohexanone, 3,3,5-trimethCyclohexanecarboxylic acid (UMUMQUM ———UNKNOWNDime thy 1 -benzene isomer2-Pentanone, 4-methyl- (8CI92-Hexanol (8CI9CI)Bonzene, ethyl- (8CI9CI)Pentanoic acid (9CI)

RT

8.885.5212.888.9412.5814.69

7.538.314.855.368.088.51

EST. CQNC

120031017017016085

746362362625

1: Q 1

J :J IJJ 1J :J I

JB 1

J 1J :J 1J

1

1

1

1

]

1

1

1

1

''4

FORM I SO-TIC 84 1/87 Rev.

IBSEMIUOLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO

Lab Name: ETCNJ

Las Code: Case No.:

Cont ract

SAS No.

Matrix: tsoil/water) UATER


Level : ( low/med) LOUI


Extraction: CSepF/Cont/SoncJ SERF

GFC Cleanup: (Y/N) N pH:

SOG No.: •

Lab Sample ID: CA215e:_:

Lab Fi le ID:' >G3339

Date Received: 10/05-'?'



Dilution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:<ug/L or ug/Kg) UG/L

1P8-95-2——————— Phenol____________________111*44-4——---—bis(2-Chloroethyl)ether____95-57-8————————2-Chlorophenol_____________541-73-1-—————1,3-Dichlorobenzene________106-46-7———>-- — 1,4-Dichlorobenzene________100-51-6 ——————— Benzyl alcohol_________'95-50-1 — ————— -1,2-Oich lorobenzene________95-48-7————-- — 2-Methyl phenol_____________108-60-1----———bis<2-Chloroisopropyl)ether_1C6-44-5 ——————— 4-Methyl phenol_____________621-64-7--------N-Nitroso-di-n-propylam me_67-72-1---------Hexachloroet hane98-95-3 —— - ——— -Nitrobenzene_______________78-59-1 ———— ——— Isophorone________________88-75-5--- ————— 2-Ni tropheno 1______________105-67-9 ———— - — 2,4-Dimethyl phenol_________65-85-0---------8enzoic acid_______________111-91-1———————b is (2-Chloroethoxy)methane_120-83-2-——————2,4-Dichlorophenol_________120-82-1———————1,2,4-Trich lorobenzene_____91-20-3———————Naphthalene______________106-47-8———————4-Chloroani 1 ma____________87-68-3—---———Hexachlorobutad iene________59-50-7——— ———— 4-Chloro-3-methyl phenol____91-57-6—————--2-MethylnaphthaIene_______77-47-4---------Hexachlorocyclopentadiene_88-06-2- —— ———— 2,4,6-Tr ichloropheno 1______95-95-4——————--2,4,5-Tr ichloropheno I______91-58-7——--———2-Chloronaphth«lene________83-74-4—— — ——— 2-Nitroani 1 ine_____________131-11-3——--——Dimethylphthalate_________208-96-8- ——— —— Acenaphthylane_____________606-20-2 —— -- —— 2,6-Dm i tro toluene_________

FORM I SVJ -1

11111111111111111111111111i:111153111111111111111111115311531111

111

85

I1UIU!UIUIUIUIUIUiUIU!UiuIUIU!UIU!UIUIUIUIUIU!UIUIUIUIUIU:UIU!UIUIU

1/37 9e

1CSEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Cont ract:

SAS No.:

Matrix: (5011/water) WATER

Sample ul/vol: 950.0 (g/mL) ML



Extraction: (SepF/Cont/Sonc> SEPF

GPC Cleanup: <Y/N) N pH:

SDG No.:


Lab File ID: >G8939

Date Received: 10x05/8*


Date Analysed: 10/28/3*



II 99-09-2 ——— - ——— 3-Nitroani 1 ine_____________83-32-9 ———————— Acenaphthene_______________51-28-5 ———————— 2,4-Dinitrophenol__________100-02-7- —————— 4-Ni trophenol______________132-64-9 —————— -Dibenzofuran_______________121-14-2—-————2,4-Dinitrotoluene_________84-66-2 — —————— Diethylphthalate___________7005-72-3—————4-Chlorophenyl-phenylether_86-73-7- ——————— Fluorene__________________100-01-6- ———— — 4-Ni troani1 ine_____________534-52-1--————4,6-Oinitro-2-methylphenol_86-30-6---------N-Nitroaodiphenylamine (1)__101-55-3--------4-Bromopheny1-phenylether__119-74-1-——————Hexachlorobenzene__________87-86-5---------Pentachloropheno 1__________85-01-8- ——— ——— Phenanthrene_______________120-12-7———————Anthracene________________84-74-2 ——————— -Oi-n-butylphthalate________206-44-0—---——Fluoranthene_______________129-00-0———————Pyrene______;_____________85-68-7————————Butylbenzy lphth*late_______91-94-1 ———————— 3,3 '-Dichlorobenzid ine.;_____56-55-3————————9«nzo(a)anthracene_________218-01-9————-—Chrysene__________________117-81-7———————bis(2-Ethylhexyl )phthalate_117-84-0———————Di-n-octylphthalate________205-99-2 ——————— Benzo(b)f luoranthene_______207-08-9———-——BenzoCk)fluoranthene_______50-32-8---------Benzo Ca Jpyrane^,___________193-39-5———————Indenotl,2,3-cd)pyrene_____53-70-3———--—-0ibenzCa,h)anthracene______191-24-2 ——————— Benzotg^h,! )perylene_______

5311535311111111115353111111531111111111112111111111111111111111

Q

IIUIUIUIUIUIUIUIU!UI LiIUIU!UIUIU1UIUIUIUIU•uIU!UIU!UIU!UIUIUIUtuIU

(1J - Cannot be separated from Diphenylamine

FORM I SU -2 86 1.-37 Re

IFSEMIUOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COnPOUNDS

ERA SAMPLE NO.



Matrix: (aoi1/water)WATER

Sample wt/vol: 950.Q (g/mL)ML


\ -o i sture: not dec. _ ._ ...... dec .


CPC Cleanup: CY/N) N pH:___

Number TICa found:

SDG No.:

Lab Sample ID: CA213e:-

Lab File ID: >G3839

Date Received: lQxQ5/:T"J

Date Extracted:10/a7/89

Date Analyzed: 10/28/S0

Dilution Factor: I____


CAS NUMBER

01.

COMPOUND NAME

UNKNOWN

RT

7.53

EST. CONC

53

. Q

JB

FORM I SU-TIC 37 1/87 Rev.

IBSEMIVOLATILE QRGANICS ANALYSIS DATA SHEET

EPA SAMPLE .NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: tsoil/water) WATER


Le-;el : < lou/med) LQUI


Extraction: ( SepF/'Con t/Sonc ) SEPF


Cant ract:

SAS No.: SDG No.:


Lab File ID: >G3840


Date Extracted: 10/07/:?0




108-95-2 —— -111-44-4 ———95-57-8 -----541-73-1 ———106-46-7 —— -100-51-6 ———95-50-1 -----95-48-7 -----infl_4tn_i_._ _106-44-5 ----621-64-7 —— -67-72-1 —— —98-95-3 -----78-59-1 ————88-75-5 ————105-67-9 ———65-85-0 ————111-91-1 ———120-83-2 ———

91-20-3 ————106-47-8 ———87-68-3 -----59-50-7 ————91-57-6 —— —77-47-4 ————83-06-2 ————95-95-4 -----91-58-7 -----88-74-4 ————131-11-3 ———208-96-8 ———606-20-2 ———

----Pheno 1— — bis(2-Chloroethyl )ether ____----2-Chlorophenol----1 .3-Dich lorobenzene----1 ,4-Dich lorobenzane----Benzyl alcohol ,-- — 1.2-Dich lorobenzane____2-Msth«jlphenol----bis(2-Chloroisopropyl)ether_____4_Methylpheno 1----N-Nitroso-d \ -n-p ropy lam i ne _----Haxachtaroethane----Nitrobenzene----Isophorone___-2-Nitrophenol— --2 . 4-D i me th\>l phenol----Senzoic acid----bia C2-Ch 1 o roe thoxy) me thane _----2 .4-Dich lorooheno 1----1 .2 .4-Tr ichlorobanzana-- — Naphthalene— __4_Ch loroan i 1 me ,----Hexach lorobutadiene-___4_Ch loro-3-methy Ipheno I ____----2-Meth«jlnaohthalane----Hexach lorocyc 1 open tad tene __----2 .4.6-Trich lorooheno 1----2 .4r5-Trich loropheno 1-_-_2-Ch loronaphtha lane----2-Ni t roan i 1 me n_ ra----Dimath-ulohthalate----Acenaphthulene----2 r6-Dinitrotoluene

111111111111111111111111111111115711111111111111111111571157111111

1 :IU 1IU ; 1IU r 1IU \IU 1!UIU 1iU iIU 1IU

' IU 1IUIU 1IU 'IU 1IU :IU 1IU :IU 1!UIU 1IU :IU 1IUIU 1IUIU 1IU !

IU 1IU :IU I!U :IU l1

£8FORM I SY -1 1/8? Rev

\

1CSEMIYOLATILE ORGANICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:


Sample wt/Vol: 880.0 CgXmD ML

Level: ClowXmed) LOU

H MQ i s ture : not dec. dec.

Extract ion: CSepFxContXSonc) SERF

GP:: Cleanup: (Y/N) N pH:

Contract!

SAS No.: SDG No.:

Lab Sample ID: CA2137L:

Lab File ID: >G384Q

Date Received: 10x05/3*

Date Extracted: 10x07x89

Date Analyzed: 10x28x89

Dilution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:(ugXL or ugXKg) UGxL

99-09-2 -----83-32-9 ————51-28-5 ————100-02-7 ——— .132-64-9 ———121-14-2 ——— -84-66-2 -----7005-72-3 ——86-73-7 ———— -100-01-6 ———534-52-1 ——— -S6-30-6 —— ---^ n i c e t1 U 1 - 7 9 - .7 - - - -118-74-1 ——— -87-86-5 ———— •85-01-8 ———— .120-12-7 ——— -84-74-2 ———— -206-44-0 ——— •129-00-0 ——— -85-68-7 ———— -91-94-1 ————56-55-3 ———— -218-01-9 ——— •117-81-7 ———117-84-0 ———one OQ n207-99-^----207-09-9 ———50-32-8 ————193-3^-5 ———53-70-3 ————191-24-2 ———

----3-Nitroaniline ,.----Acanaphthene----2 . 4-Din i t remhenn 1»__-4_Ni trophenol----Dibanzofuran. mi __ ._ ——— 2 .4-Dinitro toluene_ — -Diethulphthalate----4-Ch loropheny 1-pheny let her _----Fluorene M , ., ,----4-Nitroani 1 ma.---4, 6 -Din it ro-2-methylpheno 1 _----N-Nitrosodiphenylamine (1 )----4-Bromopheny 1-pheny 1 ether __----Hexaehlorobenzene.---Pantachlorophenol.--.Phananthrana .. ._----Anthraeana ,.---Di-n-buty Iphtha late——— Flueranthana_ „,._. ,._ ,.., ..

571157571111111111575711LI115711111111

——— Purane 11— --Buty Ihan^y Iphth* late— -^^jS'-Dieh lorobanz id ina- — -Sanôf a 1 anthracene.-.-Chryaene- —— bis(2-Ethylhexyl Jphthalate _——— Di-n-netylphthalata__-_R«nTn (h 1 f tunranthana----BanTofk Ifluor an thane——— BenznCa Ipyrena^,. .„._---- IndanoC 1 .2 .3-ed )p«urene----Dibenz(a rh)anthraeane_. — Benzoto .h . i Jperulena

112311111111111111111111

1 11U :IU 1IU :tU r tIU :IU 1IU iIU 1tuIU 1!UIU 1IU :IU 1IU :IU 1IU 'tu iIU 1IU 1:U !IU IIU :IU 1IUIU 1!U !IU 1:U :IU 1IU :IU 11 :

C1 ) - Cannot be separated from Diphenylamine

FORM I SO1 -2 89 1X87 Re

IFSEMI VOLATILE ORGAN ICS ANALYSIS DATA SHEET


EPA SAMPLE NO.



Matr vx: (soi 1/water iUIATER

Sample wt/vol: 880.0 <g/mL)ML

Lewel: (low/mod) LOUI

S Moisture: not dec._____ dec.____

Extract ion: (SepF/Cont/Sonc) SEPF


Number TICs found: '

SDG No.:

Lab Sample ID: CA2137:.

Lafa Fi Le ID: >G8840


Date Extracted: 10/07/:-:'J


Dilution Factor: /


CAS NUMBER

01.

COMPOUND NAME

UNKNOWN

,

RT

7.53

EST. CQNC

73

1. Q

JB :

t

1

11

1

1

1

1

i

1

1

t

I

1

I

FORM I SVJ-TIC 1/87 Rev.

IBSEHIUOLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE .NO.

Lab Name: ETCNJ

Lab Code : Case No. '•

MatPix: C soil /water) WATER

Sample wt/vol: 920.0 Ig/mL) ML

Leêl: Clow/mad) LOW

S tto i s tupe: not dec. dec.



Cont ract:

SAS No.: SDG No.:


Lab File :D: :£3841

Data Received: 10/05/89



Dilution Factor: 1

CftS NO. conPOUNDCONCENTRATION UNITS:Cug/L OP ug/Kg) UG/L

108-95-2 ——————— Phenol____________________111-44-4———————bi»(2-Chlopoethyl Jet hep____95-57-8 ———————— 2^Chlopophenol_____________541-73-1———————1,3-Dichlopobenzene________106-46-7— ————— 1,4-DichloPobenzene________100-51-6 —— ——— -Benzyl alcohol_____________95-50-1 — -- ———— 1,2-DichloPObenzene________95-48-7- ————— — 2-Methyl phenol_____________108-60-1—————bis(2-ChlopoisopPopyl)ethep_106-44-5 ——————— 4-Methyl phenol____________I621-64-7--------N-NitPoso-di-n-pPOpylam me_67-72-1 — —————— Ha xachlopoe thane___________99-95-3 ———— - —— Ni tpobenzene_______________78-59-1-- — ----- I sophopone________________88-75-5 ———— -——2-NitPophenol______________105-67-9 ——————— 2,4-Di methyl phenol_________65-85-0---------Benzoic acid_______________111-91-1———————bi»(2-ChloPoethoxy)methane_120-83-2——————2,4-Dichlopophenol________120-82-1———————1,2,4-Tpichlopobenzene_____91-20-3———————Naphthalene______________106-47-8———————4-Chlopoani I ine____________87-68-3--—--——Hexachlopobutadlene________59-50-7————— —— 4-Chlopo-3-methyL phenol____91-57-6- ————— — 2-Methylnaphtha lene________77-47-4---------Hexachlopocyc1open tad iene__98-06-2————————2,4,6-TptchloPOphenol______95-95-4————————2,4,5-TpichloPOphenol______91-58-7——--———2-Chloponaphthalene________88-74-4— — ——— 2-NitPoani 1 me___________131-11-3 ——— ——— Dimethylphtha late__________208-96-8---———Acenaphthylene___________606-20-2 ——— - —— 2,6-Dm i tpo toluene_________

111111111111111111111111111111115411111111111111111111541154111111

IUIUIUIUIUIUtu!UIUIUIU!UIUiUIUIUIUIUIU!UIUIUIU;uIU;uIUIUIUIUIUIUIU


1CSEMIUOLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NC.

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: (»oiI/water) UATER


Level: Uou/med) LOU1

X Moisture: not dec. dec.

Ext pact ion: (SepF/Cont/Sonc) SEPF

GP!l Cleanup: CY/N) N pH:

Cont ract:

SAS No.: SDG No.:

Lab Sample ID: CA213SC

Lab F t l e ID: >GS341

Date Rece ived : 10/05/8*

Data Extracted: 10/07/89



CAS NO. COMPOUNDCONCENTRATION UNITS:lug/L or ug/Kg) UG/L

99-09-2--- ——— — 3-Ni troani 1 ine_____________15433-32-9--——————Acenaph thane_______________I 1151-28-5 —— -- ——— 2,4-Dinitrophenol__________154100-02-7———————4-Nitrophenol______________154132-64-9 ——————— Dibenzofuran_______________I 11121-14-2 ——— - —— 2,4-Oinitrotoluene_________I 1184-66-2 ———————— Dlethylphthalate___________I 117005-72-3 — ———— 4-Chlorophenyl-phenylether_I 1186-73-7——--- —— Fluorene__________________I 11100-01-6 ——————— 4-Ni troani 1 me_____________154534-52-1 —— — ---4,6-Dmitro-2-methylphenol_I 5486-30-6——---——N-Nitroaodiphenylamine (1)_111101-55-3--------4-8romopheny1-phonylet her__I 11118-74-1 — — ——— Hexachlorobenzene__________1 1187-86-5 ———— -- — Pentachloropheno \__________154S^-01-8 — — ——— -Phenanthrene_______________I 11120-12-7———————Anthracene________________I 1184-74-2 —— - ———— Di-n-butylphthal«te________I 11206-44-0———————Fluoranthene_______________I 11129-00-0———————Pyrene____________________I 1185-68-7--——————Butylbenzylphthalate_______I 1191-94-1 ———————— 3,3'-Dichlorobenzidine_____12256-55-3 ———————— Benzo<a)enthracene_________I 11218-01-9 ——————— Chryaene__________________I 11117-81-7———————bi»C2-Ethylhexyl )phthalate_t 11117-84-0 ——— ———Di-n-octylphthalate________I 11205-99-2--—————Benzo(b)f luoranthene_______I 11207-08-9 — ————— 8enzo(k)f luoranthene_______I 1150-32-8———- — -BenzoCa )pyrene_____________I 1119 3-39-5-- ——— --Indenoll,2,3-cd)pyrene_____I 1153-70-3---------OibenzC a,h ) anthracene_____111191-24-2- ———— — Benzotg,h,i )perylene_______I 11

__________________________________________I__(1J - Cannot be separated from Diphenylanune

FORM I SU -2

IUtUIUtuIU!UIU!UIUIU:UIU!UIU!UIUtuIU!UIU;uIUIUIUIUIU!UIU;uIU:UIU

92

IFSEMIOQLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIUELY IDENTIFIED COnPOUNDS

EPA SAMPLE NO.

Lab Name:ETCNa . Contract:

Lai Code: Case No.: SAS No.:

Matrix: (so iI/water)WATER

Sample wt/vol: 920.0 (gxmL)ML

Level: (low/med) LOU1

\ "oisture: no* dec._____ dec.____


GP" Cleanup: (Y/N) N pH:___

SDG No.:

Lab Sample ID: CA213S::

Lab File ID: >G3S41

Date Received: 10/05/Sv

Date Extracted:1QXQ7X89

Date Analyzed: 10/28.-'c:v

D i l u t i o n Factor: f____

Number TIC» found: iCONCENTRATION UNITS:

or ug/Kg)UG/L

CAS NUHBER

01.

COMPOUND NAME

UNKNOUN

RT

7.54

1EST. CQNC 1: Q

64 ! 381I1i .1IItI1I!t11111111111t!1111

FORM I 93 Rev.


ERA SAMPLE 'NO,

1Lab Name: ETCNJ

Lab Code: Case No.:



Level: ( low/mod) LOW


Extract ion: CSepF/Cont/Sonc) CONT


Cont ract:

SAS No.:

CAS NO. COMPOUND

SDG No.:


Leb File ID: >G9045-

Date Received:



Dilut ion Factor: 1


I10.8-95-2——————Phenol__________________111111^44-4———————bi»(2-Chloroethyl Set her____I 1195^7-8———————— 2-Chlorbphenol_____________111541-73-1 —————— 1,3-Oichlorobenzene_______111106-46-7——————1,4-Dichlorobenzene_______111100-51-6 ——————— Benzyl alcohol_____________11195-50-1————————1,2-Oichlorobenzene________11195-48-7————————2-Methyl phenol_____________I 11108-60-1 —————— bis(2-Chloroiaopropyl )ether_l 11106-44-5———————4-Methyl phenol_____________111621-64-7------—N-Ni troso-d i-n-propy lamina_I 1167-72-1 ——————— Hexachloroe thane__________11198-95-3————————Nitrobenzene_______________11178-59-1———————— Isophorona_________________I 1188-75-5———————2-Nitrophenol____________111105-67-9 ——————— 2 ,4-Di methyl phenol_________I 11.65-85-0————————Benzoic acid_______________153111-91-1——————bi»(2-Chloroethoxy) ma thane_111120-83-2———————2,4-Dichlorophenol_________111120-82-1——————1,2,4-Trichlorobenzene_____11191-20-3———————Naphthalene______________111106-47-8——————4-Chloroani line___________11187-68-3—— — — --Hexachlorobutad.iene_______11159-50-7————————4-Chloro-3-methyl phenol____I 1191-57-6————----2-Methy 1 naphtha lene_______.11177_47_4———————Hexachlorocyclopantadiene__11138-Q6-2---------2,4,6-Trichloropheno 1 .._ 11195-95-4————————2,4,5-Trichlorophenol______15391-58-7———————2-Chloronaphthalene_______11188-74-4————————2-Ni t roan i 1 ins_____________153131-11-3——————Dimethylph thai ate_________111208-96-8 ——————— Acenaph thy lane_____________I 11606-20-2 —————— 2,6-Oinitrotoluane________111_________ __________________I_

94FORM I S<J -1

I U -iu,tuIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

1/87 Rev,

\

1CSEWUOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Leb Name: ETCNJ

Lab Code: Case No.:

Cont ract:

SAS No.:

ria t r i x : C so i 1 /we ten) WATER

Sample wt/vol : 940.0 Cg/mL) ML

Level: (low/med) LOUI

SDG No . :


Lab File ID: >G9045

Date Received:


Extraction: (SepF/Cont/Sonc > CQNT






I99-09-2————————3-Nit roan i line_____________15387-32-9————————Acenaphthene_______________I 1151-^8-5————————2,4-Dinitrophenol__________153100-02-7———————4-Nitrophenol______________153132-64-9———————Dibenzofuran_______________111121-14-2 ————— — 2,4-Oinitro toluene_________I 1184-66-2 ——————— Die thy Iphtha late__________1117005-72-3 —————— 4-Chlorophenyl-phenyl ether_HI86-73-7————————Fluorene__________________111100-01-6 ——————— 4-Nitroani 1 ine_____________153534-52-1 ——————— 4,6-Oinitro-2-me thy I phenol_15386-30-6————————N-Nitrosodiphenylamine CD_I 11101-55-3 ——————— 4-8romophenyl-phenylether__111H8-74-1 —— ————Hexachlorobenzene__________I 1187-86-5————————Pentachlorophenol__________15385-01-8————————Phenanthrene_______________I 11120-12-7——————Anthracene_______________11184-74-2 ———————— Di-n-butyIphthalate________I 11206-44-0——————Fluor«nthene_______________I 11129-00-0———————Pyrene____________________I 1185-68-7———————Butylbenzy Iphtha late______11191-94-1————————3,3'-Dichlorobenzidine_____12156-55-3 ——————— Benzo(a)anthracene________111218-01-9———————Chrysene__________________111117-81-7———————bia(2-Ethylhexyl)phthalate_I 11117-84-0———————Oi-n-octyIphthalate________HI205-99-2——————Benzo(b)f luoranthene______111207-08-9 ————— — Benzo(k)f luoranthene_______I 1150-32-8 ————— —— B»nioCa)pyrane________111193-39-5———————Indeno(l,2,3-cd)pyr»ne_____11153-70-3---------Dibenz(a,h) anthracene_____t11191-24-2 ——————— Benro(g,h , i )perylen«_______I 11

- Cannot be separated from Diphenylamine

FORM I SU -295

IUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUruIUIUIUIU

1/87 Rev,



EPA SAMPLE NO.



Ma t P i x: (soil/we t e r)UATER

Sample wt/voli 940.0 Cg/mL)ML

Level: Clow/mad) LOU

* Moisture: not dec._____ dec.____

Extract ion: (SepF/Cont/Sonc) CONT


SDG No.:


Lab File ID: >G9045

Date Received: (

Data Extracted:10/ll/89

Data Analyzed: 11x15/89

Dilution Fector: ___/

Number TICs found:CONCENTRATION UNITS:Cug/L or ug/Kg>UG/L

CAS NUMBER

01. 141- 8-602. *03. 2233-00-304. 127-18-405. 504-02-906.

COMPOUND NAME

Acatic acid, ethyl esterACETONE DIMER1-Ppopena, 3,3,3-trichloro-E thane , tet rach loro-1,3-CyclohexanedioneUNKNOWN

RT

5.016.419.075.458.327.81

EST. CONC

2206221191212

Q

BJBJBJJJBJ

FORM I SU-TIC 96 1/87 Rev

IBSEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO

iLab Name: ETCNJ

Lab Code: Case No.:

Ma t r i x: (soil/wa ten) WATER

Sample ut/vol: 900.0 Cg/mL) ML

Lave 1: (low/med) LOW


Extract ion: CSepF/Cont/Sonc> CONT


Contract:

SAS No.: SDG No.:


Lab File ID: >G9079

Date Received: fo/





108-95-2 ——————— Phenol____________________111111-44-4———————b is C2-Chloroe thy l)ether____11195.-57-S————————2-Chlorophenol_____________111541^-73-1———————1,3-Dichlorobenzene________111106^-46-7--------1,4-Dich lorobenzene_______111100-51-6 —————— Benzyl alcohol___________11195-50-1 ———————— l ,2-Dich lorobenzene________11195-48-7———————2-Methyl phenol___________111108-60-1 ——————— bisC2-Chloroisopropyl >ether.J 11106-44-5———————4-Methylphenol_____________I 11621-64-7———————N-Nit roso-d i-n-p ropy lam ine_11167-72-1 ——————— Hexachloroe thane__________11198-95-3————————Nitrobenzene_______________I 1178-59-1 —————— — Isophorone________________I 1188-75-5 ——————— 2-Nitrophenol____________111105-67-9———————2,4-Diroethylphenol_________11165-85-0———————Benzoic acid_____________156111-91-1 —————— b is (2-Chloroethoxy)me thane_111120-83-2———————2,4-0 ich loropheno 1_________111120-82-1 —————— 1,2,4-Tr ich lorobenzene_____11191-20-3———————Naphthalene______________111106-47-8———————4-Chloroani 1 ine____________11187-68-3———————Hexachlorobutadiene_______11159-50-7———————4-Chloro-3-methylphenol____11191-57-6———————2-Methyl naphthalene_______11177-47-4————————Haxachlorocyclopentadiene__11188-06-2 ——————— 2,4,6-Tr ich loropheno 1_____11195-95-4———————2,4,5-Tr ich loropheno 1_____15691-58-7———————2-Chloronaphthalena_______11188-74-4———————2-Nitroani line___________156131-11-3 —————— Dimethylph thai ate_________111208-96-8 —————— Acenaphthylene___________111606-20-2- ————— 2,6-0 initrotoluene________111_____________________________________I_

IUIUIUIU.IUIUIUIUIUIUIUiUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI

FORM I S<J -1 97 1/87 Rev

•1CSEMI VOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Coda: Case No.:

Ma t r i x: (soil/watar) WATER

Sample ut/vol: 900.0 (g/mi_) ML

Level: Clou/mad) LOU


Extractioni (SepF/Cont/Sonc> CONT


Cont ract:

SAS No.: SDG No.:


Lab File ID: >G9Q79

Date Received:






FORM 1 SU -2

Q

99-09-2 ————83-32-9 ———— -51-28-5 ———— -10:0-02-7 ——— -132^64-9 ——— -12?-14-2 ——— -84-66-2 ————7005-72-3 —— •86-73-7 ————100-01-6 ——— •534-52-1 ———86-30-6 ———— •101-55-3 ———118-74-1 ——— -87-86-5 ————85-Q1-8 ———— .120-12-7 ———84-74-2 ———— -206-44*0 ———129-00-0 ——— •85-68-7 ————91-94-1 ———— -56-55-3 ————218-01-9 ——— -117-81-7 ———117-84-0 ——— •205-99-2 ——— •207-08-9 ——— -50-32-8 ————193-39-5 ——— -53-70-3 ————191-24-2 ——— -

— --3-Nitroani 1 ina----AcBnaphthene_. n , _----2, 4- Din it rap he no 1——— 4-Ni t raphena 1----Dibenzofuran----2,4-Dinitroto luene— — Diethylphthalate— --4-Ch loropheny 1-pheny let her _----Fluorena-___4-Ni t roani 1 ina----4,6-Dtni t ro-2-me thy 1 phenol _-- — N-Ni t rosodipheny lamine C 1 ) _----4-Bromopheny 1-pheny 1 ether __----Hexachlorobenxene-.--Pentach lorophano 1- — --Phenanthrene----Anthracene-- — Di-n-but<jlphthalate— --Fluor an thene n_----Pyrana——— Butulbanzulphthalate——— 3 .3 ' -Dich lorobenz id me——— Banzo (a lanthracena——— Chryaana-—— bi»<2-Ethylhexyl >ph the late——— Di-n-oct*jlphthalata——— Benzo(b)f luoranthana. ,.,_• —— Banzo Ck ) f luoranthena- — -Benzo(a)pyrena, .,_ .._——— IndenoCl .2 .3-cd)p<jrana—— -DibanzCa .h Janthraeana——— Banzo Cg .h r i )parulana

11561111561561111111111111111561561111111111561111111111111111111221111111111111111111111111111111

1IUt uIUIUIU.IUIUIUIUIUIUIU

• IUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIU1

981x87 Rev

IFSEMIVOLATILE ORGAN ICS ANALYSIS dATA SHEET


EPA SAMPLE NO.



Matrix: (soiI/water)UATER


Level: Clow/med) LQU

% Moisture: not dec._____ dec.____



iNumber TICs found: __

SDG No.:

Lab Sample ID: CA214QC

Lab F i l e ID: >G9079

Date Received: (O



D i l u t i o n Factor: /

CONCENTRATION UNITS:(ug/L OP ug/Kg)UG/L

CAS NUMBER

01.02. >03. 141-78-604.05.06. 127-18-407.08. 141-79-709.10.11.12.13. 625-33-214.

COMPOUND NAME

ACETONE DIMERUNKNOUNAcetic acid, ethyl esterUNKNOUNUNKNOUNEthane, tet rachloro-UNKNQUN3-Penten-2-one, 4-methyl-UNKNOUNUNKNOUNUNKNOUNUNKNOUN3-Penten-2-oneUNKNOUN

.

RT

6.6510.925.0415.2722.055.4111.515.2011.1412.0811.8613.383.6813.06

EST. CONC

1300470624787342622201815121411

Q

BJ3-BJ3JJJJJJJJJJ

FORM I SU-TIC 1/87 Rev

99

IBSEMIUOLAT1LE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO,

Lab Name: ETCNJ

Lab Code:

Cont pact:

Case No.:

Matrix: (sol 1/water) UJATER


Leve1: <low/mod) LOU

% Moisture: not dec. dec.

Extraction; (SepF/Cont/Sonc) CONT


CAS NO. COMPOUND

SAS No.: SDG No.:


Lab File ID: >G9056

Date Received: IQI

Date Extracted; 10/12/89



CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L Q

108-95-2 ———111-44-4 ———95-57-8 ————541-73-1 ———106-46-7 ———100-51-6 ———95-50-1 ————95-48-7 ————108-60-1 ———106-44-5 ———621-64-7 ———67-72-1 ————98-95-3 ————78-59-1 ————88-75-5 ————105-67-9 ———65-85-0 ————111-91-1 ———120-83-2 ———

91-20-3 ————106-47-8 ———87-68-3 ————ea en ~991-57-6 ————77-47-4 ————

95-95-4 ————91-58-7 ————88-74-4 ————131-11-3 ———208-96-8 ———606-20-2 ———

1——— Phenol 1——— bis(2-Chloroethyl ) ether ____ 1——— 2-Ch loropheno 1 _ 1——— 1 r3-Dichlorohenzene 1——— lT4-Diehlorohenzene 1----Benzyl alcohol .„. 1—— -1,2-DiehlorQbanzene 1— --2-Methy Ipheno 1 ,._ ,„ I——— bis(2-Chloroisopropyl >ether_l— — 4-Methyl phenol 1__--N-Ni t r oso- d i -n -p ropy lam ine _ 1- — -Hexach Inroethana. . M 1—— -Ni t robanzena „ 1---- Isophorone _ 1——— 2-Nitrophenol 1——— 2 r 4-D i ma thvl phenol 1----Banzoic acid _ 1----b isC2-Ch 1 o roe thoxy ) me thane _ 1——— 2 ,4-Dichloraphanol 1——— 1 .2 .4-Tr ieh 1 arobenzene t— --Naphthalene, „._, 1——— 4-Ch loroan i 1 ine , 1__--H»v«eh lornhut ad iana 1__-_4-Ch loro- 3 -methyl phenol ____ 1——— 2- Ma thyl naphtha Iana 1——— Hexach lorocycl open t ad iene __ 1———— 5 ,4,-A-Tr iehlorophanol 1_ —— 2 ,4,5-Tr iehlorophanol . _ _ 1———— -P-Th Inrnnaphf ha l*n« 1----2-Ni t roan i 1 ine ,_,. „.., 1— — Qimathylphthalata , I— --Acanaphthy Iana IIMI 1——— 2T6-Dini trotoluena I

1

121212121212121212121212121212125812121212121212121212581258121212

IIUIUIUIIIIUIUIUIUIUIUIUIUIUIU1UIUIUIUIUIUIUIUIUIUIUIUIUIUIU1UIUIUIU1

1COFORM I SY -1 1/87 Rev

1CSEMI VOLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO,

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: Csoi1/water) UATER






Contract:

SAS No.: SDG No.:


Lab File ID: >G9056

Date Received: (

Date Extracted: 10/12x89




99-09-2 ———— -83-32-9 ———— -51-28-5 ———— -100-02-7 ——— -132-64-9 ——— •121-14-2 ——— -84-66-2 ———— •7005-72-3 —— •86-73-7 ———— -100-01-6 ——— -534-52-1 ——— •86-30-6 ———— -101-55-3 ——— •118-74-1 ——— -87-86-5 ———— •85-01-8 ———— •120-12-7 ——— -84-74-2 ———— -206-44-0 ——— •129-00-0 ——— •85-68-7 ———— •91-94-1 -----56-55-3 —— --218-01-9 ——— •117-81-7 ———117-84-0 ——— •205-99-2 ——— •207-08-9 ——— •50-32-8 ————193-39-5 ——— •53-70-3 — ——191-24-2 ——— •

----3-Nitroani 1 ine_• - — Aeenaphthene ,„——— 2 T4-Dini t rophenol— — 4-Ni t ropheno 1• ---Dibenzof uran ,.——— 2,4-Dinitrotoluana——— Diethylphthalate.---4»Ch loropheny 1-pheny 1 ether _----Fluorene , , ,_.----4-Nitroani 1 i<">e- — -4, 6 -Din i t ro-2-methy Ipheno 1 ___-_N-N; t roaodipheny lamine C 1 ) _----4-Bromopheny 1-pheny let her __----Haxachlorobenzena----Pentaeh Lorophano 1----Phananthrana _—— -Anthraeana----Di-n-buty Iphtha late _-- —— Fluaranthana.-- — Pyrane——— Butylbanzulphthalate——— 3 r3 '-Dieh larobanz idina——— BanzaCa)anthracana——— Chryaana _——— bi»(2-Ethylhexyl )phthalate _——— Di-n-oct-jlDhtha late——— Banzotblf luoranthana----Banzo tk If luoranthana——— Banzo(a)pyrana——— IndenoC 1 .2 r3-cd Ipurana__--Dihanz[aTh)anthraeana——— Banzo (g .h f i loarulana

5812585812121212125858121212581212121212122312121212121212121212

11UIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI


FORM I SY -2 1 C 1 1/87 Rev,

IFSErtIVOLAT n_E ORGAN ICS ANALYSIS DATA SHEET


EPA SAMPLE NO.



Matrix: (so:1/water)WATER



S Moisture: not dec.__ dec.



SDG No.:


Lab File ID: >G9056

Date Received: {



Dilution Factor: I


CAS NUMBER

01. 141-78-602.03.

COMPOUND NAME

Acetic acid, ethyl esterACETONE DIMERUNKNOWN

RT

5.056.468.98

EST. CQNC

3707524

1G2

Q

BJBJBJ

FORM I SV-TIC 1/87 Rev,

IBSEMI VOLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Cont ract

SAS No.

Ma t r i x: (soil/wa t e r ) WATER


Level: (low/med) LOU)

S Moi3 t u r e: not dec. dec.



SOG No.:


Lab File ID: >G9057

Date Received: tol/ff,





108-95-2 ——————— Phenol____________________111-44-4———————bis(2-Chloroethyl )ether____95-57-8 ———————— 2-Chlorophenol_____________541-73-1 —— ————1,3-Dichlorobenzene________106-46-7-- ————— 1,4-DichIorobenzene________100-51-6-- —— ---Benzyl a Icohol_____________95-50-1 — — ———— 1,2-Dichlorobenzene________95-48-7————————2-Methyl phenol_____________108-60-1—————-bis(2-Chloroisopropyl)ether_106-44-5 ——————— 4-Methyl phenol_____________621-64-7--------N-Nitroso-d i-n-propy lam me_67-72-1----- — --Hexachloroe thane___________98-95-3 ———— —— -Nit robenzene_______________78-59-1--------- Isophorona _______.___....88-75-5 ———————— 2-Nitrophenol______________105-67-9 ——————— 2,4-Dimethylpheno 1_________65-85-0 ————— —— Benzole acid_______________111-91-1--- — ---bis(2-Chloroethoxy)me thane_120-83-2 ——————— 2,4-Dichlorophenol_________120-82-1 ———— —— 1,2,4-Trich lo robenzene_____91-20-3————————Naphthalene________________106-47-8 ——————— 4-Chloroan i 1 ine____________87-68-3 ——————— Hexach lorobut ad iene_______59-50-7————————4-Chloro-3-methyl phenol____91-57-6 ———————— 2-Methyl naphtha lene________77-47-4---------Hexachlorocyc1 opentadiene__88-06-2 — — ———— 2,4,6-Tr i ch lor opheno 1______95-95-4- ———— —— 2,4,5-Tr ich loropheno 1______91-58-7———--——2-Chloronaphthalene________88-74-4——— ———— 2-Ni t roam 1 ine_____________131-11-3 —————— Dimethylphthalate_________203-96-8—----—Acenaphthylene_____________606-20-2 —— - — --2,6-Dimtro toluene_________

111111111111111111111111111111115411111111111111111111541154111111

Q

IIUIUIUIU1UIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIU

FORM I SiJ -1 1C3 1/87 Rev,


ERA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: Csoi I/water) CJATER

Sample wt/vol: 920.0 <g/mL) ML


H Mo i sture: not dec. dec.



Cont ract:

SAS No.: SDG No.:


Lab File ID: >G9057

Date Received: (d



Di lution Factor: 1


99-09-2- —————— -3-NitPoanil me_____________83-32-9---———--Acenaphthene_______________51-28-5 ———————— 2,4-Dinitrophenol__________100-02-7———— — -4-Nitrophenol______________132-64-9 ——————— Dibenzofuran_______________121-14-2- ———— --2 ,4-Dmitro toluene_________84-66-2 —————— --Oiethylphthalate___________7005-72-3 —————— 4-Chloropheny1-pheny1 ether_86-73-7—————- — Fluorene___________________100-01-6-————-4-Nitroaniline_____________534-52-1 ——————— 4,6-0 in i t ro-2-methy Ipheno 1_86-30-6---------N-Nitrosodiphenylamine C1)_101-55-3--------4-Bromopheny1-phenylet her__118-74- l--------Hexachl orobenzena ________87-86-5---------Pentachloropheno1__________85-01-8- —— —. —— Phenan throne_______________120-12-7———----Anthracene_________________84-74-2-- ————— Oi-n-butylphthalate_______206-44-0 ——————— Fluor an thane_______________129-00-0 ————— — Pyrene____________________85-68-7———————Butylbenzylphthaiate______91-94-1 ———————— 3,3 '-Dichlorobenzidine_____56-55-3 ———————— BenzoCa)anthracene_________218-01-9———————Chrysene__________________117-81-7———————bis(2-Ethylhexyl )phthalate_117-84-0 —————— -Di-n-octylphthalat a________205-99-2——————Benzo(b)f luoranthena______207-08-9 ——————— Benzo(k)fluoranthene_______50-32-8-— ————— BenzoCa Jpyrena_____________193-39-5 ————— —lndeno(l,2,3-cd)pyrene_____53-70-3———----Dibenz(a,h)anthracene______191-24-2--------Benzo(g,h,i Jperylane_______

5411545411111111115454111111541111111111112211111111111111111111

IIUtuIUIUIUtuIUIUtuIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI



IFSEMIOOLATrLE ORGAN ICS ANALYSIS DATA SHEET


EPA SAMPLE NO.


Lab Coda: Case No.: SAS No.:

Matrix: Csoi1/water)WATER

Sample ut/vol: 920,0 (g/mL)ML

Leve 1 : ( low/med ) LOUI

X Moisture: not dec._____ dec.____



.1Number TICs found: _

SDG No.:


Lab Fila ID: >G9Q57

Date Received;



Dilution Factor: '


CAS NUMBER

01. 141-78-602.03.04.

COMPOUND NAME

Ace t ic acid , ethyl esterACETONE DIMERUNKNOUNUNKNOWN

*

RT

5.126.467.848.90

EST. CONC

4301301110

Q

BJBJBJBJ


IBSEMI VOLATILE ORGAN1CS ANALYSIS DATA SHEET

EPA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Cont ract

SAS No.

Matrix: (soiI/water) WATER


Level : C low/med) LOUI

HMoisture: not dec. dec.-



CAS NO. COMPOUND

SDG No.:


Lab File ID: >G9058

Date Received: (


Date Analyzed! 11/15/89

Di tut ion Factor: 1


I108-95-2 ——————— Phenol____________________112111-44-4———————bisC2-Chloroethyl Jet her____I 1295-57-8————————2-Chlorophenol_____________t 12541-73-1 ——————— 1,3-Dichlorobenzene________I 12106-46-7——————1,4-Dichlorobenzene_______112100-51-6 ——————— Benzyl alcohol_____________I 1295-50-1 ——————— -1,2-Dichlorobenzene________I 1295-48-7————————2-Methyl phenol_____________I 12108-60-1 ——————— bis<2-Chloroiaopropyl)ether_!12106-44-5———————4-Methyl phenol_____________I 12621-64-7--------N-N1t roso-d i-n-propylam me_I 1267-72-1 ———————— Hexachlo roe thane___________I 1298-95-3 ———————— Nitrobenzene_______________I 1278-59-1 —— — -—— Isophorone_________________I 1288-75-5 ———————— 2-Nitrophenol______________112105-67-9———————2,4-Di methyl phenol_________I 1265-85-0———————Benzole acid_____________159111-91-1 ——————— bia(2-Chloroethoxy)me thane__112120-83-2———————2,4-Dichlorophenol_________112120-82-1 ——————— 1,2,4-Tr ich lorobenzene_____I 1291-20-3 ———————— Naphthalene________________I 12106-47-8 ——————— 4-Chloroani 1 me____________I 1287-68-3-———————Hexachlorobutad iene________I 1259-50-7————————4-Chloro-3-methylphenol____I 1291-57-6———————2-Methylnaphthai ana_______11277-47-4---------HexachloPOcyc1 open tad iena__I 1288-06-2————————2,4,6-Trichlorophanol______I 1295-95-4————————2,4,5-Trichlorophenol______15991-58-7————————2-Chloronaphthalene________I 1288-74-4————————2-Nitroani 1 ine_____________159131-11-3-—————Dimethylphthalata_________112208-96-8— ————— Acenaphthy Iene_____________I 12606-20-2- —————— 2,6-Dmitroto luena_________I 12___ _____ ___ ____ __________I__

FORM I SU -1106

I1UIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIU

1/87 Rev

' 1CSEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Cont ract:

SAS No.:

Matrix: <soi1/water) UATER


Level : C low/mad) LOW




SDG No.:


Lab File ID: >G9053

Date Received: /*/



Dilution Factor: 1



FORM I SO1 -2

Q

99-09-2 ———— -83-32-9 ———— -51-28-5 ———— -100-02-7 ——— -132-64-9 ——— -121-14-2 ——— -84-66-2 -----7005-72-3 —— -86-73-7 ————100-01-6 ——— -534-52-1 ———86-30-6 ———— -101-55-3 ———118-74-1 ———87-86-5 ————85-01-8 ———— -120-12-7 ——— -84-74-2 ———— -206-44-0 ———129-00-0 ——— -85-68-7 ———— -91-94-1 ———— -56-55-3 ———— -218-01-9 ——— •117-81-7 ——— -117-84-0 ——— .205-99-2 ——— -207-08-9 ——— -50-32-8 ———— -193-39-5 ——— -53-70-3 ———— -191-24-2 ——— -

1• — -3-Ni t roan i 1 ine 1-_-~Acenaphthene 1----2 ,4-Din i t rophano 1 1----4-Nitrophenol 1----Dibenzof uran 1— — 2 ,4-Dinitroto luena 1——— Diethylphthalata 1— --4-Ch loropheny 1-pheny let her _ 1----Fluorana , ,.„,, 1__-_4_Ni t roan i 1 ina 1----4,6-Oini t ro-2-methy Ipheno 1 _ 1._--N-Ni t roaodi phony lam ine C 1 ) _ 1----4-Bromopheny 1-pheny let her __ 1----Hexachlorobonzene 1.---Pentachlorophenol 1-- — Phenan throne t----Anthracene t----Di-n-butvlohthalate 1----Fluor an thane 1-- — Porena 1——— Bufjlbanzulohthalata 1- —— 3.3 '-Dichlorobenzid ina I.- — BenzoCa )anthracana 1——— Chrysana ,.. t- —— bia(2-Ethylhexyl )phthalate _ 1•---Di-n-oct*jlohthalato 1----Banzo(b Jfluoranthena 1— --BenzoCk )fluor an thane 1----Benzo (a)pyrana 1-- — IndenoC 1 .2 .3-cd >ourene 1----DibenzCa .h )anthracene 1-_--Benzn(g rh r i )parylane 1

5912595912121212125959121212591212121212122412121212121212121212

1tuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1 • I

1071/87 Rev,



EPA SAMPLE NO.

Lab Name:ETCNJ

Lab Code: Case No.:



Level: (low/mod) LQU

\ Moisture: not dec. _ dec.____,

Ex t rac tion: C SepF/Con t/Sonc) CONT


Cont ract:

SAS No.: SDG No.:


Lab FiIe ID: >G9058

Date Received: /o/



Dilution Factor: _ /

Number TICs found:CONCENTRATION UNITS:<ug/L or ug/Kg>UG/L

CAS NUMBER

01. 141-78-602.03.04. 108-88-305.

COMPOUND NAME

Acetic acid, ethyl esterACETONE DIMESUNKNOWNBenzene, methyl-UNKNOUN

RT

5.106.468.924.327.86

EST. CONC

460140181311

Q

BJBJBJJBJ

FORM I SY-TIC 1C8 1/87 Rev.


EPA SAMPLE NO,

Lab Name: ETCNJ

Lab Code: Case No.:


Samp le wt/vo1: 960.0 Ig/mL) ML



Extraction: (SepF/Ccnt/Sonc) CONT


Con t ract:

SAS No.: SDG No.:


Lab File ID: >G9Q59

Date Received: /0/





108-95-2 ——————— Phenol____________________111-44-4- — ———— bis(2-Chloroethyl Jet her____'.95-57-8 ——————— -2-Chloropheno I_____________541-73-1-- ————— 1,3-Dichlorobenzene________106-46-7————-—1,4-Dichlorobenzene________100-51-6 ——— -- — Benzyl alcoho 1_____________95-50-1---————1,2-Dichlorobenzene________95-48-7---—----2-Methylphenol_____________108-60-1-———--bisl2-Chloroisopropyl)ether_106-44-5- —————— 4-Methyl phenol_____________621-64-7--------N-Nitroso-di-n-propylamine_67-72-1---------Hexachloroet hane___________98-95-3-——-----Nitrobenzene_______________78-59-1——---—-Isophorone_________________88-75-5 ———— ——— 2-Nitrophenol______________105-67-9- — - — — 2,4-01methyl phenol_________65-85-0-- —————— Benzoic acid_______________111-91-1———-——bis(2-Chloroethoxy)methane_120-83-2 ——— ——— 2,4-Dich loropnenol_________120-82-1———————1,2,4-Tr ich lorobenzene_____91-20-3————————Naphthalene________________106-47-8- — ———— 4-Ch loroani 1 ine____________87-68-3————----Hexachlorobutadlene________59-50-7—— — — --4-Chloro-3-methy1 phenol____91-57-6 —— - ———— 2-Methylnaphtha lene________77-47-4---------Hexachlorocyc1 open tadlene__88-06-2---------2,4,6-Trichloropheno195-95-4-----———2,4,5-Trichlorophenol______91-58-7— —— ——— 2-Chloronaphthalene________88-74-4————— —— 2-Nitroan i 1 me_____________

208-96-8--—----Acenaphthylene_____________606-20-2- — ———— 2,6-D mi trotoluene_________

101010101010101010101010101010105210101010101010101010521052101010

109FORM I SY -1

IUIUIUIU1UIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

1/87


EPA SAMPLE NO.

Lab Name: ETCNJ


Matrix: (soi I/water) WATER



Cont rac t:

SAS No.:


Extraction: (SepF/Cont /Sonc ) CONT

GPC Cleanup: <Y/N) N PH:

SDG No.:


Lab File ID: >G9059

Date Received: /p//P/?T



Dilution Factor: 1


99-09-2 ———————— 3-Nitroani 1 ine_____________83-32-9 —————— — Acenaphthene_______________51-28-5 ——————— 2,4-Dmi trophenol_________100-02-7———————4-Ni trophenol______________132-64-9- —————— Dibenzof uran_______________121-14-2--————2,4-Oinitrotoluene_________84-66-2- ——————— Die thy Iphtha late___________7005-72-3—————4-Chlorophenyl-phenylether__86-73-7---------Fluorene___________________100-01-6--—----4-Nitroanilme_____________534-52-1 ——————— 4,6-Dmitro-2-methylphenol_86-30-6---------N-Nitrosodiphenylamine C1)_101-55-3--------4-Bromopheny1-phenylet her__118-74-l--------Hexachlorobenzene87-86-5--- ———— -Pentachloropheno 1__________85-01-8 ———— -- — Phenanthrene_______________120-12-7——— —— -Anthracene_________________84-74-2- —————— -Di-n-butyIphtha late________206-44-0 ——————— Fluoranthene_______________129-00-0 ——————— Pyrene____________________85-68-7———————ButylbenzyIphtha late______91-94-1 ——————— 3,3'-DichloPobenzidme_____56-55-3---———-BenzoCa)anthracene________218-01-9———————Chrysen*__________________117-81-7——————bi»(2-Ethylhexyl )phthalate_117-84-0 ——————— Di-n-octy Iphtha late________205-99-2 ——————— BenzoCb)f luorenthene_______207-08-9 — ————— BenzoClOf luoranthene_______50-32-8- ——— ——— BanzoCa)pyrane_____________193-39-5--- — —— Indenod ,2 ,3-cd )pyrene_____53-70-3---------Dibenz(a,h)anthracene______191-24-2--————Benzo(g,h, i)perylsns_______

5210525210101010105252101010521010101010102110101010101010101010

Q

IIUIUIUIUtuIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI


FORM I SU -2 110 1/87

IFSEMIOOLATILE QRGANICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

Lab NamesETCNJ

Lab Code: Case No.:

Matr ix: (so i 1 / w a t e r ) W A T E R

Sample w t / vo l : 960.0 Cg/mDML

Level: (low/mod) LOW

\ Moisture: not dec.____ dec.____



Number TICs found: _____

Cont ract:

SAS No.: SDG No.:


Lab File ID: >G9059

Date Received: (tll'



D i l u t i o n Factor: _____


CAS NUMBER

01. 141-78-602.03.04.

COMPOUND NAME

Acetic acid, ethyl esterACETONE DIMERUNKNOWNUNKNOWN

RT

5.076.468.927.84

EST. CONC

3901201411

Q

BJBJBJBJ


IBSEMIUQLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: .

Lab Code: IP**' Case No.:>V . " "



Level: C low/mad) LOW


Extraction: (SepF/Cont/Sonc ) SEPF


Contract:

SAS No.: SDG No.:


Lab File ID: >G9106






108-95-2-111-44-4-95-57-8—541-73-1-106-46-7-100-51-6-95-50-1—95-48-7—109-60-1-106-44-5-

67-72-1 —98-95-3 —78-59-1—88-75-5 —105-67-9-65-85-0—111-91-1-

120-82-lS91-20-5

59-50-7—91-57-6—77-47-4—

95-95-4—91-58-7—88-74-4—131-11-3-208-96-8-A n^_on_9 —

--__ — -Phenol—————— bis(2-Chloroethyl ) ether ____———— — 2-Ch loropheno 1----- — If3-Dich lorobanzena .,_— --_ — i ,4-Dich lorobenzana _—————— Benzyl alcohol---- — -1 .2-Dich lorobenzana—————— 2-Meth-jlphanol-------bis C2-Ch loro i sop ropy 1 ) ether-------4-Mathylphanol— -__ — N-Ni t roso-d i-n-propy lamina ____-_.__ He xachloroathana--- — --Nitrobenzene,^ . immm-- — --_ laophorona--- —— -2-Ni t ropheno 1 ,„_— ———— 2 , 4-D i ma thyl phenol— —— --Banzoic acid , . „—————— b is <2-Ch lor oethoxy )me thane

gSi± ——— 1, 2, 4-Trich lorobanzena.-.———---Naphtha lan* p

^-----4-Chlornan i 1 ina

»._» —— 4-Chloro-3-methylphanol-- —— --2-M«thul naphtha lane

-------2 .4r6-Trieh loropheno 1—— -- — -5 T4,5-Tr ieh lorophano 1———— ——— 2-Ch loron»phtha lane,,. ._._ in-------2-Nitrnani line-.--__ -ni m*Hiy Iphtha lata------- Acanaph thyl ana-------9J6-rjini trntoluana

114211111111111111111112111196l 11111I 11111HI111

111111111ill111HI111HI111HI156HI156HI111I 111

11IUIUIUIUIUIUuIU1IUIUIUIUIUIU1IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU 11 1

FORM I SU -1 112 '87 Pev

1CSEMIYOLATILE ORGAN1CS ANALYSIS DATA SHEET

EPA SAMPLE NO. 1Lab Name: ETCNJ .,,

j*«jrV8f "Lab Code: T*3!f Case No.:



Leve1: (low/mod> LQU

Cont ract:

SAS No.:


Extraction: (SepF/Cont/Sonc ) SERF


CAS NO. COMPOUND

5DG No.:


Lab File ID: >G91Q6

Data Received: 10/10/89





99-09-2 ——————— 3-Nit roan i line___________:5683-32-9————————Acanaphthene_______________11151-28-5 ———————— 2,4-Dinitrophenol__________I 56100-02-7———————4-Nitrophenol______________156132-64-9 —————— Dibenzofuran_____________111121-14-2 —————— 2,4-Dinitrotoluene________11194-66-2————————Die thy Iphtha late___________147005-72-3 —————— 4-Chlorophenyl-phenyl ether_11186-73-7————————Fluorene__________________I 11100-01-6 ———— —-4-Nitroani line_____________156534-52-1 ——————— 4,6-Dinitro-2-roethy 1 phenol_i 5686-30-6 ————— —— N-Nitrosodiphenylamine (1)_111101-55-3-—-—--4-8romophenyl-phenylether__i11118-74-1 —————— Hexachlorobenzene_________11187-86-5 ———————— Pentachlorophenol__________ i 5685-01-8 ——————— Phenanthrene_____________111120-12-7——————Anthracene_______________11184-74-2———————Oi-n-buty Iphtha late_______til206-44-0———--Fluor en thene_____________111

-——Pyrene__________________111£——Butylbenzy Iphtha late______111

91-94-1-^*-———J,3'-Dichlorobenzidine_____1225 6-55-3 jy-frfo——B*nzo (•) anthracene________ill218-01-9^-^.———Chry»ene_________________111117-81-7———————bi*(2-Ethylnexyl )ph the late_til117-84-0——————Di-n-octylphthe late_______111205-99-2——————-Benzo(b)fluo ran thene_______I 11207-08-9——————BenzoCk)f luoran thene______11150-32-8 ———————— BenzoCa Jpyrene_____________I 11193-39-5——————— Indenod ,2 ,3-cd )pyren*_____I 1153-70-3———————Oibenz(a,h)anthr«cene______111191-24-2——————Benzo(g,h, i )perylene______111

(!) - Cannot be separated from Diphenylamine

FORM I SY -2

IIIIIU1UIUIUIU10IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

113

IFSEMIUOLATILE ORGANtCS ANALYSIS DATA SHEET

IDENTIFIED COMPOUNDS

EPA SAMPLE NO.-

***•Lab Name:ETCNJ

Lab Coda: *• Caaa No.:

Matrix: (aoiI/water)WATER



S Moiature: not dec._____ dec.___

Extract ion: CSepF/Cont/Sonc) SEPF


Number TICs found: 2/

Cont ract:

SAS No.: SDG No.:

Lab Sample ID: CA215QC

Lab File ID: >G9106


Data Extracted:11/06/89

Data Analyzed: 11/1?'89

Dilution Factor: I___


CAS NUMBER

01.02. 103-82-203. 98-89-504. 142-62-105. 108-93-006. 501-52-007. 111-14-800. 100-93-009^ 109-52-4

11. 111-14-0 —12-.° 503-74-2

IA> 124-07-2

la-/ 127-18-4;,l^f 98-89-5 J18-y loe-io-i^l!*?> '-K«/' '21/U12-Q5-033-, —————————j?. toe so j —zo**! IQ#~t9~±

\\ " COMPOUND NAME

1 UNKNOWNiBenzeneacet ic ac id1 Cyc lohexanecarboxy 1 ic ac idIHexanoic acidICyc lohexano 1IBenzenepropano ic ac idHeptanoic acid

tCyclohBAanul ———————————————Pentanoic acid

1 UNKNOWN

IButanoic acid, 3-methyl-1 UNKNOWNlOctanoic acid1 UNKNOWN

££IEth«n«, tet rachloro-jitCyclohexanecarboxy 1 ic acidi|jZ-P«n t anona , 4- mm t hy 1 -SWfiWkNOWNÛNKNOWN

iNonanoic acidIUHKMOUH ——————————————————IDeneene, methyi ———————————— 1

•tojtt-Jtw-tOBt^-.j^* s***0Lj( -

•i ' C

RT

9.9716.2514.1111.40

7.5117.5713.15

11.5810.95

1 —— 12.95 i8.186.27

14.8414.78

5.1913.56

3.464.76

10.6016.37

1 —— 10.0? 11 ——— 4.03 1

SO.**V. a^

41026023012087130110

3224

1818262213181210811_

<r•?•

tcore i Q

uui j13IJ131 J

1 J1 J

1 J' JB1 J1 JU1 J1 JU1 J1 J

——————— h3—

11 T1 T1t111

1



ERA SAMPLE NO,

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: (soi1/water) WATER






Cont rac t:

SAS No.: SDG No.:


Lab File ID: >G9060

Date Received: fO/ft/tf



Di l u t i o n Factor: 1


108-95-2 ——————— Phenol____________________111-44-4—- ———— bisC2-ChloroethylJet her____95-57-8 ————— — -2-Chloropheno 1_____________541-73-1 —————— 1,3-Dich lorobenzene_______106-46-7--------l,4-Dichlorobenzene________100-51-6 ——————— Benzyl alcohol_____________95-50-1 ———— ——— 1,2-Dich lorobenzene________95-48-7—-------2-Methylphenol_____________108-60-1- — —— --b is(2-Ch1oroisop ropy 1)ether_106-44-5 ——————— 4-Methyl phenol_____________621-64-7--------N-Nitroso-di-n-propylam me_67-72-1 — — - — — Hexachloroe thane___________98-95-3- — - ——— -Ni trobenzene_______________78-59-1-——————— Isophorone_________________88-75-5————————2-Nitrophenol______________105-67-9 —— - ——— 2,4-Dimethyl phenol_________65-85-0 — — ———— Benzoic acid_______________111-91-1-——————bis(2-Chloroethoxy)methane_120-83-2 ——————— 2,4-Dichloropheno 1_________120-82-1---- ——— 1,2,4-Tr ichlorobenzene_____91-20-3————————Naphthalene________________106-47-8 ——————— 4-Chloroani 1 ine____________87-68-3 ———————— Hexach lorobutadiene________59-50-7————————4-Ch loro-3-methylphenol____91-57-6- — ————— 2-Methyl naphtha lene________77-47-4---------Hexachlorocyc1 open tad iene__88-06-2 ————— - — 2,4,6-Trichloropheno 1______95-95-4——- ———— 2 ,4,5-Tr ich loropheno 1______91-58-7—— ————'. -Chloronaphthalene_______88-74-4—— ————— 2-Nitroani 1 ine_____________131-11-3----———Dimethylphthalate__________208-96-8--————Acenaphthylene_____________606-20-2----- —— 2,6-Dmitroto luene_________

111111111111111111111111111111115711111111111111111111571157111111

IUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUJ_

FORM I SU -11 1 5

1/87 Rev

1CSEMI VOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Con t ract:

SAS No.:





Extraction: ISepF/Cont/Sonc) CONT


SDG No.:


Lab File ID: >G9060

Date Received: /0//0/M





11) - Cannot be separated from Diphenylamine

FORM I SY -2

Q

99-09-2 ————83-32-9 ————51-28-5 ———— -100-02-7 ——— -132*64-9 ——— •121-14-2 ——— -84-66-2 ————7005-72-3 —— •86-73-7 ———— -100-01-6 ——— -534-52-1 ——— -86-30-6 ———— -101-55-3 ———118-74-1 ———87-86-5 ————85-01-8 ———— -120-12-7 ——— -84-74-2 ———— -206-44-0 ——— -129-00-0 ——— -85-68-7 ————91-94-1 ————56-55-3 ————218-01-9 ———i i T a i ^11/-81-7-----117-84-0 ——— -205-99-2 ———207-08-9 ——— •50-32-8 ————193-39-5 ———53-70-3 ————m _9A_2___-

----3-Nitroani 1 ine----Acenaphthene ,„„----2 ,4-Dinitrophenol----4-Nitrophenol----Dibanzofuran----2;4-Dinitrotoluane-- — Diethulphthalate----4-Ch loropheny 1-pheny let her _•---F luorene----4-Nitroani 1 me- — -4,6-Oinitro-2-methylpheno 1 _----N-Ni trosodiphenylamine C 1 ) _----4-Bramophenvl-ohenvjlether----Hexachlorobenzene----Pentachloroohenol----Phananthrene----Anthracene , ,,,,,.„----Di-n-butvlohtha late— --Fluoranthane----Pyrane——— Butylhanzulphtha 1 a t a-- — 3 .3 ' -Dieh larobanz id ina----Banzo t a )an t hracana— — Chry&ana _„„,.,, ,——— bis(2-EthyIhexyl )phthalate _----Di-n-oct-ulDhthalate--- -Banzo (h )fluoranthana----Banza(k)fluoranthane----BenznC«)pvrane.----IndannCl .2 .3-cd Ip^rana____Oih«n*ta .hlanthracana____aaniotg rh. i )oerwlana

5711575711111111115757111111571111111111112311111111111111111111

1IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

1161/87 Rev

IFSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET


ERA SAMPLE NO.




Sample wt/vol: 880.0 (g/mLJML


S Moisture: not dec ._____ dec . ____



.1Number TICs found:

SDG No.:


Lab File ID: >G9060

Date Received: /*/


Date Analyzed: 11/15''39


CONCENTRATION UNITS:lug/L or ug/KgJUG/L

CAS NUMBER

01. 141-78-602.03.04.

COMPOUND NAME


RT

5.116.468.947.88

EST. CONC

430733613

Q

BJBJBJBJ

FORM I SU-TIC 117 1/87

IDPESTICIDE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO

Lab Name: ETCN3

Lab Code: Case No.:


Sample wt/vols 910.0 Cg/mL) ML


SMoisture: not dec. dec.

Extraction: ISepF/Cont/Sonc) SEPF


Cont ract:

SAS No.: SD6 No.:

Lab Sample ID: CA1379G

Lab File ID: >HA292

Date Received: O<?/a<?//9

Date Extracted: 10-'Q4"89


Dilution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UG/L Q

319-64-6 -----319-65-7 ————319-86-8 ————58-89-9 —— ——76-44-8 ------309-00-2 -----1024-57-3 ———959-98-8 -----60-57-1 — -- —72-55-9 ------72-20-8 - —— —33213-65-9 ——72-54-8 —————1031-07-8 ———50-29-3 —— ——72-43-5 —————53494-70-5 ——5103-71-9 ———5103-74-2 ———8001-35-2 ———12674-11-2 ——

- 11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-82-5 ——

—— aloha-BHC—— beta-BHC—— delta-BHC---oamma-BHCCLindane )---Heptach lorm---Aldr in— — — Hep tachlor epoxide---Endosu 1 fan I- - - D i e 1 d r i n—— 4.4'-DDE---Endr in ,,,—— Endoaulfan I I—— 4.4'-DDD---Endosu 1 fan aulfate—— 4.4'-DDT---Methoxyehlor---Endrin ketone .,„„,,.---* Ipha-Ch lordane „_. „---gamma-Ch lordane „ , „., ,„---Toxaphene , , .„—— Aroc lor-1016—— Aroclor-1221 ,.,. „—— Aroclor-1232 „_ — Aroclor-1242——— Aroc lor-1249---Aroe lor-1254_ii _., ,—— Aroclor-1260

.055

.055

.055

.055

.055

.055

.055

.055

.110

.110

.110

.110

.110.110.110.550.110.055.0552.200.550.550.550.550.5501.1001.100

1IDIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU 1IU IIUIUIUIUIUIUIUIU1

FORM I PEST l-'37 Rev

118

IDPESTICIDE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:





Ex tract ion: (SepF/Cont/Sonc) SEPF


Cont rac t:

SAS No.: SDG No.:


Lab File ID: >HA293

Date Received: O9/


Date Analyzed: 1Q/31'89



319-64-6 -----319-65-7 ————319-86-8 ————59-89-9 —————76-44-8 ------309-00-2 ————1024-57-3 ———959-98-8 ————60-57-1 ------72-55-9 —————72-20-8 ------33213-65-9 ——72-54-8 —— — -1031-07-8 ———50-29-3 —————72-43-5 —————53494-70-5 ——5103-71-9 ———5103-74-2 ———8001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-82-5 ——

1

—— aloha-BHC—— beta-BHC—— dalta-BHC---aamma-BHCCLindane )---Heptach lor— -Aldr in---Heptach lor epoxide---Endoau 1 f an I n— -Dieldr in—— 4.4'-DDE---Endr in---Endoaul fan I I—— 4r4'-DDD---End omul fan au 1 f a te—— 4r4'-DOT---Mathoxyehlor---Endrin k«tone._ ,.,,__— -a lph«-Ch lordan* _ ,_,---gamma-Ch lordana— -Toxaphena _. _„ i i m i ,—— Aroclor-1016—— Arnclor-1221 _, „..., .—— Aroclor-1232..,, ,,..„„.,- — Aroelor-1242- — Apoc\or-1248—— Aroclor-1254—— Aroclor-1260

.057

.057

.057

.057

.057

.057

.057

.057

. 110

.110

. 110

.110

.110

.110

.110

.570

.110

.057

.0572,300.570.570.570.570.5701.1001. 100

1IUIUIUIUIU!UIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

FORM I PEST 1/87 Re>

1 19

IDPESTICIDE QRGANICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: CaoiI/water) WATER

Sample ut/vo 1 : 810.0 (g/mL) ML





Cont rac t:

SAS No.: SDG No.:


Lab File ID: >HA288

Date Received: oq/a«/t*l

Date Extracted: 10/Q*+-'39



CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg 3 UG/L

319-64-6 -----319-65-7 ————319-86-8 -----58-89-9 ----- -76-44-8 —————309-00-2 -----1024-57-3 - ——959-98-8 -----60-57-1 —————72-55-9 —————72-20-3 —————33213-65-9 ---72-54-8 ------1031-07-8 «--50-29-3 —————72-43-5 ------53494-70-5 ——5103-71-9 ———5103-74-2 ———8001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-32-5 ——

—— alpha-BHC—— beta-BHC—— delta-BHC---qamma-BHCCLindane )---Heptaeh lor , nniii

—— Aldr in---Heptachlor epoxide---Endosul fan 1---Die Idr in_--4.4'-DDE---Endr in---Endoaulfan II—— 4.4'-DDD---Endoaul fan aulfate—— 4.4l-DDT---Methoxychlor—— Endrin katone---« Ipha-Ch lordana n_ n m i i i--- gamma- Ch lordana _, _.- - ~ To x A p h e n e_--Apoclor-1016——— Aroelor-1221 „,,,„„,—— Aroclor-1232---Aroclor-1242— -Aroelor-1248——— ArQelor-1254——— Aroelor-1260

.062

.062

.062

.062

.062

.062

.062

.062

.120

.120

. 120

.120

.120

.120

.120

.620

. 120

.062

.0622.500.620.620.620,620.6201.2001.200

I1UIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

FORM I PEST 1/37 Rev.

120


ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Ma t P i x: (soil/wa t e r) WATER


Leva 1: Clow/mad) LQU




Contract :



Lab File ID: >HA326

Date Received:

Date Extrected: 10/06X89

Date Analyzed! 11/02/99



FORM I PEST

Q

319-64-6 ————319-65-7 ————319-86-8 ————58-89-9 —————76-44-8 —————309-00-2 ————1024-57-3 ———959-98-8 ————60-57-1 —————72-55-9--- ——72-20-8 —————33213-65-9 ——72-54-8 —————1031-07-8 ———50-29-3 —————72-43-5 —————53494-70-5 ——5103-71-9 ———5103-74-2 ———8001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-82-5 ——

—— alpha-BHC—— bet*-BHC—— delta-BHC---gamma-BHCCLindane )---Hap t ach lor .,__—— Aldrin---Haptaehlor epox ide—— Endosulfan I---Dia Idr in—— 4r4'-DDE---Cndr in—— Endosulfan II—— 4r4'-DDD---Endosu 1 fan su 1 f ate—— 4r4'-DDT— -Mathoxych lor---Endrin katona—— a Ipha-Ch lordane---qamma-Chlordana niniiii MII _---Toxaphena—— Aroclor-1016—— Aroelor-1221- — Aroelor-1232—— Aroelor-1242—— Aroclor-1248—— Aroelor-1254—— Aroe lor-1260

.053

.053

.053

.053

.053

.053

.053

.053

.110

.110

.110

.110

.110

.110

.110

.530

.110

.530

.5302.100.530.530.530.530.5301.1001.100

1IUIUIUIUIUIUIUIUIU1UIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

1/87 Rev121


SPA SAMPLF NO,

Lab Name: ETCNJ

Lab Code:

Cont ract:

Case No.:

Ma t r i x : (soil /wa t e r ) UATER

Sample wt/vol: 940,0 Cg/mL) ML

Level : ( low/mad) LOU



Lab File ID: >HA327

Date Received:


Extraction: (SepF/Con t /Sonc ) CONT


CAS NO. COMPOUND



Di lut ion Factor

CONCENTRATION UNITS:(ug/L or ug/Kg> UG/L

319-64-6 ——————— alpha-BHC________319-65-7———————beta-BHC_________319-86-8 ——————— delta-BHC________58-89-9 ——————— -gamma-BHCCLindane).76-44-8 —— - ———— Heptachlor_______309-00-2 —————— Aldrin__________1024-57-3 —————— Heptachlor epoxide959-98-8 ——————— Endosulfan I_____60-57-1————————Dieldrin_________72-55-9 ———————— 4,4'-DDE_________72-20-8 ———————— Endrin___________33213-65-9—————Endosulfan II_____72-54-8 ———————— 4,4'-ODD_________1031-07-8 ——— —— Endosulfan sulfate50-29-3————————4,4'-DOT_________72-43-5————————Methoxychlor_____53494-70-5 ————— Endrin ketone_____5103-71-9—————alpha-Chlordane__5103-74-2————-gamma-Chlordane___8001-35-2——————Toxaphene________12674-11-2—————Aroclor-1016_____11104-28-2—————Aroc lor-1221______11141-16-5—————Aroclor-1232______53469-21-9 ————— Aroc lor-1242______12672-29-6 ————— Aroclor-1249______11097-69-1—————Aroclor-1254______11096-82-5 ————— Aroclor-1260______

.053

.053

.053

.053

.053

.053

.053

.053

.110

.110

.110

.110

.110

.110

.110

.530

.110

.530

.5302.100.530.530.530.530.5301.1001.100

IIUIUtuIU1UIUIUIUIUIUIUIUIUIUIUIUIUIUIUmIUIUIUIUIUIUIUI

FORM I PEST 1/87 Rev

122

IDORGAN1CS ANALYSIS DATA SHEET

EPA SAMPLE NO,

Lab Name: ETCNJ-"

Lab Code: Case No.:

Ma t r i x: (soilXwa t e r) UATER


Level: tlow/med) LOW

Con t ract:

SAS No.:




CAS NO. COMPOUND

SDG No.:


Lab File ID: >JA487

Date Received: *»/•«"*



Dilution Factor : 1


1319-64-6 -----319-65-7 -----319-86-8 ————58-89-9 —————76-44-8 —————309-00-2 -----1024-57-3 ———959-98-8 ————6Q-57-1 -----72-55-9 -----72-20-8 —————33213-65-9 ——72-54-8 —————1031-07-8 ———50-29-3 —————72-43-5 —————53494- 7U-5 ——5103-71-rf ———

8001-35-&— —12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-82-5 ——

—— alpha-BHC—— beta-BHC—— delta-BHC---aamma-BHCCLindane )---Heptach lor— -Aldr in---Heotach lor eoox ide---Endosulfan I---Dieldrin ,_B—— 4.4'-DDE---Endrin ,_---Endoau 1 fan I I—— 4.4'-DDO---Endosul fan sul f ate—— 4r4'-DDT---Mathoxyeh IQP— -Endp in katona- —— alpha-Ch lopdane „ .,— — •gamma-Ch lopdantt „ __—— Toxaphene ,—— Aroclor-1016—— Arnclop-1221— -Arnclop-1232—— Aroelop-1242—— Aroclop-1248——— Apne lop-1254—— ApnelQp-1260

.052

.052

.052

.052

.052

.052

.052

.052

.100

.100

.100

.100, 100.100.100.520.100.052.0522.100.520.520.520.520.52011

1mIUIUIUIU1UIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

FORM I PEST123

1/87

IDORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETCNj'"

Lab Code: Case No.:

Matrix: (»oi I/water) WATER


Level: Clow/mod) LOLJ




Cont rac t:

SAS No.: SDG No.:


Lab File ID: >JA488

Date Received: /a/0"/**





319-64-6 ——————319-65-7 ——————319-86-8 ——————58-89-9 ———————76-44-8 ———————309-00-2 ——————1024-57-3 —————959-98-8 ——————60-57-1 ———————72-55-9 ———————72-20-8 ———————33213-65-9 ————72-54-8 ———————1031-07-9 —————50-29-3 ———————72-43-5 ———————53494-7&r9-—— —5103-7l£» —————5103-74*2 —————8001-35 5 ————12674-11-2 ————11104-28-2 ————11141-16-5 ————53469-21-9 ————12672-29-6 ————11097-69-1 ————11096-82-5 ————

-alDha-BHC-beta-BHC-delta-BHC-qamma-BHCCLindane )-Heptach lor-Aldr in— Hep tachlor epoxide-Endosul fan I ,.-Dieldrin-4.4'-DDE-Endr in-Endoau 1 fan I I-4r4'-DDD-Endosulfan aulfate-4r4'-DDT-Mathoxych lor ,_-Endr in katone „-a Lpha-Ch lardane-g«mm*-Ch lordane-Toxaphane ,__-Aroelor-1016-Aroclor-1221-Aroclor-1232-Aroelnr-1242-Aroelor-1248-Aroclor-1254-Aroclor-1260

.057

.057

.057

.057

.057

.057

.057

.057

.110

.110

.110

.110

.110

.110

.110

.570

.110

.057

.0572.300.570.570.570.570,5701.100I. 100

1IUIUmIUIUIUIUIU .IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

' IUIU1

FORM I PEST124

1/87 Rev


EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:


Sample wt/vol: 900,0 Cg/mL) ML


X Moisture: not dec. dee.

Extraction: (SepF/Cont/Sonc) SERF-


Cont ract:

SAS No.: SDG No.:

Lab Sample . ID: CA1897G

Lab File ID: >JA489

Date Received: "••*/**



Dilution Factor: 1


319-64-6 ——————— alpha-BHC________319-65-7———————beta-BHC_________319-86-8——————delta-BHC_______58-89-9 —————— --gamma-BHC(Lindane).76-44-8————————Heptachlor_______309-00-2 —————— Aldrin__________1024-57-3 —————— Heptachlor epoxide.959-98-8 ——————— Endosulfan I_____60-57-1 ———————— Oicldrin_________72-55-9 ———————— 4,4'-DDE_________72-20-8————————Endrin___________33213-65-9 ————— Endosulfan II_____72-54-8 ———————— 4,4'-ODD_________1031-07-8———-—Endosulfan sulfate.50-29-3 ———————— 4,4'-DOT_________72-43-5-s——————M«thoxychlor_____53494-70-9-————Endrin ketone____5103-71^*—————alpha-Chlordane__51Q3-74RS-—————g«mma-Chlord«ne___8001-39-2-—————Toxaphene________12674-11-2—————Aroclor-1016_____11104-28-2—————Aroc lor-1221_____11141-16-5—————Aroc lor-1232_____53469-21-9 ————— Aroc lor-1242_____12672-29-6—————Aroc lor-1248_____11097-69-1—————Aroc lor-1254_____11036-82-5 ————— Aroc lor-1260_____

.056.056.056.056.056.056.056.056.110.110.110.110.110.110.110.560.110.056.0562 . 2 0 0.560.560.560.560.5601.1001.100

ID!UIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI


125

IDJ9PC9TICIDE ORGANICS ANALYSIS DATA SHEET

ERA SAMPLE NO

Lab Name: ETCNJ?

Lab Code: Case No.:



Level: (low/med) LQLJ

Cont ract:

SAS No.:




SDG No.:


Lab File ID: >JA490

Date Received: "



Dilut ion Factor: 1


319-64-6 ——————— alpha-BHC________319-65-7———————beta-BHC_________319-86-8———————delta-BHC________58-89-9--————gamma-BHCCLindane).76-44-8———————-Heptachlor_______309-00-2———————Aldrin___________1024-57-3——-——Heptachlor epoxide959-98-8 ——————— Endosulfan I_____60-57-1————————Oieldrin_________72-55-9 ———————— 4,4'-DDE_________72-20-8 ———————— Endrin___________33213-65-9 ————— Endosulfan 1 I____72-54-8 ———————— 4,4'-DOO_________1031-07-8-————-Endosulfan sulfate50-29-3————————4,4'-DOT_________72-43-5-———————Methoxychlor______53494-70>-S-—-——Endrin ketone_____5103-71-*-—————alpha-Chlordane___51Q3-74j»J<-"—--—gamma-Ch lordane__8001-3^2---———Toxaphene_______12674-11-2—————Aroc lor-1016_____11104-28-2 ————— Aroc lor-1221_____11141-16-5—————Aroc lor-1232_____53469-21-9 ————— Aroc lor-1242_____12672-29-6 ————— Aroc lor-1248_____11097-69-1 ————— Aroc lor-1254_____11096-82-5—————Aroc lor-1260_____

.053

.053

.053

.053

.053

.053

.053

.053

.110

.110

.110

.110

.110

.110

.110

.530

.110 •

.053

.0532.100.530.530.530.530.5301.1001.100

IIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU


126

IDdtBBTICIDE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: ETCN3' ~

Lab Coda: Case No.:



Level: Clow/medi LOW


Extract ion: (SepFVCont/Sonc) SEPF


Cont ract:

SAS No.: SDG No.:


Lab File ID: >JA492

Date Received: /o/o*/'9





319-64-6 ——————— alpha-BHC________319-65-7———————b«ta-BHC_________319-86-8 ——————— delta-BHC________58-89-9--————--gamma-BHC(Lindane).76-44-8————————Hep tech lor_______309-00-2———————Aldrin___________1024-57-3 —————— Heptachlor epoxide959-98-8 ——————— Endosulfan I_____60-57-1 ———————— Dieldrin_________72-55-9 ———————— 4,4'-ODE_________72-20-8 ———————— Endr in___________33213-65-9 ————— Endosulfan II____72-54-8————————4,4'-ODD_________1031-07-8—— ——— Endosulfan sulfat*50-29-3 ———————— 4,4'-DOT_________72-43-5-.———————Methoxychlor_____53494-70-5-—-—Endrin ketone____5103-71-$-;—————alpha-Chlordane___5103-74-r2-f---——g«mma-Chlordane___8001-3#-2—————Toxaphene________12674-11-2—————Aroc lor-1016_____11104-28-2—————Aroc lor-1221_____11141-16-5—————Aroc lor-1232_____53469-21-9—————Aroc lor-1242_____12672-29-6—————Aroc lor-1248_____11097-69-1 ————— Aroc lor-1254_____11096-82-5—— ---Aroclor-1260_____

.051

.051

.051

.051

.051

.051

.051

.051

.100

.100

.100

.100

.100

.100

.100

.510

.100

.051

.0512.510.510.510.510.51011

IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI UIUIUIUI


127

IDICIDE QRGANICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETC!

Lab Code: Case No.:



Level: Uaw/med) LQU


Extraction: (SepF/Cont/Sonc> SERF


Contract:

SAS No.: SDG No.:

Lab Sample 10: CA2138G

Lab File ID: >JA493

Date Received: /o/»«//f



Dilution Factor: 1


319-64-6—319-65-7—319-86-8—58-89-9 ——76-44-8 ——3D9-OQ-2--1024-57-3-959-98-8--60-57-1 ——72-55-9 ——72-20-8 ——33213-65-972-54-8 ——1031-07-8-50-29-3-r-72-43-5 ——53494- 7&951Q3-7ft|f5103-74£g8001-39»£12674-11*811104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

————— alpha-BHC————— beta-BHC————— delta-BHC_ ———— qamma-BHCCLindane)————— Heptachlor_ ———— Aldrin————— Heptachlor epoxide------Endosu 1 f an I— -_ — Oieldr in „ „ _————— 4 r4'-DDE--- ——— Endrin, m

------ Endoaulfan 1 1————— 4.4--ODD——— -- Endosu 1 fan su If ate————— 4.4'-DDT

*{5^—— Cndrin k«tona_ in i i ia_ ,i-- — — «lph«-Ch lordana^•••'•-qaama-Ch lordane

&u ———— Aroelor-1016 .,————— Aroelor-1221 „„,————— Aroelor-1232—————— ftrnelflr-1242 .—————— Araclor-1249,—————— Aroe lor- 1254—————— Arnelor-1260

.053

.053.053.053.053.053.053.053.110. 110.110.110.110,110.110.530.110.053.0532.100.530.530.530.530.5301.1001.100

1IUIUIUIUIUtuIUIU

• iuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI


128


EPA SAMPLE NO,

Lab Name: ETCNJ Contract:


Matrix: <soi1/water) WATER Lab Sample ID: CA2139G

Sample wt/vol: 900.0 (g/mL) ML Lab File ID: >JA501

Level: Clow/med) LOU Date Received: '

SMoiature: not dec. dec. Date Extracted:

Extraction: (SepFxCon t /Sonc ) SEPF

GPC Cleanup: (Y/NJ N pH:

CAS NO. COMPOUND

Date Analyzed: 11/08



319-64-6 ————319-65-7 ————319-86-8 ————58-89-9 —————76-44-8 —————309-00-2 ————1024-57-3 ———959-98-8 ————60-57-1 —————72-55-9 —————72-20-8 —————33213-65-9 ——72-54-8 —————1031-07-8 ———50-29-3-, ————72-43-5 —————53494-70-5 ——5103-71-9 ———5103-74-2 ———8001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-82-5 ——

—— aloha-BHC—— beta-BHC—— delta-BHC---qamma-BHCCLindane )---Heptach lor ,—— Aldr in---Heptach lor epox ide---Endosu 1 fan I---Die Idr in ,—— 4.4'-DDE---Endr in---Endoaul fan II—— 4f4'-DDD---Endosu 1 fan au 1 f ate—— 4.4--DDT---Methoxych lor , i n i - i IM- — Endrin ketona _---alpha-Ch lordane— -qamm*-Ch lordane _ ,, MI _---Toxaphene .— -Aroelor-1016—— Aroclor-1221—— Aroclor-1232—— Aroelor-1242-,_Aroclnr-124a— -Aroc Lop-1254——— Aroelor-1260

.056

.056

.056

.056

.056

.056

.056

.056

.110

.110

.110

.110,110.110.110.560.110.056.0562.200.560.560.560.560.5601.1001.100

1IUIUIUIUIUIU!UIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

FORM I PEST

1291x87 Rev


EF'A SrtMPLE NO.

Lab Name: ETCNJ

Lab Code: Case Ho.:

Mat P ix: (501 l/uater ) UIATER

Sample wt/vol: 900 .0 t g-'mL) ML

Level: ( low/med) LOW

S M o i s t u r e i n o t d e c . dec.

Extract ion: (SepF/Cont /Sonc ) SERF

GPC Cleanup: (Y/NJ N pH:

Lon tract:

SnS No.: SDG No.:

Lab Sample ID: CA214QG

Lab Ftle ID: >JA502

Date Received: i

Date Extracted:


D i lut ion Factor: 1


319-64-6 ————319-65-7 ————319-86-8 ————58-89-9 ------76-44-8 ------309-00-2 ————1024-57-3 ———959-98-8-----60-57-1 —————72-55-9 ------72-20-3 —— ——33213-65-9 ——72-54-8 —————1031-07-8 ———50-29-3-.. ————72-43-5 —————53494-70-5 ——5103-71-9 ———5103-74-2 ———9001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ---12672-29-6 ——11097-69-1 ——11096-32-5 ——

—— alpha-BHC—— beta-BHC—— delta-8HC---aamma-BHCCLindane j---Hept ach lor---Aldr in---Heptachlor epoxide---Endosu 1 fan I---Dieldrin—— 4.4'-DDE---Endr in---Endosu 1 fan I I—— 4.4'-DDD---Endosu If an sulfate—— 4.4--DDT---Methoxychlor---Endrin katone---alpha-Ch lordane---gamma-Ch lordane---Toxaphane aimm , , ,—— Aroclor-1016——— Aroclor-1221 „ _„, , ,—— Aroclor-1232---Aroclor-124'2— -Hrcc lor-1243__.Aroc lor-1254—— Aroc lor-1260

.056

. 056,056. 056.056. 056.056. 056.110. 110. 110.110.110. 110. 110.560.110. 056. 0562.200.560.560.560.560.5601. 1001.100

1 1IU 1IU IIU 1IU 1IU 1IU 1tu tIU 1IU 1IU 1IU 1IU 1tu iIU 1IU tIU 1IU 1IU 1IU I1 U 1IU iIU :IU iIU 1IU 1IU 1IU 11 1

FORM I PEST 1301/37

IDPESTICIDE ORGAN ICS ANALYSIS D' TA SHEET

ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:







Cont ract:

SAS No.: SDG No.:


Lab File ID: >HA552

Date Received: lO/'C-/*

Date Extracted: lQ/12'89




319-64-6 ————3-19-65-7 ————319-86-8 ————58-89-9 —————76-44-8 —————•309-00-2 ————1024-57-3 ———959-98-8 ————60-57-1 —————72-55-9 —————72-20-8 —————33213-65-9 ——72-54-8 —————1031-07-8 ———50-29-3 —————72-43-5 —————53494-70-5 ——5103-71-9 ———5103-74-2 ———8001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-82-5 ——

—— alpha-BHC---beta-BHC—— delta-BHC---aamma-BHCCLindane )---Heptach lor—— Aldr in— ——Hep t ach lor epoxide---Endosu 1 f an I ,.,---Die Idr in „—— 4.4'-DDE---Endr in— -Endosulf an I I—— 4.4--DDD—— Endosu If an sulf ate—— 4.4--DDT---Methoxyehlor---En dp in ketone---a Ipha-Ch lopdane mm_- — gamma-Ch lordana IM i i m > i i nii- - - To x a p h a n •—— Apoclor-1016—— Apeelor-1221—— Apoclor-1232—— Aroelor-1242—— Apoelor-1248_-_Arcielop-1254——— Apoelor-1260

.060

.060

.060

.060

.060

.060

. 060

.060

.120

.120

.120

.120

.120

.120

.120

.600

.120

.060

. 0602.400.600.600.600.600.6001.2001.200

1IUIDIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1


131

1ID

PESTICIDE ORGANICS ANALYSIS DATA SHEETEPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:


Sample wt/vol: 940.0 Cg/mD ML





Cont ract:

SAS No.: SDG No,:


Lab File ID: >HA553

Date Received: io/jo/8^

Date Extracted: 10/12'89


Dilut ion Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/KgJ UG/L

319-64-6 ————719-65-7 ————319-86-8 ————58-89-9 —————76-44-8 —————309-00-2 ————1024-57-3 ———959-98-8 ————6Q-57-1 —————72-55-9-- ———72-20-8 —————33213-65-9 ——72-54-8 —————1031-07-8 ———50-29-3 —————72-43-5 —————53494-70-5 ——5103-71-9 ———5103-74-2 ———8001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-82-5 ——

— -alpha-BHC—— beta-BHC—— delta-BHC---gamma-BHCCLindana )—— Heptachlor---Aldr in---Haptach lor eoox ide---Endosu 1 f an I mnii imin---Dieldrin „„ .,—— 4.4'-DDE---Endr in---Endosu 1 fan I I—— 4.4--DDD— -Endosu If an aulfate—— 4.4'-DDT---Methoxyehlor---Endr in Uetona---alpha-Chlardana n i m i i i i i i mi M

-• — gamma-Ch lordana _„ iinii_ n , . ,.,—— Toxaphana——— Aror lor-1016—— Aroelor-1221—— Arnelar-1232——— Areelnr-1242——— Arnelor-1248——— Aroclar-1254——— Arne lnr-1260

.053

.053

.053

.053

.053

.053

.053

.053

.110

. 110

.110

.110

.110

.110

.110

.530

.110

.053

.0532.100.530.530.530.530.5301. 1001. 100

iIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIU1


132


EPA SAMPLE NO.

Lab Name: ETCNO-,

Lab Coda: Case No.:


Sample wt/voli 990.0 Cg/mL) ML





CAS NO. COMPOUND

Cont ract:

SAS No.: SDG No.:


Lab File ID: >HA554

Date Received: l°/'°





319-64-6 ——————— alpha-BHC________319-65-7———————beta-BHC_________319-86-8 ——————— delta-BHC________58-89-9————-—-gamma-BHC(Lindane).76-44-8 ———————— Heptachlor_______309-00-2 ——————— Aldrin___________1024-57-3——————Heptachlor epoxide959-98-8 ——————— Endosulfan I_____60-57-1 ———————— Dieldr in_________72-55-9———————4,4'-DDE_________72-20-8 ———————— Endr in___________33213-65-9 ————— Endosulfan II____72-54-8————————4,4'-DDO_________1031-07-8 ————— -Endosulfan sulfate50-29-3 ———————— 4,4 '-DOT_________72-43-5———————-Methoxychlor_____53494-70-5 ————— Endrin ketone____5103-71-9 —————— alph.-Chlordane___5103-74-2--———gamma-Chlordane___8QQ1-35-2---———Toxaphene_______12674-llr2—————Aroclor-1016_____11104-2t--2—————Aroc lor-1221_____11141-16-5—————Aroclor-1232_____53469-21-9 ————— Aroc lor-1242_____12672-29-6—————Aroc lor-1248_____11097-69-1 ————— Aroc lor-1254_____11096-82-5—————Aroc lor-1260_____

,051.051,051.051.051.051.051.051.100.100.100.100.100.100.100.510.100, 051.0512.510.510.510.510.51011

IIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1UIUIUIUIUIUIUIUIUIU1UI


133


ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:


Sample wtxvol: 950.0 (g/mL) ML

Level: tlow/med) LQLJ

?4 Moisture: not dec. dec.

Extraction: CSepF/Cont/Sane) SEPF


Cont ract:

SAS No.: SDG No.:


Lab File ID: >HA555

Date Received: ltf/io/9^

Date Extracted: 10/12-'89

Date Analyzed: 11/15''39

Dilution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UG'L

319-64-6 ————319-65-7 ————319-86-8 ————58-89-9 —————76-44-8 —————309-00-2 ————1024-57-3 ———959-98-8 ————6Q-57-1 —————72-55-9 —————72-20-8 —————33213-65-9 ——72-54-8 —————1031-07-8 ———50-29-3 —————72-43-5 —————53494-70-5 ——5103-71-9 ———5103-74-2 ———8001-35-2 ———12674-11-2 ——11104-29-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-82-5 ——

—— alpha-BHC—— beta-BHC—— delta-BHC---aamma-BHCCLindane )- — Haptachlor „,,„ „. ,—— Aldr in---Haotachlor eoox ide---Endoaul fan 1 ,,---Die Idr in—— 4.4'-DDE---Endrin—— Endoaulf an I I—— 4.4'-DDD—— Endoaulf an aulf ate .—— 4.4'-DDT---Me thnx«jch lor—— Endrin katone---a Ipha-Ch lordane „—— qamma-Ch lordane , .. ,---Toxaphene „, ,„, „„, „..—— Aroelor-1016—— Aroclor-1221—— Aroclor-1232—— Aroelor-1242—— Apoclor-1248—— Aroclor-1254—— Aroelor-1260

.053

.053

.053

.053

.053

.053

.053

.053

.110

.110

.110

. 110

.110

.110

.110

.530

.110

.053

.0532.100.530.530.530.530.5301. 1001.100

11UIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

FORM I PEST 1 '87

134


ERA SAMPLE' NO.

Lab Name: ETCN3

Lab Code: Case No.:





Extraction: CSepF/Cont/Sonc> SEPF


Contract:

SAS No.: SDG No.:


Lab File ID': >HA566

Date Received: 10x10/99





319-64-6 -----319-65-7 ————319-86-8 ————58-89-9 ------76-44-8 —————309-00-2 ————1024-57-3 ———959-98-8 -----60-57-1 —————72-55-9 —————72-20-8 —————33213-65-9 ——72-54-8 —————1031-07-8 ———50-29-3 —————72-43-5 —————53494-70-5 ——5103-71-9 ———5103-74-2 ———8001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-82-5 ——

—— alpha-BHC—— beta-BHC—— delta-BHC---gamma-BHC(Lindane )---Heptach lor---Aldr in „ ,„— — — Heptaehlor epoxide—— Endoaulfan I---Qia Idr in.,,—— 4r4'-ODE---Endr in „ ,,---Endoau 1 fan I I—— 4.4--DDD---Endoaulfan aulfate—— 4.4l-DDT---Methoxychlor---Cndr in keton*— -alpha-Ch lordane __.. ,_,--- gamma -Ch lordane---Taxaphene—— ArQelop-1016—— Aroclor-1221 „—— Aroclor-1232—— Aroclor-1242——— Aroelor-1248——— Aroelnr-1254 , n——— Aroclor-126n

.054

.054

.054

.054

.054

.054

.054

.054

.110

.110

.110

.110

.110

.110

.110

.540

.110

.054

.0542.200.540.540.540.540.5401.1001.100

1IDIUIDIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIU1


135

ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET

Lab Name: ETCNJfl•Of.

Lab Code: Caae No.:

Matrix: (soil/watep) UATER

Sample wt/vol: 950.0 Cg/roL) ML





Contract:

SAS No.: SDG No.:


Lab File ID: >HA556

Date Received: 10/1





319-64-6 ——————— alpha-BHC________319-65-7———————beta-BHC_________319-86-8 ——————— delta-BHC________58-89-9 —————— — gamma-BHCCLindane).76-44-8 ——————— -Heptachlor_______309-00-2 ——————— Aldpin___________1024-57-3—————Heptachlop epoxide.959-98-8———————Endosulfan I_____60-57-1————————Dieldrin_________72-55-9 ———————— 4,4'-DDE_________72-20-8 ———————— Endpin___________33213-65-9 ————— Endoaulfan II____72-54-8 ———————— 4,4'-ODD_________1031-07-8 ————— Endosulfan sulfate.5Q-29-3 ———————— 4,4'-DOT_________72-43-5---------Methoxychlop_____53494-70-5—————Endrin ketone____5103-7X-9——————alpha-Chlordane__5103-74-2*---———gamma-Chlordane___

-2*-——•—-Toxaphene________t-r2—————Apoclop-1016_____

11104-28^2—————APOC IOP-1221_____11141-16-9————APOC 1 op-1232_____53469-21-9—————APOC IOP-1242_____12672-29-6—————Apoclor-1248_____11097-69-1 ————— APOC IOP-1254_____11096-82-5—————APOC 1 op-1260_____

.053

.053

.053

.053

.053

.053

.053

.053

.110

.110

.110

.110

.110,110.110.530.110.053.053 -2.100.530.530.530.530.5301.1001.100

IUIUIUtuIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIU


136

2AWATER UOLATILE SURROGATE RECOVERY

Lab Name: ETC Corp. 4-iLeuui alui y Contract:

Lab Code: Case No.: . SAS No.: SDG No

1 EPA1 SAMPLE NO.

01lQC70070y02IQC70070VJ031QC70Q70U041CA1372U05ICA1372US061CA1372<JR071CA1373U08ICA1374U09ICA1376U10ICA1375U11IQC70070U12ICA1377VJ13ICA1382'J14IQC70070U15ICA1378U16ICA2068U17ICA1379U18ICA1380U19ICA2067U1 tfT,201CA2070U »M^211221231241251261271281291301

SI(TOD*

99101989810099979897979999981001009999979896

52(BFB)*

100999997991009695999798989897989696959698

S3(DCE)*

1009810197

10110110510010610310095103969594~96949494

OTHER TOTOUT

00000000Q00000000000

page 1 of

51 (TOL) • Taluene-d852 (BFB) • Bromofluorobenzene53 (DCE) - l,2-Dichloroethane-d4

QC LIMITS(88-1103(86*119)(76-114)

* Column to be used to flag* Ualues outside QC limits0 Surrogates diluted out

recovery values

FORM II UOA -1 137 1X87 Rev

2AWATER VOLATILE SURROGATE RECOVERY

4*T '0/1 •//<*?Lab Name: ETC Corp. f LaLutaLuj./ " Contract:

Lab Code: Case No.: SAS No.: SDG No

page 1 of

01020304050607080910111213

1415161718192021222324252627282930

S]s:s:

EPASAMPLE NO.

QC70076VCA1380V — 'CA1381VCA1383VCA2026VCA2029VCA2032VCA2032VSCA2032VRQC70076VCA2033VCA2031VCA2034VQC70076VCA2027VCA2035VCA2036VCA2037VCA2038VCA2039VCA2040VCA2042VCA2043V

SI(TOL)I

99

99•9898989798989898989898999898989897989992

S2(BFB)|

97

9797979696989898979797989698989796979897107

S3(DCE)|

100

101101103100102100991011001021031049910510410510410599102104

*

OTHER

—————

——————————

—————

——————————

——————————

TOTOUT

0

00000

°0000000o0II0

——

<?•

QC LIMITSL (TOL) - Toluene-d8 (88-110)1 (BFB) - Bromofluoroberuene (86-115)j (DCE) - l,2-Dichloroethane-d4 (76-114)

I Column to be used to flag recovery values* Values outside QC limitsD Surrogates diluted out

FORM II VOA -1 138 1/87 Rev,


Lab Name: ETC Corp. 1 Laboratory Contract:


010203040506070809'101111213114,15116'17i18:1912021122123124125126127128129 I30!

ERASAMPLE NO.

QC70079VQC70079UCA1894UCA1893VCA1893USCA1893URCA1895VCA1897VCA1896UQC70079VCA1897UCA1896UCA2136UCA2137UCA213BVP#2.D*hfV

SI(TOD*

9898989799989787 *939410099979898?7

S2(BFB)*

95959897979797104951029797999798/0&

S3( DCE ) #

9999

1Q310210210299101103112104106103107111too

OTHER TOTOUT

000000010000000

1 -

page 1 of

SI CTOL) - Toluene-d832 CBFB) - BromofluorobenzeneS3 (DCE) - l,2-Dichloroethane-d4

QC LIMITS(88-110)C86-115)C76-114)

t Column to be used to flag* Values outside QC l i m i t sD Surrogates d i l u t e d out

recovery values

FORM II UOA -1 1/87 Rev

139


Lab Nama: ETC Corp. I Laboratory Contract:

Lab Coda: Caaa No.i SAS No.: SDG No.i

1 EPA1 SAMPLE NO.

011QC7Q081U02ICA1778U03ICA1779U04ICA178QU09ICA1783U06IQC70081UQ7ICA1778USQ8ICA1778UR09ICA1790V10ICA1796U11ICA1799U121CA2140U13ICA2140VS -14ICA2140UR1511611711811912012112212312412912*12?' Jj>- ————2B1 f ,' W-991 V!.•?ni ^Jif

SI(TOD*

1001001001019810010010010010098999999

52(BFB)*

97959595949999999898100100100100

S3(DCE)*

1061021051041071001019910010099100102100

OTHER TOTOUT

00000000000000

paga 1 of

SI (TOD * Toluana-dS32 (BFB) * BromofluorobanzanaS3 (DCE) » l,2-Dichloroathana-d4

QC LIMITS(88-110)(86-115)(76-114)

* Column to ba uaad to flag* Ualuas outsida QC limitsD Surrogataa dilutad out

racovary valuas

140FORM II UOA -1 1/87 Rev


Lab Name: ETC Corp. Contract:


010203040506070809101112131415161718192021222324252627282930

EPASAMPLE NO.

QC70083VCA2141VCA2142VCA2143VCA2149VCA2151VCA1891VCA2145VCA2152VCA2153V

———————————

——————————— i

SI(TOL)|

991001001001019796969797

—————

—————1

—————

——— —— i

S2(BFB)I

1021011071021039899105102101

—————

—————

————— i

S3(DCE)#

95939599104100978999100

i

OTHER TOTOUT

0000000000

————— ——

page 1 of

51 (TOL) - Toluene-d852 (BFB) - Bromofluorobenzene53 (DCE) - l,2-Dichloroethane-d4

QC LIMITS(88-110)(86-115)(76-114)

I Column to be used to flag recovery values* Values outside QC limits0 Surrogates diluted out

141FORM II VOA -1 1/87 Rev,


Lab Name: ETC Corp. | Laboratory Contract:

Lab Code: Case No.: SAS No.: SDG NO

010203040506070809101112131415161718192021222324252627282930

, EPASAMPLE NO.

QC70085VQC70085VCA2150VCA2147VCA2144V

———————————

. .

——— ... . — ... ——

SI(TOL)#

104105102104101

—————"

——————————

....... —

S2(BFB)#

98102999291

— ———

S3(DCE)|

104113105101114

—————

———————————————

—————

—————

—————

OTHER

-" •——————————

—————

—————

TOTOUT

00000

——

11

page 1 of

51 (TOL) - Toluene-dS52 (BFB) - Bronofluorobenzene53 (DCE) - 1,2-Dichloroethane-d4

QC LIMITS(81-117)(74-121)(70-121)

i Column to be used to flag recovery values* Values outside QC limitsD Surrogates diluted out

142FORM II VGA -1 1/87 Rev

Lab Name: ETCNJ

Lab Code:

, 2CWATER SEMIUOLATILE SURROGATE RECOVERY

Cont ract:

Case No.: 5AS No.: SDG No

1 EPA1 SAMPLE NO.

01IQC70081C021CA1381CS03ICA1381CR04ICA1379CQ5ICA1380CQ6ICA1381C07109)09 1101111121131141151161171Ifll191201211221231241251261271281291301

SI(NBZ)*

860376777784

S2( FBP ) t

757464707171

S3(TPH)#

139108120121112143 »

S4(PHD*

715048634549

S5C2FP)#

684935673944

56CTBP)#

584958514746

OTHER TOTOUT

000001

•

51 CNBZ) - Nitrobenzene-d552 CFBP) - 2-Fluorobiphenyl53 (TPH) - Terphenyl-dl454 (PHL) - Phenol-d555 C2FP) - 2-Fluorophenol56 CTBP) • 2,4,6-Tribromophenol

QC LIMITS(35-114)(43-116)(33-141)(10- 94)(21-100)(10-123)

t Column to be used to flag* Ualuea outside QC limitsD Surrogates diluted out

recovery values

page 1 of143

FORM II SO -1 1/87 Rev

2CUATER SEMIVOLATILE SURROGATE RECOVERY

Lab Name: ETC Corp, Contract:


1 EFA1 SAMPLE NO.

01IQC70Q82C02ICA1859CS03 ICA1859CR04ICA1893C05ICA1894C06ICA1859C07109 1091101l i t12113114115116117118119120121 122123124125126 1271281291301

SI(NBZ)#

91939092100102

S2(FBP)#

758578788777

S3(TPH)#

119112108117135110

S4(PHD*

3945419 «

3038

S5(2FP)#

665557484558

36(TBP>#

389685847668

OTHER TOTOUT

0001Q0

page 1 of

51 CNBZ) • Nitrobenzene-d?52 (FBP) - 2-Fluorobiphenyl53 CTPH) - Terphenyl-dl454 (PHL) - Phenol-d535 C2FP) - 2-FluorophenolS6 CTBP) • 2,4,6-Tribromophenol

QC LIMITS(35-114)(43-116)(33-141)(10- 94)(21-100)(10-123)

# Column to be used to flag* Ualuca outside OC lim i t sD Surrogates d i l u t e d out

recovery values

144

FORM II SU -1 1/87

Lab Name: ETCNJ

Lab Code:

2CWATER SEMIVOLATILE SURROGATE RECOVERY

Contract:

Case No.: SAS No.: SDG No

010203040506070809101112131415161718192021222324252627282930

EPASAMPLE NO.

QC70086CCA1895CCA1896CCA1897CCA2136CCA2137CCA2138C

——————————————— : ———————

————————————

———————————————————————

———————————

. ———— . . ———— . _ i

SI(NBZ)|

83868680768474

S2(FBP)*

77848580788676

———————————————

——————————

S3(TPH)#

113118117120121124117

—————

——————————

—————

-——————————

. .._

S4(PHL)|

28302438343323

—————

—————

—————

S5(2FP)#

56503943515437

—————

S6(TBP)|

60636980686659

—————

—————

•——————————

—————

OTHER

—————

_

TOTOUT

0000

00

——

. __ 1

51 (NBZ)52 (FBP)53 (TPH)54 (PHL)55 (2FP)56 (TBP)

Nitrobenzene-d52-FluorobiphenylTerphenyl-dl4Phenol-d52-Fluorophenol2,4,6-Tribromophenol

QC LIMITS(35-114)(43-116)(33-141)(10- 94)(21-100)(10-123)

i Column to be used to flag recovery values* Values outside QC limitsD Surrogates diluted out

145

Lab Name: ETCNJ

Lab Code:,

2CWATER SEMIVOLATILE SURROGATE RECOVERY

Cont rac t:

Case No.: SAS Mo.: No

V

1 EPA1 SAMPLE NO.

01IQC70037CQ2ICA1907CR03iCA2139C04ICA1907CS05ICA1907CQ6:CA2140C071OS:09110111112113114:15116! k17118:19:20121!22:23:24125:26127!29129 :30:

SI(N8Z)#

849082837976

S2CFBP)#

823883757070

S3(TPH)#

13312678125129104

S4(PHD*

66604 *717560

3512FP>#

74631 *757561

36ITBPJ*

61630 »787659

U : H£R

•

TO' 'OUTI

'0 I0 :3 10 10 '0 1

:1:1;

t

1

• 1;

tI

tII

I

I

II

51 (NBZ) - Nitrobenzene-d552 (FBP) - 2-Fluorobiphenyl53 CTPH) - Terphenyl-dl454 (PHD - Phenol-d535 (2FP) • 2-FluorophenolS6 ITBP' • 2,4,6-Tribromophenol

page 1 of

Column to be used to flag'-'alues outside QC l i m i t sSurrogates d i luted out

recovery

QC LIMITS(35-114)t43-116)(33-141J110- 945121-10U'110-123)

FOWM M SU -1

Lab Name: ETCNJ

Lab Code:

2CWATER SEMIv-QLATILE SURROGATE RECOVERY

Contract•

Case No.: SAS No.: SOG No

1 EPA1 SAMPLE NO.

01IQC87921C02ICA2139C03ICA2273C04ICA2273CS05ICA2273CR061071081091101111121131141151 >161171181191201211221231241251261271281291301

SICNB2)#

76747676ai

S2(FBP)#

7975727975

S3(TPH)#

114109113105110 '

S4CPHL)#

390 *343636

S5(2FP)#

561 *474549

S6CTBP)#

7720646675

OTHER TOTpur02000

• 1

51 (N8Z>52 (FBP)53 (TPH)54 <PHL>55 <2FP)56 (TBP)

Ni trobenzene-d52-FluorobiphenylTerphenyl-dl4Phenol-d92-FIuorophenol2,4,6-Tribromophenol

OC LIMITSC35-114)(43-116)C33-141)CIO- 94)C21-100)C10-123)

# Column to be used to flag* Values outside QC limits0 Surrogates diluted out

recovery values

page 1 of

FORM II SU -1 147 1x87 Rev.

Lab Name: ETCMJ

Lab Codei »»

2C. WATER SEMIUQLATILE SURROGATE RECOVERY

Contract:


1 EPA1 SAMPLE NO.

01IQC70092C02ICA1889C03ICA1890C04ICA1892C09ICA1908C06ICA2141C07ICA2142C08ICA2143C09ICA2149C1QICA2151C11ICA1891C12ICA2144C13ICA2145C14ICA2146C15ICA2192C1611711811912012112212312412512612712812913fll

51(NQZ>*

716773778870669081717673797677

»

52CFBP)*

696369748964598875707373807877

S3(TPH)#

1181161181131411129997106107112977888114

54( PHL ) *

6874716573746662717136552 •4 •76

S5(2FP)#

7069716378777065707641630 •1 •80

56(TBP)«

5056575548546655926133700 »0 •

58

OTHER TOTOUT

000000000000330 -1

52 CFB*)53 (TPH)54 (PHL)S9 (2FP)56 (TBP)

Nitrobenzene-d92-FluorobiphenylTerphenyl-dl4Phenol-d52-Fluorophenol2,4,6-Tribromophenol

QC LIMITS(39-114)(43-116)(33-141)(10- 94)(21-100)(10-123)

# Column to be used to flag* Values outside QC l i m i t sD Surrogates d i l u t e d out

recovery values

page 1 of

FORM II SU -1 148 1/87 Rev

Lab Name: ET

Lab Code:

2CWATER SEri I VOLATILE SURROGATE RECOUERY

Contract:


1 EPA1 SAMPLE NO.

01IQC70098C '021CA2150C03104105106 t071081091101lit121131141151161171181191201211221231241251261271281291 - 1301 ""1

SIC NBZ ) *

8476

i

S2( F8P ) *

7676

S3(TPH)#

107108

54(PHL)#

3633

S5(2FP)#

5644

56(TBP)#

7067

OTHER ITOTOUT

Q0

51 (NBZ)52 CFBP)53 CTPH)54 (PHD55 C2FP)56 (TBP)

Nitrobenzene-d52-FluorobiphenylTerphenyl-dl4Phenol-d52-Fluorophenol2 ,4,6-Tr ibromopheno 1

QC LiniTS(35-114)C43-116)(33-141)(10- 94)(21-100)(10-123)

* Column to be used to flag* Values outside QC l i m i t s0 Surrogates diluted out

recovery values

page 1 of 149FORM II S«J -1 1/87 Rev

Lab Name: ETCNJ

Lab Code:

2EWATER PESTICIDE SURROGATE RECOVERY

Cont rac t:


1 EPA1 SAMPLE NO.

011QC70030G02ICA1907G03ICA1907GS04ICA1907GR05ICA2139G06ICA2140G0710910911011111211311411511611711811912012112212312412512612712fll2913D1

SICDBO*

956187777063

OTHER TOTOUT

000000

SI (DBC) - D i b u t y l c h l o r e n d a t e

ADUISORYQC LIMITS(24-154)

page 1 of

*'Column to be used to flag recovery values* Ualues outside QC lim i t sD Surrogates diluted out

FORM II PEST-1 150 1/87 Rev

Lab Name: ETCNJ

Lab Code:


Cont rac t :


1 EPA1 SAMPLE NO.

01IQC70045G02ICA1381G03ICA1381GS04ICA1381GR05ICA1379GQ61CA138QG07ICA1374G08109110111112113114115116117113119 t201211221231241251261271281291301

SICDBC)*

122127721388492216 •

OTHER TOTOUT

0000001

SI CDBC) - Dibutylchlorendate

ADVISORYQC LIMITS(24-154J

page 1 of

# Column to be used to flag recovery values* Ualues outside QC l i m i t sD Surrogates diluted out

FORM II PEST-1 1/87 Re>

151

Lab Name: ETCNJ

Lab Code:

2EUATER PESTICIDE SURROGATE RECOVERY

Cont ract:


1 EPA1 SAMPLE NO.

01IQC70046G02ICA1661GS03ICA1861GR04ICA1893G05ICA1894G061CA1861G071081091101111121131141151161171181191201211221231241251261271281291301

SI( Dec ) *114142137109145126

OTHER TOTOUT

000000

SI (DBC) - Dibutylchlorandata

ADUISORYQC LIMITS(24-154)

# Column to be used to flag* Values outside QC limitsD Surrogates diluted out

recovery values

page 1 of

FORM II PEST-1 1/87 Rev

152


Contract:

No.: SAS No. : SDG No

1 EPA1 SAMPLE NO.

01IQC70048G021CA1S95G03ICA1896G041CA1897G05ICA2136G06ICA2137G07ICA2138G08109 1101111121131141151161171181191201211221231241251261271281*S9I30 r

SICDBO*

241301281213180300 »244 »

OTHER TOTOUT

1111111

Dibutylchlorendate

ADVISORYQC LIMITS(24-154)

* Column to be used to flag* Values outside QC limitsD Surrogates diluted out

recovery valuea

page 1 of

FORM II PEST-1 1/87

153

Lab Name

Lab Code


Contract'

No.: SAS No.: SOG No

1 EPAI SAMPLE NO.

Q1IQC70050G02ICA1889G031CA1890G04ICA1892G05ICA1908G061CA2141G07ICA2142G08ICA2143G09ICA2149G10ICA2191G111CA1691G121CA2144G131CA2149G14ICA2146G15ICA2192G16117118119120121!221231241251261271281291JOI

SIC DBC ) *

253 •258 •295 •253 •8190284 *104413 •1001129314987354 »

OTHER TOTOUT

111100I01000001

Dibutylchlorendate

AOUISORYQC LiniTS(24-154)

* Column to be used to flag* Ualue* outside QC l i m i t *0 Surrogate* d i l u t e d out

recovery value*

page 1 of

FORM II PEST-1 1x87 Rev.

154

Lab Name: ETCNJ" -'uis-

Lab Code:


Contract:


t EPAI SAMPLE NO.

Q1IQC70Q55G02ICA2150G03 IQ4IQ5-I06107108109110111112113114115116117118119120 1211221231241251261271281291301

SICDBO#

134218 *

OTHER TOTOUT

01

1

SI (D8C) - Oibutylchlorendate

ADVISORYQC LIMITSC24-154J

t Column to be used to flag* Values outside QC lim i t sD Surrogates diluted out

recovery values

page 1 of

FORM II PEST-1 1/87 Rev

155

3AWATER UOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

&>T ,f/4/j~iLab Name: ETC Corp. 4—Labuialflry Contract:

tab Code: Case No.: SAS No.: SDG No.:tfT*-*

Matrix Spike - £PA Sample No.: CA1372US

COMPOUND

1 rl-DiehloroathenaTr ichloroethana .,BenzenaTo luanaCh lorobanzana ._,

SPIKEADDEDCug/L>

90.00090.00090.00090.00090.000

SAMPLECONCENTRATION

Cug/L)

Q.OQO0.0007.46739.6360.000

MS 1CQNCENTRAT I ON I

Cug/L) 1

91.026 143.279 194.019 184.708 146.240 1

1

MSSREC

10287939092

1 QC 11 LIMITS!

*l REC. 1

161-149 1171-1201176-1271176-1291179-13011 1

COMPOUND

1 ?l-Dich loroethanaTr i eh loroa thane „BenzeneTo luanaCh lorohenzane _ . ,.. _, __

SPIKEADDED(ug/LJ

90.00090.00090.00090.00090.000

MSD •CONCENTRATION

(ug/L)

47.61941.47091.81282.03944.891

nso*REC *

"9583898990

HRPD *

74963

1QC LIMITS iRPO 1 REC. 1

14 161-149114 171-120111 176-127113 176-125113 175-1301

1 1

4 Column to be used to. flag recovery and RPD values with an asterisk

* Ualuas outsida of limit*

RPD: 0 out of 9 outside limits'Spike Recovery: 0.. out of 10 outside limits

Comments: ____

FORM 111 UOA -1 1/87 Rev.

156

3AWATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Name: ETC Corp. I Laboratory Contract:


Matrix Spike - EPA Sample No.: CA1893US

COMPOUND

1 ,1-Dich loroetheneTriehleroetheneBenzeneToluene ,_mCh lorohenzAne iira , ,. _

SPIKEADDEDCug/L)

50.00050.00050.00050.00050. 000

SAMPLECONCENTRATION

Cug/L)

0.0000.000Q.OOQ0.0000.000

MS 1CONCENTRATION!

Cug/L) 1

37.913 136.477 141.451 142.908 145.078 t

1

MS%

REC

7673838690

I QC1 LIMITS

#1 REC.

161-145171-120176-127176-125175-1301

Vi

COMPOUND

1 ,1-Dich loroethaneTr inn loroetheneBenzeneTo lueneCh 1 nrohenzene

SPIKEA&eeoCug/L)

50.00050. 00050.00050.00050.000

MSDCONCENTRATION

Cug/L)

36.97736.42941.79742.72644.973

MSO 1* 1 HREC *l RPD *

74 1 273 1 084 1 185 1 090 1 0

QC LRPD

1414111313

MITSREC.

61-14571-12076-12776-12575-130V

# Column to be used to flag recovery and RPD values with an asterisk

* Ualues outside of l i m i t s

RPD: 0 out of 5 outside limitsSpike Recovery: 0 out of 10 outside l i m i t s

Comments: _____________________________________________________

FORM I II UQA -1 1/87 Rev.

157


Lab Name: ETC Corp. | Laboratory Contract:

Lab Code: Case No.: . . SAS No.: SDG No.:trrt* &r '0/2*/6*f

Matrix Spike - SPA Sample No.: CA2032VS

V

COMPOUND

1 , 1-DichloroetheneTrichloroetheneBenzeneTolueneChlorobenzene

COMPOUND

1 , 1-DichloroetheneTrichloroetheneBenzeneTolueneChlorobenzene

_ _ . _ . _ _ . _

SPIKEADDED( ug/L )50.00050.00050.00050.00050.000

.

SAMPLECONCENTRATION

(ug/L)0.0000.0001.9480.0000.000

MSCONCENTRATION

(ug/L)35.96735.35343.54943.87744.882

MS

REC I

7271 *838890

SPIKEADDED(ug/L)

50.00050.00050.00050.00050.000_ _ .._

MSDCONCENTRATION

(ug/L)36.36436.58346.74245.80947.203

_ .. — . —— —————

MSD !

REC *| RPD I

73 j 173 390 792 494 ! 5

QC L:RPD

1414.111313

—————

QC jLIMITSREC. j

61-145J71-12076-12776-12575-130

i

iCMITS ]REC.

61-145!71-12076-12776-12575-130

'

I Column to be used to flag recovery and RPD values with an asterisk

* Values outside of limits

RPD: 0 out ofSpike Recovery:

5 outside limits1 out of 10 outside limits

Comments:

FORM III VOA -1 1/87 Rev.

158


Lab Name: ETC Corp. I 'Laboratory Contract:


Matrix Spike - EPA Sample No.: CA2140US

COMPOUND

1 rl-Dichloreethene „ nTr iehloroetheneBenzene _._ MiiTo luene ,. ,_, , ,Ch Inrabenzena _ . ., _

SPIKEADDEDCug/L)

90.00090.00050.00090.00090.000

SAMPLECONCENTRATION

(ug/L)

0.00014.6621.6090.0000.000

MSCONCENTRATION

(ug/L)

39.02091.96349.00944.11947.162

MS 1 QC. S ILIMITSREC *l REC.

70 161-14974 171-12087 176-12786 176-12994 179-130

1

COMPOUND

1 , 1-Dich lornetheneTr ichloroetheneBenzeneTolueneCh lorobenzene ,_ , . , _

SPIKEADDED(ug/L)

90.00090.00090.00090.00090.000

MSOCONCENTRAT I ON

CugXL)

36.83192.63149 . 43449.27848 . 472

MSD.%REC *

7476889197

XRPD *

93133

QC LIMITSRPD I REC.

14 161-14514 171-12011 176-12713 176-12513 175-130

1v# Column to be used to flag recovery end RPD values w i t h an asterisk

* Ualues outside of limits

RPO:Spike

0 out ofRecovery:

outsideout of

l i m i t s10 outside 1imi ts

Comments

FORM III UOA -1 1/87 Rev.

159

3CUIATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Name: ETCNJ . Contract:


Matrix Spike - &tf Sample No.: CA1381CS

COMPOUND

Phanol2-Chlo-rophenol1 ,4-0 ich lorobenzene ____N-Nitroso-di-n-prop. Cl)_1 ,2 ,4-Tr ich lorobenzene __4-Cn loro-3-me thylpheno 1_Acenaphthene4-Ni t ropheno 12 ,4-DinitrotoluenePent ach lorophenolPvrene

SPIKEADDEDCug/L)

204.082204.082102.041102.041102.041204.082102.041204.082102.041204.082102.041

SAMPLECONCENTRATION

Cug/L)

0.0000.0000.0000.0000.0000.000o.ooo0.0000.0000.0000.000

MSCONCENTRATION

(ug/L)

112.274122.99080.02875.55482.46473 . 27379.493120.47652.78532.51782.366

MS 1 QC I% ILIMITSI

REC *l REC.

55 112- 8960 127-12378 136- 9774 141-11681 139- 9836 123- 9778 146-11859 110- 8052 124- 9616 1 9-10381 126-127

1

COMPOUND

Phono 12-Chloroohenol1 ,4-Dich lorobenzene ____N-Ni t roso-d i-n-prop . (1 )_1 ,2 ,4-Tr ich lorobenzene _ „4-Ch loro-3-me thy I phenol_Acenaphthene,4-Ni t ropheno 1 ,,,.2 .4-Dinitrotolu«n«_,Pantaeh 1 o rophanflrl.^ , _M _Pvrene

.<%•

SPIKEADDED(ug/L)

212.766212.766106.383106.383106.383212.766106.383212.766106.383212.766106.383

MSDCONCENTRATION

(ug/L>

115.129123.41077.62474.105BO. 70592.76776.592141.10762.50255.25885.035

MSDHREC *

5458737076447266592680

\RPO *

2476619a1213481

QC LIMITSRPD 1 REC.

42 112- 8940 127-12328 136- 9738 141-11628 139- 9842 123- 9731 146-11850 110- 8038 124- 9650 1 9-10331 126-127

1

CD N-Ni t roso-di-n-p ropy lam ine

# Column to be used .to flag recovery and RPD values with an asterisk


RPD: 0 out of 11 outside limitsSpike Recovery: 0 out of 22 outside limits

Common t s '•

FORM III Sv -1 160 1/87 Rev.

3CWATER SEMIUOLATILE MATRIX SPIKE/MATRIX SPIKE OUPLtr.ATE. RECOUERY


Lab Code: Case No.: SAS No.: SDG No.:£F7C~

Matr ix Spike -.fiPTTSample No.: CA1859CS

COMPOUND

Phsna 12-Ch loropheno 11 ,4-Dich lorobenzcne ____N-Nitroso-di-n-prop. ( 1 >_1 ,2 ,4-Tr ich lorobenzene _4-Ch loro-3-methylphenol_Aeenaphthene4-Ni t ropheno 1 ,2,4-DinitrotoLuenePentach loropheno 1 _ , ,ptjrene

SPIKEADDEDlug/D

200.000200,000100.000100.000100,000200.000100.000200.000100.000200.000100.000

SAMPLECONCENTRATION

tug/L)

0.0000.0000.0000.0000.0000.0000.0000.0000.0000.000O.-OQO

MSCONCENTRATION

Cug/L)

90.260180.29877.54493.90880.931164.46882.69659.43874.110134.711102.536

MSS

REC *

40907884818283307467103

QCLIMITSREC.

12- 3927-12?36- 9741-11639- 9823- 9746-11810- 8024- 96

9-10326-127

COMPOUND

Pheno 12-Ch loropheno 1 mii ,_, . „„1 ,4-Dich lorobenzene ____N-Nitroso-di-n-prop. Cl)_1 ,2 ,4-Tr ich lorobtnzane _4-Ch loro-3-methy 1 phenol _Acenaph thene4-Ni t ropheno 12 .4-Din i t rotolu«n« wnPentach lo ropheno 1Purene

SPIKEADDED(ug/L)

200.000200.000100.000100.000100.000200.000100.000200.000100.000200.000100.000

MSDCONCENTRATION

(ug/L)

81.091151.06876.62070.14678.867154.77981.19425.72372.85681.21296,880

MSD\REC #

4176777079778113734197

HRPD #

1181

1836279 •2

506

QC LIMITSRPD 1 REC.

42 112- 8940 127-12328 136- 9738 141-11628 139- 9842 123- 9731 146-11850 110- 8038 124- 9650 1 9-10331 126-127

1

(1) N-Nitroso-di-n-propylamine



RPD: 1 out of 11 outside limitsSpike Recovery: 0 out of 22 outside li m i t s 161Comments :

FORM in sg -i 1x87 Rev.

3CWATER SEMIYOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOUERY.


Lab Code: Case No.: SAS No.: SDG No,:

Matrix Spike - EPA Sample No.: CA1907C^

COMPOUND

Phenol2-Ch loropheno I1 ,4-Dich I orobenzene ____N-Nitroso-di-n-prop. tl)_1,2,4-Trich 1 orobenzene _4-Chloro-3-methylphenol_Acenaphthene _4-Ni t ropheno 12 ,4-Oin i troto luenePentach loropheno 1P-orena

&

SPIKEADDED(ug/L)

208.333208.333104. 167104.167104.167208.333104.167208.333104. 167208.333104.167

SAMPLECONCENTRATION

Cug/L)

0.0000. 0000.0000.0000.0000.0000. 0000. 0000.0000.0000.000

MSCONCENTRATION

(ug/L)

142.452161.71379.31587.08U79, :'5Q164.26187. 1*9100.57874. H41157.17981.310

MS I QC% ILIHITSI*EC. *i *EC.

68 : 12- 3-~ '78 127-12.! l76 : 36- 9 '84 141-116177 ! 59- 9*79 123- 97184 : 46-11:-' '48 110- 80172 124- 9r. :75 1 9-103178 -I26-12-"

-1- 1

COMPOUND

Pheno 12-Ch loropheno 11 ,4-D i ch 1 orobenzene _N-Nitroso-di-n-prop. ( 1 )_1,2,4-Trich lorobenzene_4-ChlopQ-3-methylpheno 1_Acenaph thene4-Ni t rophano 1 m n , , ., .2 ,4-Dinitroto luanaPen t*ch lopophanol niii „ BParana

SPIKEADDED(ug>'L)

208.333208.333104.167104.167104.167208.333104.167208.333104.167208.333104.167

MSOCONCENTRATION

Cug/L)

134.212138.37481.13871.57084.395132.13189.25397.37567.66984.37682.941

MSD%

REC #

6467786981638647654180

\RPD #

6152

2G622231060 »2

1QC LIMITS 'RPU 1 PhC. 1

42 i ii- a* i40 127-11'28 136- 9~M38 !4l-llr.

28 13"- 98 l42 123- v31 146-118150 i 10- y •38 12-i- 9o :50 1 9-10 ' '31 126-1271

I

(1 ) N-Nitroso-di-n-propylamine

$ Column to be used to flag recovery and RPD values with an

* values outside of l i m i t s

RPD: 1 out of 11 outside l i m i t sSp •• ke Recovery: 0 out of 22 outside l i m i t s

Comment s:162

FORM III SU -1 L.'87 Re

3EUATER PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY



Matrix Spike - EPA Sample No.: CA1381GS

COMPOUND

g a mma - BHC ( L i n d a n e )Hept ach lorAldrinD i e 1 d r i n . ,Endr in4.41 -DOT

SPIKEADDED(ug/L>

.220

.220

.220

.549

.549

.549

SAMPLECONCENTRATION

Cug/L)

O.QOO0.0000.0000.0000.000Q.OOO

MSCONCENTRATION

Cug/L)

.151

.153

.143

.423

.483

.437

MS 1 QC% (LIMITS

REC *l REC.

69 156-12370 140-13165 140-12077 152-12688 156-12180 138-127

1

COMPOUND

g a mma- BHC C Lindane)Hept ach lorAldr inD le Idr in ,Endr in „ .4.4--DDT

SPIKEADDEDCug/L)

.220

.220

.220

.549

.549

.549

riSDCONCENTRATION

Cug/L)

.296

.286

.269

.798

.909

.844

MSD 1\ 1

REC #1

135 * 1130 1122 »l145 • 1165 »l154 •!

\RPD *

65 *61 *61 *62 *61 »63 *

QC LRPO

15• 2022182127

1IM ITS 11 REC. I

156-12? 1140-1311140-1201152-126 I156-1211138-12711 I

ft Column to be used to flag recovery and RPD values with an asterisk

* Uelues outside of limits

RPD: 6 out of 6 outside l i m i t sSpike Recovery: 5 out of 12 outside limits

Commen t s:

FORM III PEST-1 1/87 Rev.

163

3EWATER PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECQUERY




COMPOUND

qamma-BHC CLindane JHept ach lorAldr in •Die Idr inEndr in4.4--DDT

SPIKEADDEDCug/L)

.200

.200

.200

.500

.500

.500

SAMPLECONCENTRATION

Cug/L)

0.0000.0000.0000.000o-,ooo0.000

MSCONCENTRATION

Cug/L)

.322

.290

.236

.788

.991

.891

MS 1 QC 1* ILIMITSI

REC #t REC. l...... |...... |161 * 156-1231145 -140-1311143 »I40-120 1158 *I52-1261198 »I56-121 1178 * 138- 1271

1 1

V

COMPOUND

qamma- BHCCL i ndane )Hep t ach lor i i r a i i

Aldr inDieldr inEndr in4.4'-DDT

SPIKEADDEDCug/L)

.200

.200

.200

.500

.500

.500

MSOCONCENTRATION

Cug/L)

.317

.285

.278

.786

.900

.869

MSDS

REC *

159 »142 *139 *157 »180 »174 «

SRPD #

1230

102

QC LIMITSRPD 1 REC.

15 156-12320 UQ-13122 140-12018 152-12621 156-12127 138-12-7

1

V

0 Column to be used to flag recovery and RPD



lues with an asterisk

Co mm*, n t s :

FORM III PEST-1 1/87 Rev

164

3EWATER PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Nam«: ETCNJ Contract:



COMPOUND

gamma-BHCCL indane )Heptach lorAld r i nDie Idr inEndr in4.4'-DDT

SPIKEADDEDCug/L)

.213

.213

.213

.532

.532,532

SAMPLECONCENTRATION

<ug/L)

0.000O.OOQ0.0000.0000.0000.000

.

MSCONCENTRATION

Cug/L)

,187.173.192.487.369.520

MS 1 QC\ 1 LIMITS

REC *l REC.

88 156-12381 140-13190 140-12092 152-12669 156-12198 138-127

1

COMPOUND

qamma-BHC(L indane )HeptachlorAldrinD i e 1 d r i nEndr in4. 4 '-DOT

SPIKEADDEDCug/L)

.213

.213

.213

.532

.532

.532

MSDCONCENTRAT I ON

Cug/L)

.183

.169

.191

.447

.376

.489

MSDH

REC #

867990847192

HRPD ft

221926

QC LRPD

152022182127

[HITSREC.

56-12340-13140-12052-12656-12138-127




Commen ts:

FORM III PEST-1 1/87 Rev.

165

4AVOLATILE METHOD BLANK SUMMARY

Lab Name: ETC Corp.

Lab Code: Ca*e No.:

Lab File ID: >C7233

Date Analyzed 1QXQ2/89


Instrument ID: GC/MS C

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSDi

Contract:

SAS No.: SDG No.:

Lab Sample ID: QC7Q070U

Time Analyzed: 2028

Level:(low/med) LQU

v1 EPAI SAMPLE NO.

Oil02103104105106107109 10911011111211311411511611711811912012112212312412519AI -p"--571 -M- f..291 *-291301

LABSAMPLE ID

QC70070U

LABFILE ID

>C7234

TIMEANALYZED

2123

Comments•

page 1 ofFORM IU UOA 1/97 Rev

166


Lab Name: ETC. Corp.

Lab Code: Case No,:

Lab File ID: >C7241

Date Analyzed 10/03/89

Matrix: (901 I /water) WATER


THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:

Contract:

SAS No.: SDG No.:


Time Analyzed: 1138

Leva I: C 1 ow/med ) LOUi

Comments

iof

1 EPA1 SAMPLE NO.

Oil02103104105106107108109110111112113114115116117118119120121122123124125 1 .«•**>•5*1 "?*»271 ~mSk*~~

291301

LABSAMPLE ID

CA1372VCA1372USCA1372VRCA1373UCA1374UCA1376UCA1375U

LABFILE ID

>C7243>C7244>C7245>C7247>C7248>C7250> C725 1

TinEANALYZED

1444153916351824191921102207

FORM IU UOA 1/87 Rev,

167

4A 'VOLATILE METHOD HLANK SUMMARY

Lab Name: ETC Corp.

Lab Code: Case No.:

Lab File ID: >C7255


Matrix: CsoiI/water) UATER



Contract:

SAS No.: SDG No.:

Lab Sample ID: QC70070<J

Time Analyzed: 1631

Level:(low/med) LQU

V

I EPAI SAMPLE NO.

Oil02!03104109106107108109110111112113 t141151161171181191201211221231241251261271281291301

I LABI SAMPLE ID

CA1377UCA1382UCA1374UCA1376U

LABFILE ID

>C7256>C7257>C7258

' >C7259

TIMEANALYZED

1842193820332128

Comments

page -4* ofFORM IU UOA 1/87 Rev

168

Lab Name: ETC Corp.

Lab Code: Case No.

Lab File ID: >C7265

4AMETHOD BLANK_SUMMARY

Contract:

SAS No.: SDG No.:


Time Analyzed: 1625

Level:Clow/mad) LOW


Ma t r i x: C so i1/wa tec) WATER



1 EPA1 SAMPLE NO.

O i l021031041051061071oa i09 1101111121131141151161171181191201211221231241251261271281291301

LABSAMPLE ID

CA1375UCA1378UCA2068UCA1379UCA138QIJ,CA206W1 *7«yJCA2070U M/7

LABFILE ID

>C7266>C7267>C7268>C7269>C7270

U >C7273~. >C7274

TIMEANALYZED

1932202721222217231201570251

Comments

paga -*• of VFORM IU <JOA 1/87 Rev

169


Lab Name: ETC Corp.

Lab Code: Case No.:

Lab Pile ID: >C7277





Contract:

SAS No.: SDG No.:

Lab Sample ID: QC70076V

Time Analyzed: 1155Level:(low/med) LOW

Comments:

page l of j»_

01020304050607080910111213

1415161718192021222324252627282930

EPASAMPLE NO.

———————————

——————————————————————

———————————————————————————————————————————————————————

.

LABSAMPLE ID

CA1380V U**'C3)CA1381VCA1383VCA2026VCA2029VCA2032VCA2032VSCA2032VR

—————————————

.-

LABFILE ID

>C7278>C7279>C7280>C7281>C7283>C7285>C7286>C7287

—————————————

TIMEANALYZED

13431438153216281818200821032158

" "" -

•

FORM IV VOA 1/87 Rev,170


Lab Name: ETC Corp.Lab Code: Case No.:

Lab File ID: >C7290


Matrix: (soil/water) HATER



Contract:

SAS No.: SDG No.:


Time Analyzed: 1101

Level:(low/mad) LOW

Comments

**page , of

010203040506070809101112"1415161718192021222324252627282930

| EPA1 SAMPLE NO.

———————————————— ; ———

——————————————————————————————————————————————————————————————————————————————————————————

LABSAMPLE ID

CA2033VCA2031VCA2034V

—————————————

—————————————

LABFILE ID

>C7292>C7293>C7294

—————————————

TIMEANALYZED

132814241519

"" • "

i

FORM IV VOA 1/87 Rev,

171


Lab Name: ETC Corp.

Lab Code: Case No.:

Lab File ID: >C7303





Contract:

SAS No.: SDG No.:


Time Analyzed: 1020

Level:(lov/med) LOW

V

Comments:

page >T of

010203040506070809101112131415161718192021222324252627282930

EPASAMPLE NO.———— —— ———

———————————

———————————

——————————————————————

— —— ————— .

LABSAMPLE ID

CA2027VCA2035VCA2036VCA2037VCA2038VCA2039VCA2040VCA2042VCA2043V

— . ———————————

LABFILE ID

>C7304>C7305>C7306>C7307>C7308>C7309>C7310>C7312>C7313

_

TIMEANALYZED

1156, 12521347144215381633172919192014

—————————

————————— i

FORM IV VOA 1/87 Rev,

172

4AUOLATILE METHOD BLANK SUMMARY

Lob Name: ETC Corp.

Lab Code: Case No.:

Lab File ID: >C7326

Date Analyzed 10/11x89

Ma t r i x : (soil/wa t e r) WATER


THIS METHOD BLANK APPLIES TO THE FOLLOUING SAMPLES, MS AND MSD:

Cont rac t :

SAS No.: SDG No.:

Lab Sample ID: QC70079U

Time Analyzed: 1444

Leve1:C1ow/med) LOU

V

y

Comments:

page 1 of

1 EPA1 SAMPLE NO.

Oil02 103104105106107109 1091101111121131141151161171181191 '201211221231241251261271281291301

LABSAMPLE ID

CA1894UCA1893UCA1893USCA1893URCA1895UCA1B97UCA1896U

LABFILE ID

>C7330>C7331>C7332>C7333>C7334>C7335>C7336

TIMEANALYZED

2028212322182314000901040200

FORM IU OQA 1731/87 Rev,

Lab Nan*;

Lab Cod*:

VOLATILE METHOD BLANK SUMMARY

ETC Corp.' ——______;________ Contract:

_____ Cast No.: ____ SAS No.: SDG No.:Lab Fil* ID: _

Dat* Analysed:

Matrix: (soil/vat«r) ___

In»trua«nt ID: _&

Lab_Sanpl* ID:

Tin* Analyz*d:

L*v«l:(lov/B«d) '&W

THIS MZTHOD BLANK APPLIES TO THE FOLLOWING-SAMPLES, MS AND MSD

EPASAMPLE NO.

LABSAMPLE ID

Oil02 J03|04|05|06107|08|.09 |101"

tt

**» -. I TIME IFILE ID***/Y ANALYZED |

7152-

V

"l!151

282930,

COMMENTS:

p*g« _ of __FORM IV VOX

174l/«7 Rev


Lab N«mei ETC Corp.*

Lab Code: Case No.:

Lab File ID: >C7362




THIS METHOD BLANK APPLIES TO THE FOLLOW INC SAMPLES, MS AND MSD:

Contract:

SAS No.: SDG No.:

Lab Sample ID: QC7p081'J

Time Analyzed: 1014

Level:Clow/med) LCU

v1 EPA1 SAMPLE NO.

Oil02103104105106107108109110111112113114!15116117118119120121122123124125124 1 •271 • .2fil291301

LABSAMPLE ID

CA1778UCA1779UCA1780UCA1783U

LABFILE ID

>C7363>C7364>C7365>C7366*

TIMEANALYZED

1121121713131409

Comments:

page 1 ofFORM IU UOA 1/87

175


Lab Name: ETC Corp.

Lab Code: Casa No.:

Lab File ID: >C7369

Data Analyzed 10/13/89

Ma t P i x: C so i1/we tar) UATER



Contract:

SAS No.: SDG No.:

Lab Sample ID: QC7Q081'J

Time Analyzed: 1649

Level:(low/mad) LOU

v1 EPA1 SAMPLE NO.

Dll02103104105 t06107108109110111112113114115116117118 1191201211221231241 .'251 . *%:261271281291301

LASSAMPLE ID

CA1770USCA1778YRCA179QUCA1796UCA1799UCA2140UCA2140USCA2140UR

LABFILE ID

>C7370>C7371>C7372>C7373>C7374>C7375>C7376>C7377

TIMEANALYZED

17421838193420302126222323190014

Comments:

page 1 ofFORM IU UOA 1/87 Rev,

176




Lab File ID: >D8036



Instrument ID: GC/MS D


SDG No.:


Time Analyzed: 1444

Level:(low/med) LOW

V

Comments:

page 1 of

010203040506070809101112131415161718192021222324252627282930

EPASAMPLE NO.

———————————

———————————

——————————————————————

LABSAMPLE ID

CA2141VCA2142VCA2143VCA2149VCA2151VCA1891VCA2145VCA2152VCA2153V

—————————————

—————————————

LABFILE ID

>D8038>D8039>D8040>D8041>D8042>D8043>D8044>D8045>D8046

—————————————

—————————————

—————————————

—————————————

TIMEANALYZED

163517271816190719582048213922302320

—————————

—————————

—————————

—————————

FORM IV VOA177

1/87 Rev,


Lab Name: ETC Corp.

Lab Code: Case No.:

Lab File ID: >I8246



Instrument ID: GC/MS I


Contract:

SAS No.: SDG No.:


Time Analyzed: 2331

Level:(low/med) LOW

V

Comments:

01020304050607080910111213141516I?18192021222324252627282930

j EPASAMPLE NO.

——————————————————————————————————————————————————————————————————————

——————————

——————————•

————————————————————————————————————————

——————————

——————————-

LABSAMPLE ID

CA2150VCA2147VCA2144V

——————————————————————————

——————————————————————————

....... ..._ ...

LABFILE ID

>I8248>I8250>I8252

—————————————

—————————————

_

TIMEANALYZED

011002500429

——————————————————

—————————————————————————————————————————————————————————————————————————————————————————

—————————————————————————————————————————————

e

FORM IV VOA178

1/87 Rev,

4BSEMIVOLATILE METHOD BLANK SUMMARY

Lab Name: ETC Corp.

Lab Code: Case No.

Lab File ID: >G8653




Contract:

SAS No.: SDG No.:

Lab Sample ID: QC70082C

Extraction:(SepF/Cont/Sonc) SEPF

Time Analyzed: 1424

Level:(low/med) LOW

Instrument ID: GC/MS G


01.0203040506070809101112131415161718192021222324252627282930

EPASAMPLE NO.

——————————

——————————

t

——————————

LABSAMPLE ID

CA1859CSCA1859CRCA1893CCA1894CCA1859C

————————————

..... . ..

LABFILE ID

>G8654>G8655>G8656>G8657>G8658

DATEANALYZED

10/13/8910/13/8910/13/8910/13/8910/16/89

Comments:

page 1 of __FORM IV SV 179 1/87 Rev

4BSEMIVOIATILE METHOD BLANK SUMMARY

Lab Name: ETCNJ

Lab Code: Case No.

Lab File ID: >G8835




Contract:

SAS No.: SDG No.:


Extraction:(SepF/Cont/Sonc) SEPF

Time Analyzed: 0727

Level:(lov/med) LOW



Comments

page 1 of f.

010203040506070809101112131415161718192021222324252627282930

! EPASAMPLE NO.

————————————————————

——————————

——————————

. ...

LABSAMPLE ID

CA1895CCA1896CCA1897CCA2136CCA2137CCA2138C

._..... —— . . —— ..._;

LABFILE ID

>G8836>G8837>G8838>G8839>G8840>G8841

, ...—

—————————————

DATEANALYZED

10/28/8910/28/8910/28/8910/28/8910/28/8910/28/89

—————————

FORM IV SV 1 SO 1/87 Rev,

SEMIUQLATILE METHOD BLANK SUMMARY

Lab Name: ETCNJ

Lab Code: Case No.

Lab File ID: >G9Q12



Ma t r i x : (soil /wa ten) UIATER

Cont Pact:

SAS No.: SDG No.t

Lab Sample ID: QC7Q081C

Extract ion:(SepF/Cont/Sonc) CONT

Time Analyzed: 1624

Level: Uow/med) LOW



1 EPA1 SAMPLE NO.

Oil021031041051061071081091101111121131141151161171181191201211221231241251261271 "<r -281291301

LABSAMPLE ID

CA1381CSCA1381CRCA1379CCA138QCCA1381C

LABFILE ID

>G9013>G9014>G9015>G9016>G9017

DATEANALYZED

11/13/8911/13/8911/13/8911/13/8911/13/89

Comments:

page 1 ofFORM IU SU 1/87 Rev

131

48SEN I VOLATILE METHOD BLANK SUMMARY

Lab Name: ETCNJ

Lab Code: Case No.:

Lab File ID: >G9041



haîx: (soil/water) WATER

Instrument ID: -GC/MS G


Cont ract:

SAS No.: SDG No . :

Lab Sample ID: QC7003/

Extract ion:(SepFxContxSonc) CONT

Time Ana 1yred: V140

Level : ( low/med ) '

t EPAt SAMPLE NO.I--......--..

O i l02 !03104!

.051•Q6 1*»!08!09110!Ill12 t13114!IS t16117118!19120 I21122123124125126127128 129130!

LABSAMPLE ID

CA1907CRCA2139CCA1907CSCA1907CCA2140C

LABFILE ID

>G9043>G9045>G9077>G9078>G9079

DATE 1ANALYZED !---------- 111/14X89 111/15/89 111/16/89 111/16/89 111/16/89 1

1I1I1

1t1

1;1i111i1I1II[

1

Comment s:

page 1 of IFORM IU SO

182

48 'SEMIVOLATILE METHOD BLANK SUMMARY

•-, Caa* No.:. *

Lab Name: ETCNJ

Lab Cod*:

'Lab Fi1* ID: >


Oat* Analyzed 11X15x89

Matrix: C»oilx w«t*r) UIATER

Contract:

SAS No.: SOG No.:


Extract ion:<S*pFxContxSonc> CONT

Tim* Analyzed: 0618

Level:(low/med) LOU


THIS METHOD BLANK APPLIES TQ THE FOLLOWING SAMPLES, MS AND MSD

I EPA1 SAMPLE NO.

Oil02103104105106107108 109110111112113114115116117118119120121122123 1 IJM*V241 iHJIIPt —29 1 Hlk.26 1 fc*T''271 -2SI291301

LABSAMPLE ID

CA1889CCA1890CCA1892CCA19Q8CCA2141CCA2142CCA2143CCA2149CCA2151CCA1891CCA2144CCA2145CCA2146CCA2152C

LABFILE ID

>G9092>G9053>G9094>G9099>G9056>G9097>G9098>G9059>G9060>G9061>G9064>G9069>G9066>G9067

DATEANALYZED

11X15X8911X15X8911X15X8911x15x8911X15X8911X15X8911X15X8911X15X8911X15X8911x15x8911x15x8911x15x8911x15x8911X15X89-

Comm*nt»:

page 1 of _j_FORM IU SO 1X87 Rev

133

4B •SEMIUOLATILE METHOD BLANK SUMMARY

Cos* No.

Lab Name: ETCNJ

Lab Code:

Lab Pi Is 101 >

Date Extracted:"^?'1 11/06/89



Contract:

SAS No.: SDG No.:


Extract ion:(SepF/Cont-"Sonc) SERF

Time Analyzed: 2301




Comments:

1 EPA1 SAMPLE NO.

Oil021031041051•06107108109110111112113114115116117118119120121122123 1 -*-$'5i£''<1 -241 • BF*-.. .25 1 -af -%'"-26 1 -*3|Mtfe-271 ?&&*&*•• '281291301

LABSAMPLE ID

CA215QC

.

LABFILE ID

>G9106

DATEANALYZED

11/17/89

page 1 of /FORM W SU 1/87 Rev

134

4CPESTICIDE METHOD BLANK SUMMARY

Lab Name: ETCNJ

Lab Code: Case No

Lab Sample ID: QC70Q45G



Date Analyzed CD: 10/31/89

Time Analyzed CD: 1302

Instrument ID CD: HA

GC Column ID IDs 2250/2401

Cent ract :

SAS No.: SDG No . :

Lab File ID: >HA286

Lcvc1:Clow/med) LQU

Extract ion:CSepF/Cont/Sonc) SERF

Date Analyzed (2>: 89/11/17

Time Analyzed C2): 1213

Instrument ID (2) '• KB

GC Column ID (2): 3SSP2100

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSO:

1 EPAI SAMPLE NO.

Oil02103104105106107108109 I10111!121131141151161171181191201211221231241251261

LABSAMPLE ID

CA13S1GCA13B1GSCA1381GRCA1379GCA1380GCA1374G

DATEANALYZED 1

10/31/8910/31/8910/31/8910/31/8910/31/8910/31/89

DATEANALYZED 2

11/17/8911/17/8911/17/89

11/17/89

Comments:

page 1 ofFORM PEST 1 85 1''87 Re-


Lab Name: ETCNJ

Lab Code: Case No

Lab Sample ID: QC70046G



Date Analyzed C1't: 11/02/89

Time analyzed CD: 0909

Instrument ID (1): HA

GC Column ID (1): 2250/2401

Cont ract :

SAS No.: SDG No.:

Lab Fila ID: >HA323

Lave 1:Clou/med) LOU

Extract ion:(SepF/Cont/Sonc) CONT

Date Analyzed C2):

Time Analyzed (2) :

Inst rument ID (2):

GC Column ID (2) :


1 ERA1 SAMPLE NO.

01 1021031041051061071081091101lit12113114115116 1171181191201211221231241251261

LABSAMPLE ID

CA1S61GSCA1961GRCA1893GCA1894GCA1361G

DATEANALYZED 1

11/02/8911/02/8911/02/8911/02/8911/02/89

DATEANALYZED 2

Commen t s:

page 1 of _|_FORM IU PEST 136 1/87 Rev,

Lab Name: ET

Lab Code: 4Kf Caae No

Lab Sample ID: QC7005QG

Matrix: (aoi1/water) WATER



Time Analyzed (D: 1135


GC Column ID CD: 2250/2401


Contract:

SAS No.: SDG No.:

Lab File ID: >HA546

Level: C lou/med) LOUt

Extract ion:CSepF/ContxSonc) SEPF

Date Analyzed (2): 11/28/89


Instrument ID C2): K3

GC Column ID C2): 3%SP2100

THIS METHOD BLANK APPLIES TO THE FOLLOW ING SAMPLES, MS AND MSO:

1 EPA1 SAMPLE NO.

Oil021031041051061071081091101111121131141151161171 n. f.IB I Jtffi.3*-

191 aBF •'•20 t"~" Br2 1 1 iff? 'T221231241251261

LABSAMPLE ID

CA1889GCA1890GCA1892GCA19Q8GCA2141GCA2142GCA2143GCA2149GCA21516CA1891GCA2144GCA2145GCA2146GCA2152G

DATEANALYZED 1

11/15/8911/15/8911/15/8911/15/8911/15/8911/15/8911/15/8911/15/8911/15/8911/15/8911/15/8911/15/8911/15/8911/15/89

DATEANALYZED 2

11/28/89

Comments:

pag« 1 ofFORM IU PEST 1/87 Rev,

137

Lab Name:

Lab Code: v t Case No

Lab Sample ID: QC7QQ55G

Matrix: CsoiI/water) WATER



Time Analyzed CD: 0203


GC Column ID CD: 2250/2401


Contract:

SAS No.: SDG No.:

Lab File ID: >HA565

Level:Clow/med) LOW

Extract ion:CSepF/Cont/Sonc) SERF

Date Analyzed C2): 11/28/89


Instrument ID (2): KB



0102030405060708091011121314151617181920212223242526

ERASAMPLE NO.

•

LABSAMPLE ID

CA2150G

DATEANALYZED 1

11/16/89

DATEANALYZED 2

11/28/89

Comments:

page 1 ofFORM IU PEST 138 1/87 Rev

Lab Names E _„__~ IJBiVBXM* •--' JT^B^^*^*

Lab Coda: . !*fi£f • Case No•••* e'*,

Lab Sample 10: QC70Q48G




Time Analyzed (1): 0000

Instrument ID (1): JA

GC Column ID (1): 2250/2401

4C{[ 1C IDE METHOD BLANK SUMMARY

Contract:

SAS No.: SDG No.; .

Lab File 10: >JA486

Leve 1 : C1 ow/med ) LOUI

Extract ioniCSepF/Cont/Sonc) SERF•

Date Analyzed (2 ): -

Time Analyzed (2): 0031

Instrument ID (2): KB


THIS METHOD BLANK APPLIES TO THE FQLLOUIING SAMPLES, MS AND MSD:

1 EPA1 SAMPLE NO.

Oil02103104105106107108109 11011111211311411511*1- -wi*17l- Sp«fv- •181 #a&r:191 *»?,:.201 '-T-l .211221231241251261

LABSAMPLE ID

CA1895GCA1896GCA1897GCA2136GCA2137GCA2138G

DATEANALYZED 1

11/08/8911/08/8911/08/8911/08/8911/08/8911/08/89

DATEANALYZED 2

11/21/8911/21/8911/21/89

Comments:

page 1 of _J_FORM IU PEST 139 1/87 Rev


Lab Name: ETCNJ

Lab Code: Case No.:


Matrix: Csoi1/uater> WATER


Date Analyzed (1): 11/08/89

Time Analyzed CD: 0947 Time Analyzed C2): 0252

Instrument ID (1): JA Instrument ID (2): KB

GC Column ID CD: 2250/2401 GC Column ID (2): 3SSP2100


Cont rac t:

SAS No.: SDG No.:

Lab File ID: >JH495

Leve 1 : C low/med ) LOW

Ex tract ion:CSepF/Cont/Sonc) SERF

Date Analyzed C2>:

1 EPA1 SAMPLE NO.

Oil02103104!05106 t07108109110111112113114115116117118 1191201211221231241 -'251261

LABSAMPLE ID

CA1907GCA1907GSCA1907GRCA2139GCA2140G

DATEANALYZED 1

11/08/8911/08/8911/08/8911/08/8911/08/89

DATEANALYZED 2

11/21/89

11/21/89

Comments:

page 1 ofFORM 1U PEST 190 1/87 Rev

IfiUQLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: ETC Corp.

Lab Code: Case No.:

Matrix: (soi 1/water) LJATER





Cont rac t:

SAS No.: SDG No . :

Lab Sample ID: QC7Q07Qg

Lab File ID: /C7233so/±

•Data Received:


Dilution Factor: 1


I74-87-3 ———————— Chlorome thane______________I 1074-83-9 ——— - —— -Bromome thane_______________I 1075-01-4————————Uinyl Chloride_____________11075-00-3 ——————— Chlo roe thane_____________11075-09-2 ——————— Methylene Chloride________1867-64-1 ———————— Acetone___________________I 1075-15-0———————Carbon Disulf ide__________1575-35.4———————1,1-Dichloroethene________1575-34-3————————1,1-Oichloroe thane_________15540-59-0———————1,2-Dichlorethene (total )__1567-66-3————————Chloroform________________15107-'06-2———————1,2-Dichloroethane_________1578-93-3 ———— —— 2-Butanone_______________11071-55-6 ———————— 1,1,1-Tri chlo roe thane______1556-23-5-- ——— —— Carbon Tet rach lor ide_______15108-05-4———————<Jinyl Acetate______________I 1075-27-4---------Bromodich loromethane______1578-87-5 — —————— 1,2-Dichloropropane________1510061-01-5————cim-l,3-Dichloropropene____1579-01-6———————Tr i chlo roe thene__________15124-48-1 ————— --Dibromoch lorome thane_______1579-00-5———————1,1,2-Triehloroethane______1571-43-2———————Benzene_________________1510061-Q2-6--———tran»-l,3-Dichloropropene__1575-25-2—-•—————Bromoform_________________15108-10-1——————4-Methyl-2-Pentanone______110591-78-6——————2-Hexanone_______________110127-18-4———————Tetrachloroethene__________1579-34-5 ——————— 1,1,2,2-Tet rach loroe thane__15108-88-3 —————— Toluene_________________15108-90-7———————Chloroberuene______________15100-41-4——————Ethylbenzene_____________15100-42-5——————Styrene_________________151330-20-7—————Xylene (total)___________15__ ___ ___ ___ _______________I__

Q

IIUIIIIIIIIIIIDIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIU

'

FORM I191

1/87 Rev,

109-99-9 T«tr»hydrofuran.

192

TtXTATIYlLl

_ Contract:

Saaplo wt/vol:t«v«lt (low/m«d)% Moisturei not die.Column: (pick/cap)

see NO.Jtab Saaplo XOiUb Filo XOi __Data ftocoivad: /oA*-/^Data Analyxodi Vw>»LDilution Factort *

coHctmuTionorNuatoor TIC* foundi

1/17

193

• 1AVOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO,

Lab Name: ETC Corp.

Lab Code: Case No.:

Matrix: Caoi1/water) WATER




Column: (peck/cap) PACK

Contract:

SAS No. '-

II_____

SDG No.:

Lab Sample ID: QC70070v

Lab File ID: >C724l

Date Rece ived'

Data Analyzed: 10/03/89



74-87-3 ——— — —— Chlorome thane______________11074-83-9———————Bromome thane_____________11075-01-4————————Uinyl Chloride_____________11075-00-3————————Chlo roe thane_______________I 1075-09-2————————Methylene Chloride_________1467-64-1————————Acetone___________________11075-15-0————————Carbon Diaulfide ______1575-35-4———————1,1-0ichloroethene________1575-34-3 ——————— 1,1-D i chio roe th»ne________-15540-59-0——————1,2-0 ich lore thene (total)__1567-66-3———————Chloroform107-06-2 ——————1,2-0 ichloroe thane________1578-93-3———————2-Butanone_______________11071-55-6 ——————— 1,1,1-Trichloroe thane______1556-23-5———————Carbon Tet rach lor ide______15108-05-4———————vinyl Acetate______________11075-27-4———————Bromodichloromethane_______1578-87-5—————•——1,2-Dich loropropane________1510061-01-5————cis-l,3-Dichloropropene____1579-01-6-——-———Trich loroethene___________15124-48-1———----Dibromoch lorome thane_______1579-00-5———————1,1,2-Tr ich loroethene______1571-43-2———————Benzene_________________1510061-Q2-4?»-——tr«n«-l, 3-D i chlo ropropene__1575-25-2--J*'--—— Bromo form________________15108-10-1--A————4-M«thyl-2-Pentanone______110591-78-6——————2-Hexanone_______________12-127-18-4——————Tet rach loroethene_________1579-34-5———————1,1,2,2-Tetrachloroethane__15108-88-3——————Toluene_________________15108-90-7————•——Chlopntaenzane________15100-41-4——————Ethyl benzene_____________15100-42-5———————Styrene___________________151330-20-7—————Xylene (total)___________15_____________________________________I

IIUIUIUIUtoIUIUIUIUIU

IUIUIUIUIUIUIUIUIUIUIUIUIUIUtuL>IUIUIUIUIUtuIUI

FORM I OOA 1/87 Rev194

Mtrixs (SMtl* Vt/V*ll

OtlMI ( 0 ,££££

109-99-9 T«tr*hydrofur«n.

195

VOLATXLI OKAKICS'AWALYSXS DATA SHItTTWATXVIW XDINTXmD COMPOUNDS

eaatMet!

SAS N O . t

SAflP«£ JO.

No.

Saapla vt/vol:Lavals (low/mad)% Moiaturas notColuant (pack/cap)

Nuabar TICa founds

Ub Saapla IDsLab Pila XOsData Itacaivadi „Data Analysads _Dilution factori

CONCXNTJUTXON UNITS:(uf/t or

196

• • . . ' 1ft .vMDLATILE ORGANICS ANALYSIS DATA SHEET

ERA SAMPLE NO

Lab Name: ETC Corp.

Lab Code: Caae No.:



Leve 1 : C 1 ow/med) LOUI



Contract '•

SAS No.: SDG No . :

Lab Sample ID: QC7QQ70U

Lab File ID: >C7255so/*

Dete Received:


Dilution Factor: 1


74-87-3 ———————— Ch loromethane______________11074-83-9—————-—Bromome thane_______________11075-01-4————————Uinyl Chloride_____________11075-00-3———————Chloroethane_____________11075-09-2 ———————— Methylene Chloride_________1667-64-1 ——————— Acetone_________________11075-15-0———————Carbon Diaulf ide____^______1575-35-4———————1,1-Dichloroethene________1575-34-3———————1,1-Dichloroe thane______ 15540-59-0———————1,2-Dichlorethene (total)__1567-66-3———————Chloroform_______________15107-06-2——————1,2-Di chloroe thane________1578-93-3———————2-Butanona_______________11071-55-6———————1,1,1-Tri chloroe thane_____1556-23-5———————Carbon Tat rachlor ide______15108-05-4——————Uinyl Acetate____________11075-27-4—----- —— Bromodich loromethane______1578-87-5——————1,2-Dichloropropana_______1510061-01-5---——ci»-l,3-Dichloropropene____1579-01-6———————Trichloroethene__________15124-48-1——————Oibromoch lorome thane______1579-00-5———————1,1,2-Trichloroethane______1571-43-2———————Benzene_________________1510061-02-4—-——tranm-1,3-0 ichloropr opene__I575-25-2———----Bpomoform ____._! 5108-10-1—*--———4-n»thyl-2-Pentanone______110591-78-6——————2-Hexanone_______________110127-18-4——————Tetrachloroe thane_________1579-34-5———————1,1,2,2-Tetrachloroethane__15108-88-3——————Toluene________________15108-90-7——————-Chlorobenzene^_^________15100-41-4——————Ethylbenzene_____________15100-42-5——————Styrene_________________151330-20-7—————Xylene (total)___________15

______ ___ _________________I__

IU1UIUIUIIUIUIUIUIUiuIUIUIUIUtuIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIU

FORM I UOA 197 1X87 Rev.

8 6 L

VOLATXLZ OMAWXCS, ANALYSIS DATA SMttTvwb**-* ***?_— ._ _._.«•••*•« 'AAM^tinma

Lab CodosMatrix:Sanpla vt/voltLoval: (lov/mad) JLgtj_I Moisturos not doc.Column: (pack/cap)

Numbor TICa founds

Mo.:

ContractsSAS Ho.s SM M

Lab saaplo XDs _Lab Fila IDs _Data Xocaivcd: _Data Analysads .Dilution Factor: I

CONCSHTIUTXOIIor

row x X/17

199


EPA SAMPLE NO

Lab Name: ETC Corp. Contract: I_____


Matrix: (soi l/uiater) UATER Lab Sample ID: QC70G70U





Lab File ID: >C7265

Date Received:


01lut ion Factor: 1


74-87-3- ——————— Chlorome thane______________I 1074-83-9 —————— •—Bromome thane_______________11075-01-4———————Uinyl Chloride____________11075-00-3 ———————— Chloroe thane_______________I 1075-09-2———————Methylene Chloride________1567-64-1————————Acetone___________________1775-15-0————————Carbon Disulf ide ______1575-35-4———————1,1-Dichloroethene________1575-34-3————————1,1-Dichloroethane_________15540-59-0 —————— 1,2-Dichlorethene (total)__1567-66-3————————Chloroform_________________15107-06-2——————1,2-Oichlo roe thane________1578-93-3————————2-Butanone_________________11071-55-6 ——————— 1,1,1-Tri chloroe thane______56-23-5 ——————— Carbon Tat rachlor ide______15108-05-4———————Uinyl Acetate______________I 1075-27-4———-----Bromodichloromethane______1578-87-5 ———— ----1,2-Dichloropropane_______1510061-01-5————ci»-l,3-0ichloropropene____1579-01-6—————Trichloroethene___________12 S~124-48-1 —————— -Dibromoch lorome thane_______1579-00-5———————1,1,2-Tricnloroethene______1571-43-2---JJJ--—Beniane 151QQ61-02-4»J5E7—— tren»-l,3-Dichiorapropene__.15

108-10-l-*St——•4-Plethyl-2-Pentanone_M____l 10591-7B-A————---2-He*anan«____!•*- fO127-18-4——————Tetrachloroethene_________1579-34-5———————1,1,2,2-Tetrachloroethane__15108-88-3——————Toluene_________________15108-90-7—————'-Chlorobenzene..^.._________15100-41-4------—Ethulbanzene _____u_ 15100-42-5 ——————— Styrene___________________151330-20-7—————Xylene (total)___________15

Q

IU1UIUIUIJIJIUIUIUIUIUIUIUw-IUtuIUIUIUW-IUIUIUIUIUIUt-*IUIUIUIUIUIUIU1

<rr

FORM I t- ,-,w U

1/Q7 Rev.

OMMBCi AMUflXS

109-99-9 T«tr»hydrofuran,

l/it R«V

201

VOt>.TXU OfcOUUM ANALYSIS DATA SHUT«HTA«Vlt» XOCNTX?ISO COMPOUND*

SAJlP.i

Lab Codo:

C0#P*

Cato No.: _ Sit No.l tSOO No.

Staple vt/voli

Lovol: (low/mod)I Moitturoi notColumn: (pack/cap)

TXC« found:

Lab Saaplo XDi .Lab Filt X0i _Dato Jtoeoivodi _Oato Analysod: _Dilution Factor:

CONCtimUTION UNITS:or uf/Kf)

CAJ NUM1CK

l.a..3..4.».4.7.t."t."

10..11.12-.13.14.1*'-«•-"•-"-.!»•-30-,21.22.'23.24.25.24.27.'2t.29.30.

COMKOND NAMt 1ST. CONC.

202


'_ab Nama: ETC Corp.

SAMPLE NO.-

Lab Code: Case No,:


Sample wt/vol: 9.0 Cg/mL) HL

Lave 1: t 1ow/med) LOW



Contract:

SAS No.: SDG No.:

Leb Sample ID: QC70076U

Lab File ID: >C7277

Date Received: Q9->'?0/99<J*



CAS NO. COMPOUNDCONCENTRATION UNITS:(uq/L or ug/Kg) UG/L

74-87-3———————Chlorome thane____________11074-83-9 ——————— -Bromome thane_______________I 1075-01-4———————Uinyl Chloride____________11079-00-3———————Chloroe thane_____________11079-09-2———————Methylene Chloride ____1667-64-1————————Acetone___________________11075-15-0 ——————— Capbon Disulf ide__________1575-35-4———————1,1-Dichloroe thane________1575-34-3———————1,1-Oichloroe thane________15540-59-0——————1,2-Dichlorethene (total)__1567-66-3————————Chloroform________________15107-06-2———————1,2-0 ichlopoe thane_________1578-93-3 ——————— 2-Butanone_______________11071-59-6 ——————— 1,1,1-Trichloroe thane______1556-23-5——————Carbon Tet rachlor ide______19108-05-4——————Uinyl Acetate____________11075*27-4—------ -Bromod ich lorome thane______1578-87-5 ————— — 1,2-Oich loropropane_______1910061-01-9—————cis-1,3-Dichloropropene____1579-01-6———————Trichloroathana^__________15124-48-1——————Dibromoch lorome thane______1579-00-9———————1,1,2-Trichloroe thane______1571-43-2———————Benzene_________________1510061-02-6—•——tran»-l,3-Dichloropropene__1575-25-2———————Bromoform^______________15108-10-1——————4-ttethyl-2-Pentanone______110591-78-6——————2-Haxanone_______________110127-18-4——————Tatrachloroethena_________1579-34-5 ——————— 1,1,2,2-Tetrachloroethane__15108-88-3——————Toluene_________________19108-9Q-7-- ———— Chlorobenzene____________19100-41-4———————Ethyl benzene_______________19100-42-5 —————— Styrene_________________151330-20-7——————Xylene (total)____________19

___________I__

Q

IIIIUIIIIIIIIIIIUIUIUIIIIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU


*»M i.I/I

IEVOLATILE ORGAN ICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

ERA SAMPLE NO.

LabuiuLeb Name:ETC Corp.

Leb Coda: Case No.:

Me t r i x: (soil/we tar)WATER



H Moisture: not dec._____

Co 1umn: (pack/cap)

Contract:

SAS No.: SDG No.:


Leb File ID: >C7277

Date Received: 09>'M/89


Dilution Factor: '___

Number TICa found:CONCENTRATION UNITS:(ug/L or ug/Kg)UG/L

CAS NUMBER COMPOUND NAME

•n/*+, F+t^*/.

FORM I YOA-TIC

RT EST. CONC

i/a;

205

Q

? Rev.


SAMPLE NO

ILab Name: ETC Corp.

Lab Coda:* Case No.:

Ma t r i x: (soil/wa tar) WATER


Level: Clow/mad) LOW



Contract:

SAS No.: SDG No.:

Lab Sampla IDs QC70Q76VJ

Lab File ID: >C7290/*/»

Data Racaivad: 09.'30/99

Data Analyzed: 10x09x89

Dilution Factor: 1

CAS NQ. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UG/L

I74-87-3———————Chloroma thane____________11074-83-9——•———Bromomethane_____________11075-01-4———————Uinyl Chloride____________11075-00-3———————Chloroa thane_____________11075-09-2———————Me thy lane Chloride________1767-64-1———————Acetone_________________11075-15-0———————Carbon DUulf ide__^______1575-35-4———————1,1-Dichloroe thane________1575-34-3———————1,1-Oichloroe thane________15540-59-0——————1,2-Dichlorethene (total)__1567-66-3———————Chloroform_______________15107-06-2——————1,2-Diehloroethene________1578-93-3———————2-Butanone_______________11071-55-6———————1,1,1-Trichloroethane______1556-23-5———————Carbon Tetrachlor ide_______15108-05-4——————Uinyl Acetate____________11075-27-4——————Bromodichloromethane______1578-87-5——"———-l,2-Dichloropropane_______l510061-01-5————cia-l,3-Dichloropropene___l579-01-6———————Trichldroe thane___________15124-48-1———^—— PitarQBmehlQraiMthana 1579-00-5——————1,1,2-Trichloroethane______1571-43-2———————Benzene_________________1510061-02-6*—»- —— tran»-l,3-Dichloropropane__l575-25-2————-——Bronoform________________15108-10-1——————4-Mathyl-2-Pentanone______12591-78-6——————2-Haxanona_______________110127-18-4——————Tetrachloroethene_________1579-34-5———————1,1,2,2-Tetrachloroethane__15108-88-3——————Toluene_________________15108-90-7-—-——•-Chlorabangena 15100-41-4——————Ethylbenzene_____________15100-42-5——————Styrene_________,________151330-20-7—————Xylene (total)___________15_____________________________________I__

I1UIUIUIUIIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIJIUIUIUIUtuIUtuIU

FORM I UOA 206 1/87 Rev.

•"•UNO,

109-99-9 T«tr»hydrofuran,

I/It »«v,

207


EPA SAMPLE NO.

ILab Nama:ETC Corp. i- Laaai aluiy/

Lab Coda: Caaa No.:

Matrix) (aoi1/watar)UATER

Sampla ut/vol: 9.0 (gxmL)ML

Laval: (low/mad) LOU

*S Moisturat not dac._____

Column: (pack/cap)

Numbar TIC* found: O

Contract:

SAS No.i SDG No.:

Lab Sampla ID: QC70076U

Lab Fila ID: >C729Q

Data Racaivad:

Data Analyzad: 10x09/89

Dilution Factor: _|___

CONCENTRATION UNITS:(ug/L or ug/Kg)UC/L

CAS NUMBER

—————— i. »

COMPOUND NAME

tl**s, r**~+^J .

-T-l1'-- - " -C.VIf-ffFT

.

RT EST. CONC

.

Q

FORM I UOA-TIC

1AVOLATILE ORGAN1CS ANALYSIS DATA SHEET

SAMPLE NO.

Lib Nama: ETC Corp.

Lab Code: Caaa No.:

Ma t r i x: (soilxw« tar) WATER

Sampla wt'voli 9.0 (gxmL) ML

Lava It (low/mad) LOU

S Moiatura: not dac.


Contract

SAS No. i SOG No.:


Lab Fila ID: >C7303'f//oData Racaivad: 09»'3Q;'99


Dilution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:(ugxL or ugxKg) UGxL

I74-87-3———————Chloromathana____________11074-8.3-9-——-——--Bromomathana ____________11075-01-4———————Yinyl Chlorida____________11075-00-3 ——————— Chloroathana_________ IIP75-09-2———————Mathylana Chlorida________1567-64-1———————Acatona_________________11075-15-0———————Carbon Diaulf ida__________1575-35-4———————1,1-Dichloroathana________1575-34-3 ——————— 1,1-Dichloroathana________15540-59-0——————1,2-Oichlorathana (total)__15

107-06-2— —— ---1,2~0ichloroathana________1578-93-3———————2-Butanona_______________11071-55-6———————1,1,1-Trichloroathana______1556-23-5--————Carbon Tatraehlorida 15108-05-4——————Uinyl Acatata____________I1075-27-4——•—----BromadiehloroiMthana 1578-87-5———-----1,2-0 ichl crop ropana^_____1510Q61-01-5---«-ei»-l*3-Dichloropropana^___l579-01-6——TSff—Triehioroathana___________15134-Afl-t- jiff. OtbpQaaehlQroMthana 1579-00-5—*qfe*"l»l>2-Tr i oh loroathana 15

10061-02-4—»——tr«n»-l, 3-Oichloropropana__t 5

108-10-1——————4-Mathyl-2-Pantanona______110591-78-6——————2-Haxanona_______________110127-18-4——————Tatrachloroathana_________1579-34-5———————1,1,2,2-Tatrach loroathana__15108-88-3——————Toluana_________________15108-90-7——————Chlorobanzana____________15100-41-4——————Ethylbanzana_____________15100-42-5——————Styrana_________________151330-20-7—————Xylana (total)___________15

IUIUIUigIIUtuIUIUIUIJIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

*0/2

FORM I UOA 1X87 Rav.

109-99-9 Tvtrahydrofuran.

210

IEUOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

Lab Name:ETC Corp

Lab Coda:

Lauui al ru/ *"

Caaa No.:

Matrix: (soi1/watar)UATER

Sampl* wt/voli 9.0 (g/mDML

Lavali Clou/mad) LOU

X hoistura: not d«c.

Columni (packxcap)

Numbar TICa found:

Con-tract:

SAS No.:

CAS NUMBER

SDG No,:


Lab Fila ID: >C730?

Data Racaivad: 0*rJ6*'69

Data Analyzadt 10/10x89

Dilution Factor* I

CONCENTRATION UNITS:Cug/L or ugxKg)UG/L

COMPOUND NAME RT EST. CONC

FORM I UOA-TIC 2111X87 Raw


ERA SAMPLE NO,

Lab Name: ETC Corp. Contract: I ————————


Matrix: CaoiI/water) WATER Lab Sample ID: QC7Q079U

Sample uit/vol: 5.0 Cg/mL) ML



Column: (peck/cap) PACK

Lab File ID: >C7326

Date Received:


Dilution Factor: 1


74-87-3 —————74-83-9 ————75--01-4 —————75-00-3 —————75-09-9------67-64-1 ——————75-15-0 —————75-35-4 ————75-34-3--- _ -540-59-0 ————67-66-3 —————107-06-2 ————78-93-3 —————71-55-6 —————56-23-5 —————108-05-4 ————75-27-4------78-87-5 ————10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5---'- —71-43-2 —————10061-02-6 ——75-25-2 ————108-10-1 ————591-78-6 ————

79-34-5 —————108-88-3 ————108-90-7 ———100-41-4 ————100-42-5 ————1330-20-7 ———

i---Ch loromethane _ 1- — Bromomethane „, 1—— Uinvl Chloride 1- — Chloroethana „ „ 1— -Methulene Chloride 1---Acetone. ,_._, _ 1—— Carbon Disulfide, . ._,. ,,_.__ 1- — 1 rl-rjichloroethana 1---1 . 1-Dieh la roe thane 1—— 1,2-Dichlorethene (total ) __ 1— -Chloroform .. , 1—— 1 .2-Dich loroe thane 1— -2-Butanone , 1——— 1 rl .1-Triehloroa thane I---Carbon Tet rach lor ide. , _,. , 1—— Uinyl Acetate 1—— Bromod ich lor one thane 1—— Ir2-Dichlarapranane 1—— ci«-l ,3-Dichloropropene ____ 1—— Tr iehlnroathana_ 1——— Qifaromachlapomethane^ „ n .1——— 1 ;lr5-Triehlopo«thane 1— -Benzene , 1- —— t ran»-l ,3-Dich loropropene __ 1—— Bromoform I——— 4-Mathyl-2-Pentanone. ,,.„,._ _ 1—— 2-Hexanone 1- —— Tat raehloroathena m 1—— 1, 1, 2, 2-Tet rach lo roe thane __ 1---To luene..,, Mm 1—— Ch lorohenzene 1——— Ethylhanzena in n 1---Styrane m_ 1——— Xylena (total ) , 1

1

10101010710 ^55555510551055555555510105555555

1IUIUIUIU1IUIUUJIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIU1


uVOUTXU OMMTXCi MUUTSXI *AWU NO,

Mttrixi (MSupK

C

109-99-9 Tetrahydrofuran.................. '

t/17 ««v

213

IEVOLATILE ORGANIC* 'ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE XO

Lab Nama; -£7ZT^te Cod*!

/:Casa No.: __

Pft«tr»et:

s&A No.: SSOC No.:

Matrix: («oil/vatar)Sanpla vt/vol:

Laval: (low/mad)% Moistura: not dae.Colunn: (pack/cap)

Nunbar TIC« found:

Lab Saapla XO:Lab Pilt IDtData Racaivad: /#//// £9Data Analysad:Dilution factor:

CONCENTRATION UNITS._ . 7//fc

rom x VOA-TIC 2141/17


EPA SAMPLE NO,

Lab Name: ETC Corp.

Lab Code: Case No.:

Ma t r i x: (soil/uia t e r) UATER


Level: Clow/mod) LOW



Contract:

SAS No.: SDG No.:


Lab File ID: >C7342

Date Received:


Dilut ion Factor: 1


74-87-3 — - ————— Ch lorome thane___________74-83-9---- — ---Qromome thane____________75--01-4————————Yinyt Chloride__________75-00-3 ———————— Chloroethane____________75-09-2————-—Methylene Chloride______67-64-1 ——————— Acetone_______________75-15-0 — ————— Carbon Diaulf ide_______75-35-4———————1,1-0ich loroethene______75-34-3———— —— -1,1-Di Chloroethane______540-59-0—————1,2-Dichlorethene (total),67-66-3——— ———— Chloroform______________107-06-2 —————— 1,2-0 i Chloroethane______78-93-3 — —————— 2-Butanone______________71-55-6- —— -----l1111-Tr ichloroe thane___56-23-5--- — ----Carbon Tetrachlor ide____108-05-4——————Uinyl Acetate__________75-27-4------—-Bromodichloromethane____78-87-5 ——————— 1,2-Dichloropropane_____10061-01-5*————cia-1,3-Dichloropropene__79-01-6 ——————— Tr ich loroethene________124-48-1——————Dibromoch lorome thane____79-00-5——'————1,1,2-Tr ich loroe thane___71-43-2 ——————— Benzene_______________10061-02-6—————trans-1,3-Dichloropropene.75-25-2———————Bromoform_____________108-10-1 —————— 4-Methyl-2-Pentanone____591-78-6 —————— 2-Hexanone_____________127-18-4——————Tet rach loroethene______79-34-5 ——————— 1,1,2,2-Tet rach loroe thane.108-88-3 —————— Toluene_______________108-90-7——————Chlorobenzene__________100-41-4——————Ethyl benzene___________100-42-5 ———— —— Styrene_______________1330-20-7——————Xylena (total)_________

.110

.110

.110

.110

.13

.110

.15

.15

.15

.151515.110.15.15.110.15.15.15.15.15J5.15.15.15110.110.15.15.15.15.15.1515

IUIUIUIUuIUIUIUIUIUIUJUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

215FORM 1 UQA 1/87 Rev

1AV9IAT2U OMMTXCS AJULVSXS QAXft


2" '1 /*i 6

Lab Name:Lab Code:

IIVOLATILE ORGANICS ANALYSIS OATA SHEET

nNTATIVELY'lDENTIFIED COMPOUNDS

Contract:SAS NO.:

EPA SAMPLE HO.

Cast So. SDG No.:Matrix: (aoil/vatar)Sampla vt/vol:

Level: (lov/aed)% Moisture: not dec.Colunn: (pack/cap)

Number TICs found:

Ub Saapla IDi

Lab rilt ID:Dat« tacaivad:Data Analyxad:Dilution factor:

CONCENTRATION UNITS(ug/L or

CAS NUMBER

1.a.3.4.5.ft.7.t.».

10.11.12.13.14.15.K.17.IS.1».20.21.22.23.24.25.2*.27.'2t.29.30.

•

—————————— —————— - —————— "COMPOUND NAXE

Wlttmtuin/vspan /riMta^ ————

, ._._

————

RT

/§//,£»

•• 1——^^—

1ST. CONC.

55^*7

•

0

————— ..

__

__n-^ ———

rom x TOA-TXC 217 1/17 Rtv

1AVOLATILE ORGANIC? ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETC Corp.

Lab Code: Case No.:

Matrix; (soiI/water) UATER



\ Hoist

Column:

Cont ract

SAS No. SDG No. :

Lab Sample ID: QC7Q081'J

Lab File ID: >C7362

Date Received:

sture: not dec. Date Analyzed: 10x13x89

n: (pack/cap) PACK Dilution Factor: 1

CONCENTRATION UNITS:CAS NO. COMPOUND Cug/L or ug/Kg) UGXL Q

74-87-3 ———74-83-9 ———75-01-4 ———75-00-3 ———75-09-2 ———67-64-1 ———75-15-0 ———75-35-4 ———75-34-3 ———540-59-0 ——67-66-3 ———107-06-2——79-93-3 ———71-55-6 —— -56-23-5 ———108-05-4 ——75-27-4 ———78-87-5 ———10061-01-5-79-01-6 ———124-48-1——79-00-VJJSJ71-43-2-2310061-07 175-25-2--SI108-10-1 ——591-78-6 ——

79-34-5 ———108-88-3 ——108-9Q-7 ——100-41-4 ——100-42-5 ——1330-20-7—

--- — Chloromethana——— -Bromomathana ,———— Uinyl Chloride ,.,,,...----- Chloroethane „- — — Methylane Chloride———— Acetone ,, , , .. ——— Carbon Diaulf ide i i i i i i i H———— 1 r 1-Dichloroathena- ——— 1 r 1-Dich lor oe thane——— 1, 2-0 ich lore then* (total ) __— _-_Ch loroform.———— 1 f 2-D i chl or oa thane— -.-2-Butanone ,.„__.„.„ ,———— 1-1 - 1-Tri eh laraa thane_. —— Carbon Tat rach lor ide.....Uinyl Acetate ,.„__„„-. —— Bromadi eh 1 aroma thane... — 1,2-Dichloropropane

— —— Triehlaroethene ,..___. , „.„„

~«- 1,1,2-Tr ichlaraa thane . ,M— -Banzana immm_fc—— tran»-l,3-Dichloropropene___

.....A'-Mathyl-2-Pantanana-, —— .2-Haxanana _ , _MII ,

—— • — 1, 1 , 2, 2-Tat rach loroa thane __ .-. ——— Taluana——— -Ch lorabenzana—— ..Ethylhanzana ,_.. — —— Styrana^,^,^, _, n————— Xylana (total ) .„„,,.,._..,

1110110110110131101515151515151101515110151515151515151515110110151515151515151

1IUIUtuIUUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIU1

FORM I UOA 218 1x87 Rev

109-99-9 Tttrahydrofuran,

I/IT

219

IEUOLATILE ORGAN ICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

Lab Name:ETC Corp. I Laboratory

Lab Code: Case No.:


Sample wt/vol: 5.Q (g/mL)ML

Level: ( lou/med) LQLJ


Column: (pack/cap) u

Contract:

SAS No.:

I

SDG No.:

Lab Samp la ID: QC70081U

Lab File ID: >C7362

Data Received: («/f3/9


Di lut ion Factor: \


CAS NUMBER

01.02.

' -*ti/• • JW.i'miic

»• —— JB*j&i

COMPOUND NAME

CARBON DIOXIDEUNKNOUN

1!£••.. .

pp* •t'

RT

1.571.30

EST. CONC

7432

?2n

Q

JJ



ERA SAMPLE NO.

Lab Name: ETC Corp.

Lab Code: Case No.:

Ma t P i x: (soil/ua ten) UATER

Sample wt/voU 9.0 Cg/mL) ML

Lave1: C1ow/med) LOU

H Moisture; not dec.


Cont ract

SAS No.

CAS NO. COMPOUND

SDG No.:

Lab Sample ID: QC70081'J

Lab File ID: >C7369

Date Received: lo/'«/«*


Oilut ion Factor: 1

CONCENTRATION UNITS:Cug/L OP ug/Kg) UG/L

74-87-3———————Chlorome thane____________11074-83-9——————-Bpomome thane_____________11075-01-4———————Vinyl Chloride____________11075-00-3———————Chloroe thane______.______11075-09-2———————Methylene Chlopide^______1467-64-1 ——————— Acetone__________________11075-15-0———————Carbon Disulf ide__________1575-35-4———————1,1-Dichlopoethene________1575-34-3 ——————— 1,1-Dichlopoe thane________15540-59-0 —————— 1,2-Dichlopethena (total)__1567-66-3————————Chlopofopm_________________15107-06-2 —————— 1,2-0 ichlopoe thane________1578-93-3———————2-8utanone_______________11071-55-6———————1,1,1-Tpichlopoethane______1556-23-5—-—————Carbon Tat rachlorida 15108-05-4——————Uinyl Acetate____________11075-27-4——————Bromod ichloromethane___ 1578-87-5—-————-l,2-0ichlopoppopane_____ 1510061-01-5-—-—ci»-l,3-0icnlopoppopene____l579-01-6———————Tpichloroethene___________15124-48-1—————Pi brBiBoehloroiM thane 1579-00-5^——————1,1,2-Trichlopoethene______1571-43-2———————Benzene__________________1510061-02-6------tr«n»-l,3-Dichlopoppopane__1575-25-2———————Bromeform________________15108-10-1——————4-M«thyl-2-Pentanone______110591-78-6——————2-H«xanon«_______________I10127-18-4——————Tetpachlopoethene_________1579-34-5 ——————— 1,1,2,2-Tatrachlopoethane__15108-88-3 —————— Toluene__________________15108-90-7——————--Chlnrah«n»«n* 15100-41-4——————Ethylbenzene_____________15100-42-5——————Stypene__________________151330-20-7—————Xylene (total)___________15

IIUIUIUIUIJIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUtuIUIUIUIU

rrrFORM I UOA 1/87

r

iM

f

otoI«toItO

ftN•»

*<anoHIcH

ror-o f

IEUOLATILE ORGAN ICS ANALYSIS DATA SHEET


ERA SAMPLE NO.

Lab Neme:ETC Corp. I Laboratory


Matrix: (301 1 /water ) WATER

Sample wt/vol: 5.0 <g/mL>ML


H Moisture: not dec. _____

Column* (pack/cap)

Coot ract:

SAS No.: SOG No.:


Lab File ID: >C7369

Date Received: io/ia/9*?


Dilution Factor: 1

Number TICa found: ICONCENTRATION UNITS:(ug/L or ug/Kg)UG/L

CAS NUMBER

01.

——————— 4*9*-"-•• . .

COMPOUND NAME

CARBON DIOXIDE

Lf''

RT

1.54

EST. CONC

95

223

Q

J


VOLATILE ORGAN ICS ANALYSIS DATA SHEETEPA SAMPLE NO.

Lab Name: ETC Corp.

Lab Code: Case No.:

Ma t pi x: (soil/wa t e r) WATER


Level: (low/mod) LOLJ



Cont ract:

SAS No.: SOG No.:


Lab File ID: >D8036XT-

Date Received: 10/VQTV89

Dete Analyzed: 10/17/89



74-87-3————————Chlorome thane______________11074-83-9 ——————— -Bromome thane_______________I 1075-01-4————————vinyl Chloride_____________I 1075-00-3 ——————— Chloroe thane_____________11075-09-2————————Methylene Chloride_________1867-64-1 ———————— Acetone___________________1975-15-0———————Carbon Disulf ide__________1575-35-4———————1,1-Dichloroethene________1575-34-3 ——————— 1,1-Dichloroethane________15540-59-0——————1,2-Oichlorethene (total)__1567-66-3 ———————— Chloroform_________________15107-06-2———————1,2-Dichloroe thane_________1578-93-3———————2-Butanone_______________11071-55-6 ———————— 1,1,1-Trichlo roe thane______1556-23-5 ———————— Carbon Tet rach lor ide_______15108-05-4———————vinyl Acetate______________I 1075-27-4———————Bromodichlorome thane______1578-87-5 ——————— 1,2-Dichloropropane_______1510061-01-5—————c is-1,3-Dichloropropone____1579-01-6—"——————Trichloroethene____________15124-48-1-- — -——Dibromoch lorome thane_______1579-00-5 ——————— 1,1,2-Trichloroe thane______1571-43-2———————Benzene_________________1510061-02-6—————tran»-l,3-Dichloropropene__1575-25-2- ——————— Bromoform_________________15108-10-1——:————4-Methyl-2-Pentanone_______I 10591-78-6———————2-Hexanone_________________\ 10127-18-4——————Te t rach lo roe then*_________1579-34-5———————1,1,2,2-Tet rach loroe thane__15108-88-3——————Toluene_________________15108-90-7——————Chlorobenzene____________15100-41-4——————Ethylbenzene_____________15100-42-5——————Styrene_________________151330-20-7—————Xylene (total)___________15

Q

IUIUIUIUI13IUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU


szz

AM it/TVO* Z

IEVOLATILE ORGANics ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

Lab Name:ETC Corp.

Lab Code: Case No.:

Matrix: tsoi1/water)WATER

Sample wt/vol: 5.0 Cg/mDML

Level : C low/mod) LOW


Column; (pack/cap)

Number TICs found:

Cont ract:

SAS No.: SDG No. :


Lab File ID: >08036X3Date Received: 10/Vfl^89

Date Analyzed: 10/17x89

Dilution Factor: I____

CONCENTRATION UNITS:CugxL or ug/Kg)UG/L

CAS NUMBER COMPOUND NAME RT EST. CONC Q

FORM I UOA-TIC 1/87 Rev,

226


EPA SAMPLE NO

Lab Name: ETC Corp.

Lab Code: Case No.:


Sample vt/vol: 5.0 (g/»L) ML

Level: (low/raed) LOW



Contract:

SAS No.:; SDG No.:

Lab Sample. ID: QC70085V

Lab File ID: >I8246'Date Received:


Dilution Factor: l


74-87-3——————Chloromethane74-83-9——--—-Bromomethane75-01-4——————Vinyl Chloride75-00-3——————Chloroethane75-09-2——————Methylene Chloride67-64-1--——™Acetone__75-15-0——————Carbon Disulfide75-35-4——————l, 1-Dichloroethene75-34-3——————1,1-Dichloroethane540-59-0—————l, 2^Dichlorethene (total)67-66-3——————Chloroform107-06-2—————1,2-Dichloroethane78-93-3———————2-Butanone71-55-6——————l, 1,1-Trichloroethane56-23-5——————Carbon Tetrachloride108-05-4—————Vinyl Acetate75-27-4——————Broaodlchloronethane78-87-5——————1,2-Dichloropropane10061-01-5————cis-1,3-Dichloropropene79-01-6———-—Trichloroethene124-48-1—-———DibroMOchloromethane79-00-5--——-—l,1,2-Trichloroethane71-43-2-———-——Benzene10061-02-6——'-trana-1.3-Dichloropropene7 5-2 5-2——-——Bromof orm108-10-1—————4-Methyl-2-Pentanone591-78-6-————2-Hexanone127-18-4—————Tetrachloroethene79-34-5———-——l,1,2,2-Tetrachloroethane108-88-3—————Toluene108-90-7———-—Chlorobenzene100-41-4—————Ethylbenzene100-42-5—————Styrene1330-20-7—————Xylene (total)

i

101010107101055510510551055555555510105555555

;Uu

109-99-9 T«trahydro£uran

228

V3LXTIU OMA»X<-S1>NAWSXS OATA SHUTCOMPOUNDS

centrtct:SAS Mo.i

vt/vol:Lavol:% Moisturai notColumn: (pack/cap)

Nuabar Ties foundi _£

Datt Analysed t _Dilution factor:

COHCfHTJUTIOHor

CAS NUMltX

1.2.3.4.i.• .7.t.».10.11.12.13.14.15.

17.It.It.20.31.33.23.34.35.3«.37."21.2t.30,

rom x io»-txc 229 1/17

SEMIUQLATILE ORGAN ICS ANALYSIS DATA SHEET



Matrix: (soil/water) LJATER Lab Sample ID: QC70Q81C

Sample wt/vol: 1000. Cg/mL) ML Lab File ID: >G9012

Level: Uow/irad) LOW Date Received: W 79/89


Extraction: (SepF/Cont/Sonc ) CONT






I108-95-2———————Phenol____________________I 10111-44-4———————bis(2-Chloroethyl )ether____110?5-57-8———————— 2-Chlorophenol_____________110541-73-1———————1,3-Dichlorobenzene________110106-46-7———————1,4-Dichlorobenzene________I 10100-51-6——————Benzyl alcohol____________11095-50-1———————1,2-Dichlorobenzene_______11095-48-7———————2-Methylphenol____________110108-60-1 ——————— bis(2-Chl ore i sop ropy 1 )ether_l 10106-44-5 ——————— 4-Methyl phenol_____________110621-64-7-- — ——N-Ni t roso-di-n-propy lamine_11067-72*1 ———————— Hexachloroe thane___________I 1098-95*3 ———————— Nitrobenzene_______________I 1078-59*1————————Isophorone_________________I 1088-75-5———————2-Nitrophenol____________110105-67-9 —————— 2,4-Di methyl phenol________11065-85-0———————Benzole acid_____________150111-91-1——————b is (2-ChloPoethoxy)me thane_110120-83-2———————2,4-Dichlorophenol_________110120-82-1———————1,2,4-Trich lorobenzene_____11091-20-3 ——————— Naphthalene______________110106-47-8——————4-Chloroaniline___________11087-68-3———————Hexachlorobutadiene_______11059-50-7————————4-Ch I oro-3-methyl phenol____HO91-57-6————'———2-Methylnaphthalene_______HO77-47-4———•———Hexachlorocyclopentadiene__11088-06-2———————2,4,6-Trichlorophenol______11095-95-4———:———2,4,5-TrichIorophenol______15091-58-7————-—2-Chloronaphthalene_______11088-74-4————————2-Ni t roan i line_____________150131-11-3——————Dimethylph thai ate_________110208-96-8 —————— Acenaphthylene____________110606-20-2——————2,6-Dinitro toluene________110______________________________________I__

FORM I SU -1230

IIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIU

1/87 Rev

- 1CSEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO.



Metrix: (soil/water) UIATER Lab Sample ID: QC70081C

Sample wt/vol: 1000. Cg/mL) ML Lab File ID: >G9012

Level: (low/mad) LQUI Date Received: ,OK29/89




Data Extracted: 10/04/89



CAS NO. COMPOUNDCONCENTRATION UNITS:tug/L or ug/Kg) UG/L

99-09-2 —— -83-32-9 —— -51-28-5 —— -lt)Q-02-7——132-64-9 ——121-14-2 ——84-66-2 —— -7005-72-3—86-73-7 —— -100-01-6——534-52-1——86-30-6 —— -101-55-3——118-74-1——87-86-5 —— -B5-Q1-8 —— -120-12-7——84-74-2 —— -206-44-0 ——129-00-0 — -85-68-7"*.—91-94-l- £56-55-3-ijr218-01-9«S|117-81-7*2117-84- 0--'-

• 207-08-9—-50-32-8 —— -193-39-5——53-70-3 —— -191-24-2 — -

— ----3-Ni t roani 1 ine _ _— —— - Ac a nap h than a———— -2 ,4-Dini t rap hen o 1------4-Nitraphenal._ — — Dibenzofuran------2 r4-Din i t rota luana. ———— Diathvlphthalata------4-Ch loroohensjl-phenylether------Fluorene._-- — 4-Ni t roen i 1 ine „_ ,„_„.------4, 6 -Din it ro-2-methy Ipheno 1 _•- — --N-Ni t rosod iphanylamine (1) _. — — -4-Bromophenyl-phenylether __------Hexachlorobanzana•- —— -Pantach loroohenol•-- —— Phananthrana.__ —— Anthracana mia- ———— Di-n-hutylphthalata. ———— -Fluoranthana _ , iin.. —— .-Pyrana

S,£ .-3,3 '-Oichlornbanz idina&»*-Banzn(a)anthraeane tBi'-fi — Chrysenai**-——b \*(2-Ethylhaxyl)pht ha late _Bri»— Oi-n-octylphthalata.- ——— Banzo(h)f luoranthena. — . — -Banzn(k)f luoranthana.-- —— BanzoCa)pyrana ..__ — -Indartof 1 .2 r3-ed ) pur ana————— .D i han^t a rh) anthracene. — . ——— BanzoCg rhr i Iperulene

1150110150150110tio1101101101501501101101101501101101101101101101201101101101101101101101101101101

1IUIUIU *IUIU .IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1 1

CD - Cannot be separated from Diphenylamina

FORM I SU -2231

1/87 Rev

IFSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET


ERA SAMPLE NO.

Lab Name:ETCNJ

Lab Code: Case No.:

Matrix: Csoi 1/wa ter )LJATER

Sample wt /vo l : 1000. (g/mL)ML

Level: ( low/mad) LQLJ

\ Moisture: not dec._____ dec.___



Number TICs found: -S

Cont ract:

SAS No,: SDG No.:


Lab File ID: >G9Q12

Date Received: 0* 29/89



Dilution Factor: /___


CAS NUMBER

01. 141-78-602.03.04.05.

•

>f*9*j

'

COMPOUND NAME

Acetic acid, ethyl eaterUNKNOWNUNKNOWNUNKNOWNTr ichloropropene iaomer

* 'ft ' '

'&. •• •:&'' * *

•

-

RT

5.256.477.916.799.13

EST. CONC

77067322114

. Q

JJJJJ

FORM I SV-TIC 232 Rev

SEMIVOLATILE QRGANlEs ANALYSIS DATA SHEET SAMPLE NC

Lab Name: ETC Corp.


Matrix: (soi I /water) WATER

Sample wt/vol: 1000. Cg/mL) ML


Cont ract:

SAS No.: SDG No.:

Lab Sample ID: OC70082C

Lab F t l e ID: >G8653

Date Received:


Extraction: ( SepF/Cont /Sonc ) SERF

GPC Cleanup: (Y'N) N pH:




CAS NO. COMPOUNDCONCENTRATION UNITS:lug/L or ug/Kg> UG/L Q

108-95-2 ———11 1-44-4-..--95-57-8 ————541-73-1 ———106-46-7 ———100-51-6 ———95-50-1 ————95-48-7 ————108-60-1 ———106-44-5 ———621-64-7 ———67-72-1 ————98-95-3 ———— -78-59-1 ————88-75-5 ———— •105-67-9 ———65-85-0 ———— -111-91-1 ——— •120-83-2 ——— -120-82-1 ——— •91-20-3 ———— -106-47-8-—**87-68-3 ———— -59-50-7 ———— •91-57-6 ———— •77-47-4 ———— -

95-95-4 ———— -0 1 KQ •? _.

88-74-4 ———— -131-11-3 ——— -208-96-8 ——— -606-20-2 ——— -

——— Phenol t- — -b i»<2-Chloroethyl )ether ____——— 2-Chloraphenol 1----1.3-Dichlorobenzene 1----1 .4-Dich lorobenzene . 1----Benzvl alcohol ,, I----1.2-Dichlorobenzene 1——— 2-Methvlphenol 1----bis(2-Chloro is op ropy 1 )ether_l----4-Methvjlphenol 1----N-Ni t roso-di -n-p ropy lam ine _ 1----Hexachloroethane 1~---Ni t robenzene 1----Isophorone 1----2-Nitrophenol I——— 2 .4-Dimethvlphenol 1----Benzoic acid ,,. , 1•- — bis C 2-Ch 1 o roe thoxy) me thane _ 1——— 2 r4-Diehlnrophanol 1----Ip2r4-Triehlorabenzene 1——— Naphthalene ,„_ immm 1

._ — 4-Chlara-3-meth«jlpheno 1 1----2-Mathy 1 naphtha lena 1----Hexach lorocyclopentadi one __ „ 1.---2 J4J. A-Tr ieh lorophano 1 1.---2 ,4r5-Tr ichlopophanol 1.-_-2-Ch laron aphtha lana 1. —— 2-Nitroani 1 ina ,_„, i- ——— Dimathylphthalata t•---Acenaphthylene , __ mam 1•---2.6-Dinitrotoluene 1

t

101010101010101010101010101010105010101010101010101010501050101010

1lu-ll)IU1UIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

FORM I SU -1 233 1/37 Rev.

1CSEMIUOLATILE ORGANICS ANALYSIS DATA SHEET

SAMPLE NO,

Lab Name' ETC Corp. • Contract: t___




Level: (low/m«d) LOU

HMoisture: not dec. dec.




Lab File ID: >G8653

Da te Rece i ved: /P/VW'/rt





99-09-2 ———————— 3-Nitroani 1 ine_____________15083-32-9-- —— —— -Acenaphthene_______________I 1051-29-5- ——— ——— 2,4-Dinitrophenol__________150100-02-7- —— — --4-Ni trophenol______________150132-64-9 ———— — Dibenzofuran_____________110121-14-2 ———— —— 2 .4-Din.itrotoluene______I 1084-66-2 ———————Diethylphthe late__________HO7005-72-3————4-Chlorophenyl-phenylether_11086-73-7———————-Fluorene__________________110100-01-6 ——————— 4-N i t roan i line_____________150534-52-1 ——————— 4,6-D in itro-2-methy1 phenol_15086-30-6—--—---N-Nitroaodiphenylamine (1)_110101-55-3 —————— -4-Bromophenyl-phenylether__I 10118-74-1 —— — —— Hexachlorobenzene__________I 1087-86-5 ——————— Pentachlorophenol_________15085-01-8 ———————— Phenanthrene_______________I 10120-12-7——————Anthracene_______________11084-74-2 ——————— Di-n-butylphthalate_______110206-44^-0 ———— *—Fluoranthene_______________I 10129-00-0 ——————— Pyrene____________________I 1085-68-7———————Butylbenzylphthalate______11091-94-1———————3,3'-Dichlorobenzidine_____12056-55-3--—-—•—B«nzo(a)anthracene________I10218-01-9——————Chrysene____________ 110117-81-7——————bia(2-Ethylhexyl)ph thai ate_HO117-84-0———————Di-n-octylphthalate________I 10205-99-2 — ————— B«nzoCb)f luoranthene_______I 10207-08-9- — ————Benzotk)f luoranthene_______t 1050-32-8———————Benzo(a)pyrene____________110193-39-5——————IndenoU,2,3-cd)pyrene_____11053-70-3———————DibenzCa ,h )anthracene______110191-24-2-- ————Benzo(g,h , i )perylene______110


FORM I SU -2

IUiUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI

1/87 Rev

234

IFSEMIUQLATILE ORGANICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

Lab Name:ETC Corp.

Lab Code: Case No.:

Matrix: (soiI/water)UATER

Sample ut'voli 1000. <g/mL)ML

Level: ( low/med) LOU1

% Moisture: not dec.__;____ dec.___

Ex tract ion: (SepF/Cont/Sonc) SEPF


Number TICs found: 3___

Cont ract:

SAS No.: SDG No.:


Lab File ID: >G8653

Date Received:

Date Extracted:10x06/89


Dilution Factor: J____

CONCENTRATION UNITS:tug/L or ug/Kg)UG/L

CAS NUMBER

01.02. ioe-ee-303.

COMPOUND NAME

UNKNOUNBenzene, methyl* (9CI)UNKNOUN

RT

5.233.152.54

EST. CONC

6211 . .7

Q

JJJ

*

FORM I SU-TIC 1/87 Rev,

235

• IBSEMIUQLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO:

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: Csoi1/water) UATER

Sample ut/vol: 1000. Cg/mL) ML




CPU: Cleanup: (Y/N) N pH:

Cont ract

SAS No . : SDG No.:


Lab File ID: >G8835

Date Received: 10/&9/£V





FORM I SU -1

Q

108-95-2 ———

95-57-8 ————541-73-1 ———

100-51-6 ———95-50-1 ————95-48-7 -----108-60-1 ———106-44-5 ———621-64-7 ———67-72-1 —— --98-95-3 - —— -78-59-1 — ——88-75-5 —— —105-67-9 ———65-85-0 -----111-91-1 ———120-83-2 ———1 ori — fto— 1 _ ___91-20-3 ————106-47-8 ———

KO c n *y91-57-6 ————77.47-4 ————

95 95-4 ————91-58-7 ————88-74-4 -----131-11-3 ———208-96-8 ———

_ —— Pheno 1— — bis(2-Chloroethyl )ether ____----2-Ch loropheno 1 , .,_ „ .,„----1 .3-Dichlopobenzene----lJ4-Dichlnpobanzen«----Benzyl alcohol iin nii ., |1IB_----1 r2-Diehlopahanzena——— 2-Methylpheno 1----bisC2-Chloro i sop ropy 1 )ether_----4-Mathylpheno 1 . ni m_----N-Ni t roao-d i-n-propy lamine _----Haxanhlopoethane___-Ni t pobanzane , ni_ „----Isnphopana E_mmm m_——— 2-Ni t ropheno 1 , _ „ „_——— 2 ,4-Di methyl pheno 1----Banzoic acid----bis t2-Ch loroe thoxy ) me thane _——— 2 ,4-Oiehlorophenal----1;2 r4-Trichlopobenzene——— Naphtha lane——— -4-Chlaroani 1 me im ,__— --Haxach Inrohutadiane—— -4-Ch loro-3-me thy! pheno 1 ____—— -2-rtathul naphtha lane----Hexach lorocyc lopentadiena __----2j4T6-Tpich lopophano 1-__-2;4.5-Tpich lopopheno 1_-__2_Ch loponaphtha lan«-_--2-Ni t poan i 1 ina, t , iim ,----Dimathulphtha late----Aeanaphthylene .„, _----^jA-ninitPOto luane

101010101010101010101010101010105010101010101010101010501050101010

1 1IU :IU 1IU 'IU . 1IU • iIU tIU iIU 1IU IIU 1IU 'IU 1IU :IU 1lU :IU 1IU !IU 1IU :IU 1IU :IU IIU :IU 1IUIU 1iU !IU 1IU !IU 1IUIU 1IU1 1

1/37 Re236


EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: (soil /water) LJATER



Cont ract:

SAS No.:


Extraction: (SepF/Cont /Sonc ) SEPF

GP': Cleanup: (Y/N) N pH:

SDG No.:


Lab File ID: >G8835

Date Received: 10/05/8'-'


Date Analyzed: 10/2S--'S9

Dilution Factor: 1

CftS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UG/L

99-09-2 —— -- ——— 3-Nit roan i 1 ine_____________ 5083-32-9 — --- ——— Acenaphthene_______________ 1051-28-5 ——————— -2,4-Dinitrophenol__________ 50100-02-7---- ——— 4-Nitrophenol______,_______ 50132-64-9- — ————Dibenzofuran_______________ 10121-14-2 —— - ——— 2,4-Din i tro toluene_________ 1084-66-2---- ———— Diethylphtha late___________ 107005-72-3 —— - —— 4-Chloropheny1-phenylet her_ 1086-73-7———--- — Fluorene__________________ 10100-01-6 ———— —— 4-Nitroani1 me_____________ 50534-52-1- —————— 4,6-Dmitro-2-methylphenol_ 5086-30-6 — --- —— -N-Nitrosodiphenylamme (1)_ 10101-55-3--------4-Bromopheny1-phenylet her__ 10118-74-l--------Hexachlorobenzena 1087-86-5 —————— --Pentach loropheno 1__________ 5085-01-8 ———————— Phenanthrene_______________ 10120-12-7———————Anthracene________________ 1084-74-2 ——— — ——Di-n-butylphtha late________ 10206-44-0———————F luoranthene_______________ 10129-00-0———————Pyrene_______;_____________ 1085-68-7————————Butylbenzylph thai ate_______ 1091-94-1 ———————— 3,3'-Dichlorobenzidme^_____ 2056-55-3 ———— ---BenzoCa )anthracene________ 10218-01-9 ——————— Chrysene__________________ 10117-81-7———————bisC2-Ethylhexyl Jphthalate_ 10117-84-0— ————— Di-n-octylphthalate________ 10205-99-2 ——————— Benzo(b)f luoranthene_______ 10207-08-9 — ------BenzoCk)f luoranthene_______ 1050-32-8 ——————— -BenzoCa )pyrene_____________ 10193-39-5--- —— --IndenoCl,2 ,3-cd)pyrene_____ 1053-70-3 — —— ----DibenzCa,h)anthracene______ 10191-24-2--------Benzo(g,h,i Jperylene_______ 10_________________________________________I__

(. 1 / - Car.not be separated from Diphenylamme

FORM I S"J -2

Q

IIUIUIUIUIUtuIUIUIUtuIUIUIUIUIUIUIUIU!UIUIUIUIUIUtuIUIUIUIU'. U!UIU

237


TENTftTIUELY IDENTIFIED COMPOUNDS

ERA SAMPLE NO.



Matrix: (soi1/water)WATER

Sample wt/vol: 1000. Cg/mL)ML

Level: Clou/med) LOW


Extraction: CSepF/Cont/Sonc) SERF


Number TICa found: '

SDG No.:

Lab Sample ID: QC70086T

Lab File ID: >G8835

Date Received: lO/O^/o^



Dilution Factor: _/____


CAS NUMBER

01.

COMPOUND NAME

UNKNOWN

RT

7.52

EST. CONC

69

, Q iJ i

i

i

i

i

i

i

i

i

t

i;1

1

1

1

I

FORM I SU-TIC 238 l.'S


EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: (soil/waten) WATER


Level: Clow/mod) LOU


Extract ion: (SepF/Cont/Sonc1 CONT


Contract:

SAS No.: SDG No.:


Lab File ID: >G9041

Date Received: \o



Oi lut ion Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L'••*

108-95-2 —————— Phenol__________________110111-44-4———————bis(2-Chloroethyl )ether____11095-57-8 ———————— 2-Chlorophenol_____________110541-73-1 —————— 1,3-Dichlorobenzene_______110106*-46-7———————1,4-Dichlorobenzene________110100-51-6——————Benzyl alcohol___________11095-50-1———————1,2-Dichlorobenzene_______11095-48-7———————2-Methyl phenol___________110108-60-1——————bis(2-Chloroisopropyl >ether_l 10106-44-5 ——————— 4-Methylphenol_____________HO621-64-7——-———N-Nitroso-di-n-propy lamine_11067-72-1 ———————— Hexachloroe thane___________11098-95-3 ———————— Nitrobenzene_______________I 1078-59-1———————— Isophorone________________I 1088-75-5————————2-Nitrophenol______________110105-67-9 ——————— 2,4-Dimethylphenol_________11065-85-0———————Benzoic acid_______________150111-91-1——————b is (2-Chloroethoxy)me thane_110120-83-2——————2,4-Dichlorophenol________110120-82-1———————1,2,4-Tr ichlorobenzene_____11091-20-3————————Naphthalene________________I 10106-47-8——————4-Chloroaniline___________HO87-68-3—----——Hexachlorobutadiene_______11059-50-7————————4-Chloro-3-methylphenol____I 1091-57-6———————2-Methyl naphtha lane_______11077-47-4————————Hexachlorocyc lopentadiene__I 1088-06-2———————2,4,6-Trichlorophenol_____11099.99.4———————2,4,5-Trichlorophenol_____15091-58-7———————2-Chloronaphthalene_______HO88-74-4————————2-Nitroani 1 ine_____________150131-11-3 ——————Dimethylphthe late_________110208-96-8 ——————— Acenaph thy lane_____________I 10606-20-2 —————— 2,6-Dinitrotoluene________110_____________________________________I_

tuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I SU -1239

1/87 Rev,


EPA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Ma t r i x: (soil/wa tar) WATER

Sample wt/vol: 100Q. Cg/mL) ML


% Moiature: not dec. dec.


GPC Cleanup^ (Y/N) N pH:

Cont ract:

SAS No.: SDG No.:


Lab File ID: >G9041

Date Received: i



Dilut ion Factor: 1


99-09-2 ———————— 3-Nitroani 1 ine_____________I 5083r32-9———————— Acenaph thane_______________I 1051-28-5———————2,4-Dinitrophanol_________150100*-02-7———————4-Nitrophenol______________150132-64-9 —————— Dibenzofuran_____________110121-14-2——————2,4-Oinitrotoluene________11084-66-2———————Diethylphthalate__________1107005-72-3—————4-Chlorophenyl-phenylether_11086-73-7————————Fluorene__________________110100-01-6———————4-Nitroani 1 ine_____________150534-52-1 ——————— 4,6-Dinitro-2-methylphenol_15086-3 0-6- ——————— N-NitrosodiphenyI*mine (1)_110101-55-3 —————— 4-Bromophenyl-pheny lethar__110118-74-1——————Hexachlorobanzane_________11087-86-5———————Pentachlorophenol_________15085-01-8- —————— Phenanthrene_____________110120-12-7——————Anthracene_______________11084-74-2 ——————— Di-n-butylphthalate_______110206-44-0———————Fluo ran thane_______________I 10129-00-0———————Pyrena____________________I 1085-68-7——•————Butylbanzylphthalate______11091-94-1————————3,3'-Dichlorobanzidine_____12056-55-3-——————BenzoCaJanthracene________110218-01-9——————Chryaene_________________110117-81-7——————bia(2-Ethylhaxyl)phthalata_110117-84-0—------Di-n-octylphthe late_______133205-99-2 — - ———— BenzoCb)f luoranthane_______t 10207-08-9——————BenzoCkJf luoran thena______11050-32-8———————Benzo(a)pyrana___________110193-39-5———————Indano(l,2,3-cd)pyrane_____I 1053-70-3- —————— D i benz (a, h) anthracene______110191-24-2——————Benzo(g,h, i )parylene______110

_______,1__(1) - Cannot be separated from Diphenylamine

IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIIUIUIUIUIUIU


IFSEnI VOLATILE ORGAN ICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

Lab Name:CTCNJ . Contract:


Ma t r i x: (soil/w» t e r)WATER

Sample wt/vol: 1000. (g/mL)ML

Level: (low/mod) LOW

H Moisture: not dec._____ dec.____



. INumber TICa found: _

SDG No.:


Lab Ftle ID: >G9041

Date Received: f



Dilution Factor: /


CAS NUMBER

01. 141-78-602. >03.04. 2233-00-3

COMPOUND NAME

Acetic acid, ethyl esterACETONE DIMERUNKNOWN1-Propene, 3,3,3-trich loro-

RT

5.156.547.949.14

EST. CONC

2702302613

Q

JJJJ

FORM I SV-TIC 1/87

241


ERA SAMPLE NO,

Lab Name: ETCNJ

Lab Code: Case No.:

Matr ix : C s o i 1/water) LJATER

Sample wt/vol: 1000. Cg/mD ML

Leve 1: ( low/mod ) LOU1




Contract:

SAS No.: SDG No.:

Lab Sample 10: QC7Q092C

Lab File 10: >G9Q51

Date Received:



Dilut ion Factor : 1


108-95-2 ———111-44-4 ———99-57-8 ————541-73-1 ———

100-51-6 ———95-50-1 ————95-48-7 ————108-60-1 ———X06-44-5 ———621-64-7 ———67-72-1 ————9B-95-3-----78-59-1 ————88-75-5 ————105-67-9 ———65-85-0 ————111-91-1 ———

91-20-3 ————106-47-8 ———87-68-3 ————59-50-7 ————91-57-6 ————77-47.4 ————

95-95-4 ————91-58-7 ————88-74-4 ————131-11-3 ———208-96-8 ———606-20-2 ———

1——— Phenol 1— — bisC2-Chloroethyl ) ether ____ 1——— 2-Chlorophenol . 1----1 ,3-Dichlorobenzena 1----1 r4-Dieh lorohenzane , 1——— Benzyl alcohol .,„ , 1——— 1 .2-OiehlorGhenzena 1----2-Methy Iphenn 1 „, „ 1——— bis(2-Chloroisopropyl )ether_l----4-Methy Iphenol __ _ 1——— N-Ni t roao-d i-n-propy lamina _ 1——— Hexach loroathane ,„„ 1——— Nitrobenzene , 1——— laophorona t——— 2-Nitrophenol , 1———— 5 ,4-Dimft thy Iphenol 1——— Benzoic acid , 1-- — bis(2-Ch loroethoxy)me thane _ 1———— 5 ,4-rJiehlaraphenol I— --1 ,2 ,4-Tr ichlorohenzene 1— — — Naphthalene , , , . , , 1. —— .-4-Ch Inroani 1 ina mn 1----Haxaehlarahutadiana , 1

—— .-9_M.*hvl naphtha l«n« im 1——— Hexachlorocyclopentadiene. _ 1———— 2 J4f A-Tr ich lornphano 1 I— --2r4.5-Trieh loropheno 1 1———— 2-Chlaran«phth*lene . 1- — -2-Ni t roan i 1 me im , 1——— Dimethtjlphthalata „ 1----Acenaphthy lene „,. 1——— 2r6-Dinitroto luene M 1

1

101010101010101010101010101010105010101010101010101010501050101010

1IUIUIUIUIU -IUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

FORM I SU -1242

1/87 Rev

SEMIOOLATILE ORGAN ICS ANALYSIS DATA SHEETERA SAMPLE NO.

Lab Name: ETCNJ . '

Lab Code: Case No.:

Matrix: (sol 1/water) UATER


Lave 1: Clow/med) LOU


Extraction: (SapF/Cont/Sonc) CONT

GPC Cleanup: CY/N) N pHJ

CAS NO. COMPOUND

IContract: I_______

SAS No.: SDG No.:


Lab Fila ID: >G9051

Data Received:



Dilut ion Factor: 1

CONCENTRATION UNITS:CugxL or ugxKg) UGxL Q

99-09-2 ——————— 3-Ni troani 1 ine____________83-32-9———————Acenaph thane_____________51-23-5————————2,4-Oinitrophenol__________100-02-7———————4-Nitropnenol______________132-64-9——————Dibenzofuran_____________121-14-2————•—2,4-Dinitrotoluena^_______84-66-2———————Diethylphthalate__________7005-72-3—————4-Chlorophenyl-phenylether_86-73-7————————Fluor ana__________________100-01-6——————4-Nitroani 1 ina___________534-52-1 ——————— 4,6-Dinitro-2-methyl phenol_86-30-6 ———————— N-Ni trosodiphenylamine (1)_101-55-3--- — ---4-Bromopheny1-pheny1 ether__118-74-1 ————— — Hexachlorobenzene__________87-86-5---------Pentachloropheno1_________85-01-8———————Phenan throne_____________120-12-7——————Anthracene_______________84-74-2———————Oi-n-butylph thai ate_______206-44-0-——•——Fluor an thane____„_________129-00-0———————Pyrane____________________85-68-7———————Butylbenzylphthe late______91-94-1—— --——3,3 '-Dichlorobanzidina_____56-55-3——---—-BanzoCa)anthrecene________218-01-9——————Chryeene_________________117-81-7—————bi»(2-Ethylhexyl >ph thai ate_117-84-0——————Di-n-octylph thai ate_______205-99-2——————8enzo(b)f Iuoran thane______207-08-9———————Banzo£k)f luoranthane_______50-32-8—•—————Benzo(a)pyrene__,_________193-39-5——————Indeno(l,2,3-cd)pyrena_____53-70-3———————>Dibenz(e,h )anthracene______191-24-2 —————— 8enzo(g,h, i Jperylene______

5010505010101010105050101010501010101010102010101010101010101010

IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI

(1) - Cannot be separated from Diphenylamina

FORM I SU -2 Rev

243

IFSEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

Lab Name:ETCNJ

Lab Code: Case No.:

Matrix: (soiI/water>UATER

Sample wt/vol: 1000. <g/mL)ML

Leva 1: (1 ow/med) LOW

\ Moisture: not dec.___mm. dec.____


GPC Cleenupi CY/N) N pH:___

Number TICs found: 4r

Contract:

SAS No.: SDG No.:


Lab File ID: >G9Q51

Date Received:





CAS NUMBER

01. 141-79-602.03.04.

COMPOUND NAME


RT

5.106.448. 907.84

EST. CONC

3901102014

Q

JJJJ


IBSEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO. *. -(

Lab Name: ETI

Lab Coda: ";39HRr.Case No.:

Matrix: Csoi l/wat«r> WATER


Level: ( low/mod) LQUI


Extraction: (SepF/Conl/Sonc) SERF


Contract:

SAS No.:

>G9105

SDG No . :


Lab File ID:

Date Received:





108-95-2 ——111-44-4 ——95-57-8 ———541-73-1 ——106-46-7 ——100-51-6 ——95-50-1 ———95-48-7 ———108-60-1 ——106-44-5 ——621-64-7 ——67-72-1 ———98-95-3 ———78-59-1 ———88-75-5 ———105-67-9 ——65-85-0 ———111-91-1 ——

'1-20- E

91-57-6-- -77.47.4 ———

95-95-4 ———91-58-7 ———88-74-4 ———131-11-3 ——208-96-8 ——606-20-2 ——

———— Phenol— —— bis (2-Ch loroethyl )ether ____———— 2-Chlorophanol———— 1 f3-Dichlorobanzene-- —— 1 ,4-Dieh lorobenzena „ , „———— Benzyl alcohol———— 1 r2-Diehlorohanzana———— 2-Methyl phenol ,_-- — bis (2-Ch loro i sop ropy 1 )ether_———— 4-Methyl phenol- —— -N-Ni t roso-di-n-propy lamme _

—— _-Ni t rohanzene—— -- Imophorona———— 2-Nitrophanol ,————— 2,4-Dimathylphanal— — -Benzaie acid , _. — --bi» (2-Ch loro* thoxy)methane_

^*-_t 2 ,4-Tr i eh larobanzane _»£— --NaphthaleneMW—— 4-Chloro»ni 1 i ne«:-.--H« «eh lornhutadiana»— >--4-ChlQro~3-m«thuloh«nQ 1

————— 2 J4r5-Tr iehlaraohanal. ——— 2-Ch laronaph the lane— ---2-Ni t rnani 1 inm ^ _————— DimethylphthaLata _

— - — 2 ,^-Din it ro toluene _„

1110110no110no110no110no110no110no110no110150110110110no110no110no110no150110150HO110no1

1IUIUtu .IUIUIUIUIUIUIUIUIU

' IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI

FORM I SU -1 Rev.


EPA SAMPLE NO.

ILab Nama: ETCNj&-~ . •-

«aSv-Lab Coda: '*"-3Btt:€••• No.:wjr:fla t r i x : (soil /wal»r"> UATER

Sample wt/vol:'1000. (g/mL> ML

Level: Clow/mad) LOUI


Extract ions (SepF/Cont/Sonc) SEPF


CAS NO. COMPOUND

Cont ract:

SAS No.: SDG No.:

Lab Sample 10: QC70Q98C

Lab File ID: >G9105






99-09-2————————3-N it roani line_____________15083-32-9————————Acenaphthene_______________11051-28-5———————2,4-Dinitrophenol_________150100-02-7——————4-Nitrophenol____________150132-64-9——————Dibenzofuran_____________HO121-14-2——————2,4-Dinitro toluene________11084-66-2———————Diethylphthalate__________1107005-72-3 ————— 4-Chlorophenyl-phenylether_11086-73-7————————Fluorena__________________I 10100-01-6——————4-N it roani line___________150534-52-1———————4,6-Oinitro-2-methylphenol_15086-30-6———————N-N it rosodipheny lamine CD_110101-55-3———————4-Bromophenyl-phenylether__I 10118-74-1——————Hexachlorobenzene_________11087-86-5———————Pentach loropheno I_________;5085-01-8————————Phananthrana ___________110120-12-7——————Anthracene_______________: 1084-74-2———————Oi-n-butylphthalete_______110206-44-0————-Fluoranthene_______________I 10129-00-ae^"&--r-Pyr«ne__________________110

" Butylbenzylphthalate______HO-3,3'-Dichlorobenxidine_____120

---Benzo (e )anthracene________1102ia-Dl-*>£-r-- >"-*3-'-Chry».ana ^-^_____________110117-81-7———-——bi»(2-Ethylhexyl)phthalata_14117-84-0——————Di-n-octylphthalate_______110205-99-2——————Benzo <b)f luoranthane______HO207-08-9——————Benzo <k)fluoranthene______11050-32-8———————Benzo(a)pyrene___________110193-39-5——————IndenoU,2,3-cd>pyrene_____11053-70-3 ——————— DibenzCajh)anthracene_____,,1 10191-24-2 —————— Benzo(g,h, i )perylene^_____110

______________________________________I__(1) - Cannot be separated from Diphenylamina

FORM I SU -2

1IUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIJIUIUIUIUIUIUIU1

1/87 Rev,

246

\

IFSEniUOL<W:M-E ORGAN 1CS ANALYSIS DATA SHEET

ITIUCLY IDENTIFIED COMPOUNDS

ERA SAMPLE NO.

Lab Name:ETCNJ

Lab Code: " " •'• Case No.:

Ma t r i x: (soil /wa t e r ) UJATER

Sample wt/vol: 1000. Cg/mL)ML


H Moisture: not dec._____ dec.___



Cont ract:

SAS No.: SDG No.:


Lab File ID: >G9105

Date Received: 'tt)/«J>89

Date Extracted:11/06x89


Dilution Factor: _L

CONCENNumber TICa found: 1 .. tuqXL

CAS NUMBER

01.

COMPUUND N«ME

UNKNOWN

.-. 4 - .••-.•xjfup*.*^•tjjjjgjji^î fSllfcr*-.-..: (8fiif "^ ' * ' ' ••" rSeyJ SSIt'*; •. • 'r • •

TRATIQN UNITS:or ug/Kg)UG/L

RT

6.18

.

EST. CQNC

30

•

Q

J

FORM 1 SU-TIC 2471/87 Rev


F-PA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Mat r i x : C s o i l / w a t e r ) LJATER


Level: Clow/med) LGU




CAS NO. COMPOUND

Cant rac t:

SAS No.: SDG No . :


Lab File ID: >JA495/*/"/

Date Received: o»/j )/ro/ri /*4Date Extracted: 09 ••g?"0


Di lut ion Factor


519-64-6 ————319-65-7 ————319-86-8 ————58-89-9 —————76-44-8 —————309-00-2 ————1024-57-3 ———959-98-8 ————60-57-1 —————72-55-9 —————72-20-8 —————33213-65-9 ——72-54-8 —————1031-07-8 ———50-29-3 —————72-43-5 —————53494-70-5 ——5103-71-9 ———5103-74-2 ———8001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-82-5 ——

—— alpha-BHC— -beta-BHC—— delta-BHC---aamma-BHC(Lindane )---Heptach lor---Aldr in---Heot ach lor epox ide---Endosu 1 f an I---Die Idr in—— 4.4'-DDE---Endr in—— Endoaulfan II—— 4.4l-DDD---Endoaul fan sulfate—— 4.4--DDT---Mathnxyehlor— -Endr in Uatons— -alpha-Ch lordane.---gamm«-Ch lordane—— Toxaphene—— Aroelor-1016—— Aroclnr-1221—— Aroelor-1232——— Aroelnr-1242——— Arnelor-1248——— Aroelor-1254—— Aroclor-1260

.050,050.050.050.050.050.050.050.100.100.100.100.100.100.100.500.100.050-.0502.500.500.500.500.50011

1IUIUIUIUIUIUIU .IUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIU1


248

IDPESTICIDE O.RGANICS ANALYSIS DATA SHEET

ERA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

MatPix: (soil/wat«p) WATER


Level: (low/med) LQU

>i Moisture* not dec. dec.



Cont ract:

SAS No.: SDG No.:


Lab File ID: >HA296

Date Received: vo/o4/f4





319-64-6 ——————— alpha-BHC________319-65-7———————beta-BHC_________319-86-9 ——————— delta-BHC________58-89-9- — ————— gamma-BHCCLindane).76-44-8- ——————— Heptachlor_______309-00-2 ——————— Aldr in___________1024-57-3-------Heptachlor epox ide.959-9Q-9 ——————— Endosulfan I_____60-57-1 —— —— ---Dieldr in_________72-55-9 ———————— 4,4'-DDE_________72-20-8 ———————— Endr in___________33213-65-9 ————— Endosulfan II____72-54-8 ———————— 4,4'-ODD_________1031-07-8-———--Endosulfan sulfate.50-29-3 ———————— 4,4'-DOT_________72-43-5 ———————— Methoxychlor_____53494-70-5—————Endrin ketone_____5103-71-9——————alpha-Chlordane___5103-74-2----—-gamma-Chlordane___8001-35-2——— —— Toxaphene________12674-11-2 ————— Apoclop-1016_____111Q4-28-2 ————— Aroc toP-1221_____11141-16-5 ————— Aroclor-1232_____53469-21-9 ————— Aroc 1 OP-1242_____12672-29-6—————Aroc IOP-1248_____11097-69-1—————Aroc IQP-1254_____11096-82-5 ————— APOC IQP-1260_____

.050.050,050. 050.050.050,050.050.100.100.100.100.100, 100.100.500. 100.050.0502.500.500.500.500.50011

IUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I PEST 1/97 Re'

249

\


ERA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:



Level: Clou/mod) LOW

HMoisture: not dec. dec.



Contract:

SAS No.: SDG No.:


Lab File ID: >HA323

Date Received: -i*/*3/#*l





319-64-6 ——————— alpha-BHC________319-65-7———————beta-BHC_________319-86-8 ——————— delta-BHC________58-89-9- —— ———— gamma-BHCCLindane).76-44-8 ———————— Heptachlor_______309-00-2———————Aldrin___________1024-57-3——————Heptachlor epoxide.959-98-8———————Endoaulfan I_____60-57-1————————Dieldrin_________72-55-9 ———————— 4,4'-DDE_________72-20-8————————Endrin___________33213-65-9 ————— Endosulfan II_____72-54-8 ———————— 4,4'-ODD_________1031-07-8——————Endosulfan sulfate50-29-3 ———————— 4,4'-DOT_________72-43-5———————Methoxychlor_____53494-70-5 ————— Endrin ketone_____5103-71-9——————alpha-Chlordane___5103-74-2 —————— gamma-Ch lordane___BO 01-35-2—————Toxaphene________12674-11-2—————ArocloP-1016______11104-28-2—————Aroc lor-1221______11141-16-5—————Aroc lor-1232______53469-21-9—————Aroc lor-1242______12672-29-6 ————— Aroc lor-1248______11097-69-1—————Apoclor-1254______11096-82-5 ————— APOC lor-1260______

.050

.050

.050

.050

.050

.050

.050

.050

.100

.100

.100

.100

.100

.100

.100

.500

.100

.500

.5002.500.500.500.500.50011

IUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI


250

IDICIOE ORGANICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETCMC

Lab Code: Case No.:

Ma t r i x : (soil /uia ten) WATER


Level: (lou/med) LOU




Contract:

SAS No.: SDG No.:

Lab Sample ID: QC7004SG

Lab File ID: >JA486

Date Received: oq/»T/**?





319-64-6-319-65-7-319-86-8-58-89-9 —76-44-8—309-00-2-1024-57-3959-98-8-6Q-57-1 —72-55-9--72-20-8——33213-65-72-54-8—1031-07-850-29-3-T72-43*f |K53494«4K)5103-2QHI5103-7W8001-79W12 674- 11- J11104-28-11141-16-53469-21-12672-29-11097-69-11096-82-

—————— alpha-BHC—————— beta-BHC ,. ————— delta-BHC—————— gamma-BHCCLindane ) ,_ ,_------- Heptachlor————— -Aldrin. — __ — Heptachlor epox ide , MI. in ._, ,--- — --Endosu 1 f an I-__-__-Di« Idr in ,._—————— 4.4'-DDE»__--_-Cndr inJ ————— Endosu If an I I. ————— 4.4'-DDD—————— -Endoaul fan sulfate^,,, „,_, .—————— 4r4'-DOT*--^---M«thoxychlap ip

g— ---Endrin k«ton«R -I —— •lph«-Chlardanam .._. _l^-»—— q«mm*-Ch lord*nB&-i- — -Tax«ph«ne»—— ; ———— Aroelor-10163 —————— Aroclor-12215 —————— Arnelar-12329 ————— Aroe lap- 1242& —————— Aroelor-12481 —————— Apnelop-12545 ————— Apoelop-1260

.050

.050

.050

.050

.050

.050

.050

.050

.100

.100

.100

.100

.100

.100

.100

.500

.100

.050

.0502.500.500.500.500.50011

1IUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1



EPA SAMPLE NO,

Lab Name: £'

Lab Code: *^: . Case No.:

Ma t r i x : (soil /we tar) U1ATER

Sample ut/vol: 1000. (g/mL) ML

Level: Clou/mad) LOUI




Contract:

SAS No.: SOG No . :


Lab File ID: >HA546

Date Received: 10 /" '*^

Date Extracted: lQ/12'99



CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg> UG/L

319-64-6--319-65-7--319-86-8--58-89-9 ——76-44-8 ——309-00-2--1024-57-3-959-98-8--60-57-1 ——72-55-9 ——72-20-8 ——33213-65-972-54-8 ——1031-07-9-50-29-3 ——72-43-5 ——53494-70-55103-7X-9-

' 51Q3-74T2*

' 2674>-iSS'104-Kj4t-SH9-2r*f-29-669-12-5

————— alpha-BHC————— bata-BHC————— dalta-BHC--~---qamma-BHC(Lindane ) ,————— Heptaehlor————— Aldrin

--_ — -Endoaulfan I- —— — Dieldr in a__ ia_————— 4.4'-DDE------Endr in,în————— Endoaulfan 1 1 ,————— 4.4--DDD————— Endoaulfan aulf ate ,_.,.————— 4r4'-DDT.,,— _- — Mathoxych lor . ,„,,,_. — .- — Endrin ketone— — - — alphi-Chlordane... — .-gamnia-Chlordane••—•---ToxaphanaK. ——— Aroelor-1016Kp ——— Aroelor-1221•t— --Aroelop-1232_G. ———— Aroelor-1242, „ ,, , ,- ———— Aroelor-1248 .—————— Aroelor-1254 _ . ..—— - — Aroc lor- 1260 ._

,050.050.050.050.050.050.050.050.100.100.100.100.100.100.100.500.100.050.0502.500.500.500.500.50011

1IUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

FORM I PEST 1/87 R*v

252

\


EPA SAMPLE NO

Lab Name: ETCNJV,

Lab .Code: " ,'; Case No.:



Level: C low/mod) LQU)

Cont rac t:

SAS No.:

Moisture: not dec dec



CAS NO. COMPOUND

SDG No.:

Lab Sample 10: QC7QQ55G

Lab File ID: >HA565






319-64-6 ——————— alpha-BHC________319-65-7———————beta-BHC_________719-86-8 ——————— delta-BHC________58-89-9—-—--—gamma-BHCCLindane).76-44-8———————Heptachlor_______309-00-2 ——————— Aldnn___________1024-57-3—————-Heptachlor epoxide.959-98-8 ——————— Endoaulfan I_____60-57-1 ———————— Dieldrin_________72-55-9 ———————— 4,4'-DDE_________72-20-8 ———————— Endrin___________33213-65-9 ————— Endosulfan II____72-54-8 ———————— 4,4'-DDO_________1031-07-8----——Endosulfan sulfate.50-29-3 ———————— 4,4'-DOT_________72-43-5 ———————— Methoxychlor_____53494-70-5 ————— Endrin katone5103-71-9 —————— alpha-Chlordane___5103-74-2—————- gamma -Ch lordane___8001-35-2—-———Toxaphene_______12674-11^2—————Aroc lor-1016_____11104-2a-2————Aroc lor-1221_____11141-le>$—————Aroc lor-1232_____53469-21-9—————Aroc lor-1242_____12672-29-6—————Aroc lor-1248_____11097-69-1 ————— Aroc lor-1254_____11096-82-5 ————— Aroc lor-1260_____

,050.050,050.050,050.050,050.050.100,100,100,100,100,100100,500100,050050

>500,500500,500500

ItuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I PEST 1/87 Pev.

f\ r ~LZ o o

8AVOLATILE INTERNAL STANDARD AREA SUMMARY

Lab Name: ETC Co,-p.' Contract:


Lab File ID (Standard): >C7231 Data Analyzed: 10/02/89

Instrument ID: GC/MS C Time Analyzed: 1837

Matrix:Csoil/water) WATER Leve1:(low/med) LOW Column:(pack/cap)

II1 12 HOUR STO

1 UPPER LIMIT

1 LOUER LIMIT

1 EPA SAMPLE1 NO.

Q1IQC7Q07QV02IQC70070U031041051061071081091101111121131141151161171181191201 ^* 191 I .*»22! •«

ISl(BCM)AREA *

66550

133100

33275

7174695347

rt ————————

RT

13.47

13.4613.50

IS2CDFB)AREA *

317584

635168

158792

335419460323

RT

24.05

24.0324.03

IS3CCBZ)AREA *

233201

466402

116601

252458340604

RT

29.47

29.4529.45

151 CBCM) - BVowochloromethane152 (DFB) - 1,4-Difluorobenzene153 (CBZ) • Chlorob»nzene-d5

UPPER LIMIT - * 100*of internal standard areaLOUER LIMIT - - 50*of intarnal standard area

* Column used to flag internal' standard area values w i t h an asterisk.

page _£_ of j£_

FORM UIII UOA 1/87 Rev

254

80UOLATILE INTERNAL STANDARD AREA SUMMARY

Lab Namei ETC Corp. Contract!

Lab Code: Case No.: SAS No.: SOG No.:



Matrix: Csoi I/water) UATER Level:(low/med) LQU1 Co lumn : (pack/cap ) _^_

111 12 HOUR STO

1 UPPER LIMIT

1 LOWER LIMIT

1 EPA SAMPLE1 NO.

01IQC70070U02ICA1372U03ICA1372YS04ICA1372v*RQ5ICA1373U06ICA1374U07ICA1376U08ICA1379U091101111121131141151161171181191201211 ,f221 «J

ISKSCM)AREA *

104163

208326

92081

989041029881022819944886247786798277180120

ft

RT

13.49

13.4813.4713.4613.4913.9313.4413.4913.90

IS2COFQ)AREA *

493901

987002

246791

468434906908499899499360436618377663399940376306

RT

24.00

24.0224.0924.0324,0324.1024.0224.0224.08

IS3CCB2)AREA *

366536

733072

183268

394218378884366479339304344391306929309309296629

RT

29.41

29.4729.4729.4929.4629.5329.4029.4529.50

151 CBCM) • Mtoehloromethane152 CDFB) • r^PDifluorobenzen.153 (CBZ) - Chlorobenz«ne-d9

UPPER LIMIT - * 100*of internal itandard areaLOWER LIMIT - - 90Sof intarnal standard araa

% Column usad to flag irvternal standard ar*a value* with an asterisk.

page *• of */

FORM UUI UOA 1/87 Rev

255

8AUOLflTILE INTERNAL SlftKDARD «REA SUMMARY

Lab Name: ETC Corp. ' Contract:




Matrix:(soi1/water) UATER Level:(low/med) LOW Column:(pack/cap) ___

111 12 HOUR STO

1 UPPER LIMIT

1 LOUER LIMIT

1 EPA SAMPLE1 NO.

OHQC7007QU02ICA1377U03ICA1382U041CA1374U05ICA1376U061071081091101111121131141151161171181191201 d?n j£991 Ê

IS1CBCM)AREA *

96969

193930

48483

8785294004808378437182902

Urp>•ti _______

RT

13.30

13.3513.3013.4713.3513.40

IS2CDFB)AREA *

452236

904472

226118

405893445624383433404983399-296

RT

23.73

23.7823.7623.8623.7823.82

IS3CCBZ)AREA *

349207

698414

174603

316491346441302824319337313414

RT

28.92

28.9828.9529.0828.9628.98

151 CBCM)152 (DFB) -153 CCBZ) - Chlorobenzene-d5

UPPER LIMIT - * 100*ef internal standard area.LOUER LIMIT - - 90Sof internal standard area.

* Column used to flag internal standard area values with an asterisk,

page 3 of ^

FORM UIII UOA 1/87 Rev

256

SHVOLATILE, INTERNAL STANDARD A?E. SUMrARV

Lab Names ETC Corp. Ccrtract:

Lab Code: Case No.: SAS No.: SDG No,:



Matrix: Csoi i/water) WATER Leve 1: Uow/med ) LOW Co lumn: (pack/cap ) ___

t11 12 HOUR STD

1 UPPER LIMIT

1 LOWER LIMIT

1 EPA SAMPLE1 NO.

Q11QC70070U02ICA1375UQ3ICA1378U04ICA2068UQ91CA1379U06ICA138QU07ICA2Q69U *T)08ICA2070U * T0911QI111121131141151161171181191201

IS1CBCM)AREA *

81199

162398

40599

860669356587125870668883489531

PA 878601 83851

91 ' Ifif92 I .-db*i<-

RT

13.29

13.2813.3213.3413.2813.2613.3113.2913.27

IS2CDFB)AREA *

396694

793388

198347

413918430516416935408155428207432395423437390901

RT

23.68

23.7023.7423.7623.7423.7223.7323.7123.69

IS3CCBZ)AREA *

318670

637340

159335

334768346538335343328515343889346602342101315422

RT

28.83

28.8928.9328.9428.8929.9028.8828.8928.88

151 (8CM) - •IHftehioromethane152 (DFB) * 1%4-Oi 11uorobenzene153 CCBZ) * Chlorob«nzene-d5

UPPER LIMIT - * 100*of internal standard areaLOWER LIMIT - - 50*of internal standard area

t Column uftad to flag in-tarnal standard ara* values with an asterisk,

page _£_ of JL

FORM UUI UOA 1X87 Rev

257






Matrix:(soil/water) WATER Level:(low/med) LOW Column;(pack/cap) gyVuA

01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO,

QC70076VCA1380VCA1381VCA1383VCA2026VCA2029VCA2032VCA2032VSCA2032VR

ISl(BCM)AREA I

89814

179628

44907

856058689983905816598447478789746718304778301

_ .. —— . ——— _ —

RT

13.28_— — _

>,,-.-

13.2713.3313.2813.2813.3113.3013.3313.2713.26

—————

IS2(DFB)AREA I

395016

790032

197508

397299406819399478385540396587378526353331379984354630

_________

RT

23.71

23.6923.7223.7023.7023.7323.7223.7123.7323.72

IS3(CBZ)AREA I

318244

636488

159122

325240332209324826317723329066312545295815313320288101

—————————

— -•-

RT

28.85

28.8828.8728.8928.8928.9128.9128.8728.9128.90

__ ——— i

151 (BCM) - Broaochloromethane152 (OFB) - 1,4-Difluorobenzene153 (CBZ) * Chlorobenzene-d5

UPPER LIMIT » + 100%of internal standard areaLOWER LIMIT - - 50%of internal standard area

I Column used to flag internal standard area values with an asterisk.

page<rr FORM viii VOA 2 5 a/87 Rev,





Instrument ID: 6C/MS C Time Analyzed: 1005

Matrix:(soiI/water) WATER Level:(low/med) LOW Column:(pack/cap) 3u/

01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

QC70076VCA2033VCA2031VCA2034V

_ _ — — ._...

ISl(BCM)AREA 1

89788

179576

44894

82645840908188780831

—————————

_ _. — — ..... —

RT^13.28

—————

13.2613.2813.2613.32

—————

—————

—————

IS2(DFB)AREA I

404864

809728

202432

383173378342379314375628

—————————

—————————

— ————————

RT

23.67

—————

23.7223.7423.7223.74

—————

—————

IS3(CBZ)AREA *

325000

650000

162500

314897316576315572311845

—————————

RT

28.86

—————

28.8728.9228.9328.94

—————

—————_ _

151 (BCM) - Bronochloronethane152 (DFB) - 1,4-Difluorobenzene153 (CBZ) - Chlorobenzene-d5

UPPER LIMIT - + 100%of internal standard areaLOWER LIMIT - - 50%of internal standard area

I Column used to flag internal standard area values with an asterisk.JL '

FORM VIII VOA 1/87 Rev

259


Lab Name: ETC Corp. Contract: .




Matrix:(soil/water) WATER Level:(low/med) LOW Column:(pack/cap)1

01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

ISl(BCM)AREA I

83796

167592

LOWER LIMIT 41898

EPA SAMPLENO.

QC70076V 78302CA2027V 70595CA2035V 72584CA2036V 72618CA2037V 73309CA2038V 72249CA2039V 68513CA2040V 62592CA2042V 72984CA2043V 67845

1

RT

13.33

13.3313.3013.2913.2813.3113.3413.2913.2713.3113.29

IS2(DFB)AREA I

384911

769822

192455». — -*

366424337199346414342888349013347239321119290119365271342843

—————————

RT

23.76

23.7523.7223.7123.7423.7323.7623.7223.7323.7323.71

—————

IS3(CBZ)AREA I

330704

661408

165352

320617291648301227298653301481300988283603252359309470262351 •

iRT

28.92

28.9328.9228.8628.8828.8828.9428.9028.9128.9128.89

——

—————

IS1 (BCM) - Bromochloromethane UPPER LIMIT * + 100%IS2 (DFB) - 1,4-Difluorobenzene of internal standard area.IS3 (CBZ) - Chlorobenzene-d5 LOWER LIMIT - - 50%

of internal standard area.

I Column used to flag internal standard area values with an asterisk./ I

page -g of &FORM VIII VGA 1/87 Rev,




Lab File ID (Standard): >C7325 Data Analyzed: 10/11/-89

Instrument ID: GC/M1S C Time Analyzed: 1349

Matrix: (soil/water) WATER Leve 1 : ( low/mod > LOUI Co lumn; (pack/cap ) flf£0£-

111 12 HOUR STD

1 UPPER LIMIT

1 LOWER LIMIT

1 EPA SAMPLE1 NO.

01IQC700791J02ICA1894V03ICA1893U041CA1893US05 ICA1893UR06ICA1895U07ICA1897U08ICA1896U09 110111112113!14115116 117118!191201211221

ISl(BCM)AREA *

77565

155130

38783

7368265502663266506264093548966365066433

RT

13.26

13.3013.3013.2713.3013.2613.2613.3013.29

IS2(OFB)AREA *

354708

709416

177354

342335300052309512312346302555248321307006317115

RT

23.73

23.7223.7223.7323.7223.7223.7223.7223.71

I S3 ( CBZ )AREA *

307253

614506

153626

296687265182273550268274261181220662250798282191

RT

28.87

28.9028.9028.9128.9028.9028.9028.9028.89

I SI (BCM) • Brofflochloromethane152 CDFB) • 1,4-0ifluorobenzene153 (CBZ) - Chlorobenzene-d5

UPPER LIMIT - * 100Xof internal standard areaLOWER LIMIT - - 50*of interne 1 standard area

t Column used to flag internal standard area values with an asterisk261page __ of __

1/87

SAVOLATILE INTERNAL STANDARD AREA SUMMARY



Lab File ID (Standard): >C7338 Deta Analyzed: 10/12/89


Matrix: lso\I/water) WATER Leva I :( low/med ) LOW Co lumn : (pack/cap ) MC'r*

111 12 HOUR STD

1 UPPER LIMIT

1 LOWER LIMIT

1 EPA SAMPLE1 NO.

01IQC7QQ79tJ02 103104105106107109 109110111 I12113114115!16117118119120121)221

IS1C8CM)AREA *

58085

116170

29043

56046

RT

13.26

13.27

IS2(DFB>AREA *

245073

490146

122536

268726

RT

23.73

23.73

IS3(CBZrAREA #

213526

427052

106763

251428

RT

28.92

28.91

151 CBCM) - Sromochloromethane152 CDFB) " 1,4-Difluorobenzene153 (C8Z) - Chlorobenzene-d5


f Column used to flag internal standard area values utith an

page __ of __

8AUQLATILE INTERNAL STANDARD AREA SUMMARY




Instrument ID: GC/MS C T ime Analyzed: 1751

Mat rix:(soi1/water) WATER Leve1:(low/mad) LOW Column;(pack/cap)

01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

CA1897UCA1896U

,

ISKBO1)AREA *

51476

102992

25738

5844156845

RT

13.26

13.2713.27

I S2 ( OFB )AREA #

229097

458194

114549

27422826S091

RT

23.69

23.7323.73

IS3CC9Z)AREA *

204634

409268

102317

244862240868

RT

28.87

28.9128.87

151 iBCM) - Bromochloromethane152 CDFB) - 1,4-Difluorobenzene153 (CBZ) - Chlorobenzene-d5

UPPER LIMIT - * 100%of internal standard area.LOWER LIMIT - - 5QX 263of internal standard area.

t Column used to flag internal standard area values with an asterisk,

page __ of __

8AUOLATJLE INTERNAL STANDARD AREA SUMMARY



Lab File ID (Standard): >C7361 Data Analyzed: 1Q/13/S9


Matrix: (so; I/water) UIATER Leve 1 : C low/med) LOU Co lumn : (pack/cap ) "PA(LK

111 12 HOUR STD

1 UPPER LIMIT

1 LOWER LIMIT

1 EPA SAMPLE1 NO.

01IQC70081U02ICA1778V03ICA1779U04ICA1780U05ICA1783U06 1071081091101111121131141151161171181191201 *-•211 <;<?221

IS1CBCM)AREA *

55460

110920

27730

5331152320528295278650736

UrI 'r

RT

13.30

13.2613.2713.3113.3013.27

IS2CDFB)AREA *

242331

484662

121166

248819247233248137251096241352

RT

23.73

23.7223.7323.7323.7223.73

IS3CC8Z)AREA *

220400

440800

110200

225292223243224157221168219232

RT

28.91

28.9128 .9128.9228.9128.91

151 (BCM) - Bromochloromethane152 (OFB) • 1,4-Oifluorobenzena153 (CBZ) - Chlorob0nzene-d5

UPPER LIMIT - + 100*of internal standard areaLOWER LIMIT - - 5OHof internal standard area

* Column used to flag internal standard area values with an asterisk

page _L. of 3

FORM V I I I UOA 1/87 RevO s264


Lab Name: ETC Corp. ' Contract:


Lab File ID (Standard): >C7368 Data Analyzed: 10/13/S9


Matrix: Csoi I/water ) UATER Leva 1: C low/mod ) LOU Co lumn: (pack/cap )

01020304050607080910111213141516171819202122

111 12 HOUR STD

1 UPPER LIMIT

1 LOWER LIMIT

1 EPA SAMPLE1 NO.

IQC70081UICA-1778VSICA1778URICA1790UICA1796U1CA1799UICA2140UICA2140VJSICA214QUR11t1111I1I11 . <._1

isi(BCM)AREA *

92016

104032

26008

516255149453796507654998040937491764922745782

r:.

RT

13.27

13.2713.3013.2613.2613.3013.2713.2713.3013.26

IS2CDFB)AREA *

245863

491726

122932

242346247516250076243845232974184003229667224327216221

RT

23.69

23.7323.7623.7223.7223.7223.7323.7323.7223.72

I S3 t CB2 )AREA *

225086

450172

112543

219558222247224379219814212266170567209765205187194271

IRT

28.87

28.9128.9028.i9028.9028.9028.9128.9128.9128.90

151 (SCM) • Bromochloromethane152 (DFB) - 1,4-Difluorobenzene153 CCBZ) * Chlorobenzene-d5

UPPER LIMIT - + 100*of internal standard areaLOWER LIMIT - - 50*of internal standard area

* Column used to flag internal standard area values with an asterisk,

page 3 of _3-_

FORM UIII v*OA 1/87 Rev

265




Lab File ID (Standard): >D8035 Data Analyzed: 10/17/89

Instrument ID: GC/MS D Time Analyzed: 1353

Matrix:(soil/water) WATER Level:(low/med) LOW Column:(pack/cap) _____

01020304050607060910111213141516171819202122

I

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

QC70083VCA2141VCA2142VCA2143VCA2149VCA2151VCA1891VCA2145VCA2152VCA2153V

——————————————————————

•

. ———— . ——————

ISl(BCM)AREA *

39166

78332

19583

41410421103719237641382233366537042414403397638085

RT

12.59

12.5812.5812.5812.6212.6212.6112.6412.6112.6912.68

—————

IS2(DFB)AREA I

142356

284712

71178

148994152698133875133042140077120299131855137967120773123053

————————

RT

23.24

23.2323.1923.2223.2323.2723.2223.2523.2623.3023.29

IS3(CBZ)AREA I

114710

229420

57355

1145561212331074091083611119649801010726110690097900100167

RT

28.21

28.4028.1528.2328.3128.3128.2628.2928.3028.3128.33

—————————— i

151 (BCM) * Bromochloroaethane152 (DFB) - 1,4-Difluorobenzene153 (CBZ) - Chlorobenzene-d5

UPPER LIMIT - + 100%of internal standard area,LOWER LIMIT - - 50%of internal standard area.

I Column used to flag internal standard area values with an asterisk,

page _(_ of _j_

FORM VIII VOA 266 1/87 Rev



Lab Coda: Casa No.: SAS No.: SDG No.:

Lab File ID (Standard): >I8245 Data Analyzed: 10/18/89

Instrument ID: GC/MS I Time Analyzed: 2242

Matrix:(soil/water) WATER Level:(low/med) LOW Column;(pack/cap)

01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

QC70085VQC70085VCA2150VCA2147VCA2144V

"U—————— 23

—————————

ISl(BCM)AREA I

33721

67442

16861

3248129675313123113030945

————————————————————————————————————————————————————————————————————————

£*•Rf..-v -K" * ———

— . —— _ ——— -

RT

10.84

10.8410.8910.8610.9310.89

_____

IS2(DFB)AREA 1

217291

434582

108645

211363203617205895195838204243

____- ___

RT

21.47

21.5021.5121.5121.5521.51

IS3(CBZ)AREA i

201421

402842

100711

186150176154181340172652180528

iRT

26.30

e

26.3626.4026.3726.4026.37

151 (BCM) - Bromochloromethane152 (D;'B) - l,4-Difluorobenzene153 (CBZ) * Chlorobenzene-d5

UPPER LIMIT - + 100%of internal standard area,LOWER LIMIT - - 50%of internal standard araa.

f Column used to flag internal standard area values with an asterisk.

page _l_ of _(_PORM VIII VOA 267 1/87 Rav,

SBSEMIVOLATILE INTERNAL STANDARD AREA SUMMARY



Lab File ID (Standard): >G8652 Data Analyzed: 10/13/89

Instrument ID: GC/MS G Time Analyzed: 1330

01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

QC70082CCA1859CSCA1859CRCA1893CCA1894CCA1859C

,

—— . ——————

ISl(DCB)AREA *

108807

217614

54404

92112119444121403103066106214122794

—————————

RT

9.44

9.429.449.469.439.529.41

IS2(NPT)AREA I

163203

326406

81601

146946188998174011182269188053186731

____ , ———

RT

13.14

......

13.1213.1213.1413.1313.2313.11

IS3(ANT)AREA *

82089

164178

41045

767749041384764975779289894726

—— ——————

iRT

18.48

18.4718.5018.4918.4918.6018.48

————— ,————— 1

——— !

——— I——— 1

151 (DCB) - l,4-Dichlorobenzene-d4152 (NPT) - Naphthalene-d8153 (ANT) - Acenaphthene-dlO

UPPER LIMIT » + 100%of Internal standard area.LOWER LIMIT « - 50%of internal standard area.


page

FORM VIII SV -1 268 1/87 Rev,

8CSEMIVOLATILE INTERNAL STANDARD AREA SUMMARY





01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.


,

——————————

IS4(PHN)AREA i

110139

220278

55070

112916124556122928139214135671136155

—————————

RT

22.84

22.8322.8522.8522.8422.9622.82

—————

IS5(CRY)AREA 1

51762

103524

25881

561487899778887781937255089698

_ _______

RT

30.68

30.6730.6730.6830.6830.7930.67

—————

IS6(FRY)AREA i

28634

57268

14317

321055694553954486884286271167*

—————————

—————————

_________

RT

34.59

——. 1

34.5734.5934.5934.5834.7034.57

—————

————— i

154 (PHN)155 (CRY)156 (PRY)

Phenanthrene-dl0NaphthaIene-d8Perylene-dl2

UPPER LIMIT - + 100%of internal standard areaLOWER LIMIT - - 50*of internal standard area

i Column used to flag internal standard area values with an asterisk,

page _/_ of _[_

FORM VIII SV -2269

1/87 Rev,

SBSEMIVOLATILE INTERNAL STANDARD AREA SUMMARY

Lab Name: ETCNJ . Contract:Lab Code: Case No.: SAS No.: SDG No.:



01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

QC70084CCA1858CCA1858CSCA1858CRCA1372CCA1373CCA1374C

-_ ——————————

ISl(DCB)AREA I

195845

391690

97922

116519110303175981158739113749109175146394

—————————

—————————

RT

9.42

9.419.449.449.469.489.469.44

—————

—————

IS2(NPT)AREA I

300632

601264

150316

213884181150271426188464205298192800256659

_ ______

RT

13.15

13.1113.1113.1413.1413.1613.1413.13

—————

—————

153 (ANT)AREA I

141907

283814

70953

1263869184411705597003109353110130112783

RT

18.50

18.4718.4818.4918.5018.5118.5018.50

111111 —— •

151 (DCB) - l,4-Dichlorobenzene-d4152 (NPT) - Naphthalene-d8153 (ANT) • Acenaphthene-dlO

UPPER LIMIT - + 100%of internal standard areaLOWER LIMIT - - 50%of internal standard area


page / of _FORM VIII SV -1 1/87 Rev

270

scSEMIVOLATILE INTERNAL STANDARD AREA SUMMARY

Lab Name: ETCNJ . • Contract:



Instrument ID: GC/MS G Tine Analyzed: 0928

01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

QC70084CCA1858CCA1858CSCA1858CRCA1372CCA1373CCA1374C

•

— ————————

IS4(PHN)AREA I

196834

393668

98417

192962138884177124137970176466172580181549

—————————

RT

22.86

22.8422.8322.8622.8522.8622.8522.85

— ———

ISS(CRY)AREA *

100295

200590

50148

1108449854512399794972125394111421126809

————————

RT

30.70

30.6730.6730.6830.7030.7030.7030.68

——————————

———————————————— . ——

IS6(PRY)AREA 1

73151

146302

36575

79609721518339361214894338041179158

————————

————————

..

RT

34.59

34.5734.5734.6034.6034.6134.6034.58

154 (PHN)155 (CRY)156 (PRY)

- Phenanthrane-dlO- Naphthalene-dS- Perylene-dl2

UPPER LIMIT - -»• 100%of Internal standard area,LOWER LIMIT - - 50%of internal standard area

I Column used to flag internal standard area values with an asterisk

pageFORM VIII SV -2 1/87 Rev.

271

8CSEMIVOLATILE INTERNAL STANDARD AREA SUMMARY

Lab Name: ETCNJ * Contract:




01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.


..._. ———— ._

IS4(PHN)AREA 0

167014

334028

83507

14055511063111270412474310981393329102388

———————————————————————————

RT

25.69

25.6725.6925.6825.6925.6825.6925.69

——————————

_ ————

ISS(CRY)AREA 1

109315

218630

54658

89027660268103392680616075700864076

RT

33.82

33.7833.8033.8133.8133.7933.7933.80

IS6(PRY)AREA 1

83744

167488

41872

73387560026157881111460224359150934

. ....

RT

37.90

37.8837.8837. $937.8937.9037.9037.90

—————

154 (PHN)155 (CRY)156 (PRY)

Phenanthrene-dl0Naphthalane-daPerylene-dl2

UPPER LIMIT - + 100%of internal standard areaLOWER LIMIT • - 50%of internal standard area


page .J of

FORM VIII SV -2272

1/87 Rev,

8BSEMIVOLATILE INTERNAL STANDARD AREA SUMMARY

Lab Name: ETCNJ *. Contract:




01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.


_ . —————————

ISl(DCB)AREA 1

181980

363960

90990

.

132750146364129870138487128998133011133750

•""——————————————————

—————————

. _ ———— . _ ——

RT

11.87

, ————

11.8511.8511.8511.8711.8611.8611.87

_ . ——

IS2(MPT)AREA 1

309905

619810

154952

230753235923221880253606217273213012226652

—————————

—————————

RT

15.69

15.6715.6715.6915.6915.6815.6815.69

—————

IS3(ANT)AREA |

134778

269556

67389

1073278657087083101639881617531085644

——————————————————

iRT

21.21

... ——

21.1921.21021.2021.2221.1921.1921.22

—————

151 (DCB) * l,4-Dichlorobenzene-d4152 (NPT) - Naphthalene-d8153 (ANT) - Acenaphthene-dlO

UPPER LIMIT - + 100%of internal standard areaLOWER LIMIT « - 50%of internal standard area.


page l, of is

FORM VIII SV -1273

1/87 Rev,

8BSEMIVOLATILE INTERNAL STANDARD AREA SUMMARY

Lab Name: ETCNJ . ' Contract:



Instrument IDs GC/MS G Time Analyzed: 1509

01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.


»-»-JWJAfi.•fflwa

ISKDCB)AREA *

253845

507690

126922

196782215568227596202838199757183596

hr." •&•*RE---

RT

10.69

10.6810.6710.7010.6810.6910.70

IS2CNPT)AREA *

373359

746718

196680

336431307104331172335050333406302683

RT

14.47

14.4614.4514.4814.4614.4714.46

IS3XANT)AREA *

105884

211768

52942

10364575300940411032819938590824

RT

19.92

-

19.9219.9219.9319; 9319.9219.93

151 (DCB)152 (NPT)I S3 (ANT)

OftenIorobenzene-d4

Acenaphthene-dlO

UPPER LIMIT - + 100*of internal standard ar«aLQUIER LIMIT - - 50*of internal standard area

Column used to flag internal standard area values with an asterisk

FORtl UIII SU -1 1/87 Rev

274

, acSEMIVOLATILE INTERNAL STANDARD AREA SUMMARY



Lab File 10 (Standard): >G9011 Data Analyzed: 11/13/89


II1 12 HOUR STD

1 UPPER LIMIT

1 LOWER LIMIT

1 EPA SAMPLE1 NO.

01IQC70081C02ICA1381CS03ICA1381CR04ICA1379C05ICA138QC06ICA1381C07108109110111112113114115116117118119120121122 1 J

IS4CPHN)AREA *

95587

191174

47794

929065948686039879528559672529

!•:••'

RT

24.38

24.3824.3724.3824.3824.3724.38

IS5CCRY)AREA *

41029

82058

20514

311362959035320363143518723862

RT

32.40

32.4032.4132.4132.3932.4232.41

IS6CPRY)AREA *

26689

53378

13344

207252243724947273242556814399

.

RT

36.43

36.4336 . 4436.4536.4336.4436.43

154 (PHN) - »*hanthrene-dlO155 (CRY) • M*>hth«len«-d8156 (PRY) * P«ryl«n«-dl2


# Column used to flag internal standard area values with an asterisk,

page 1 of 1*

FORM UIII SU -2 1/87 Rev

275

SBSEMIUOLATILE INTERNAL STANDARD AREA SUMMARY

Lab Name: ETCNJ . ' Contract:


Lab F i l e ID (Standard): >G9036 Data Analyzed: l

Instrument ID: EC/MS G Time Analyzed: 1703

01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

QC700S7CCA1907CRCA2139C

*

IS1CDCB)AREA *

282541

965082

141270

255355288674254550

RT

10.65

10.7010.6410.62

IS2CNPT)AREA *

535163

1070326

267581

518146514242532142

RT

14.44

14.4914.4214.40

I S3 I ANT)AREA »

189412

373324

94706

175698172977187300

1•RT !

19. SV!

;

i1

19.93119.8** :19.871

i- *-. 1

1;

.1

1

1

1

1

1

1

IS1 CDCB) - l,4-Dichlorobcnzene-d4[S2 (NPT) - Naphth«lena-d8IS3 (ANT) - Acenaphthene-dlO

UPPER LIMIT - * 100Sof internal standard are-LOWER LIMIT - - 50*of internal standard are.

! olumn used to flag internal standard area va lues with an asterisk,

page 7 o f

FORM V I I I SU -1 1/87 Rev

276

8CSEÎOOLATILE INTERNAL STANDARD AREA SUMHARY


Lah Code: Case No.: SAS No.: SDG No.:

Lab File ID (Standard): >G9036 Data Analyzed: H/14/-V1-'

Instrument ID: GC/MS G Time Ana lyzed: 170-3

111 ............1 12 HOUR STD|. ...........1 UPPER LIMIT1 ............I LOWER LIMIT1 ............1 EPA SAMPLE1 NO.

02ICA1907CR03 :CA2139C04105 :061 >07!08109:10111:12113:14115:16117!18119:20 121 !22 1

IS41PHN)AREA *

187149

374298

93575

160667158911167522

RT

24.30

24.3724.2824.30

IS5(CRY)AREA .*

99167

198334

49584

754777767582871

RT

32.32

32.3732.2932.30

IS6LPRY j

32054

1641 U3

41027

50574537456*060

RT

36..K'

36.3836.3!.:36.31

-• » .

IS- CPHN) - Phenanthrene-dlOIS5 (CRY) - Naphthalen»-d8ISr. (PRY) - Perylene-dl2

UPPER LIMIT - * 100Sof internal standard are.LOWER LIMIT - - 50Sof internal standard are

# Column used to flag internal standard area values w i t h an asterisk,

page > of *"

FORM UJI I SU -2 1/87 Rs

277

8BSCMIVOLATILE INTERNAL STANDARD AREA SUMMARY

Contracti

.i SAS No.: SDG No.:

. >ef090 Data Analyzad: 11/19/89

Tima Analyzad: 0922

111 12 HOUR STD

1 UPPER LIMIT

1 LOWER LIMIT

1 EPA SAMPLE1 NO.

01IQC70092C02ICA1889C03ICA1890C04ICA1892C09ICA19Q8C06ICA2141C07ICA2142C08ICA2143C09ICA2149C10ICA2191C11ICA1891C121131141191161171181191 aaaioni *J H911 'J H22 1 _ '.z^^m

IS1COCB)AREA *

296991

913102

128276

240999230417246079239441242717239102249428244996237764240162240419

^ Ev~

RT

10.69

10.6210.6910.8910.7710.6410.7310.6910.6710.6610.7110.63

IS2CNPT)AREA *

471741

943482

239870

471802462180498070499829490791902344497082479863487364473907902004

RT

14.44

14.4014.4114.6914.9714.4014.9314.4114.4314.4914.4914.41

IS3CANT)AREA *

141099

282118

70930

168640170199179642180192163346181473184494169610173464176429179644

1RT 1

19.871

1

1

11

19.87119487120*131

\ 2 Of 02119117 119.97119.87119.90119.91119.93119.881

111111111I1

151 C152 (153 CANT) •

banzana-d4de

•riaphthana-dlO

UPPER LIMIT - * 100*of intarnal standard araa.LOWER LIMIT - - 5OHof intarnal standard araa.

Column uaad to flag intarnal standard araa valuas w i t h an astarisk

FORM U I I I SU -1 1/87 Rav

278

sc.SEniUOLATlLC INTERNAL STANDARD AREA SUMMARY

Lab NMMI ETCH1 Contract!

SAS No.» SOG No.:

Data Analyzed: 11X19/89

Tim* Analyzed: 0922

111 12 HOUR STD

1 UPPER LIMIT

1 LOWER LIMIT

1 EPA SAMPLE1 NO.

01IQC70092C02ICA1889C03ICA1890C04ICA1892C09ICA1908C06ICA2141C07ICA2142C08ICA2143C09ICA2149C10ICA2191C11ICA1B91C121131141191141171iai191

1S4CPHN)AREA *

114814

' 229628

97407

127020138009149919149382120831144621169279143921137686147269144641

2 0 1 n-M^hfc i if f2 1 1 ZZ33 ^ ^ ^ C22 1 D ^ ^ ^ KI

RT

24.28

24.3024.2824.9624.4924.2824.4124.3024.7624,3224.3724.31

IS9CCRY)AREA *

44817

89634

22409

3414996608946096138643046496237912394998999766070494223

RT

32.31

32.2832.2932. *732.4632.3032.4132.3132.3432.3332.3732.32

IS6CPRY)AREA *

30368

60736

19184

1895839187*4298544149423102*-279219984132869391193827439908

RT

36.32

34.31t-36.29t<"£*>' '«f48|r 36f3lViWtt36.3236.3936.3436.3836.32

UPPER LIMITof internalLOWER LIMITof intarnal

- * 100*standard araa- - 90*standard araa

Column ua*d to flag- internal standard araa valuas with an astarisk.

2L. of _1_FORM UIII SU -2 1/87 Raw

279

, *mSEMIVOLATILE INTERNAL STANDARD AREA SUMMARY

Lab Maniai ETCNJ . Contracts_^âaaWSaatajBBtla\illaBBBBBBBBBCfcjAj<efa>-

Lab Coda *&4& & ^ KBL)ta. i SAS No.: SDG No.*B ^ BjT&Lab File rti ^ ^ B$°063 Data Analyzed: 11/19/89

"" HJI BKrInstrument ID Ktl Baf?' Tima Analyzed: 1702

.'••••••••X-T*:

111 12 HOUR STD

1 UPPER LIMIT

1 LOUER LIMIT

1 EPA SAMPLE1 NO.

OHCA2144C02ICA2149C03ICA2146C04ICA2192C09106107toai0911011111211311411911611711BI191501 _ia^211 J« H221 _-1^^^

ISKDCB)AREA *

276949

" 993098

138274

191897243096239961249749

^ ^ ^ ^ ^•I'.r

RT

10.69

10.7010.6610.6910.64

IS2CNPT)AREA *

492671

989742

246339

429069910921492184930396

RT

14.44

14.4614.4414.4314.42

IS3CANT)AREA *

194274

308948

77137

132832169399164409187309*

.RT19.89

19.8819.91

- 19488l'|9'

t _

UPPER LIMIT - * 100Hof internal standard area.LOWER LIMIT - - 50*of internal standard area.

* Column used to flag internal standard araa value* with an asterisk

paga _J_ of *"

FORM UlII SO -1 1x87 Rev,

2GO

Lab Name: CTCNJ

Lab Code

Lab File i

Instrument I

, 8CINTERNAL STANDARD AREA SUMMARY

Contract:

$fe.i SAS No.i SDG No.:

63 Data Analyzed! 11/19/89

Time Analyzed: 1702

11

1 12 HOUR STD

1 UPPER L I M I T

1 LOUER L I M I T

1 EPA SAMPLE1 NO.

01ICA2144C02ICA2149C03ICA2146C04ICA2192C091041071O B I09110111112113114t191

171181191

IS4(PHN)AREA ft

133400

"" 266800

66700

129944121470128347190911

3 1 |—— -— ™««S«iJM^Mg-—

22 1 _ _^BBBBBBBBBBBBBBBB^KZ_

RT

24.33

24.3024.3224.3124.32

IS9CCRY)AREA *

93074

106148

26937

94664461004801369366

RT

32.34

32.3132.3332.5232.32

IS6CPRV)AREA ft

39046

70092

17923

RT

36.32

31172.1 3*. 3229299* KJ#*?329832 £?*f32471ir*V9*»3

* ~L TL.

UPPER LiniT - * 100*of internal standard area.LOUER LIMIT • - 90*of internal standard area.

ft Column used to flag internal standard area values with an asterisk.

page v of _*^

FORM UIII SU ~2 1/87 Rev.

8BSE*I VOLATILE INTERNAL STANDARD AREA SUMMARY

Lab Name: ETCNJ . Contract:* f

Lab Code: Case No.: SAS No.: SOG No.:

Lab File ID (Standard): >G9076 Data Analyzed: 11/16."::'-

In3,t rument ID: GCXMS G Time Analyzed: 1426

11I-. ..........1 12 HOUR STD!.-..........1 UPPER LIMIT1 ............1 LOWER LIMfT1 .............1 EPA SAMPLE1 NO.

01 ICA1907CS02ICA19Q7C03 :CA2140C04105!061 >07!08109:10111!12113:14!15 ;16 t17:18119!20121 122 1

IS1CDCB)AREA *

338478

676956

169239

288384259179252117

RT

10.61

10.6110.5810.57

IS2CNPT)AREA *

730615

1461230

365307

631399609744589730

RT

14.39

14.3814.3714.36

IS31ANT)AREA »

215733

43l-i66

107366

24^119273999244976

.RT

19.3.'

19,8319.3219.81

"• * .

I£i (DCS) - l,4-Dichlorobe-.zene-d4152 CNPT) - Naphthalene-d8153 (ANT) - Acenaphthene-dlO

UPPER LIMIT - * 10UNof internal standard areLOWER LIMIT « - 5U*of internal standard arc.

* Column used to flag internal standard area values with an asterisk.

page I_ of >_

FORM U I I I SV -1 1/87 Re

232

acSEMtUQLATILE INTERNAL STANDARD AREA SUMMARY

Lab Name: ETCNO . Contract:

La& Code: Case No.: SAS No.: SDG No.:

Lab File ID (Standard): >G9076 Data Analyzed:

Instrument ID: GC/MS G Time Ana 1yzed: 1426

01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

CA1907CSCA19Q7CCA2140C

•>

IS4CPHN)AREA *

165383

330766

82692

197290220338181325

RT

24.25

24.2424.2524.23

IS51CRY)AREA t

68593

137136

34296

748448138177968

RT

32.26

32.2332.2432.21

AREA *

47777

95554

23339

494825472056830

1RT :

36.2-'

1

36.24136.25:36.221

1•* - • !

1;1;1

1

1

1;1:I

IS* CPHN) - Phenanthrene-dlO155 (CRY) - Naphthalene-d8

(PRY) - Perylene-dl2

UPPER LIMIT - * 10OSof internal standard are*..LOWER LIMIT - - 50Sof internal standard area.

4 Column used to flag internal standard area values with an asterisk,

page *" of **

FORM UII I SV -2 1/87 Rev

233

SB. SEMIUQLATILE INTERNAL STANDARD AREA SUMMARY


Lab Code: Case No.: SAS No.: . SDG No.:

Lab File ID (Standard): >G9104 Data Analyzed: 11/17.'89


01020304050607OS091011121314151617IS19202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

QC70098CCA2150C

IS1CDCB)

275107

550214

137553

238409242265

RT

10.60

mmmmmm

10.4210.44

IS2CNPT)AREA #

555*49

llll-a

277*24

51579857C/68

RT

14. '.9

14.1814. -Jl

IS3CANT)

2 5"* 2 6

5 153 -2

220471

1RT 1

19.*4I

I

1

11

19.63 119.65 1

1I111111111!I111111!

151 (DCS) - l,4-Dichlorobenzene-d4152 CNPT) - Naphthalene-d8IS? (ANT) - Acenaphthene-dlO

UPPER LIMIT - * 10i]%of internal standard a r- - aLOWER LIMIT - - 50%of internal standard a-'ea

# Column used to flag internal standard area values with an asterisk

page I of JV.

FORH U I I I SU -1 1/87

234

acSEMI VOLATILE INTERNAL STANDARD AREA SUMMARY



Lab File ID (Standard): >G91Q4 Data Analyzed: 11/17"39


01020?040?0607080910111213141516171819202122

1

12 HOUR STO

UPPER LIMIT

LOWER LIMIT

EPA SAMPLEMO.

QC7Q098CCA2150C

IS4CPHN)WREA *

309958

619876

154969

272355314267

,

RT

24.26

24.0424. 07

IS5(CRY)^REA *

114529

229058

57265

125224167360

RT

32.25

32,0332. M4

IS6CPRY)*VEA #71079

142158

35539

84783*-573

1

RT

36.22

36.0336.03

;S4 tPHN) - Phenanthrene-dlOIS5 (CRY) - Naphthalcne-dS;S6 'PRY) » Perylene-dl2

UPPER LIMIT - + l:jSof internal standard area.L.'MER LiniT - - JSof internal standard area.

# Column used to flag internal standard area values with an asterisk.

page ^_ of i_

FORM (Jill SU -2 1/87 Rev

ETC

TABULATED RESULTS

NON CLP PARAMETERS

236

—— ^ sgr c i *• ——————————————————————————————————————————— ~ —— ~ ——

TABLE 1: QUANTITATIVE RESULTS and QUALITY ASSURANCE DATA

Conventional Analysis Data (QR10)

Chain of Custody Data Required for ETC Data Management Summary Reports

CA1379 WASTE MANAGEMENT. INC. 405 U1GUBURR 890928 0834 4ETC Simple No. Company Facility Sample Point D*t« Tim* Hours

NPDESNumber

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenolics, Total mg/1Cyanide. Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/cmSpecific Conductance urn/cmpH stdpH stdNitrite as N mg/1

roOO

Resul ts

Samp laConcert.

21 .0.4

< 1<.050.00135 .05 . 1

820830

7 . 0 37 .04

MOL

1 .0. 1. 1

.050.0100

1 01 0

1 0 . 01 0 . 0

. 1

NOV 10. 1989

-

-

TABLE 1: MISCELLANEOUS DATA (QR64)


CA1379 WASTE MANAGEMENT. INC. 405 W1GWBURR 890928 0834 4

ETC Simple No. Company Facility Sample Point P*ie Tim* Hours

Compound

Ammonia as NSulfate as S04Bicarbonate as CaC03Carbonate as CaC03Nitrogen. Total Kjeldahl (TSolids, total dissolved (RO

toOJoo

Resul ts

SampleConcert.

mg/1

.15< 5 . 0

428<5.0

.64663

MDLmg/1

.045 0

10.05 .0

.205

OCT 25, 1989

-

^ C 1 I —————————————————————————————————————————————————————————————————— " —————————


Field Parameters (QR16)


CA1379 WASTE MANAGEMENT. INC. 405 W1GWB14RR 690928 0634 4EJtpttd

ETC Sample No. Company F4cility Svnpla Point 0*tt Time Hours

Parameter

pH Field) stdpH i Field stdpH i Field stdPH i Field stdSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. (

CO

Resu l t s

SampleMeasure

7.497.507.507 54

766768767771

10.1

MOL

.

OCT 3. 1989

.

•

———— •liPr C ll" ——————————————————————————————————————————————————————————————————————————————————————————————


Conventional Analysis Data (QR10)Chain of Custody Data Required for ETC Data Management Summary Reports

CA1380 WASTE MANAGEMENT. INC. 405 W1GWB16RR 890928 1321 1ETC Simple No. Compjoy Facility Sample Point Date Time Hour*

NPDESNumber

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenolics, Total mg/1Cyanide. Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/cmSpecific Conductance urn/ cmpM stdpH stdNitrite as N mg/1

roo

Resu l t s

SampleConcert .

30.22

( . 1<.050

.0008926.727.2

830840

7.047.06

MDL

1.0.1.1

.050.0100

1 01.0

10.010 0

.1

•

NOV 10, 1989

•

ETCOCT 25. 1989



CA1380 WASTE MANAGEMENT. INC. 405 W1GWB16RR 890928 1321 1ETC Sample No. Company Facility Sample Point 0«t« Time Hour*

Compound


Resu l t s

SampleConcen .

mg/1

< 045.14

518<5.0

< . 2 0572

MDLmg/l

.045 .0

10.05 0

.20

C 1 4, ———————————— " —————————————————————————— " ————————————————————————————————————



Chain of Custody Data Requked for ETC Data Management Summary Reports

CAI380 WASTE MANAGEMENT, INC. 405 W1GWBI6RR 890928 1321 1CJtpMtf

ETC S*mp)« No. Company , Facility Sample Point Date Tin* Hours

Pa rame t e r

pH i Field stdpH 'Field stdpH 'Field stdpH i Field stdSpecific Conductance Field un/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/ cmSpecif ic Conductance Field urn/cmTemperature Deg. C

rovo

Retul tc

SampleMeaiure

7.947.006 997 00

915899905899

11.9

MDL

OCT 3, 1989

——— ^^^- c i *• ————————————————————————— ————————————————————————^L=^




CA1381 WASTE MANAGEMENT. INC. 405 XDUP 890928 1321 0Elap&«d

ETC Sample Mo. Company Facility Sample Poini Oai« Time Hour*

NPDESNumber

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenolics. Total mg/1Cyanide. Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/cmSpecific Conductance urn/cmpH stdpH stdNitrite as N mg/1

ho

CM

Result c

SampleConcen.

31 0.2

< 1<.050

001121.822.2

910910

7.037.03

MDL

1 .0. 1.1

.050.01001.01 .0

10 .010.0

.1

NOV 10. 1989

.

•

—— ^Hv t ii- ——



CA1381 WASTE MANAGEMENT. INC. 405 XDUP 890928 1321 0ETC S«npl« No. Company Facility Sample Point Dm Tiow Hours

Compound

Ammonia as NSulfate as S04Bicarbonate as CaC03Carbonate as CaC03Nitrogen, Total Kjeldahl (TSolids, total dissolved (RO

ro

Resul ts

SampleConcert.

mg/1

< 046.44

505<5.0

.34558

MDLmg/1

.045.0

10.05.0

.20

OCT 25, 1989

———— i ^ C 1C ———————————————————————————— ——— ——————— •• —————————————— ——— ————————————— - —— •-


Field Parameters (QR16)Chain of Custody Data Required for ETC Data Management Summary Reports

CA1381 WASTE MANAGEMENT. INC, 405 XDUP 890928 1321 0E *p»«tf

ETC S«npl« No. Company F*cility Smpl« Point 0*t« Tim* Hours

Parameter

pH i Field stdpH i Field stdpH i Field stdpH Field stdSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. C

NO

cn

Resu l t s

SampleMeasure

7.947.006.997.00

915899905899

11.9

MDL

-

»•

OCT 3, 1989

—— •1 " c ' u —————————— —————————— ———— .-— — - ———————————————————



CA1893 WASTE MANAGEMENT. INC. 405 W1GWP3A 891002 0947 5ETC Swnpla No. Company Facility S«npl« Point D*(« Timt Hours

NPDESNumber


roON

Resul ts

SampleConcen .

2.6.2

<.050.00065

4.14.2

550560

7.487.48

MDL

1.011

.050.01001.01.0

10 010.0

.1

NOV 10, 1989

•

•

-_

i

———— ^ HP - C 1 *. —— ' — '•T-LJ



CA1893 WASTE MANAGEMENT, INC. 405 W1GWP3A 891002 0947 SFTC SMP!« No, rrnnn*")1 Facility Samplt Point fiat* Iln»» itour»

Compound

Ammonia as NSulfate as S04Bicarbonate as CaC03Carbonate as CaC03Nitrogen, Total KJeldahl (TSolids, total dissolved (RO

ro

Result*

SampleConcen,

mg/l

<.0429.9

3020<.20

323

MDLmg/l

.045 0

10.0

.2010

DEC 4, 1989

——— «lgpr n , b ———————————————————————— ., —— ... , ——————————————————————————————— __™ —— OCT 5. 1989




CAT893 WASTE MANAGEMENT. INC. 405 W1GWP3A 891002 0947 5ei»(u4d

ETC S«mpl« No. Company Ftcillty Sample Point D*t* TIM Hour*

Parameter

pH i Field stdpH I Field stdpH Field stdpH 'Field stdSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmGroundwater Elevation Feet

CO

Remits

SampleMeasure

7.477.467.477.49

543543549550

10.5

MDL

-

.

-

— ^PH " c ——————————————————————————————TABLE 1: QUANTITATIVE RESULTS and QUALITY ASSURANCE DATA



CA1894 WASTE MANAGEMENT, INC. 405 W1GWP3B 891002 1603 2E J*p»d

ETC Samp In No. Company FtcUity Svnpl* Point Date Tirot Kauri

NPDESNumber

Chloride mg/1Fluoride mg/1Nitrate as N mg/1PhenoUcs. Total mg/1Cyanide. Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specif ic Conductance urn/cmSpecific Conductance urn/cmpH stdpH stdNitrite as N mg/1

ro\Q

VO

Results

SampleConceit.

7.6.1.4

< .050.00069

2 .83.0

550550

7.667 66

MDL

1.0. 1.1050

.01001 .01 .0

10.010.0

1 .0

NOV 13. 1989

-

HP^ tlL



CA1894 WASTE MANAGEMENT. INC. 405 W1GUP3B 891002 1603 2ETC Smplt Mo. Compjny Facility Sample Point Date Time Hours

Compound


O

R e s u l t s

SampleConcen .

mg/i< 04

28.8296

0< . 2 0

324

MDLmg/1

.045.0

10 .0

.2010

OCT 31 . 1989

———— f fclF C 11, ———————————————————————— "'" ————— '" —— ' '" "" ——————————————— " ————————




CA1894 WASTE MANAGEMENT. INC. 405 W1GWP3B 8910021603 2ETC Simple No. Company Facility Sample Point Date Tim Hours

Parameter

pH i Field stdpH i Field stdpH i Field stdpH i Field, stdSpecif ic Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. C

C.)

Resul ts

SampleMeasure

7.487.527.517 51

555549548548

10.3

MDL

-

OCT 5. 1989

•

-

— ^• fe" c • *• ————————————————————————————— —————— —————— —————^^^p^



Chain of Custody Data Required for ETC Data Management Summary Report*

CAI895 WASTE MANAGEMENT. INC. 405 W1GWP4A 891003 0909 3ETC S«nol« No. Company Facil i ty Sample Point Date Tim* Hours

NPDESNumber

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenolics. Total mg/1Cyanide, Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/cmSpecific Conductance urn/cmpH stdpH stdNitrite as N mg/1

CK'OrO

Rtiultl

SampleConcen .

3.6.1.7

<.050.00013

7 07.6

520530

7.557.56< 1

MDL

1.0.1.1

.050.01001 01 0

10.010.0

.1

NOV 22. 1989

-



CAI895 WASTE MANAGEMENT. INC. 405 W1GWP4A 89I003 0909 3Etc Sample No. Company Facility Swnple Point Oat« Time Hour*

Compound

Ammonia as NSulfate as S04Bicarbonate as C&C03Carbonate as CaCQ3Nitrogen. Total Kjeldahl (TSolids, total dissolved (RO

O

Resu l t s

Samp 1 eConcen .

mg/1

< . 0 423.0

2790< . 2 0

308

MDLmg/1

.045.0

10.0

.2010

-

OCT 31 , 1989

——— fer tIL —————————————————————————————————————————————————————————————————————•'•' OCT 10. 1989




CA189S WASTE MANAGEMENT. INC. 405 W1GWP4A 891003 0909 3

ETC S«npl4 Mo. Company Facility 3*mpl« Point D«ie Time Hour*

Parameter

pH (Field stdpH i Field stdpH i Field stdpH (Field stdSpecific Conductance i Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. (

Ot

Result!

SampleMeasure

7.487.507.497.49

502504502499

9.7

MDL

•

.

——— " ^B^Btf C 1 1 ———————————————————————————————————— " ——————— —— ———— ™ — " ———————————————————————————




CA1896 WASTE MANAGEMENT. INC. 405 W1GWP4C 891003 1412 1EJ*pt«a

ETC S*np)t No, Compiny Facility S*mp]« Point Dm Tim* Hour*

NPDESNumber

Chloride mg/lFluoride mg/lNitrate as N mg/lPhenolic* . Total mg/lCyanide. Total mg/lTotal Organic Carbon mg/lTotal Organic Carbon mg/lSpecific Conductance urn/cmSpecific Conductance urn/cmpH stdpH stdNitrite as N mg/l

0!CDen

Reiultt

Samp 1 eConcen.

30.7

<.050.0006723.223.3

11001100

6.916 99

MDL

1 .0.1.1

.050.0100t . o1.0

10.010.0

.1

NOV 28. 1989

•

———— ^B^T~ C 1 1* ————



CA1896 WASTE MANAGEMENT. INC. 405 W1GWP4C 891003 1412 1Elapsed

ETC Sample No. Company Facility Sample Point Date Time Hours

Compound


Os'O

R«tulti

Sampl*Concert ,

mg/l

< .0415 .0

6350

.39692

MDLmg/l

.045 .0

1 0 . 0

.2010

OCT 31 . 1989

ir 1 c i L ——————————————————————————— •" —————————————————————SK=±


Field Parameters (OR 16)


CAI896 WASTE MANAGEMENT, INC. 405 W1GWP4C 891003 1412 1Elapsed

ETC Sample No. Company Facility Sample Poinl D*te Time Hours

Parameter

pH Field stdpH Field stdpH Field stdpH Field stdSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance 'Field urn/cmSpecific Conductance 'Field urn/cmTemperature Deg. C

O

Resul t s

SampleHeaiure

7.057.067.057.07

111410791098nos

10.5

MDL

OCT 10. 1989

—— ^_^ c , —————————————————————————————————————————————————• B^g^




CA1897 WASTE MANAGEMENT, INC. 405 WIGWP4B 891003 1518 2Elipted

ETC Simple No. Company Facility S*nple Point Dit« Tim* Hour*

NPDESNumber

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenolic*. Total mg/1Cyanide. Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/cmSpecific Conductance urn/cmpH stdpH stdNitrite as N mg/1

Ox1

C.)oo

Ratult t

SampleConctn.

25.2.2

< . 1< .050

.000684.34.5

530540

7.447.52< . l

MDL

1 .0.1.1

.050.01001.01.0

10.010.0

.1

NOV 22. 1989

•

—— ^^^ c ' c ——



CA1897 WASTE MANAGEMENT. INC. 405 W1GUP4B 89I003 1518 2ETC Swnplt No, Company facility Sample Point Cite Timt Hours

Compound


Ovo

Rtiult s

Sampl*Conc*n.

mg/1

< 04<5.0

2480< . 2 0

316

MDLmg/l

.045.0

10.0

.2010

OCT 31. 1989

•

" PSê 11 —————————————————————————————————————————————————


Field Parameters (OR 16)Chain of Custody Data Required for ETC Data Management Summary Reports

CA1897 WASTE MANAGEMENT. INC. 405 W1GWP4B 891003 15)8 2ETC Sample No. Company Facility Sample Point Dm Time Huuri

Parameter

pH Field stdpH Field stdpH Field' stdpH Field stdSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/ cmSpecific Conductance Field urn/cmTemperature Oeg. (

ON!

O

Result s

SampleMeaiur'e

7.527.537.567.55

508508509507

9.5

MDL

-

OCT 10, 1989

.

*

—— KB^ e i i* ——————————————————————————— ———————————————————•sr



CA2136 WASTE MANAGEMENT. INC. 405 W1GWB6RR 891004 0833 SETC Sample No. Company Faciliry Sample Point Dat« TliN Hour*

NPDESNumbtr


Resu l t s

SampleConcen.

4 .1.2.4

< 050.0003511. 511. S

790790

7.207.20

MDL

1 .0.1.1

.050.01001 01.0

10.010 0--

.1

NOV 22, 1989

.

\J

—— ^Hto- c ll» ———^Htw^



CA2136 WASTE MANAGEMENT, INC. 405 W1QUB6RR 891004 0833 5El*p**d

ETC SMipli No. Conpiny Facility 3*np)« Point 0*t« Tint Hour*

Compound


Os'

Result!

SampleConcen.

mo/1<.04

15.0510

0.21

527

MDLfflfl/1

.045 0

10.0

.2010

NOV 27, 19B9

•

•

——— Bv" CIU —————————————————————————————————————————————————————— ——————^^^^=^ OCT 10 1989



Cfiam of Custody Data Required for ETC Data Management Summary Reports

CA2136 WASTE MANAGEMENT. INC. 405 W1QWB6RR 891004 0833 5ETC S«npl< No, Company Facility Sample Point Date TlM Hours

Par-Mtttvr

pH FieldpH FieldpH 'FieldpH i FieldSpecific ConductanSpecific ConductanSpecific ConductanSpecific ConductanTemperature

CM

stdstdstdstd

ce Field urn/cmce Field urn/cmce Field urn/cmce Field urn/cm

Oeg. (

Rtiulti

SampleMeasure

7.017.017.027.05

845836832827

10.0

MDL

-

.

.

——— ^LVe^F c '*• ————————————————————————————————————————————————————————————————— " ——^ |F




CA2U7 WASTE MANAGEMENT. INC. 405 W1GWP2B 891004 1325 3ETC S*npl< No, Company Facility Scnple Poinl D*t» Time Hours

NPDESNumber

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenolics, Total mg/1Cyanide, Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/cmSpecific Conductance urn/cmpH stdpH stdNitrite as N mg/1

-Pa.

Result!

SampleConcen.

2.6.2

< 050.00040

9.910 0

530540

7.457.48

MDL

1.0

.050.01001.01.0

10.010.0

.1

NOV 27. 1989

-

-_

• l p^



CA2137 WASTE MANAGEMENT. INC. 405 W1GWP2B 891004 1325 3ETC 5«npl« No. Company F»cility S*npl« Point D*te Tim* Hours

Compound


Results

SampleConcen.

mfl/1

< 0416.4

2780

.21404

MOLmg/1

.045 0

10.0-

.2010

NOV 27. 1989

^^^ OCT 10. 1989TABLE 1: QUANTITATIVE RESULTS and QUALITY ASSURANCE DATA



CA2137 WASTE MANAGEMENT. INC. 405 WIGWP2B 89)004 1325 3ETC SMipl* Mo, Company Fidlity Svnple Point D«te Time Hours

Pcmnwtvr

pH (Field stdpH ' Field stdpH i Field stdpH i Field! stdSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. C

O-J

O\

Resul ts

SampleMeasure

7.517.507 507.52

522516516515

10 5

MDL

-

.

——— ^MfV~ C 1 I ——— ——— ————— _^____ ————— ________ — _ ——— __ ———— ____^_______. ——• H^


Conventional Analysis Data (OR 10)Chain of Cuttody Data Required for ETC Data Management Summary Reports

CA2138 WASTE MANAGEMENT. INC. 405 W1GWP2C 891004 1440 0Eliptttt

ETC S«npl« No. Company F*ciliiy S*npl« Point 0*t« Tim Hours

NPDESNumber

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenolics. Total mg/1Cyanide, total mg/1Total Organic Carbon mg/1Total Organic Carbon ' mg/1Specific Conductance urn/cmSpecific Conductance urn/cmpH stdpH stdNitrite as N mg/1

ON!

Result!

SampleConceit.

9.3

!3( 0 5 0

.0003110.210.3

880880

6.776.79< 1

MDL

1.0.1

.050.01001.01.0

10.010.0

.1

NOV 27. 1989

-

•_



CA2138 WASTE MANAGEMENT. INC. 405 W1GWP2C 891004 1440 0Eiap»<t

ETC S«npl« Mo. Cmnpaoy Facility Swnpl* Point D«U Tim* rtour*

Compound


OO

Rtiulti

SampleConcert.

mg/1

< 0430.9

5030<.20

521

MDLmg/1

.045.0

10.0

.2010

NOV 27. 1989

——— pSr c ' L ———————————————————————————————— ————————————————


Field Parameters (OR 16)Chain of Custody Data Required for ETC Data Management Summary Reports

CA2138 WASTE MANAGEMENT. INC. 405 W1GWP2C 891004 1440 0Elapt«<f

ETC S«npl« Mo. Company F»cility Sample Poini Dat« Time Hours

Parameter

pH i Field > stdpH i Field stdpH i Field stdpH i Field stdSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. C

VD

Reiult S

SampleMeasure

7.057.037.037.03

774784780780

10.5

MDL

-

OCT 10. 1989

,

;

——— ^————^ C 1C ——————————————————————— • —————————————————————————————————————————————————————


Conventional Analysis Data (OR 10)Chain of Custody Data Required for ETC Data Management Summary Report*

CA2139 WASTE MANAGEMENT. INC, 405 WIGWPIB 891005 0800 8ETC Smplf M»- Compiny F»cility S«npl< Point Dm It** Hours

NPDESNumber

Chloride mo/1Fluoride mg/1Nitrate as N mg/1Phenolics, Total mg/1Cyanide, Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/cmSpecific Conductance urn/cmpH stdpH stdNitrite as N mg/1

CK'roO

Rtiultl

SampleConcin.

4 . 7

< 050.002018.319.1

15001510

6.516.52

MDL

1.0.1.1

.050.01001.01 0

10.010.0

.1

NOV 27. 1989

•

•

— — •B^r c ' u ~"~~^^^^="TABLE 1: MISCELLANEOUS DATA (QR64)


CA2139 WASTE MANAGEMENT. INC. 405 WIGWPIB 891005 0800 8ETC Stmplt No. Comp*f>y Ftcility SmpJt Point 0«t« Time Hauri

Compound

Ammonia at NSulfate as S04Bicarbonate as CaC03Carbonate at CaC03Nitrogen. Total KJeldahl (TSolids, total dissolved (RO

R*tultc

Sampl*Concen.

<.0426.6

9930

.S31000

MDL

.045.0

10.0-

.2010

NOV 27, 1989




CA2139 WASTE MANAGEMENT. INC. 405 W I GUP IB 891005 0800 8ETC SMiplt No, Company Facility S*npl» Point 0»t» Tlnw Hour*

Parameter

pH < Field' stdpH Field stdpH < Field, stdpH i Field stdSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. C

Ov!K>ro

Results

SampleMeasure

6.766.746.766.78

1535152214961484

10.5

MDL

-

OCT 10, 1989

*

-_

^^^ DEC 19. 1989TABLE 1: QUANTITATIVE RESULTS and QUALITY ASSURANCE DATA

Conventional Analysis Data (QR1O)

Chain of CuHody Data Required for CTC Data Management Summary Report* !

CA2140 WASTE MANAGEMENT. ?NC. 405 W1GWP1C 891005 1410 1ETC SMpI« Ho, ;:.; Compwy : ' F»cility Swipl* Paint D»U Tta* rtourt

NPDES . .^ ::':';:' ; - " • . . v . . ; - ^ v ^ "Number . ^^••;;- .. -;-;- . - - . . : • -.'••• -

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenolics, Total mg/1Cyanide. Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/cmSpecific Conductance urn/cmpH stdpH stdNitrite as N mg/1

CN'

Osl

Return

SampU

2.4.1.6

<.050.003115.817.2

13701370

6.416.42

MDL

1.0.1.1

.050.01001.01.0

10.010.0

.1

-

-

——— ^ EJF C El* ———


Chain of Cuttody Data Required for ETC Data Management Summary Report*

CA2I40 WASTE MMW3EMENT; INC, 405 W1QWP1C 891005 1410 1ETC SMpJ« Ho. CoDpiny Ficility Sampl* Point Oat* Hum ttours


NJ

ftetuitt

SampleConein,•a/i

<.048.52

10400

.32868

MDLma/1

.045.0

10.0

.2010

DEC 19, 1989

-

•_

»r C IL ————————————————————————————————————————————————————————————————————————————




CA2140 WASTE MANAGEMENT, INC. 405 W1GUP1C 891005 1410 1ETC S«npl< No. Company Facility S*np)« Point D*t« time Hour*

P™.,.,

pH i Field stdpH i Field stdpH i Field stdpH 'Field stdSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. C

i "»

fUiultt

SampleMeasure

6.456.466.476. SO

1321131613181318

10.9

MDL

-

*

OCT 10. 1989

-_




CA2M1 WASTE MANAGEMENT, INC. 405 W1GWP3C 891009 0856 9ETC SMP!« No. Co*p«iy Facility 3»npl* Point 0*l« Tint Huur*

NPDESNumber


lUtultt

Smpl*Conctn.

12.7.5

6 9<.050

.000695.86.1

817.0818.0

7 567.57

MDl

1 .0.1

1.050

.01001.01.0

10.010.0--

.1

NOV 27, 1989

^^^F



CA2U1 WASTE MANAGEMENT. INC. 405 W1GWP3C 891009 0856 9EJtp*«<t

ETC SMipli No. Compiny Ficility S*npU Point D*t» Tim* Hours

Compound


Retultt t

SampleConceit.

mg/i< ,04

12.2437

0.25

455

MDLmg/1

.045.0

10.0-

.2010

NOV 27. 1989

—— ^^p^ c ' u —————————————————————————————————————————————TABLE 1: QUANTITATIVE RESULTS and QUALITY ASSURANCE DATA

Field Parameters (QR16)Chain of Custody Data Required for ETC Data Management Summary Reports

CA2141 WASTE MANAGEMENT, INC. 405 W1GWP3C 891009 0856 9ETC S«npl< No, Company Facility Sample Point D«te Time Hours

Parameter

pH Field, stdpH i Field stdpH Field stdpH < Field stdSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/ cmSpecific Conductance Field urn/cmTemperature Deg, C

Os!NJCO

Result!

SampleMeasur*

7.437.447.457.45

856860858863

12.5

MDL

OCT 16. 1989

1 —— ^^^" c ' *" "" ————————————————————————————————————— " — " ———————————




CA2U2 WASTE MANAGEMENT, INC. 405 W1GWP6A 891009 0913 3EHp*«d

ETC SMH>)« Ho- Company F*cility S*mpl« Point D«t« TltM Hour*

NPDESNumbtr

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenolici, Total mg/1Cyanide. Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/cmSpecific Conductance urn/cmpH stdpH stdNitrite as N mg/1

Os!

VO

Remit*

Sampl*Concen .

9 .7.2

18.5<.050.00095.05.3

671.0671 .0

7 .177.19

MDL

1.0.1.1

.050.01001 .01.0

10.010.0

.1

NOV 27. 1989

•

—— •Ito^ 1 11* ——^ • • • ^^^



CA2142 WASTE MANAGEMENT. INC. 405 WIGWP6A 891009 0913 3EJ»pMO

ETC Sample No. Company Ftciliiy Sample Point 0*(* Tint Maun

Compound

Ammonia as NSulfaU as SQ4Bicarbonate as CaC03Carbonate as CaC03Nitrogen. Total Kjeldahl (TSolids, total dissolved (RO

OJCD

Remits

S«mpl*Cancan.

13.1303

0<.20

433

MDLmg/1

.045 0

10.0

.2010

NOV 27. 1989

•

^ C 1 !• —OCT 16, 1989




CA2142 WASTE MANAGEMENT, INC. 405 W1GWP6A 891009 0913 3El*f>*«4

ETC Sample No. Company Ftcility Sample Point Date Time Hours

— -pH I Field)PH 'FieldpH i FieldPH FieldSpecific ConductanSpecific ConductanSpecific ConductanSpecific ConductanTemperature

OJ

stdstdstdstd

ce i Field urn/cmce Field urn/cmce Field urn/cmce Field urn/cm

Deg C

Results

Samp 1 tMeasure

7 227 227.247.25

694694694693

11 .9

MOL

-

•

f

,

—— ^8^8=" c ' *• " —————————————————————— ^ ——————————————————————————^HHB^ r



Chita of Custody Data Required for ETC Data Management Summary Reports

CA2143 WASTE MANAGEMENT. INC. 405 WIGWP7A 891009 1442 2Cliptttf

ETC S«np]< No. Cwnpcny Facility 3«npl< Point Ditt Tint Hours

NPDESNumbe r

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenolics, Total mg/1Cyanide, total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/cmSpecific Conductance urn/cmpH stdpH stdNitrite as N mg/1

CK'OsJNO

Results

SampleConcen.

9.5.3

< . l<.050.00155 95.9

686.0687.0

7.507.51O

MDL

1 .0.1.1

.050.01001.01 .0

10.010.0

.1

NOV 27, 1989

*

.

^^^^^F


Chain of Custody Data Required for ETC Data Management Sunwnary Reports

CA2143 WASTE MANAGEMENT. INC. 405 W1GWP7A 891009 1442 2El«pt*Ct

ETC Swuplt No. Cwnpiny F*ctlity S*npl» Point D*t» Tim* H«uri

Compound

Ammonia as NSulfate as SQ4Bicarbonate as CaC03Carbonate as CaC03Nitrogen, Total Kjeldahl (TSolids, total dissolved (RO

OJ04

Resul t t

SampleConcen ,

me/1< .04

50,9325

0.23

500

MDLmg/1

.045.0

10.0

2010

NOV 21 . 1989

*

• p^ "




CA2143 WASTE MANAGEMENT, INC. 405 W1GWP7A 891009 1442 2

ETC S«nplf No. Comp«ny . F»cility S«mpl« Point D*t« TliM Hour*

Parameter

pH (Field stdpH Field stdpH Field stdpH Field stdSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. C

Resul ts

SampleMeasure

7.427.447.447.44

670670670670

11.2

MDL

--------

OCT 16. 1989

•

•

—— ' ^^^" c ' u ————————"" — —— —————————— ___ ———— __ ————— _ —————— _ ———




CA2I49 WASTE MANAGEMENT. INC. 405 XDUP 891009 0913 3

ETC Sampl* No. Company Facility S*npl* Point Dat« Tim* Hour*

NPDESNumber

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenolics, Total mg/1Cyanide, Total mg/1Total Organic Carbon mg/1 .Total Organic Carbon mg/1Specific Conductance urn/cmSpecific Conductance urn/cmpH stdpH stdNitrite as N mg/1

CD

Resul ts

SampleConcert .

.216.8<.050

< 01006.36.5

691 .0693.0

7.177.20

MDL

1.0.1.1.050

.01001 01.0

10.010.0

.1

DEC 20. 1989

-

-

———— âinj r C 1 1* ————



CA2M9 WASTE MANAGEMENT. INC. 405 XDUP 8910090913 3ETC Simple No. Company Facility 3«npl« Point Dm Time Hour*

Compound


Os'OJON

Resul ts

SampleConcert.

mfl/1

< 0413.2

3150<.20

434

MDLmg/1

.045.0

10.0

.2010

NOV 3. 1989

•

—— ^Mr c ' L —————————————————————— ———— —————————————————0BE=E=




CA2149 WASTE MANAGEMENT. INC. 405 XDUP 891009 0913 3ETC S«npl« No. Company Facility Simple Point Date Time Hour)

Parameter

pH i Field' stdpH 'Field stdpH 'Field' stdpH IField stdSpecific Conductance Field um/c(nSpecific Conductance Field urn/ cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. C

C/J

Resu l t s

SampleMeasure

7.227.227.247.25

694694694693

1 t . 9

MDL

-

OCT 20, 1989

•

•_

—— •»r c IU —————————————————————————————————————————————————TABLE 1: QUANTITATIVE RESULTS and QUALITY ASSURANCE DATA

Conventional Analysis Data (QR10)Chain of Custody Data Required for ETC Data Management Summary Reports : i:

CA2150 WASTE MWWGEMENT, INC, 405 XDUP 8910100836ftETC SwnpJt No. Company P*clllty 3**pl* taint Dit» TJUwt • flour*

NPOES " • • • :-.:: % , "' ' '• ' '^'^' • , ' • 'NllMfatr • . .::•:;-:: ;• . :' ' ;'. ••" - . .y; • ; f

Chloride mg/1Fluorlde mg/1Nitrate as N mg/1Sulfate as S04 mg/1Phenolics, Total mg/1Cyanide, Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/cmSpecific Conductance urn/ cmpH stdpH stdNitrite as N mg/1

OD

Remits

Sampl*Conc*n,

67.6

'.2<S.O<.oso

<. 01000179.4181.7

1319.01334.0

6.786.79

MO I

1.0.1.1

5.0.050

.010001.01 .0

10.010.0

".1

DEC 20, 1989

•

•

•

.' •::i-.-.yv..---

^^^="



CA2I50 WASTE MANAGEMENT. INC. 405 XDUP 891010 0830 1ETC S«nple No. Company Facility 3<mpj« Point D*t» Tim Hour!

Compound


OJ

Osl

Result s

SampleConcen .

mg/1

< . 2 0<5.0

72701.04

1030

MOLmg/1

.20S . O

10.0

.20to

NOV 3, 1989

•

———— __^. c j L —————————————————————————— , —————————————————————————————————————————^K=F




CA2I50 WASTE MANAGEMENT, INC. 405 XDUP 891010 0830 1El*f>**d

ETC Sanplt No. Conpiny Facility S«mpl< Point Oit* Time Hours

Par«m*t«r

pH (Field stdpH Field stdpH Field stdpH > Field stdSpecific Conductance (Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. C

O

Retulti

SampleMeasure

6.976.987.007.01

1408141114061404

10 7

MDL

-

OCT 16. 1989

t

•

1 ——— ^KP- C 11 ————————————————————————————————————————————————————————————————————^^^f^ NOV 10, 1989TABLE 1: QUANTITATIVE RESULTS and QUALITY ASSURANCE DATA



CA2151 WASTE MANAGEMENT. INC. 405 X03FB 8910091700 1Eltpt*d

ETC Swnplt No. Company Facility Sample Point D«t« , Time Hour*

NPDESNumber

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenolics. Total mg/1Cyanide. Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/cmSpecific Conductance urn/ cmpH stdpH stdNitrite as N mg/1

Remits

SampleConceit.

<1 .0< , l< J

< 050.0014< 1 .0< 1 010.310.38.048.10

MDL

1.0.1.1

.050.01001.01 0

10.010.0--

.1

.

.

^K=^



CA2151 WASTE MANAGEMENT. INC. 405 X03FB 891009 1700 1£lBpM«

ETC SMH>]« No, Comotny Facility S*wpl» Point 0»t» Timt Hour*

Compound


U-J

fteiultt

Samp ItConctn.

< 04<5.0

00.00<.20

HDLma/1

.045.0

10.0

.2010

•

NOV 21 , 1989

Documents

53 PELA ————