GC/MS reportHealing Solutions Black Pepper

This GC-MS analysis con�rms the chemical distribution for this pure black pepper matches that expected for the botanical name Piper nigrum. All the constituents are within range and no adulterants were found.

Page 1 of 4

D:\GC Data\GC Data\Essential oils\Black pepper oil.gcd

2 / 4

Sample InformationUser NameSample NameSample TypeData Name

: $Admn.$: Black pepper oil: $Organic$: D:\GC Data\GC Data\Essential oils\Black pepper oil.gcd

Chromatogram D:\GC Data\GC Data\Essential oils\Black pepper oil.gcd

min

Intensity

10 20 30 40 50

0

250000

500000

750000

1000000

1250000

1500000

1750000

2000000

2250000

2500000

2750000

3000000

8.5

80

8

.91

0

9.4

05

10

.56

3

10

.68

5

11

.18

7

11

.74

3

12

.06

9

12

.26

5 12

.65

8

13

.00

0

13

.68

6

14

.15

2

14

.55

1

15

.40

0

15

.49

7

15

.98

0

16

.09

3

17

.03

9

17

.88

5

18

.90

2 1

9.6

61

2

0.2

95

26

.87

8

27

.35

5

28

.04

4

28

.61

7

29

.15

2

29

.99

0

30

.76

2

30

.88

7

31

.18

5

31

.85

8

32

.11

9

32

.29

0

32

.75

1

32

.94

5

33

.16

0

33

.58

3

33

.74

9

34

.10

2

34

.39

0

34

.70

6

35

.00

7

35

.35

7

35

.79

8

36

.18

4 3

7.0

31

38

.79

1

39

.42

1

D:\GC Data\GC Data\Essential oils\Black pepper oil.gcd

3 / 4

Peak Table - Channel 1 Peak# Ret.Time Area Area% Name

1 8.580 1060221 0.8769 Alpha-Thujene 2 8.910 10255490 8.4819 Alpha-Pinene 3 9.405 265894 0.2199 Camphene 4 10.563 13058983 10.8006 Sabinene 5 10.685 8408022 6.9540 Beta-Pinene 6 11.187 1862104 1.5401 Myrcene 7 11.743 1222479 1.0111 Alpha-phellandrene 8 12.069 8191035 6.7745 Delta-3-carene 9 12.265 129497 0.1071 Alpha-Terpinene

10 12.658 381580 0.3156 m-Cymene 11 13.000 19546963 16.1666 Limonene 12 13.686 209328 0.1731 Beta-Ocimene 13 14.152 291156 0.2408 Gamma-terpinene 14 14.551 174148 0.1440 4-thujanol 15 15.400 89951 0.0744 2-Carene 16 15.497 376906 0.3117 Alpha-terpinolene 17 15.980 114171 0.0944 Menth-2-en-1-ol cis-para 18 16.093 511340 0.4229 Linalool 19 17.039 46123 0.0381 Menth-2-en-1-ol- trans-para 20 17.885 26987 0.0223 Cis-verbenol 21 18.902 28967 0.0240 6-(1-Hydroxy-1-methylethyl)-3-methyl-2-cyclohexen-1-yl acetate 22 19.661 543714 0.4497 Terpinen-4-ol 23 20.295 82024 0.0678 Alpha-terpineol

24 26.878 2700131 2.2332 Delta-Elemene 25 27.355 316321 0.2616 Alpha-Cubebene 26 28.044 150351 0.1243 Cyclosativene 27 28.617 5397142 4.4638 Alpha-Copaene 28 29.152 908326 0.7512 Beta-copaene 29 29.990 150959 0.1249 Alpha-Gurjunene 30 30.762 33816666 27.9685 Trans-Caryophyllene 31 30.887 169755 0.1404 Muurola-4(14),5-diene<trans 32 31.185 55182 0.0456 Alpha-guaiene 33 31.858 1703857 1.4092 Alpha-humulene 34 32.119 17753 0.0147 Cis-beta-Farnesene 35 32.290 28124 0.0233 Beta-Elemene 36 32.751 82176 0.0680 Isogermacrene D 37 32.945 392113 0.3243 Germacrene D 38 33.160 264014 0.2184 Beta-selinene 39 33.583 692819 0.5730 Bicyclogermacrene 40 33.749 475219 0.3930 Guaia-6,9-diene 41 34.102 2969139 2.4557 Beta-Bisabolene 42 34.390 254050 0.2101 Cubebol 43 34.706 1801458 1.4899 Delta-Cadinene 44 35.007 60844 0.0503 Cadina-1,4-diene trans 45 35.357 83627 0.0692 Bisabolene (E)-alpha

D:\GC Data\GC Data\Essential oils\Black pepper oil.gcd

4 / 4

Peak# Ret.Time Area Area% Name 46 35.798 93034 0.0769 Allo-Aromandendrene epoxide 47 36.184 46961 0.0388 Nerolidol (E) 48 37.031 1092467 0.9035 Caryophyllene oxide 49 38.791 183752 0.1520 Spathulenol 50 39.421 126559 0.1047 Delta-Cadinol

Total 120909882 Total 100.0000