4955 Yarrow Street Avda, CO 80002

i

STLSTL Denver4955 Yarrow StreetAvda, CO 80002

TEl: 303 736 0100 Fax: 303 431 7171www.stHnc.com

ANALYTICAL REPORT

URENCO Project

Lot#: D4D030176

Purchase Order 018511-0403003

Frank Bellini/Carl Jackson

Lockwood Greene1500 International DriveSpartanburg, SC 29304

SI DENVER

Project Manager

April 29,2004

Severn Trent LoMWIM Inc.

Table Of ContentsStandard Deliverables

Report Contents Total Numberof Pages

Standard DeliverablesThc Cover Letter and the Report Cover page are considered integralparts of this tdardDeliverablepackage. This report i incompleteunless all pages bniated in this Table of Contents are included

* Table of Contenlts

* Case Narrative

* Executive Summary - Detection Highlights

* Methods Summary

* MethodlAnalyst Summary

* Lot Sample Summary

* Analytical Results

* QC Data Association Summary

* Chain-of-Custody

N:-PMs\Fors\toc suddoc

Lot#: D4D030176

Case NarrativeEnclosed is the report for eight samples received at STL's Denver laboratory on Apri 3, 2004. Theresults included in this report have been reviewed for compliance with STL Denver's Laboratory QualityManual. The test results shown in this report meet all requirements of NELAC and any exceptions arenoted below.

Dilution factors and footnotes have been provided to assist in the interpretation of the results. Eachsample was analyzed to achieve the lowest possible reporting limit within the constraints of the method.In some cases, due to interferences or analytes present at concentrations above the linear calibrationcurve, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilutionrequired.

STL utilizes USEPA approved methods in all analytical work. The samples presented in this report wereanalyzed for the parameters listed on the analytical methods summary page in accordance with themethods indicated. A summary of quality control parameters is provided below.

This report shall not be reproduced except in fiul without the written approval of the laboratory.

Quality Control Sunmmary for Lot D4D030176

Sample Receiving

> The cooler temperature upon receipt at the Denver laboratory was 2.3 C.

> All sample bottles were received in acceptable condition.

Holding Times

> All holding times were met.

Method Blanks

> The analytes Acetone, Naphthalene, and Toluene by Method 8260B were detected in the MethodBlank below the established reporting limits. No corrective action is taken for any values in MethodBlanks that are below the requested reporting limits.

S> All other Method Blanks were within established control limits.

Laboratory Control Samples

> The LCS and LCSD recoveries were above the upper control limits for all compounds except for theDemeton LCSD by Method 8141A. In addition the relative percent difference (RPD) was outsidecontrol Emits for Demeton (total). The associated sample results are still considered valid becausenone of the target compounds were detected.

> The LCS recovery was above the upper control limit for 2,4-D by Mcthod SISlA at 93%. Inaddition the surrogate recovery for DCAA was above the upper control limit for the LCS. Theassociated sample results are still considered valid because 2,4-D was not detected.

> All other Laboratory Control Samples were within established control limits.

Lot#: D4D030176

Matrix Spike (MS) and Matrix Spike Duplicate (MSD)

> The Matrix Spike and Matrix Spike Duplicate recoveries were outside control limits for allcompounds except Ethyl parathion by Method 8141A; for all compounds in the MS by Method8151A; and for Arsenic, Lead, Selenium, and Silver in the MS by Method 601OB. The RPD wasoutside control limits for all Method 6010B metals except Chromium. In addition the surrogaterecovery of DCAA was outside control limits in the MS by Method 8151A Because thecorresponding Laboratory Control Samples and the Method Blank samples were within controllimits, these anomalies may be due to matrix interference.

> The MS/MSD recoveries, surrogate recoveries, and RPD could not be determined for Methods8270C and 808 IA because of the dilutions performed on the samples.

) All other MS and MSD samples were within established control limits.

Organics

> The relative percent difference between the primary and confirmation columns exceeded 40%/. for4,4'-DDD in samples SS-6, SS-9, SS- 1, and SS-12. The lower of the two results is reported.

> Samples SS-13, SS-15, and SS-16 were analyzed at a dilution for Pesticides by Method 80S8A due tothe presence of interfering, non-target compounds. Continuing Calibration Verification (CCV)standards for 4,4'-DDT and Methoxychlor failed when these samples were run without dilution.Therefore, it was necessary to analyze with dilution to obtain passing QC samples. The reportinglimits were raised according to the dilution level. As a result of the dilutions, the surrogaterecoveries could not be determined.

> The surrogate recoveries for DCAA in samples SS-13 and SS-15 were above the upper control limitin Method 815IA. The sample results are still considered valid because no target analytes weredetected.

> The internal standard recoveries for 1,4-Dichlorobenzene-d4 were outside control limits for sampleSS-6 and the MS/MSD performed on this sample by Method 8260B. Because the failed recoverieswere confirmed repeatedly on sample SS-6, matrix effects are confirmed.

> The Continuing Calibration Verification (CCV) standards for Demeton-S, 0,0,0-Triethylphosphorothioate, Dichlorvos, Azinphos-methyl, Mevinphos, Dimethoate, Malathion,Tetrachlorvinphos, and Naled by Method 8141A exceeded the percent difference limits in variousruns and columns. However, the overall mean percent difference is within control limits, therefore,the CCV is also in control and no corrective action was necessary. Additionally, the associatedsamples were non-detect.

> The Continuing Calibration Verification (CCV) standards for Dichloroprop, MCPP, DCAA,Dicamba, Dinoseb, MCPA, and 2,4-DB by Method 8151A exceeded the percent difference limits invarious runs and columns. However, the overall mean percent difference is within control limits,therefore, the CCV is also in control and no corrective action was necessary. Additionally, theassociated samples were non-detect.

> The Continuing Calibration Verification (CCV) standards for Heptachlor, 4,4'-DDE, Endrin, 4,4'-DDD, 4,4'-DDT, DCB, Methoxychlor, Endosulfan 1, Eadrin aldehyde, Endosulfan sulfate, and delta-BHC by Method 8081A exceeded the percent difference limits in various runs and columns.However, the overall mean percent difference is within control limits, therefore, the CCV is also incontrol and no corrective action was necessary. Additionally, the associated samples were non-detect below the reporting limit.

EXECUTVE SUMMARY - Detection H igg

D4D030176

REPORTINGLIMIT

ANALYTTCALME'THODPARAMETER RESULT UNITs

-

8S-2 04/01/04 12:30 001

ArsenicLeadBariumChromiumSilverAcetoneXylenes (total)1,2,4-Trimethylbenzenem-Xylene & p-Xyleneo-XylenePercent Moisture

0.76 B2.8225.90.099 B4.2 J,B0.93 J0.30 J0.56 a0.37 J1.6

1.00.811.01 .01.0205.15.12.52.50.10

mg/kgmg/kgmg/kgmg/kgmg/kgug/kgug/kgug/kgug/kgug/kg

&W8468W8468W846SW8468W8468W8468W846SW846&W846SW846MCAWW

6010B6010B6010B6010B6010B8260B8260B8260B8260B8260B160.3 MOD

SS-6 04/01/04 10:40 002

4,4' -DDD

ArsenicLeadBariumChromiumsilverAcetoneXylenes (total)1,2,4-Trimethylbenzenem-Xylene a p-Xyleneo-XylenePercent Moisture

0.44Qualifiers:

0.76 B

2.2153.10.10 B5.6 J,B1.0 J0.33 J0.73 J0.28 J1.3

1.7JCOL

1.00.811.01.01.0205.15.12.52.50.10

ug/kg

mg/kgmg/kgmg/kgmg/kgmg/kgug/kgug/kgug/kgug/kgug/kgt

SW846 8081A

8W8466W8466W8468W8468W8468W8468W846BW8468W84651(846

DACAWN

6010B6010B6010B6010B6010B8260B8260B8260B8260B8260B160.3 MOD

8S-9 04/01/04 15s15 003

4,4' -DDD

LeadBariumChromiumSilverAcetoneXylenes (total)o-XyleneFluoridePercent Moisture

0.39Qualifiers:

3.3533.40.085 B3.9 .,B0.72 J0.32 J1.0 B1.2

1.7J,COL

0.811.01.01.0205.12.51b0.10

ug/kg

mg/kgmg/kgmg/kgmg/kgug/kgug/kgug/kgmg/kgt

8W846 8081A

8W8468W8468W8468W8466W846

W81466W846SW846MCAWN

6010B6010B6010B6010B8260B8260B8260B9056160.3 MOD

(continued on next page)

EXC1IVE SUNM4ARY - Detection 1ig4light

D4D030176

REPORTINGL3MIT

ANALYTICALMETHODPARAMETER RESULT WNITS

&S-ll 04/01/04 10s00 004

4,4'-DDD

ArsenicLeadBariumChromiumSilverAcetoneSylenes (total)1,2,4-Trimethylbenzenem-Xylene & p-Xyleneo-XyleneFluoridePercent Moisture

0.79Qualifiers:

0.89 B2.8193.40.11 B3.8 J,B0.73 J0.23 J0.43 J0.30 J1.2 B1.3

1.7J,COL

1.00.811.01.01.0205.15.12.52.5100.10

ug/g

mg/kgmg/kgmg/kgmg/kgmg/kgug/kgug/kgug/kgug/kgug/kgmg/kgt

SW846 8081A

SW846SW846SW8468WE468W8468W846SW846SW846SW8468W8468W846MCAWW

6010B6010B6010B6010B6010B8260B8260B8260B8260B826099056160.3 MOD

SS-12 04/01/04 15:40 005

4,41'-DDD

ArsenicLeadBariumChromiumSilverXylenes (total)1,2,4 -Trimethylbenzenem-Xylene & p-Xyleneo-XylenePercent Moisture

0.65Qualifiers:

0.77 B2.7193.50.10 B1.6 i0.45 J1.1 J0.50 J1.5

1.7J,COL

1.00.811.01.01.05.15.12.52.50.10

ug/kg

mg/kgmg/kgmg/kgmg/kgmg/kgug/kgug/kgug/kgug/kgt

5846 8081A

SW846 6010BSW846 6010B8W846 6010B5W846 6010B8W846 6010B8W846 8260B8W846 8260B8W846 8260B8W846 8260BMCAWW 160.3 MOD

8S-13 04/01/04 16:10 006

LeadBariumChromiumXylenes (total)1,2,4-Trimethylbenzenem-Xylene & p-Xyleneo-XylenePercent Moisture

2.6163.01.1 J0.38 J0.82 J0.31 J1.1

0.81 mg/kg1.0 mg/kg1.0 m Mg/kg5.1 ug/kg5.1 ug/kg2.5 ug/kg2.5 ug/kg0.10 k

SW846S8w468WS468W846-8W8468w8468W846MCAWW

6010B6010B60109.8260B8260B8260B8260B160.3 MOD

(Continued on next page)

EXECUTIVE SUMMARY - Detection Eiglights

D4D030176

REPORTINGLIMIT

AhLYTICALMEIHODRESULT UNITS

SS-15 04/01/04 13:10 007

LeadBariumChromiumSilverXylenes (total)1,2,4-Trimethylbenzenem-Xylene & p-Xyleneo-XyleneFluoridePercent Moisture

SS-16 04/01/04 14:4O 008

2.5173.10.10 B

1.1 .0.35 J0.78 J

0.31 J1.0 B1.2

0.811.01.01.05.15.12.52.5100.10

mg/kgmg/kgmg/kgmg/kgug/kgug/kgug/kgug/kgmg/kg

SW846SW846SW846

SW8468W846W8846

8W846SW846SW846McaswK

6010B6010B6010B6010B8260B8260B8260B8260B9056160.3 MOD

ArsenicLeadBariumchromiumSilverXylenes (total)1,2,4-Trimethylbenzenem-Xylene & p-Xylene

o-XyleneNaphthalenePercent Moisture

0.96 B2.9 -243.7

0.11 B

1.4 J0.48 J0.99 .0.44 J0.69 JB,0.81

1.00.811.01.01.05.0'5.02.52.55.00.10

mrg/kgmg/kgmg/kgmg/kgmg/kgug/kgug/kgug/kgug/kgug/kg

SW8468W8468W8468W8466W846SW846

SW8466W846SW846BW846McaWw

601036010B6010B6010B6010B8260B8260B8260B8260B8260B160.3 MOD

METHOD J ANALYSF SUMRMAY

D4D030176

ANALYTICAL3TR'rZTfln

ANALYSTID1]T& T.P

MCAW8W8468W8460W8468W8466W8468W846SW8468846

160.3 MOD6010B7471A8081A8141A8151A8260B8270C9056

Jean CarrierLynn-Anne TrudellRacey OnoMike DobranskySonya DacarHeather DybasDan AppelhansRwanda TodeaAndrita Scofield

0087636645003371008777011595038161001008005716004409

References :

MCAWW wMethods for Chemical Analysis of Water and Wastes",EPA-600/4-79-020, March 1983 and 6ubSequent revisions.

SW846 OTest Methods for Evaluating Solid Waste, Physical/ChemicalMethods*, Third Edition, November 1986 and its updates.

SAMLE SUMMARY

D4D030176

SAMPLED SAMPNO t SAMPLE# CLIENT SAMPLE ID DATE Tn4E

GDHQL 001 SS-2 04/01/04 12:30GDHQX 002 8S-6 04/01/04 lO40G=HQO 003 SS-9 04/01/04 15215GDHQ1 004 88-11 04/01/04 10:00GDHQ2 005 SS-12 04/01/04 15:40GDHQ3 006 SS-13 04/01/04 16,10GDHQ4 007 SS-lS 04/01/04 13:1OGDHQ5 008 SS-16 04/01/04 14:40

NOTE(S)X-lbe maltydeal radu ore e .h e iced above m prmd en ie iov pps.

- Alokdnms amperfomedbefore roidAg sbroaind-44ff esonh cabavesfrnks.Rsultm aoted as 'W on oat detectd stm above bie sated EmIL

rmepour mm ant be reproduced. enxt in Al. wki fte wrm aroVa of die laboratory.-Remus for e Wowing purmnets am new rped on a dry weight baft color. cormasIy. deantyffapout. Iiabi, kyys; odor,

paint miltr est . potost pese mady. rplox potmu1. vepdrr pgravi Vt Oests. sohibIty, dmp-.ai . viscoity. ad wd

METHODS SUMMARY

D4D030176

ANALYTICALPARAMETER METHOD

PREPARATIONMETHOD

Chlorinated Herbicides by GCFluorideInductively Coupled Plasma (ICP) MetalsMercury in Solid Waste (Manual Cold-Vapor)Organochlorine PesticidesOrganophosphorous Compounds by GCPercent MoistureSemivolatile Organic Compounds by GC/MSVolatile Organics by GC/MS

SW8466W846SW8468W846SW846SW846MCANWSW846SW846

815LA90566010B7471A80812k8141A160.3 MOD8270C8260B

8W8466W846SW8468W8468W846

MCAWWSW846SW846

8151A90563050B7471h3550

160.3 MOD3550B5030B/826

References:

MCAW

8W846

'methods for Chemical Analyois of Water and Wastes',EPA-600/4-79-020, March 1983 and subsequent revisions.

"Test Methods for Evaluating Solid Waste, Physical/Chemical

Methods", Third Edition, November 1986 and its updates.

Client Sample ID: 8S-2

GC/MS Volatiles

bot-&ample #...sDate Sampled...:Prep Date......:Prep Batch t...sDilution Factor:

D4D030176-00104/01/04 12:3004/12/0441042741

Work Order C...:Date Received..:analysis Date..:Analysis Time..:

GDHQL1AF04/03/0404/12/0413:46

Matrix ......... sOLID

Nethod . ... : 6W846 8260B

PARAMETERAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-Butanone (HEM)carbon tetrachlorideChlorobenzeneChloroetbaneChloroformChloromethaneDibromomethane1,2-Dibromoethane CEDB)1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDihlorodifluoromethane1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethene1,2-Dichloroethene

(total)cis-1,2-Dichloroethenetrans-1,2-Dichloroethene1,2-Dichloropropanecis-1, 3-Dichloropropenetrans-1,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1,2,4-Trichloro-

benzene

RESULT4.2 J,BNDNDED2NDllDEDEDNDlNDNDNDNDEDNDNDNDNDNDNDND

NDNDNDEDND

NDNDNDNDNDNDNDNDNDND

REPORTINGLIMIT205.15.15.110205.15.11010105.15.15.15.15.1105.15.15.15.1

2.52.55.15.15.15.1205.1205.15.15.15.15.15.1

UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgugtkgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg


lDICKHOO GEM

Client SaLMple ID: SS-2

GC/MS Volatiles

Lot-Sanple I...: D4D030176-001 Work Order e...: GDHQL1AA Hatrri .... : SOLID

1,1,1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane1,2,3-TrichloropropaneVinyl chlorideXylenes (total)n-Butylbenzenesec-ButylbenzeneIsopropylbenzene1 2,4-Trimetbylbenzene1,3,5-Trimethylbenzenen-Propylbenzenetert-ButylbenzeneDibromochloromethane2-chlorotoluene4-Chlorotoluene1,2-Dibromo-3-

chloropropane (DBCP)1,3-Dichloropropane2,2-Dichloropropane1,1-Dichloropropenenexachlorobutadiene4-IsopropyltolueneMethyl tert-butyl ether1,2,3-Trichlorobenzenem-Xylene & p-Syleneo-XyleneBromobenzeneBromochloromethbaeNaphthalene

RESULTNDNDNDNDm JND0.93 J7ND0mND0.30 JNDEDIDEDEDNDND

ND

EDEDEDND

0.56 i0.37 JEDEDED

REPORTINGLIMIT5.15.15.1105.15.15.15.15.15.15.15.15.15.15.15.15.110

5.15.15.15.15.1205.12.52.55.15.15.1

UNITSug/kgug/kgug/kg

ug/kgug/kgug/kg

ug/kgug/kgug/kgug/kg

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kg

ug/kgug/kgug/kgug/kgug/kg

ag/kgtg/kgug/kgug/kg

ug/kg

SURROGATE

Dibromofluoromethane1,2-Dichloroethane-dt4-BromofluorobenzeneToluene-dB

PERCENT

RECOVERY941029396

RECOVERYLIMITS(71 - 136)(67 - 131)(71 - 124)(77 - 129)

OTE(S) _Rksuand &e on Um skhm bmee auad y .wcId.

I Esz dult. Rem n tkI= 9taRL

B )&eUd blank c m inaro. Th asscat medid blank woubiwm be ft get i t a mprorbk kgd.

WLOD GBE

Client Sample ID: 88-6

GCUMS Volatiles

Lot-Sample C... : D4D030176-002 Work Order g ... 1Date Sampled ... : 04/01/04 10:40 Date Received..sPrep Date ......: 04/12/04 Analysis Date..:Prep Batch 1... : 4104274 Analysis Titae..:Dilution Factor: 1

GDHQX1AA04/03/0404/12/0414:09

Katri ...... : SOLID

Hethod . . : SW846 8260B

PARAMETERAcetoneBenzeneBromodichloromethaneBromofor=Bromomethane2-Butanone (MEK)Carbon tetrachlorideChlorobenzeneChloroethaneChloroformChloromethaneDibromomethane1,2-Dibromoethane (EDB)1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethene1,2-Dichloroethene

(total)cis-1, 2-Dichloroethenetrans-1,2-Dichloroethene1,2-Dichloropropaneci6 -1,3-Dichloropropenetrans-1,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1,1,1,2-Tetrachioroethane1,1,2,2-TetrachloroetbaneTetrachloroetheneToluene1,2,4-Trichloro-

benzene

RESOaT

5.6 J,BEDNDNDEDlDNDNDEDlDEDD

NDNDNDEDNDEDNDNDND

REPORTINGLIMIT205.15.15.110205.15.11010105.15.15.15.15.1105.15.15.15.1


ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

NDEDNDNDNDNDllDNDNDNDNDNDIDNDND

2.52.55.15.15.15.1205.1205.15.15.15.15.15.1


WM GREENE

Client Sanple mD: SS-6

GC/MS volatiles

Wt-Saiple I...: D4D030176-002 work order I... GDHQX1LA Hatrir .... : SOLID

PARAMETER1,1, 1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane1,2,3-TrichloropropaneVinyl chlorideZylenes (total)n-ButylbenzeneBec-Butylbenzenelsopropylbenzene1,2,4-Trimetylbeanzene1,3,5-Trimethylbenzene

n-Propylbenzenetert-ButylbenzeneDibranochloromethane2-Chforotoluene4-Chlorotoluene1,2-Dibromo-3-

chloropropane (DBCP)1,3-Dichloropropane2,2-Dichloropropane1,1-Dichloropropene

Hexachlorobutadiene4-IsopropyltolueneMethyl tert-butyl ether1,2,3-Trichlorobenzenem-Xylene & p-Xylezeo'-XylenieBromobenzeneBromochloromethaneNaphthalne

RESULTND

VDEDEDDD

ND1.0 LT

ND

NDND0.33 JNDNDNDiDD

IDND

REPORTINmLIMIT5.15.15.1105.15.15.15.15.1

5.1

5.1,5.15.15.15.15.15.110

UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug kgug/kgug/kg


ug/kgug/kgug/kgug/kgug/kgug/kgug/kg


WDNDNDNDNDNDND0.73 ;1Q.28 J

1D1DND

5.15.15.15.15.1205.12.52.55.15.15.1

SURROGATEDibromofluoromethane1,2-Dichloroethane-d44-BromofluorobenzeneToluene-d8

PERCENTRECOVERY98103

9592

RECOVERYLIMITS(71 - 136)(67 - 131)

(71 - 124)(77 - 129)

NOTE(S):Res snd pordn afts bkvc been adused zr t weighbt

I Esntmted iML balt Is less fta RL

B Mcdbd blank ammaina. TIM asoiated medod blak watains Me Irge mlyte at a rontae level.

Client Sample ID: SS-9

GC/hs Volatiles

Lot-Sample i...:Date Sanpled...:Prep Date ...... :Prep Batch I...:Dilution Factor:

D4D030176-00304/01/04 15S:1504/12/0441042741

work Order C..:Date Received..:Analysis Date. .:Analysis Time..:

GDHQ01APL04/03/0404/12/0414:32

Matrix ..... S : OLID

Method . ... : SW846 8260B

PARAMETERAcetoneBenzeneBromodichloromethaneBromoformBroamomethane2-Butanone (MEE)Carbon tetrachlorideChlorobenzeneChloroethaneChloroformChlorometbaneDibromomethane1,2-Dibromoethane (EDB)1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluoromethane1, 1-Dichloroethane1, 2-Dichloroethane1,1-Dichloroethene1,2-Dichloroethene

(total)cis-1,2-Dichloroethenetrans-1,2-Dichloroethene1,2-Dichloropropanecis-1, 3-Dichloropropenetrans-1,3-DichloropropeneEthylbenzene2-KexanoneMethylene chloride4-Methyl-2-pentanonestyrene1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1,2,4-Trichloro-

benzene

RESULT3.9 J,BEDEDNDNDEDNDEDNDEDIDNDNDNDEDNDEDEDEDEDND

NDNDlDEDINDNDNDNDNDEDNDNDNDEDED

REPORTIMG

LIMI205.15.15.110205.15.11010105.1

5.15.15.15.1105.15.15.15.1

2.52.55.15.15.15.1205.120

5.1S.15.15.15.15.1

UNITSugfkgug/kgug/kgug/kg

ug/kgug/kgug/kgug/kgug/kgug/kguglkguglkgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg



I


GC/MS Volatiles

Lot-Sample #...: D4D030176-003 Work Order t...: GDHQO1AA Matriz ......... : SOLID

PAEAMETER

1,1,2-Trichloroethane

TrichloroetheneTrichlorofluoromethane1,2,3-TrichloropropaneVinyl chlorideXylenes (total)n-Butylbenzenesec-ButylbenzeneIsopropylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenen-Propylbenzenetert-ButylbenzeneDibromochloromethane2-Chlorotoluene4-Chlorotoluene1,2-Dibromo-3-

chloropropane (DBCP)1,3-Dichloropropane2,2-Dichloropropane1,l-DichloropropeneRexachlorobutadiene4-IsopropyltolueneMethyl tert-butyl ether1,2,3-Trichlorobenzenem-Xylene & p-Xyleneo-XyleneBromobenzeneBromochloromethaneNaphthalene

RESULTNDNDNDNDNDWD0.72 JNDNDNDNDNDNDNDNDNDNDND

NDNDDNDNDNDNDND0.32 JNDNDND

REPORTINGLIMIT5.15.15.1105.15.15.15.15.15.15.15.15.15.15.15.15.110

5.15.15.15.15.1205.12.52.55.15.15.1

UNITSug/kgug/kgug/kgug/kgug/kgug/kguglkgug/kguglkgug/kguglkguglkgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgug/kgug/kguglkguglkgug/kguglkguglkgug/kguglkgugtkgugtkg

SURROGATEDibromofluoromethaine1, 2-Dichloroethane-d44-BromofluorobenzeneToluene-d8


RECOVERYLIMITS(71 - 136)(67 - 131)(71 - 124)(77 - 129)

NOTE(S):Iur and otlg lmits km ben aiuged br dry weghs.I Egbmted mh. Re* I ess 9i ILI M&odblan ma wa. Tae cae meod blnk cuos btc ge utca armb levd.

Client Sample ID: SS-lI

GC/MS Volatiles

Lot-Sample ... :Date Sampled...:Prep Date ...... :Prep Batch t...:Dilution Factor:

D4D030176-00404/01/04 10:0004/12/0441042741

Work Order #...:Date Received..:Analysis Date..:Analysis Time..s

GDHQ11AA04/03/0404/12/0414:55

NatriX .... .: SOLID

Method .... : SW846 8260B

PARAMETERAcetone

BenzeneBromodichloromethaneBromoformBromomethane2-Butanone (MEK)Carbon tetracbloride

ChlorobenzeneChloroetbxaechloroform

ChlorometbaneDibromometlane1,2-Dibromoethane (EDB)

1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluoromethane1,l-Dichloroethane1,2-Dichloroetbane1,1-Dichloroethene1,2-Dichloroethene

(total)cis-1,2-Dichloroethenetrans-1,2-Dichloroethene1,2-Dichloropropanecis-l,3-Dichloropropenetran -1,3-DichloropropeneEthylbenzene2-NexanoneMetbylene chloride4-Methyl-2-pentanoneStyrene1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1,2,4-Trichloro-

benzene

RESULT

3.B IBNDNDNDNDND

NDNDNDNDNDEDNDNDNDNDRDNDNDND

REPORTINGLIMIT20

5.15.15.110205.15.11010105.15.15.15.15.1105.15.15.15.1

UTSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg


NDNDNDNDNDNDNDNDNDNDNDNDNDNDND

2.52.55.15.15.15.1205.1205.15.15.15.15.15.1


XcKKOOD GREEKE


GC/MS Volatiles

Wt-Sample Y...: D4D030176-004 Work Order t...: GDEQ11AP Matrix .. .a SOLID

PARAMETER1,1,l-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane1,2,3-TrichloropropaneVinyl chlorideSylenes (total)n-Butylbenzenesec-ButylbenzeneIsopropylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenen-Propylbenzenetert-8utylbenzeneDibrocochloromethane2-chlorotoluene4-Chlorotoluene1,2-Dibromo-3-

chloropropane (DBCP)1,3-Dichloropropane

2,2-Dichloropropane1,1-DichloropropeneNexachlorobutadiene4-IsopropyltolueneMethyl tert-butyl ether1,2,3-Trichlorobenzenea-Xylene & p-Xyleneo-XyleneBromobenzeneBromochloromethaneNaphthalene

RESULTNDNDNDNDEDED0.73 JNDNDND0.23 ZEDNDNDNDNDEDND

REPORTINGLIMIT5.15.15.1105.15.15.15.15.15.15.15.1

5.15.15.15.15.110

UNITSug/kgug/kg


ugfkgug/kgug/kgug/kgug/kg

ug/kgug/kgug/kg

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug1kg

ug/kg

ug/kgug/kg

NDNDNDND

NDEDND0.43 40.30 JNDNDND

5.15.15.15.15.1205.12.52.55.15.15.1



RECOVERYLIMITS(71 - 136)(67 - 131)(71 - 124)(77 - 129)

NOTE(S):

R ts, sad eponlg Emhs have be jszW fr dry we k

I Esnaed la& R t s lss 3m EL

B Medod blank c mnhaioo. To associd m hod blan ontains tIe u e o te at a epo bk lvel.


GC/MS Volatiles

Lot-Sample C...s D4D030176-005 Work Order C...:Date Sampled ...: 04/01/04 15:40 Date Received..:Prep Date ...... s 04/12/04 Analysis Date.. :Prep Batch #...: 4104274 Analysis Time-.:Dilution Factor: I

GDEQ21AA04/03/0404/12/0415:19

Katrix .... SOLID

Nethod.........: SW846 8260B

AcetoneBenzeneBromodichloromethaneBromoformBromomethane2 -Butanone (MEM)Carbon tetrachlorideChlorobenzeneChloroethaneChloroformChloromethaneDibromometbane1,2-Dibromoetbane (BDB)1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluoromethane1, 1-Dichloroethane1,2-Dichloroethane1,l-Dichloroethene1,2-Dichloroethene

(total)cis-1, 2-Dicbloroethenetrans-1,2-Dichloroethene1,2-Dichloropropaneci-i,3-Dichloropropenetrans-1,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1,2,4-Trichloro-

benzene

RESULTND

NDNDNDNDNDNDNDNDNDNDNDNDEDNDNDNDNDNDNDND

REPORTINGLIMIT205.25.15.110205.15.11010105.15.15.15.15.1105.15.15.15.1

UNITSug/kgulg/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgug/kgug/kgUg/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

NDRDaDND1DNDNDNDNDNDNDNDNDEDND

2.52.55.15.15.15.1205.1205.15.15.15.15.15.1


LODD -B

Client Sanple mD. SS-12

GCIKS Volatiles

Lot-Sample #I..: D4D030176-005 Work Order t...: GDHQ21AA

1,1,1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethbne1,2,3-TrichloropropaneVinyl chlorideZylenes (total)n-Butylbenzenesec-ButylbenzeneIEopropylbenzene1, 2, 4-Trmtbymbenzene:1,3,5-Trimethylbenzenen-Propylbenzenetert-ButylbenzeneDibromochloromethane2-Chlorotoluene4-Chlorotoluene1, 2-DLbromo-3-

chloropropane (DBCP)1,3-Dichloropropane2,2-Dichloropropane1,L-DichloropropeneHexachlorobutadiene4-I6opropyltolueneMethyl tert-butyl ether1,2,3-Trichlorobenzenem-Kylene & p-Xyleneo0-yleneBromobenzeneBromochloromethane

RESULTNDNDNDEDNDND1.6 JNDNDND0.45 JNDNDNDNDNDNDND

NDEDNDEDNDlDND1.1 J

0.50 JNDEDED

REPORTINGLIMT

5.1

5.1

5.1

10

5.1

5.1

5.1

5.15.15.15.15.1SA.5.15.15.15.110

5.15.15.15.15.1205.12.52.55.15.15.1

Matrix .... . SOLID

UTSug/kgug/kgug/kgug/kgug/kgug/kg




ug/kgug/kgug/kg

ug/kgug/kgug/kgug/kgugtkgug/kgug/kgug/kgug/kgNaphthalene


PERCENTRECOVERY98

1039199

RECOVERYLIMITS(71 - 136)(67 - 131)(71 - 124)

(77 - 129)

om (s) :Rmt md v l4 IIa have ti=e 4uswd fOr dq weigthL

I Essimted Is.aL K~ft is I= tan RL.


GC/hS Volatiles

Lot-Sample #...:Date Sampled...:Prep Date ...... :Prep Batch #...:Dilution Factor:

D4D030176-00604/01/04 16:1004/12/0441042741

Work Order #... :Date Received. .:AnalysBi Date..:Analysis Tisme..:

GDEQ31AA04/03/0404/12/0415:42

HatriX......... : SOLID

Method ......... : SW846 8260B

PARAMETERAcetoneBenzeneBromzodichloromethaneBromoformBromomethane2-Butanone (MEK)Carbon tetrachlorideChlorobenzeneChloroethaneChloroformChloromethaneDibromometh ane1,2-Dibromoethane (EDB)

1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorcbenzeneDichlorodifluoromethane1,l-Dichloroethane1,2-Dichloroethane1,1-Dichloroethene1,2-Dichloroethene

(total)cis-1, 2-Dichloroethenetrans-1,2-Dichloroethene1,2-Dichloropropanecis-i,3-Dichloropropenetrans-1 , 3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyi-2-pentanonestyrene1,1,1,2-Tetrachloroethane1,1,2,2-Tetrachloroethane

TetrachloroetheneToluene1,2,4-Trichloro-

benzene

RESULTEDNDEDEDNDNDNDEDNDNDNDNDEDNDNDNDEDIDEDED

kD

REPORTINGLIMIT205.15.15.110205.15.11010105.15.15.15.15.1105.15.15.15.1



EDNDND

EDEDEDEDEDNDNDNDNDEDNDED

2.52.55.15.15.15.1205.1205.15.15.15.15.15.1


WLOD QREEME

Client Sazple ID: SS-13

GC/NS Volatiles

Lot-Sample #...: D4D030176-006 Work Order #...: GDHQ31AA Hatri ...... : SOLID

PARAMETER1,2,1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane1,2,3-Trichloropropanevinyl chlorideZylenes (total)n-Butylbenzenesec-ButylbenzeneIsopropylbenzene1,2,4-Trimethylb e1.3,5-Trimethylbenzenen-Propylbenzenetert-ButylbenzeneDibromochloromethane2-Chiorotoluene4-Chiorotoluene1,2-Dibromo-3-

chloropropane (DBCP)1,3-Dichloropropane2,2-Dichloropropane1,1-DichloropropeneHexachlorobutadiene4-I6opropyltolueneMethyl tert-butyl ether1,2,3-Trichlorobenzeneu-Xylene & p-Myleneo-ZyleneBromobenzeneBromochloromethaneNaphthalene

RESULTND

ND

EDNRD

1.1 JNDNDND

0.38 JNDNDNDNDNDNDND

REPORTINGLIMIT5.15.15.1105.15.15.15.15.15.15.15.15.15.15.15.15.110

UNITSug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgug/kgug/kgug/kguglkgug/kgug/kgug/kgugifug/kgug/kgug/kg

NDNDNDNDEDNDND0.82 J0.31 ZND

NDND

5.15.15.15.15.1205.12.52.55.15.15.1

SURROGATEDibromofluoromethane1,2-Dichloroethane-d44-BromofluorobenzeneToluene-de

PERCENTRECOVERY94

999293

RECOVERYLIMITS(71 - 136)(67 - 131)(71 - 124)(77 - 129)

FMS) t

Rels and repoi4da mhhave been adjusd for dry %hbL

J Esumftcd rulL Resut is ea M L

client Sample ID: ES-IS

GC/hS Volatiles

lot-Sample #...s D4D030176-007Date Sampled ...: 04/01/04 13:10Prep Date ...... : 04/12/04Prep Batch C...: 4104274Dilution Factors 1

Work order E...:Date Received..:Analysls Date..:Analysis Time..

GDHQ41AA04/03/0404/12/0416:06

Hatrix ..... s OLID

Method . .... : W846 8260B

PARAMTERAcetoneBenzeneBromodichloromethaneBromofoarmBromomethane2-Butanone (MEK)Carbon tetrachlorideChlorobenzeneCbloroethaneChloroformChloromethaneDibrowomethane1,2-Dibromoethane (EDB)1,2-Dichlorobenzene1,3-Dichlorobenzene1,4- DichlorobenzeneDichlorodifluoromethane1, 1-Dichloroethane1,2-Dichloroethane1, 1-Dichloroethene1,2-Dichloroethene

(total)cis-1, 2-Dichloroetbenetrans-1,2-Dichloroethene1,2-DichloropropaneCis-1, 3 -Dichloropropenetrans-1,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1,1,1,2-Tetrachloroethane1,122,2-TetrachloroethaneTetrachloroetheneToluene1,2,4-Trichloro-

benzene

RESULTNDNDNDNDNDNDNDND

NDNDNDNDNDNDNDEDEDhDEDED

REPORTING

205.15.15.110205.15.11010105.15.15.15.15.1105.15.15.1.5.1



NDIDEDNDNDNDNDWDNDEDNDEDNDNDED

2.52.S5.15.15.15.1205.1205.15.15.15.15.15.1


CRWOD


GC/HS Volatlles

Lot-Sample I...: D4D030176-007 Work Order #...t GDHQ41AA Matrix........: SOLID

PARAMETER1,1,l-Trichloroethane11, 2-TrichloroethaneTrichloroetheneTrichlorofluoromethane1, 2, 3 -TrichloropropaneVinyl chlorideXylenes (total)n-Butylbenzenesec-ButylbenzeneIsopropylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenen-Propylbenzenetert-ButylbenzeneDibromochloromethane2-chlorotoluene4-Chlorotoluene1,2-Dibromo-3-

chloropropane (DBcP)1,3-Dichloropropane2,2-Dichloropropane1,1-DichloropropeneRexachlorobutadiene4-IsopropyltolueneMethyl tert-butyl ether1,2,3-Trichlorobenzenem-Xylene & p-Xyleneo-ZyleneBromoben2zeneBromochloromethaneNaphthalene

RESULTNDNDNDNDNDND1.1 JEDNDND0.35 JNDEDEDEDNDEDND

NDNDNDNDEDNDND

0.78 JT0.31 JNDNDND

REPORTING

LIMIT5.15.15.1105.15.15.L5.15.15.15.15.15.15.15.15.15.110

5.15.15.15.15.1205.12.52.55.15.15.1

UISuglkgug/kgug/kg

ug/kgug/kgug/kguglkgug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kgug/kgug/kg


SURROGATEDibromofluoromethane1,2-Dichloroethane-d44-BronofluorobenzeneToluene-d8

PERCENTRECOVEY961049495

RECOVEY

LIMITS(71 - 136)(67 - 131)(71 - 124)(77 - 129)

POTE(S)Resok wd .prti llmhs bave been Arustad fJr jy wdehL

I Es-aid resuk. Ret bles dun RL,


GC/MS Volatiles

Iot-Sample t...: D4DW30176-008 Work Order C...Date Sampled ... : 04/01/04 14:40 Date Received..:Prep Date ...... : 04/12/04 Analysis Date..:Prep Batdh 1 ... : 4104274 Analysis Time..:Dilution Factor: 1

GDIQ51AA04/03/0404/12/0417:16

Matrix ........ : SOLID

Metbod......... : SW846 8260B

PARAMETERAcetoneBenzeneBromodichloromethaneBromoformBrwomzethane,2-Butanone (t=)Carbon tetrachlOrideChlorobenzeneChloroethanchloroformCfhloromethaneDibromomethane1,2-Dibromoetbsule (EDB)1,2-Dicblorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethene1.2-Dichloroethene

(total)cis-1,2-Dichloroethenetrans-1,2-Dichloroethene1 2-Dicbloropropanecis-1, 3-Dichloropropenetrans-1,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1,2,4-Trichloro-

benzene

RESULTNDNDNDNDNDEDEDNDNDNDNDEDEDNDNDNDND1DNDEDND

REPORTINGLIMIT205.05.05.010205.05.01010105.05.05.05.05.0105.05.05.05.0



NDhDEDND

NDEDNDNDNDNDNDNDND

NDND

2.52.55.05.05.05.0205.0205.05.05.05.05.05.0


COOD R


CC/MS Volatiles

Iot-Bample ...: D4D030176-008

PARAMETER1.1,1-Trichloroethane1,1, 2-Trichloroeth~neTrichloroetheneTrichlorofluoromethane1,2,3-TrichloropropaneVinyl chlorideXylenes (total)n-Butylbenzenesec-ButylbenzeneIsopropylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene.n-Propylbenzenetert-ButylbenzencDibremochlorometbane2-Chlorotoluene4-Cblorotoluene1,2-Dibromo-3-

chloropropane (DBCP)1,3-Dichloropropane2,2-Dichloropropane1,1-DichloropropeneNexachlorobutadiene4-IsopropyltolueneMethyl tert-butyl ether1,2,3-Trichlorobenzenem-Xylene & p-Xyleneo-ZyleneBromobenzeneBromochlorcmethaneNaphthalene

Work Order 0...: GDHQ51A&

RES=UTNDNDEDEDNDND1.4 JVDEDND0.48 vTNDNDEDNDJD

EDND

NDNDNDNDNDD

ND0.99 J0.44 JNDND0.69 JB

REPORTINGLIMIT5.05.05.0105.05.0S.05.0S.05.05.05.0S.05.05.05.05.010

5.05.05.05.05.0205.02.52.55.05.05.0

matrix . ... SOLID

UNITSug/kgug/kgug/kgug/kg

Ug/kgug/kg

ug/kgug/kgug/kgtag/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg


SURROGATEDibromofluoromethane1,2-Dichloroethane-d44-BromofluorobenzeneToluene-dS


RECOVERYLIMITS(71 - 136)(67 - 131)(71 - 124)(77 - 129)

r8 (SI):R=Ii mad repotdng Eit have been ajd fr dry wegh

I Psdam fes Rulst is Wu Ita ILB MedWd blank ecasnlson The asdated mxthod blank conais dIlw ltget u nate ta m mic level.


GC/NS Cemivola

Lat-Saxple t ... :Date Sampled ... :

Date ... .... s

Prep Batch #...:Dilution Factor:

D4D030176-00104/01/04 12:3004/07/0440976211

Work Order I...:Date Received..:Analysia Date.. 3Analysis Tim-e.:

GDHQL1AC04/03/0404/22/0415:54

Matrix . . a SOID

Method......... : 5W846 8270C

PARAMTERAcenaphtheneAcenaphthyleneAcetophenone2-Acetylamlnofluorene4-AminobiphenylAnilineAnthraceneAramiteBeazo(aWanthraceneBenzo(b)fluorantheneBenzo(k)fluorantheneBenzo(ghi)peryleneSenzo(a)pyreneBenzyl alcoholbis(2-Chloroethoxy)

methanebis(2-Chloroethyl)-

etherbis(2-Ethylhexyl)

phthalate4-Bromophenyl phenyl

etherButyl benzyl phthalate4-ChloroanilineChlorobenzilate4-Chloro-3-methylphenol2-Chloronaphthalene2-Chlorophenol4-Chlorophenyl phenyl

etherchryseneDiallateDibenz(a,h)anthraceneDibenzofuranDi-n-butyl phthalate1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-Dichlorobenzene

RESULTEDEDNDIDEDNDIDNDEDRDNDND

NDED

RPORMTILIMIT34034034034001600340340670340340340340340340340

ED 340

340ED

UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kg

ug/kg

ug/kg

ug/kgug/kgug/kguglkgug/kgug/kgug/kg


ND

NDNDNDNDNDNDND

340

340340340340340340340

NDNDEDRDEDND

ED]ND

340670340340340340340340


LOCKOOD GR

Client Sample ID: S-2

GC/MS Semivolatiles

Lot-&aWPle #...: D4D030176-001 Work Order U...: GDHQL1AC atrix ......... : SOLID

PARAMETER3,3'-Dichlorobenzidine2,4-Dichlorophenol2,6-DichlorophenolDiethyl phthalateDimetboate7,12-Dimethylben (a)-

anthracene3,3'-Dimethylbenzidine2,4-DimethylphenolDimethyl phtbalate1,3-Dinitrobenzene4,6-Dinitro-

2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-octyl phthalateDiphenylamineDisulfotonEthyl methanesulfonateFluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyclopenta-

dieneHexachloroethaneHexachioropropeneIndeno(1,2,3-cd)pyreneIsodrinI6ophoroneIsosafroleMethapyrilene3-MethylcholanthreneMethyl methanesulfonate2-MethylnaphthaleneMethyl parathion2-Methylphenol3-Methylphenol &

4-MethylphenolHaphtbalene1,4-Naphthoquinone

RESULTEDED

ND

ND

REPORTINGLIMIT1600340340670670670

EDNDEDEDPD

6703403403401600

IDEDNDNDEDNDNDNDVDNDEDIND

160034034034034016003403403403403401600

JNITS

ug/kgug/kgug/kgug/kgug/kgug/kg



ug/kgug/kgUg/kgug/kg

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgug/kgug/kg

EDNDNDNDNDIDNDNDNDNDNDIDID

340340034034034067016006703403401600340340

NDNDND

34016003401-Raphthylamine



GC/M$ Seuivolatiles

Lot-Sample #...: D4D030176-001 Work Order xI...: GDOQL1AC Hatr i .... : SOLID

PARAMETER2-Haphthylamine2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene2-Nitrophenol4-Nitrophenol4-Nitroquinoline-

l-oxideU-Nitrosodi-n-butylamineH-NitrosodiethylamineU-NitrosodimethylamineU-NitrosodiphenylamineN-Nitrosodi-n-propyl-

amineN-NitrosomethylethylamineK-NitrosomorpholineN-NitrosopiperidineN-Nitrosopyrrolidine5-Nitro-o-toluidineParathionPentachforobenzenePentachloroethanePentachloronitrobenzenePentachlorophenolPhenacetinPhenaithrenePhenolPhorate2-PicolinePronamidePyrenePyridine1,2,4,5-Tetrachloro-

benzene2,3,4,6-Tetrachlorophenol

Thionazino-Toluidine1,2,4-Trichloro-

benzene2,4,5-Trichloro-

phenol2,4,6-Trichloro-

phenol

RESULTN3lDNDNDNDNDEDND

REPORTINGLh:IT34016001600160034034016003400

IDlDNDNDND

340340340340340

NDND1DNDNDEDD

NDIDNDNDRDNDNDNDNDNDNDaD

3403403403406701600340160016001600670

3403401600670670340670340

UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kg


Ug/kgug/kgug/kgug/kgug/kg



ug/Icgug/kgug/kgug/kgug/kgug/Jcguglkg

ug/kgug/kgug/kg

ug/kgug/kg

NDNDNDED

16001600670340

340

ND 340


UXS0OD GRESM

Client Bample ID: ES-2

GC/HS Sezivolatiles

LOt-Sample #...t D4D030176-001 Work Order #...: GD0HQL1AC Matri....... s SOLID

PARAMETER.0,0, -Triethylphosphoro-

thioate1,3,5-Trinitrobenzene

RESULTND

REPORTING-LIMIT1600

UNITSug/kg

ug/kg1600

SURROGATE2-FluorophenolPhenol-dSNitrobenzene-dS2-Fluorobiphenyl.2,4,6-TribromophenolTerphenyl-d14

PERCENTRECOVPRY767575697179

RECOVERYLIMITS(28 - 95 )(35 - 90 )(39 - 89 )(35 - 86 )(11 - 111)(30 - 98 )

WOmE(S) XRb and ftpwq lim have ken WdW ro &Y wesk

E


GC/NS Semivolatiles

Lot-Sample C...: D4D030176-002 Work Order 0...:bate Sanpled.... 04/01/04 10:40 Date Received..:Prep Date...... 04/07/04 Analysis Date..:Prep Batch 1...: 4097621 Analysis Time..:Dilution Factor: 1

GDHQX1AC04/03/0404/22/0416:20

Matrix ... .: SOLID

Method ........ 8W846 8270C

PARAMETERAcenaphtheneAsenaphthyleneAcetophenone2-Acetylaminofluorene4-AminobiphenylAnilineAnthraceneAramite

en o (a)anthraceneBenzo(b)fluorantheneBenzo(k)fluorantheneBenzo(ghi)peryleneEenzo(a)pyreneBenzyl alcoholbis(2-Chloroethoxy)





etherChryseneDiallateDibenz(a,h)anthraceneDibenzofuranDi-n-butyl phthalate1,2-Dichlorobenzene1.3-Dichlorobenzene1,4-Dichlorobenzene

RESULTNDNDNDRDEDEDNDEDRDNDNDlDllDRDND

REPORTINGLIMIT33033033033001600330330670330330330330330330330

ED 330

ED 330

MTSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kg

ug/kg

ug/kg



330

RDNDNDNDNDNDND

330330330330330330330

]DIDNDEDNDEDNDND

330670330330330330330330


LKD GRM

Client Sample IDs SS-6

GCIMS Smivolatiles

. Lot-Sample 0...: D4D030176-002 Work Order #...s GDHQX1AC Hatrix ..... : SOLID

PAFAMER3,3'-Dichlorobenzidine2,4-Dichlorophenol2,6-DichlorophenolDiethyl phthalateDinethoate7,12-Dimethylbenz(a)-

anthracene3,3'-Dimethylbenzidine2,4-DimethylphenolDimetbyl phthalate1,3-Dinitrobenzene4,6-Dinitro-

2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-octyl phthalateDiphenylamineDisulfotonEthyl methanesulfonateFluorantheneFluoreneEexachlorobenzeneRexachlorobutadieneHexachlorocyclopenta-

dieneHexachloroetbaneHexachloropropeneIndeno(1,2,3-cd)pyreneIsodrinIsophoroneIsosafroleMethapyrilene3-MethylcholanthreneMethyl mnethanesulfonate2-MethylnaphtbaleneMethyl parathion2-Methylphenol3-Methylphenol &

4-MethylphenolNaphthalene1,4-NaphthoqiinoneI-Naphthylamine

RESULTlDlDDD

NDRD

ND


670

NDNDtDNDED

670

3303303301600

NDNDNDNDNDNDNDNDNDNDEDND

160033033033033016003303303303303301600

UNITSug/kgug/kgug/kgug/kgug/kg

ug/kg


ug/kgug/kguglkgug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kgug/kg


uglkgug/kgug/kgug/kgug/kgug/kgug/kg

uglkgug/kgug/kg

NDNDNDEDD

NDEDEDNDND

IDND

330330033033033067016006703303301600330330

NDNDED

3301600330



GC/hS Semivolatiles

Lat-Sample 0...: D4D030176-002 Work Order t...: tDHQX1AC Natrix ........ SOLID

PARM4T2-Kaphthylamine2-Nitroaniline3-Nitroaniline4-KitroanilineNitrobenzene2-Nitrophenol4-Nitrophenol4-Nitroquinoline-

1-oxideN-Nitrosodi-n-butylamineN-NitrooodiethylamineN-NitrosodimethylamineN-NitrosodiphenylamineX-Nitrosodi-n-propyl-

amineN-NitrosomethyletbylamineN-NitrosomorpholineN-NitrosopiperidineN-Nitrosopyrrolidine5-Nitro-o-toluidineParathionPentachlorobenzenePentachloroethanePentachloronitrobenzenePentachlorophenolPhenacetinPhenanthrenePhenolPhorate2-PicolinePronamidePyrenePyridine1,24, 5-Tetrachloro-

benzene2,3,4, 6-TetrachlorophenolThionazino-Toluidine1,2,4-Trichloro-


phenol

2,4,6-Trichloro-phenol

RESULTNDNDNDEDIDNDEDND

.REPORTINGLIMIT33016001600160033033016003300

EDNDIDEDED

330330330330330

UDNDNDEDNDNDNDNDED13DNDNDEDNDEDNDNDNDND

33033033033067016003301600160016006703303301600670670330670330

UNITSug/kguglkgug/kgug/kgug/kg

ug/kgug/kgug/kg


ug/kgugtkgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg


ug/kg

ug/kg

IDEDEDED

16001600670330

330

330


CNOD GR


GC/KS Semivolatiles

Lot-SaMple #...t D4D030176-002 Work Order *...: GDHQXIAC Matrix.........: SOLID

PARAMETER0,0,0-Triethylphosphoro-


RESUfLTIND

REPORTINGLIMIT1600

UNITSug/kg

ug/kgID 1600

SURR~OGATE2-Fluorophenolphenol-dSNitrobenzene-d52-Fluorobiphenyl2,4,6-TribromophenolTerphenyl-dl4


RECOVERYLIMITS(28 - 95 )(35 - 90 )(39 - 89 )

(35 - B6 )(11 - 111)(30 - 98 )

6679

NOTE(S):Rewtz wd rqenh4 Etsb Im t= sawd for ft w2I.

Client Sample mD: SS-9

GCIKMSeiotle

Lot-Sample 0 ... sDate Sampled ... :Prep Date ...... tPrep Batch t ... sDilution Factort

D4D030176-00304/01/04 15:1504/07/0440976211

Work Order 0...:Date Received..:Analysis Date..:Analysis Time..:

GDHQOlAC04/03/0404/22/0416:47

Hatrir ........ z SOLID

Method ..... SW846 8270C

PARAMETERAcenaphtheneAcenaphtbyleneAcetophenone2-Acetylaminofluorene4-AmninobiphenylAnilineAnthraceneAramiteBenzo(a)anthraceneBenzo(b)fluorantheneBenzok) fluorantheneBenzo(ghi peryleneBenzo(a)pyreneBenzyl alcoholbio(2-Chloroethoxy)

methanebisl2-Chloroethyl)-



etherButyl benzyl phthalate4-Chloroanilinechlorobenuilate4-Chloro-3-methylphenol2-Chloronaphthalene2-Chlorophenol4-Chlorophenyl phenyl

etherChryseneDiallateDibenz(ah)anthraceneDibenzofuranDi-n-butyl phthalate1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-Dichlorobenzene

RESULIIDNDNDNDNDNDJDNDNDIDSDEDIDlDND

REPORTINGLIMIT33033033033001600330330670330330330330330330330

ND 330

1D 330

UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/igug/kgug/kgug/kgug/kgug/kgug/kg

ug/kg

ug/kg

ug/kg



ND 330

*EDEDEDEDEDEDND

330330330330330330330

RDEDNDEDNDNDED

ND

330670330330330330330330



GC/hS enlatles

Work Order #...: GDHQO1ACLot-SamPle #...: D4D030176-003 MatriX ..... : SOLID

3,3'-Dichlorobenzidine2,4-Dichlorophenol2,6-DichlorophenolDiethyl phthalateDimethoate7,12-Dimethylbenz(a)-

anthracene3,3'-Dimethylbenzidine2,4-DimethylphenolDimethyl phthalate1,3-Dinitrobenzene4,6-Dinitro-

2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDL-n-octyl phthalateDiphenylamineDisulfotonEthyl methanesulfonateFluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyclopenta-

dieneNexachloroethaneHexachloropropeneIndeno(1,2,3-cd)pyreneIodrinIsophoroneIsosafroleMethapyrilene3-MethylcholanthreneMethyl methanesulfonate2-MethylnaphthaleneMethyl parathion2-Metbylphenol3-Methylphenol &

4-MethylphenolNaphthalene -1,4-Naphthoquinonel-Naphthylamine

RESULTODtDNDEDEDND

REPORTINGLIMT1600330330670670670

EDVDNDNDND

6703303303301600

NDNDEDNDEDNDEDNDRDNDNDED

160033033033033016003303303303303301600

UNITSug/kgugfkgug/kgug/kgug/kgug/kg

ug/kgugfkgug/kgug/kguglkg

ug/kgug/kgug/kg

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/ksug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgug/kgug/kg

NDNDNDNDNDNDND

NDNDNDNDlDND

330330033033033067016006703303301600330330

lNDNDND

3301600330


LOWD GR

Client sazwle ID: ss-9

GC/MS Semivolatiles

lot-S8ample #...: D4D030176-003 Work Order t...: GDHQOIAC Matrr ......... z SOLID

PAMMER2-Naphthylamine2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene2-Nitrophenol4-Nitrophenol4-Nitroquinoline-

l-oxideN-Nitrosodi-n-butylamineN-HitrosodietbylamineN-NitrosodimethylamineN-NitrosodiphenylamineN-Nitrosodi-n-propyl-

amineN-NitrosomethylethylamineN-NitrosomorpholineN-NitrosopiperidineN-Nitrosopyrrolidine5-Nitro-o-toluidineParathionPentachlorobenzenePentachloroethanePentachloronitrobenzenePentachlorophenolPhenacetinPhenanthrene.PhenolPhorate2-PicolinePronamidePyrenePyridine1,2,4,5-Tetrachloro-

benzene2,3,4,6-TetrachlorophenolThionazino-Toluidine1,2,4-Trichloro-



phenol

RESULT

NDNDNDNDNDNDNDVD

REPORTINGLIMIT33016001600160033033016003300

EDNDEDNDND.

330330330330330.

NDVD

ND

ND

ND

ND

NDND

NDND

ND

ND

ND

ND

ND

21DND

ND

ED

33033033033067016003301600160016006703303301600670670330670330

Unms



ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgugfkgug/kgug/kgug/kgug/kgug/kgug/kgug/kg


ug/kg

ug/kg

EDEDND

ND

16001600670330

330

ND 330


Clent Sample ZD: SS-9

Ga/NS Semivolatiles

Lot-Sample 1 ... : D4D030176-003 Work: Order 0.... s GDHQO1AC Hatrix......... : SOLID

PARAMETER00, O-Triethylphosphoro-

thioate1, 3,5 -Trinitrobenzene

RESULTND

REPORTINQLIMIT1600

MTSug/kg

ug/kgND 1600

SURROGATE2-PluoropheiolPhenol-dsNitrobenzene-d52-Fluorcbiphenyl2,4, 6-TribromophenolTerphenyl-d14


RECOVERYLIMITS(29 - 95 )(35 - 90 )

(39 - 69 )(35 - 86 )(11 - 111)(30 - 98 )

MOE(S) @Rem and prt g riks hame bee mjsod ftw dq WihL

LOslrOOD GR


GC/S semidvolatiles

Lot-Sample 0... sDate Sampled ... :Prep Date ...... :Prep Batch #...:Dilution Factors

D4D030176-00404/01/04 10:0004/07/0440976211

Work Order #...:Date Received..:Analysis Date..:Analysis Time..:

GDHQ1lAC04/03/0404/22/0417:13

Matrix .... a SOLID

Method .... *....z SW846 8270C

PARAMETERAcenaphtheneAcenaphthyleneAcetophenone2-Acetylaminofluorene4-AminobiphenylAnilineAnthraceneAramiteBenzo (a)nthraceneSenyo (b) fluorantheneBenzo(k)fluorantheneBenzo(ghi)peryleneBenzo(a)pyreneBenzyl alcoholbis(2-Chloroethoxy)




etherButyl benzyl phthalate4 -hloroanilineChlorobenzilate4-Chloro-3-metbylphenol2-Chloronaphthalene2-Chlorophenol4-Chlorophenyl phenyl

etherChryseneDiallateDibenz(a,h)anthraceneDibenzofuranDi-n-butyl phthalate1,2-Dichlorobenzene1,3-Dichlorobenzene

RESULTVDND

*NDNDNDNDNDNDNDNDNDEDNDNDND

REPORTINGLIMIT33033033033001600330330670330330330330330330330

ND 330

ND 330


ug/kg

ug/kg

ug/kg



ND 330

IDNDNDNDNDNDND

330330330330330330330

NDNDNDNDIDNDNDND

3306703303303303303303301,4 -Dichlorobenzene


client Sauple ID: CS-1l

6c/MS ivlatlen

Lot-Sample U...a D4D030176-004 Work Order #. .. GDHQI1AC Matri .... SOLID

PARMETER3,3'-Dichlorobenzidine2,4-Dichlorophenol2,6-DichlorophenolDiethyl phthalateDimethoate7,12-Dimethylbenz(a)-

anthracene3,3'-Dimethylbenzidine2.4-DimethylphenolDimethyl phthalate1,3-Dinitrobenzene4,6-Dinitro-

2-methylphenol2,4-Dinitrzphenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-octyl phthalateDiphenylamineDisulfoton,Ethyl methanesulfonateFluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyclopenta-

dieneHexachloroethaneHexachloropropeneIndeno(1,2,3-cd)pyreneIsodrinIsophoroneIsosafroleMethapyrilene3-MethylcholanthreneMethyl methanesulfonate2-MethylnaphthaleneMethyl parathion2-Methylphenol3-Methylphenol &

4-KethylphenolNaphthalene1,4-Naphthoquinone

I-Naphthylamine

RESULTlNDEDNDNDEDND


UNITSug/kgug/kgug/kgug/kgug/kguglkg

NDNDNDNDND

6703303303301600

NDNDEDNDNDNDNDNDNDND

EDND

1600330.33033033016003303303303303301600

ug/kgug/kgug/kguglkgug/kg

ug/kgug/kgug/kgug/kguS/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgug/kgug/kg

ND

RD

ED

ND

ND

NDND

ND

ND

ED

JIDND

ND

330330033033033067016006703303301600330330

NDND

ND

3301600330



GC/kS semivolatiles

Lot-Sample *...: D4D030176-004 Work Order #...s GDHQ11AC Katri ......... SOLID

PARAM1ETER2-uaphthylamine2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene2-Nitrophenol4-Nitrophenol4-Nitroquinoline-

1-oxideN-Nitrosodi-n-butylamineN-NitrosodiethylamineN-NitrosodimethylamineN-NitrosodiphenylamineN-Nitrosodi-n-propyl-

amineN-NitrosomethyletbylamineN-NitrosomorpholineN-NitrosopiperidineN-Nitrosopyrrolidine5-Nitro-o-toluidineParathionPentachlorobenzenePentachloroethanePentachloronitrobenzenePentachlorophenolPhenacetinPhenanthrenePhenolPhorate2-PicolinePronamidePyrenePyridine1,2,4,5-Tetrachloro-




phenol

RESULTNDNDND

NDMDND

EDED

REPORTINGLIMIT33016001600160033033016003300

MDEDMD

NDWD

330330330330

330

NDHDNDEDEDNDNDNDNDXDIDNDNDVDNDNDNDNDND

33033033033067016003301600160016006703303301600670670330670330



ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg


ug/kg

ug/kg

NDND

NDND

1600

1600670330

ED 330

330



GCiMS evolaes

Lot-Sample #...: D4D030176-004 Work Order O...: GDHQ11AC Matrix .... : SOLID

PARAMETER00, O-Triethylphosphoro-

thioate1,3, 5-Trinitrobenzene

RESULTND

REPORTINGLIMIT1600

UNITSug/kg

ug/kgND 1600

SURROGATE2-FluorophenolPhenol-d5Nitrobenzene-ds2-Fluorobiphenyl2,4,6-TribromophenolTerphenyl-d14

PERCENTRECOOVRY747574677075

RECOVERYLIMITS(28 - 95 )(35 - 90(39 - 89 )(35 - 86 )(11 - 111)(30 - 98 )

NOTE(B) sRmft azid zeps H have bfen dusd for ft %*kL

wacD GRE


Cc/Hs Semivolatiles

Lot-Sample C...:Date Sampled...:Prep Date ...... :Prep Batch #...:Dilution. Factor:

D4D030176-00S04/01/04 15:4004/07/0440976211

Work Order 0. . . tDate Received..:Analysis Date..:Analysis Time. . :

GDHQ21AC04/03/0404/22/0417:40

Matrix ..... : SOLID

Method ..... SW846 8270C

PARAMKERAcenaphtheneAcenaphtbyleneAcetophenone2-Acetylaminofluorene4-AminobiphenylAnilineAnthraceneAramiteBenzo (a)anthraceneBenzo(b)fluorantheneBenzo(k) fluorantheneBenzo(ghi)peryleneBenzo(a)pyreneBenzyl alcoholbis(2-chloroethoxy)

methanebis (2-Chloroethyl) -


phthalate4-Sromophenyl phenyl


etherChryseneDiallateDibenz(a,h)anthraceneDibenzofuranDi-n-butyl phthalate1,2-Dichlorobenzene1,3 -Dichlorobenzene1,4-Dichlorobenzene

RESULT

NDNDiDNDNDNDED

IDNDNDNDEDNDED

REPORTINGLIMIT34034034034001600340340670340340340340340340340

340

ND 340


ug/kg

ug/kg

ug/kg


ug/kgug/kg


ug/kgug/kg

ND 340

NDEDEDEDED2DND

140340340340340340340

NDNDWD21DNDND

ND

ND

340670340340340340340

340


Client Sample ID: &S-12

GC/NS Semivolatiles

Wot-SamPle 0...s D4D030176-005 Work Order #...: 0)HQ21AC Matrix . . s SOLID

PARAMETER3,31-Dichlorobenzidine2,4-Dichlorophenol2,6-DichlorophenolDiethyl phthalateDimethoate7,12-Dimethylbenz(a)-


2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-octyl phthalateDiphenylamineDisulfotonEthyl methanesulfonateFluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneEexachlorocyclopenta-

dieneHexachloroetbaneNexachloropropeneIndeno(1,2,3-cd)pyreneIsodrinIsophoroneIsosafroleMethapyrilene3-MethylcholanthreneMethyl methanesulfonate2-MethiylaphthaleneMethyl parathion2-Methylphenol3-Methylphenol L

4-Methylphenol

Naphthalene1,4-Naphthoquinonel-Naphthylamine

RESULTNDNDRDVDNDND


NDNDNDNDED

6703403403401600

NDNDNDNDNDNDNDNDND

NDNDND

160034034034034016003403403403403401600

UWITSug/kgug/kgug/kgug/kgug/kgug/kg


ug/kg


us/kgug/kgug/kgug/kgug/kgug/kg

uglkgug/kg

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgug/kg

ug/kg

EDNDNDNDNDEDNDNDNDNDNDNDND

340340034034034067016006703403401600340340

NDNDND

3401600340



GC/MS Semivolatiles

Lot-Sample 0...: D4D030176-005 Work Order #...: GDHQ21AC Hatr ..... : SOLID

PARAMETER2-Naphthylamine2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene2-Ritrophenol4-Nitrophenol4-vitroquinoline-

I-oxideN-Nitrosodi-n-butylamineN-NitrosodiethylamineN-NitrosodimethylamieN-UitrooodiphenylamineN-Nitrosodi-n-propyl-

amineN-NitrosomethylethylamineN-NitrosomorpholineR-NitrosopiperidineN-Nitrosopyrrolidine5-Nitro-o-toluidineParathionPentachlorobenzenePentachloroethanePentachloronltrobenzenePentachlorophenolPhenacetinPhenanthrenePhenolPhorate2-PicolinePronamidePyrenePyridine1,2,4,5-Tetrachloro-




phenol

RESULTEDEDEDNDNDNDNDND

REPORTINGLIMIT

3401600

1600160034034016003400

NDNDNDNDND

340

340340340340

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

34034034034067016003401600160016006703403401600670670340670340



uglkgug/kgug/kgug/kgug/kg

ug/kgug/kg

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgus/kgug/kgug/kgug/kg


ug/kg

ug/kg

NDNDNDND

16001600670340

340

340



GC/MS Semivolatiles

LOt-S0amle #...s D4DO30176-005 work Order #... t GQ2 1AC Matrix ........ : SOLID

PARAMETE

0,0, 0-Trietbylphosphoro-thloate

1,3, 5-Trinitrobenzene

RESULTND

REPORTINGLD1IT1600

UNITSug/kg

ug/kgKD 1600

SURROGATE2-FluorophenolPhenol-dSNitrobenzene-d52-Fluorobiphenyl2,4, 6-TribromophenolTerphenyl-dI4

PERCENT

RECOVERY757575697281

RECOVERYLIMITS(28 - 95 )(35 - 90 )

(39 - 89 )(35 - 86 )(11 - 111)(30 - 98 )

OTE(S):Rm Fonwimtfs have been Justed for dtyw

UCD GREE

Client Sapple ID: SS-13

GC/hS Semivolatiles

Lot-Sanple # ... : D4D030176-006Date Sampled ... : 04/01/04 16:10Prep Date ...... s 04/07/04Prep Batch 1... : 4097621Dilution Factor: 1

Work Order Q. ..Date Received..:Analysis Date..:Analysis Time.. :

GDH231AC04/03/0404/22/0418:07

Matrix .... : SOLID

Method .. . 81(846 8270C

PARAM R

Acenaphthene*Acenaphthylene

Acetophenone2-Acetylaminofluorene4-AminobiphenylAnilineAnthraceneAramiteBenzo(a)anthraceneBenzo(b)fluorantheneBenzo(k)fluorantheneBenzo(ghi)peryleneBenzo(a)pyreneBenzyl alcoholbis(2-Chloroethoxy)




etherButyl benzyl phthalate4-ChloroanilineChlorobenzilate4-Chloro-3-methylphenol2-Chloronaphthalente2-Chlorophenol4-Chlorophenyl phenyl

etherChryseneDiallateDibenz(a,h)anthraceneDibenzofuranDi-n-butyl phthalate1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-Dichlorobenzene

RESULTNDEDEDEDNDNDEDNDEDNDNDNDEDEDND

REPORTINGLIMIT33033033033001600330330670330330330330330330330

330

330

UNITSuglkgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kcg

ug/kg

ug/kg



ND 330

NDNDNDNDMDImND

330330330330330330330

NDNDEDNDNDNDNDND

330670330330330330330330


Client Sanple mD: SB-13

6c4s Semivolatiles

ot-Sample I...2 D4D030176-006 Work Order #...: GDEQ31AC Matrix .. .: SOLID

PARAMETER3,3'-DJ.chlorobenzidine2,4-Dichlorophenol2,6-DichlorophenolDiethyl phthalateDimethoate7,12-Dimetbylbenz(a)-


2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-octyl phthalateDiphenylamineDioulfotonEthyl methanesulfonateFluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyclopenta-

dieneRexachloroetbaneRexachloropropeneIndeno(l,2,3-cd)pyreneIsodrinIsophoroneIsosafroleMethapyrilene3-MethylcholantbreneMethyl methanesulfonate2-MetbylnaphthaleneMethyl parathion2-Methylphenol3-Metbylphenol &

4-MethylphenolNaphthalene1,4-Naphthoquinonel-Naphthylamine

RESULTNDNDNDNDEDND


MD2DNDNDND

6703303303301600

NDNDNDNDNDIDNDRDNDNDNDHD

160033033033033016003303303303303301600

WNITSug/kgug/kgug/kgug/kgug/kguglkg


ug/kgugtkgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgugfkgug/kgug/kgug/kg

ug/kgug/kgug/kg

NDNDNDNDNDNDNDNDBDNDEDNDND

330330033033033067016006703303301600330330

NDNDND

3301600330


Client Sample IDt ES-13

aclks Senivolatiles

Lot-&ample #...a D4D030176-006

PAAMWETER2 -Naphthylamine2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene2-Nitrophenol4-Nitrophenol4-Nitroquinoline-

Work order t...: GDHQ31AC

RESULTEDNDNDNDNDNDNDND

REPORTINGLIMIT33016001600160033033016003300


UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgl-oxide

N-Nitrosodi-n-butylamineN-NitrosodiethylrineN-NitrosodimetbylamineK-NItrosodiphenylamineN-Nitrosodi-n-propyl-

amine,N-NitrosaometbylethylamineN-NitrosomorpholineN-NitrosopiperidineV-Nitrosopyrrolidine5-NJitro-o-toluidineParathionPentachlorobenzenePentachloroethanePentachloronitrobenzenePentachlorophenolPhenacetinPhen~athrenePhenolPhorate2-PicolinePronamidePyrenePyridine1,2,4,5-Tetrachloro-


benzene2,4,5-TrichLoro-


phenol

NDNDNDNDND

330330330330330

NDNDNDNDNDlDNDNDNDNDNDNDNDNDNDNDNDEDED

330330330

3306701600330160016001600670330330

1600670670330670330


Ug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgug/kguglkgug/kg

ug/kg

ug/kg

NDNDEDND

16001600670330

ED 330

330ED



GC/MS Semivolatiles

Lot-SaMple I...a D4D030176-006 Work Order 0...: GDHQ31AC Matrix .... : SOLID

RESULTREPORTINGLIMIT1600

ag - - c--oo-

0,0,0-Triethylphosphoro-thioate

1,3,5-Trinitrobenzene

UNITSug/kg

ug/kgND 1600

SURROGATE2-FluorophenolPhenol-dSMitrobenzene-dS2-Fluorabiphenyl2,4,6-TribromophenolTerphenyl-d14


RECOVERYLIMITS(28 - 95 )(35 - 90 )(39 - 89 )(35 - 86 )(11 - 111)(30 - 98 )

Rehdt and cepoftqdng Minkm bcco asmnd for wdrbL


GC/HS semivolatiles

Lot-Sample #...: D4D030176-007Date Sampled-: 04/01/04 13:10Prep Date ...... s 04/07/04Prep Batch #...t 4097621Dilution Factors 1

Work Order t...:Date Received..:Analysis Date..:Analysis Time..:

GDHQ4 lAC04/03/0404/22/0418:33

Matrix .... s 8OLID

Method ... .: 6W846 8270C

PARAMETERAcenaphtheneAcenaphthyleneAcetophenone2-Acetylaminofluorene4-AminobiphenylAnilineAnthraceneAramiteBenzo(a)anthraceneBenzo (b) fluorantheneBenzo(k)£luorantheneBenzo(ghi)peryleneBenzo(a)pyreneEenzyl alcoholbis(2-Chloroethoxy)


etherbis(2-Ethyihexyl)

phthalate4-8romophenyl phenyl


etherChryseneDiallateDibenz (a,h)anthraceneDibenzofuranDi-n-butyl phthalate1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-Dichloroben ene

RESULTNDNDNDEDNDNDNDNDNDNDNDNDNDNDND

REPORTING

LIMIT33033033033001600330330670330330330330330330330

ED 330

ND 330


ug/kg

ug/kg

ug/kg



ND 330

EDlDNDNDNDNDND

330330330330330330330

NDNDVDNDNDNDND2D

330670330330330330330330



GC/hs Semivolatiles

Lot-Saizple #...: D4D030176-007 Work Order #...g GDHQ41AC HatriX .. .. : SOLID

PARAMETER3,3'-Dichlorobenzidine2,4-Dichlorophenol2,6-DichlorophenolDiethyl phthalateDimethoate7,12-Dimethylbenz(a)-

anthracene3,31 -Dimethylbenzidine2,4-DitnethylphenolDimethyl phthalate1,3-D W trobenzene4,6-Dinitro-

2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-octyl phthalateDiphenylamineDivulfotonEthyl methanesulfonateFluorantheneFluoreneNexachlorobenzeneHexachlorobutadieneRexachlorocyclopenta-

dieneHexachloroethaneHexachloropropene

RESULTNDNDNDNDNDND


NDNDNDNDND

6703303303301600

NDNDlDNDEDNDNDNDNDNDEDND

160033033033033016003303303303303301600


us/kgug/kgug/kgu1/kgug/kg



ug/kgug/kgug/kg

Indeno(1,2,3-cd)pyreneIsodrinIsophoroneIsosafroleMethapyrilene3-MethylcholanthreneMethyl methanesulfonate2-MethylnaphthaleneMethyl parathion2-Methylphenol3-Methylphenol &

4-MethylphenolNaphthalene1,4-Naphthoquinonel-Naphthylamine

NDNDNDND

21DND

ND21DND

NDND

ND11D

330330033033033067016006703303301600330330

NDNDND

3301600330


Client Sample ID: BS-15

GC/MS Semivolatiles

Lot-SaMple 2...: D4D030176-007

PARAMETER2-Naphthylamine2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene2-Nitrophenol4-Nitrophenol4-Nitroquinoline-

l-oxideN-Nitrooodi-n-butylamineN-NitrosodiethylamineN-NitrosodimethylamineN-NitrosodiphenylamineN-Nitrosodi-n-propyl-

amineU-NitrosomethylethylamineN-NitrosomorpholineN-VitrosopiperidineN-NitrosopyrrolidineS-Nitro-o-toluidineParathionPentachlorobenzenePentachloroethanePentachloronitrobenzenePentachlorophenolPhenacetinPhenanthrenePhenolPhorate2-PicolinePronamidePyrenePyridine1,2,4,5-Tetrachloro-




phenol

work Order g...: GDHQ41AC

RESULTNDNDNDPDNDEDEDND

REPORTINGLIMIT33016001600160033033016003300

IDIDEDEDED

330330330330330

EDlND2DNDNDNDNDNDtDNDEDEDEDEDEDNDEDEDND

3303303303306701600

3301600160016006703303301600670670330670330

Matri.i.. . -SOLID



ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg


ug/kg

NDEDNDED

16001600670330

330

ND 330

(Continued oan next page)

BAWDO G-R


GC/NS Semivolatiles

1ot-gample U...2 D4D030176-007 Work Order I... : GDH41AC MatriX .... : SOLID

,0,0,0-Triethylphosphoro-thioate


RESULTND

REPORTINGLIMIT UNITS1600 ug/kg

ND 1600 ug/kg

2-FluorophenolPhenol-d5Nitrobenzene-dS2-Fluorobiphenyl2,4,6-TribromophenolTerphenyl-dH4

N0TE(S):


RECOVERY

(28 - 95 )(35 - 90 )(39 - 89 )(35 - 86 )(11 - 111)(30 - 98 )

legui Wd ipordz Infhavebeen asWdf~rdiywd~bt


aC/MS Semivolatiles

lot-Sample C.. .sDate S.amp... .2Prep Date ...... sPrep Batch #... sDilution Factor:

D4D030176-00804/01/04 14:4004/07/0440976211

Work Order ... :Date Received..Analysis Date..:Analynis Time..s

GDHQ51AC04/03/0404/22/0419:00

Matrix. ...... s SOLID

Method ......... iSW846 8270C

PARAMETER

AcenaphtheneAcenaphtbyleneAcetophenone2-Acetylaminofluorene4-AminobiphenylAnilineAnthraceneAramiteBenzo ()anthraceneBenzob) fluorantheneBenzo (kfluorantheneBenzo(ghi)peryleneBenzo(a)pyrcneBenzyl alcoholbis(2-Chloroetboxy)


etherbis(2-Etbylhexyl)


etherButyl benzyl phthalate4-ChloroanilineChlorobenzilate

RESULTRD

RDNDNDRDWDNDNDNDRDNDNDRDNDRD

REPORTINGLIMIT33033033033001600330330670330330330330330330330

ND 330

ND 330


ug/kg

ug/kg

ug/kg

ugfkgug/kgug/kgug/kgug/kgug/kgug/kg


ND 330

4-ChlOro-3-methylphenol2-Chloronaphthalene2-Chlorophenol4-Chlorophenyl phenyl

etherChryseneDiallateDibenz(ah)anthraceneDibenzofuranDi-n-butyl phthalate1,2-Dicblorobenzene1,3-Dichlorobenzene1,4-Dichlorobenzene

NDRDNDNDRDEDED

330330330330330330330

VDlDNDNDRDNDlDED

330670330330330330330330



GC/kS Semivolatiles

Lot-Sample ... * D4D030176-008

PARAMTER3,3'-DiCblorobenzidine2,4-Dichlorophenol2,6-DichlorophenolDiethyl phthalateDimethoate7,12-Dimethylbenz(a)-

anthracene3,3'-Dimethylbenzidine2,4-Dimethylphenol

Dimethyl phthalate1,3-Dinitrobensene4,6-Dinitro-

2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-octyl phthalateDiphenylamineDisulf otonEthyl methanesulfonateFluorantheneFluoreneNexachlorobenzeneEexachlorobutadieneNexachlorocyclopenta-

dieneHexachloroethaneRexachloropropeneIndeno(1,2,3-cd)pyreneIsodrinIsophoroneIsosafroleMethapyrilene3-MethylcholanthreneMethyl xetbanesulfonate2-MethylnapbthaleneMethyl parathion2-Methylphenol3-Methylphenol &

4-MethylphenolVaphtbalene1,4-Naphthoquinonel-Naphthylamine

Work Oder #...: GHAC

RESULTNDNDNDNDNDED

REPORTINGLIMIT

1600330330670670670

NDNDEDEDED

6703303303301600

NDEDNDWDND

NDNDNDVDHDNDND

160033033033033016003303303303303301600

MatriX ..... : SOLID

UNITS

ug/kguglkgug/kgug/kgug/kgug/kg




ug/kgug/kgug/kg

NDEDEDNDNDNDNDNDNDNDNDNDND

330330033033033067016006703303301600330330

NDND

ND

3301600330


C GRR

Client 8agple mD: 8S-16

GC/HS Semivolatiles

Lot-Sample #...: D4D030176-008 Work Order I.... GDHQSlAC Hatris ..... : SOLID

PARAMERTER2-Naphthylamine2-Nitroanlline3-Nitroaniline4-NitroanilineNitrobenzene2-Nitrophenol4-Nitraphenol4-Nitroquinoline-

I-oxideN-Nitrosodi-n-butylamineN-NitrosodiethylamineN-NitrosodimetbylamineN-NitrosodiphenylamineN-Nitrosodi-n-propyl-

amineU-NitrosomethylethylamineN-NitrosomorpholineN-NitrosopiperidineN-Nitrosopyrrolidine5-Nitro-o-toluidineParathion ,PentachlorobenzenePentachloroethanePentachloronitrobenzenePentachlorophenolPhenacetinPhenanthrenePhenolPhorate2-PicolinePronamidePyrenePyridine1,2,4,5-Tetrachloro-


benzene2,4,5-Tricbloro-


phenol

RESULTNDNDNDNDND

NDMD

REPORTING

3301600

160033033016003300

EDNDNDNDIRD

330330330330330

NDND17DNDNDNDNDNDNDNDNDNDVDNDNDNDNDNDND

33033033033067016003301600160016006703303301600670670330670330



ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgug/kgug/kg


ug/kg

ug/kg

NDNDIDND

16001600670330

330

ND 330


1OCO -


GC/MS Evolaes

Lot-Sample I...: a4D030176-008 Work Order #...: GDHQ51AC Matrix.........: SOLID

PARAMETER0,0, 0-Triethyiphosphoro-


RESULTND

REPORTINGLIMIT1600

UNITSug/kg

ug/kgND 1600

SURROGATE2-Fluorophemol

Phenol-d5Kitrobenzene-ds2-Fluorobiphenyl2,4,6-'TribromophenolTerphenyl-dU4

PERCENTRECOVERYCs

6867636476

RECOVERYLIMITS(28 - 95 )(35 - 90 )(39 - 89 )(35 - 86 )(11 - 111)(30 - 98 )

loTE(a):Rat su rqctg im kae beem Wdjus for dzy wdegbt

Client Samnle ID: S.-2

OCSnvoaie

Wat-Sample t... : D4D030176-001Date Sampled...s 04/01/04 12:30Prep Date ...... s 04/06/04Prep BatcI #... : 4096552Dilution Factor: 1

Work Order #...:Date Received..:Analysis Date..:Analysis Time..

GDHQLMAD04/03/0404/24/0404:06

matrix ..... SoLID

Method .... :. SW46 8081A

Aldrinalpha-BECbeta-BHCdelta-EECgamm-BEC (Lindane]Chlordane (tecbnia4,4'-DDD4,4'-DDE4,4'-DDTDieldrinEndrin

Endrin aldehydeEndosulfan IEndosulfan IIEndosulfan sulfateReptachlorHeptachlor epoxldeHethoxychlorToxaphene

I11)

RESULTHDNDNDHDNDHDNDNDNDNDNDND

NDNDEDNDNDNDNID

REPORTING

1.71.71.71.71.7171.71.71.71.71.71.71.71.71.71.71.73.4170

UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgus/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

SURROGATEDecachlorobiphenylTetrachloro-m-xylene

PERCfETRECOVERY82101

RECOVERYLIMTS(41 - 142)(50 - 127)

NOTHE(S):mb mg *epornAg Inihs hme ber a4jused br diy vcfh.

Client Sample ID: S8-6

GC sezivolatiles

Lot-Sample 8...:Date Sampled...:Prep Date ...... :Prep BatC .... sDilution Fator:

D4D030176-00204/01/04 10:4004/06/0440965521

Work Order t... sDate Received..Analysis Date..:Analysis Time..:

GDHQX1AD04/03/0404/24/0404:35

Matrix ......... : SOLID

Method . .... s W846 808LA

Aldrinalpha-BECbeta-BHCdelta-EHCgamma-BHC (Lindane)Chlordane (technical)4,4'-DMD4,4'-DDE4,4 -DDTDieldrinErerinEndrin aldehydeEndosulfan IEndosulfan !!Endosulfan SulfateHeptachlorIZeptachlor epoxideMethoxychlorToxaphene

RESULTEDNDIDND1IDND0.44 J,TLNDNDVDNDNDNDNDEDNDVDNDND

REPORTINGLIMIT1.71.71.71.71.7171.71.71.71.71.71.7

1.71.71.71.71.73.3170

UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

SURROGATE

DecachlorabiphenylTetrachloro-m-xylene

PERCERTRECOVERY8499

RECOVERYhIMITS(41 - 142)(50 - 127)

MOTE (S):Ieb ad aponWg Nits h be aKhwd AVdy Wcga.

I Estimated rslt. R s t is km don IL.COL Mom4 E. 40% VD etwn pkn nd audmaw *lU= nsul. Ue lwe Of to MO b s NPOtd.

Client Sample ID: 8s-9

GC Semivolatiles

Lot-Sawple C...: D4D030176-003 Work order P...:Date Sampled ... : 04/01/04 15:15 Date Received..:Prep Date ...... s 04/06/04 Analyois Date..:Prep Batch 4 ... s 4096552 Analysis Time..:Dilution Factors 1

GDHQOlAD04/03/0404/24/0405:04

Matrix ....... : OLID

Method.........: SW846 808A

PARAMETERAldrinalpha-BHCbeta-BBCdelta-BHCgamma.-BHC (Lindane:Cblordane (technic,4,44 -W_4,4 '-DDE4,4' -DDTDieldrinEndrinEndrin aldehydeEndosulfan IEndosulfan IIEndosulfan sulfateReptachlorHeptachlor epoxideMethoxychlorToxaphene

3.1)

RESULTNDNDNDNDNDND0.39 67,cJLNDNDNDNDNDEDlNDNDNDNDNDND

REPORTINGLIMIT1.71.71.71.71.7171.71.71.71.71.71.71.71.71.71.71.73.3170





NOTe (S)Rms ad xcp=Wg imhs lua bom mdjusted Slrdy wdglI.

I EF ftu LW ksdt I es k IdRL

COL =r dun 40% RFD belwec prkuq and onrHmado colum euits. The bwe of lhe wo rmb k upomd.

Client Sample m: ES-1l

6C Semivolatiles

Lot-Sample C...:Date Sampled...:Prep Date ..... aPrep Batch #...:Dilution Factort

D4D030176-004 Work order # ... z04/01/04 10:00 Date Received..:04/06/04 Analysis Date..:4096552 Analysis Time..:1

GDHQ11AD04/03/0404/24/0405:32

atrit......... : SOLID

Metbod . .: sBW846 80BIA

PARAMETERAldrinaipha-BECbeta-SHCdelta-BSCgamma-BEC (LindanelChlordane (tecbnici4,4' -DDD4,4'-DDE4,4'-DDTDieldrinEndrinEndrin aldehydeEndosulfan IEndosulfan 1IEndosulfan sulfateHeptachlorReptachlor epoxideMethoxychlorToxaphene

LI)

RESULTNDNDEDNDEDED0.79 TCOLNDEDNDNDEDNDNDNDEDNDNDID

REPORTINGIMI1.71.71.71.71.7171.71.71.71.71.71.71.71.71.71.71.73.3170


SURROGATE

DecachlorobiphenylTetrachloro-m-xylene

PERCENTRECOVERYE399

RECOVERYLUIITS(41 - 142)(50 - 127)

lO= (S):uks aod mpot ENadu kme been u6W 1fo y wdght

I Ednntrd XR= hu g L

O LL Mm tin 40% RFD ben puz cam wnfatn coma rSe TM owe of ti M reums Is UePO

COD GRIM

Client Sanple ID: S5-12

¢C Sedivolatiles

Lot-Sanple #...:Date Sampled...:Prep Date ...... :Prep Batch #...:Dilution Factor:

D4D030176-00504/01/04 15:4004/06/0440965521

Work arder 6...:Date Received..:AnalysiS Date..:Analysie Time..:

GDHQ21lD04/03/0404/24/0406:01


Method ..... 8W846 8082A

PA=AMETERAldrinalpha-BECbeta-BECdelta-BECgamna- -EC (Lindane)Chlordane (technical)

4,4' -D._4,4'-DDE4,4' -DDTDieldrinEndrinEndrin aldehydeEndosulfan IEndosulfan IIEndosulfan sulfateKeptachlorReptachlor epoxideMethoxychlorToxaphene

RESULT

NDNDNDNDNDND

ND0.65 J,COLEDNDNDNDDD

NDNDNDNDNDNDND

REPORTINGLIMIT1.71.71.71.71.7171.71.71.71.71.71.71.71.71.71.71.73.4170

UNITS

ug/kgug/kgug/kg



ug/kgug/kgug/kg

SURROGATEDecacalorobiphenylTetrachloro-m-xylene



NIOT(s):

R8It wd fepofiq Iit hmac be= 4usd frdry wegbrt.I EPldre raiz. Remuk I kss kn i RL

COLMmV gm111 40% RPD bcw h prhlh awd ewimonf chumm fhc Dhe Iowaofe tw Mcut s k fL

LON RM


GC Semivolatiles

Lot-Sample t...: D4D030176-006Date 8arpled...s 04/01/04 16:10Prep Date ...... s 04/06/04Prep Batch #...s 4096552

Dilution Factor: 10

Work Order # ... tDate Received..:Analysis Date..:Analynis Time..:

GDHQ3lAD

04/03/0404/27/0411:42

MatriX ..... : SOLID

Method . .... . SW846 8081A

PARPAMTERAldrinalpha-BECbeta-BHCdelta-BECgamma-BEC (Lindane:Chlordane (technici4,4 -DDD4,4' -DDE4,4'-DDTDieldrinEndrinEndrin aldehydeEndosulfan IEadosulfan II

Endosulfan sulfateHeptachlorHeptachlor epoxideMethoxychlorToxaphene

ii)

RESULTVDNDNDND

NDND1TDEDVDNDVDNDNDND

NDNDNDNDND

REPoRTINSLIMIT17171717171701717171717171717171717331700

CNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kguglkgug/kg.


PERCENTRECOVERYNC,DILNC,DIL


NC Mm ecvcr andlr RPD w kact amculateL

DML TI mcmeo b ae~md or am rqarted de dCM=oor 9k prf== s of befehg aal

Raubs wd q'fn ltse kbme 4fused for try weghL

LOC O GREENE

Client Sanple ID: 5S-15

GC Semivolatiles

Lot-&a6ple 0...: D4D030176-007Date Sampled...: 04/01/04 13:10Prep Date...;..: 04/06/04

Prep Batch 1...: 4096552Dilution Factor: 10

Work Order #...:Date Received..:Analysis Date..:Analysis Time..:

GH41AD04/03/0404/27/0412:11

Hatrix ......... : SOLID

Method, ......... x EW846 8081A

Aldrinalpba-EHCbeta-BHCdelta-BHCgamma-BHC (Lindane)chlordane (technical)4,4 ' -DDD4,4 -DDE4,4 ' -DDTDieldrinEzndrinEndrin aldehydaeEndosulfan IEndosulf an IIEndosulfan sulfateHeptachlorHeptachlor epoxideMetboxychlorToxaphene

RESULTJDNDNDNDEDIDNDNDllDEDIDEDEDIDEDNDNDNDND

REPORTINGLIMIT17171717171701717171717171717171717331700

WITSug/kgug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kg


PERCENT

RECOVERY

NC,DIL

HC, DIL

RECOVERYLIMITS

(41 - 142)(50 - 127)

NOTE(6) _NC Ue mcoy andfor RPD were ot eladd.Dl Tw ==zt k ekid or m sq=o dw m Md=k orie pmwam od Ieearh anyom

Xew sad rcpxdng lmb h e be a*tmd br dry we*tL


GC Bemivolatiles

Lot-Sample #...: D4D030176-008Date Sampled ... : 04/01/04 14:40Prep Date ...... : 04/06/04Prep Batch 0...s 4096552DilutIn Factor: 10

Work order C...:Date Received..sAnalysi. Date..:Analysis Time..:

GDHQSUM04/03/0404/27/0412:40

Matrix .... : SOLID

Kethod ... .: SN846 8081A

PARAMETERAldrinalpba-BHCbeta-BHCdelta-EECganma-BEC (LindanelChlordane (technlic4,4 '-DDD4 ,4-DDE4,4'-DDTDieldrinEdrinEundrin aldehydeEndosulfan IEndosulfan IIEndosulfan sulfateEeptachlorHeptachlor epoxideFethoxychlorToxaphene

Li)

RESULTEDEDIQDJDEDlD

EDEDEDNDED1DNDND

NDNDNDND

REPORTINGLIMIT17171717171701717171717171717171717331700

UNITS

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kg


PERCENTRECOVERY

NCDILNCDIL


NOTE (S):NC Ibe zerowry m=Uor IIPD = " alated.

DIL Ue mnoamaoo k nated or o ,cpord de w dlhnio or de prme= of Weak& amuly


GC semivolatiles

Lot-Sample i...:Date Sampled...:Prep Date ...... s

Prep Batdh i ... sDilutioa Factor:

D4D030176-00104/01/04 12:3004/04/0440951251

Work O0e r ... :Date Received..:Analysis Date.. 2Analysis Time...:

GDHQL1AE04/03/0404/12/0413.39

Matrix ... . : SOLID

Method .... : SW846 8141A

PAR7METERAzinphos-methylBolstarChlorpyrifosCoumaphosDemeton (total)DiazinonDichlorvosDimethoateDisulfotonEthopropEthyl parathionFamphurFensulfothionFenthionMalathionMerphosMethyl parathionFevinphosNaled0,0,0-Triethylphosphoro-

thioatePhorateRonnelSulfoteppThionazinTokuthionTrichloronateEPN

RESULTNDNDNDNDNDNDHDEDEDNDNDMDNDNDMDWDkDVDNDND

REPORTINGLIMIT1313131313131313131313131313131313133413

UNITS

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgug/kgug/kgug/kgug/kcgug/kgug/kgug/kgug/kgug/kg

NDNDNDEDNDHD

NDNDND

13G81313131313131313

Demeton-0Demeton-STetrachlorvinphos (Stirophos)

SURROGALTEEthyl Pir4mifosChlormefos

PERCENTRECOVERY7184

RECOVERY

LJMTS(11 - 137)

(37 - 124)

T E(S) :FRft Ed aporbtC Emk have be *Cumd for dry we ht.


OC semivolatiles

Lot-Sample #...:Date Sampled...:Prep Date ...... tPrep atch #... iDilution Factor:

D4D030176-00204/01/04 10:4004/04/0440951251

Work Order 0..:Date Recelved..:Analysis Date..sAnalysis Time..:

GDHQX1AE04/03/0404/12/0414:13

Matrix .. .: OLID

Method ......... SW846 8141A

PARAMETERAzinphos-methylBolstarChlorpyrifosCoumaphosDemeton (total)DiazinonDichlorvosDimethoateDisulfotonEthopropEthyl parathionFamphurpensulfothionFenthionM2lathionMerphos-Methyl parathionMevinphosValed0,0,0-Triethylphosphoro-

thicate

RES=TNDNDNDNDNDNDNDNDIDNDNDNDWDNDNDNDEDNDNDND

REPORTINGLIMIT1313131313131313131313131313131313133313

UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kg

ug/kqug/kgug/kgug/kgug/kgug/kgug/kguglkgug/kg

PhorateRonnelSulfoteppThionazinTokuthionTrichloronateEPNDemeton-0Demeton-STetrachlorvinphos

NDNDIDNDNDNDNDNDNDND

1368131313131.3131.313(Stirophos)

SURROGATEEthyl PirimifosChlormefos

PERCENTRECOVERY7587

RECOVERYLIMTS(11 - 137)(37 - 124)

lmuts w r*orti limis hve been a&Qjusmi br d&y weipg

WO W GREOD

Client Saiple ID: SS-9

GC Semivolatiles

lot-Sample 1 ...aDate Sampled ...:Prep Date ...... sPrep Batch t ...aDilution Factor:

D4D030176-00304/01/04 15:1504/04/04

40951251

Work Order C..: GDHQ0ODate Received..: 04/03janalysis Date..: 04/12i

wnalysis Time..: 14:46

LAE

04!/04

MatriX ..... SOLID

Method .... : SW846 8141A

PARJU4ETERAzinphos-methylBolstar

ChlorpyrifosCoumaphosDemeton (total)DiazinonDichlorvosDimethoateD1AlfotonEthopropEthyl parathionFamphurFensulfothionFenthionMalathionMerphosMethyl parathionMevinphosNaled0,0,0-Triethylphosphoro-

thiLoatePhorateRornelSulfoteppThionazin

RESULTIDNDNDEDEDEDEDNDNDNDEDEDEDNDNDNDND

NDNDIND

REPORTIMLIMIT1313

1313131313131313131313

13131313133313

UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg


ug/kgug/kg


TokuthionTrichloronateEPNDemeton-ODemeton-STetrachlorvinphos

NDNDNDNDNDNDNDkDNDND

136E1313131313131313(Stirophos)


PERCENTRECOVERY6775


NOE(S) :1s and epo eg lmi av been unuted *or d wy dghtL


GC semivolatiles

bot-Sauple #C..:Date Sampled...:Prep .... ...... s

Prep Batch 9 ... :Dilution Factor:

D4D030176-00404/01/04 10:0004/04/0440951251

Work order 9...sDate Received..:lnalysia Date..:Analysie Time..

GDHQ11AE04/03/0404/12/0415:52

Matrix .. . : SOLD

Method .... : sw846 8141A

PARAMETERAzinphos-methylBolstarchlorpyrifosCoumaphosDemeton (total)DiazinonDichlorvosDimethoateDisulfotonEthopropEthyl parathionFamphurFensulfothionFenthionMalathionMerphosMethyl parathionMevinphosNaled0,0,0-Triethylphosphoro-

thioatePhorateRonnelSulfoteppThionazinTokuthionTrichloronateEPNDemeton-ODemeton-STetrachlorvinphos (Stirophos)

RESULTNDNDNDNDIDNDNDEDNDNDNDNDNDNDNDNDNDNDNDND

REPORTINGLIMIT1313131313131313131313131313131313133313

UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg-ug/kgug/kg

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

NDNDNDEDEDNDEDED2DND

13681313131313131313


PERCENTRECOVERY7390

RECOVERYLIMITs(11 - 137)(37 - 124)

KTm(S):Resul ad rpong Imits hive been adpftd for by wcigbL

WDZOOD 6REE


CC Semivolatiles

Lot-8amQle C. . s

Date Sampled...:

Prep Date ...... s

Prep Batch #...sDilution Factor:

D4D030176-00504/01/04 15:4004/04/0440951251

Work Order t..:Date Received..:Analysis Date..:Analysis Time..:

GDHQ21AE04/03/0404/12/0416s25

Matrix ..... : SOL

Method ...... SW46 8141A

PARAMETERAzinphos-methylBolstarChlorpyrifosCoumaphosDemeton (total)DiazinonDichlorvosDimethoateDisulfotonEthopropEthyl parathionFamphurFensulfothionFenthbonMalathionMerphosMethyl parathionmevinphosNaled0,0, 0-Triethylphosphoro-

thioatePhorateRornelSulfoteppThionazinTokuthionTrichloronateEPSDemeton-0Demeton-STetrachlorvinpbos (Stlro

RESULTiDlDllDEDNDNDNDNDHD

RDNDNDNDNDNDEDNDNDND

IND

REPORTIGLIMIT1313131313131313131313131313131313133413

UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg


ND

TM

ND

ND

ND

ND

ND

ND

NDNND

13681313131313131313phos)


PERCENTRECOVERY7286


NOTE(s):Zmft ad mpw eb nEt hv bm usted fwr dry weiL


CC Semivolatiles

Lot-Sample #... :Date Sampled...zPrep Date ..... :Prep Batch #...sDilution Factor:

D4D030176-00604/01/04 16:1004/04/0440951251

Work order C...:Date Received.. sanalysis Date..:analysis Time.. i

GDHQ3 1AE04/03/0404/12/0416259

Matrix . .: SOLID

Method . . s 8W846 8141A

PARAMETERAzinphos-methylBoletarChlorpyrifosCoumaphosDemeton (total)DiazinonDichlorvosDimethoateDisulfotonEthopropEthyl parathionFamphurFensulfothionPenthionMalathionMerphosMethyl parathionMevinphosNaled0,0,0-Triethylphosphoro-

thioatePhorate

RESULTEDNDNDNDNDlDNDEDNDNDVDVD1DNDWDNDNDNDNDND

REPORTINGLIMIT1313131313131313131313131313131313133313

UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kguglkg

RonnelSulfoteppThionazinTokuthionTrichloronateEPNDemeton-0Demeton-STetrachlorvimphos

HD

ND

NDEDEDNDNDNDNDND

13

1313131313131313(Stirophos)

SURROGATEEthyl Pirimifoschlormefos

PERCENTRECOVERY

7797


NOTE(s):lenas am" pftd Ulu hve be asW dOr dry wrkfL

Client Sample D: SS-15

CC Siivoalatiles

Lt-Sample # ... tDate Sampled...:

Prep Date ...... sPrep Batch t.... :Dilution Factor:

D4D030176-007 Work Order I ... s04/01/04 13:10 Date Reeived..:04/04/04 Analysis Date. .:

4095125 - Analyss Time..:1

GDHQ41AE04/03/0404/12/0417:32

MatriX ..... : SOLID .

Method ...... 8W846 8141A

PARAMETERAzinphos-methylBoistarchlorpyrifasCoumaphosDemeton (total)DiazinonDichlorvosDimethoateDisulfotonEthpropEthyl parathionFamphurFensulfothionFenthionMalathionMerphosMethyl parathionMevinphosHaled0,0,0-Triethylphosphoro-

thioatePhorateRonnelSulfoteppThionazinTokuthionTrichloronateEPNDemeton-ODemeton-8Tetrachlorvinphos (Stiro]

RESULTNDNDNDNDRDEDND

NDllDEDND

NDNDND

NDNDEDNDND

hD

NDEDNDNDNDNDNDEDND

REPORTINGLIMIT1313131313131313131313131313131313133313

13681313131313131313

UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgUg/kg

ug/kgug/kgugs/kgug/kgug/kgug/kgug/kg

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kCgug/kgug/kgphos)


PERCENTRECOVERY7790


MOTE(S) :


GC Semivolatiles

Lot-Sample #...:Date Sampled...:Prep Date ...... :Prep Batch t...:Dilution Factor:

D4D030176-008

04/01/04 1MM4004/04/04409512S1

Work order #...:Date Received..:Analysis Date..:Analysis Time..:

GDHQ51AE04/03/0404/12/0418 05

HatriX .. .: SOLID

Hethod .... ... : SW846 6141A

PARA0MTERAzimphos-methylBolstarChlorpyrifosCoumaphosDemeton (total)DiazinonDichlorvosDimethoateDisulfotonEthopropEthyl parathionFamphurFensulfothionFenthionMalathionMerphosMethyl parathionMevinphosNaled0,0,0-Triethylphosphoro-

thioate

RESULTNDNDEDND1NDNDNDND

RDNDNDVDNDNDRDNDNDNDNDWD

REPORTINGLDT1313131313131313131313131313131313133313

uNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

PhorateRonnelSulfoteppThionazinTokuthionTrichloronateEPNDemeton-ODemeton-STetrachlorvinphos

ND

NDNDNDNDNDNDNDNDND

13691313131313131313

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg(Stirophos)

SURROGATEEthyl Pirimifos

Chlormefos

PERCENTRECOVERY7391

RECOVERYLIMITS

(11 - 137)(37 - 124)

NOTE(S):Reml od r'orfg Emm have be idjused Or dry wet.


GC Seaivolatiles

Lot-Sample ... 2Date Sampled....Prep Date ......:

Prep Batch I...sDilution Factor:

D4D030176-001

04/01/04 12:3004/08/044098553

Work Order #...:Date Received..:Analysis Date..:Analysis Time.-

GDHQL1AF

04/03/0404/13/0419:43

Matrix . .... : SOLID

Method......... : 8W846 8152A

PARAMETER2,4-D2,4-DB2,4,5-T2,4,5-TP (Silvex)DalapoaDicambaDichlorpropDinosebM[CPAHCPP

RESULT

NDNDNDlDIDIDEDNDNDND

REPORTINGLWI8181

20204141811281008100

UNITS


SURROGATEDCAA

PERCENTRECOVERY83

RECOVERYIMITS(39 - 96 )

NOTE(s):Resuk ad avofbng lmft bave bee ad~usWe for day wed&.


GC Bemvolatiles

Lot-Sample t ... s D4D030176-002Date Sampled...: 04/01/04 10:40Prep Date ...... : 04/08/04Prep Batch 1...: 4098553Dilution Factor: 1

Work Order #...:Date Received..:Aialysis Date..:Analysis Tne..*

GDHQX2AF

04/03/0404/13/0420:24

Matrlx.........: SOLID

Method.......2 SW846 8151A

PARAMETER2,4 -D2,4-DB2,*4,5 -T2,4,5-TP (Silvex)DalapoanDicamba,DichlorpropDinoseb?4CPAJ4CPP

RESULTMDE DWDNDWDED

IEDEDEDED

REPORTING

LIMIT81

202041418112

81008100

UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kcgug/kguglkg

SURROGATEDC&A

PERCENTRECOVERY90

RECOVERYLIMITS(39 - 96 M

NOTE(s):Results ad MrpothIg Umkslhave bease adusted for dry wedgta.


GC Semivolatiles

Lot-SaaPle t...: D4D030176-003Date Sampled ... : 04/01/04 15:15PZep Date ...... s 04/08/04Prep Batch C...: 4098553Dilutioui Factor: 1

Work order #...sDate Received. .Analysis Date..:Analysis Time..:

ODHO01AF04/03/0404/13/0421:05

Matrix .. S. : SLID

Method .... : SW846 8151A

PARAMETER2,4-D2,4-DE2,4,5-T2,4,5-TP (Silvex)DalaponDicauibaDichlorpropDinosebMCPAMCPP

RESULTRDVDEDNDNDND

ND]ND

NDND

REPORTINGLIMIT818120204040811291008100

DNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

SURROGATEDCAA

PERCENTRECOVERY89

RECOVERYLIMITS(39 - 96 )

NOTE(S):

OHD GRENE

Client Sample ID: SS-l1

OC Seinivolaviles

Lot-Sample #...:Date Sampled... 2Prep Date ...... :Prep Batch C...:Dilution Factor:

D4DO30176-00404/01/04 10:0004/08/044098553

Vork Order C..:Date Received..snalysis Date. *:

Analysis Time..:

GDRQ1lAF04/03/0404/13/0421:47

Matrix ..... s SOLID

Metbod ..... SW846 8151A

PARAMETER2,4-D2,4-DB2,4,5-T2,4,5-TP (1ilvex)DalaponDicambaDichlorpropDinosebMCPAMCPP

RESULTNDWDWDNDNDlNDVDNDNDID

REPORTINGLIMIT81e120204141811281008100

UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

SURROaATEDCAA

PERCENTRECOVERY95


IK= CS) :

Client Sanple ID3 E5-12

GC Semivolatiles

Lot-Sample # ... :Date 8ampled ... :Prep Date ...... :Prep Batch I... :Dilution Factor:

D4D030176-005

04/01/04 15:4004/08/04

4098553

1

Work Order 0...: oDHQ21AFDate Received..: 04/03/04

Analysio Date..: 04/13/04

Analysis Time..: 22:29

Matrix ..... : SOLIm

Method ...... 8W846 8151A

PARAMETER2,4-D2,4-DB2,4,S-T2,4,5-TP (SilveX)DalaponDicambaDichlorpropDinosebMCPAMCPP

RESULTNDNDNDNDEDNDNDNDNDND

REPORTINGL8M1T8181

20204141811281008100

UNITSug/kgug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kgug/kg

SURROGATEDCxA

PERCENTRECOVERYE7


NOTE(S) :lteS m d rqpoti linus laxc b 1 ted br dy wigh


GC semivolatiles

Lot-Sample #...: D4D030176-006Date Sampled.....: 04/01/04 16:10Prep Date .. :.... 04/08/04Prep Batch #...: 4098553Dilution Factor: 1

Wozk Order #...sDate Received..:Analysis Date..tAnalysis Time..:

GDHQ31AF04/03/04

04/13/0423:10

Matrix .. ... : SOLID

Ketbod .... : SW846 815iA

PARAMETER

2,4-D

2,4-DB2,4,5-T2,4,5-TP (Silvex)DalaponDicambaDichlorpropDinosebMCPAKCPP

RESWIdTNDNDMDNDNDNDNDNDEDED

REPORTINGLIMIT81

8120204040el1281008100


ug/kgug/kgug/kg

SURROGATEDCAA

PERCENTRECOVERY98 *


NOTH (S).> Sunapw recovM J Ouside sasfd cmWl liaos

Fesus and veporg limnts hke ben #AusW br wy wel&.

Client Sample TD: SS-15

GC Sesivolatiles

Lot-Sample #...: D4D030176-007Date Sampled ... s 04/01/04 13:10Prep Date ...... s 04/08/04Prep Batch C...: 4098553Dilution Factor: 1

Work Order I...:Date Received..:Analysis Date..:Analysis Time..:

GDHQ42AP04/03/0404/13/0423:51

MatriX ... .: SOLID

Method .... : S W846 8151A

PARAMETER2,4-D2,4-DB2,4,5-T2,4,5-TP (Silvex)DalaponDicambaDichlorpropDinosebMCPAMCPP

RESULTNDNDNDNDND1DNDNDNDND

REPORTINGLIMIT818120204040811281008100

UNITSug/kgug/kgug/kg'ug/kgug/kgug/kgug/kgug/kgug/kgug/kg

SURROGATEDCZA

PERCENTRECOVERY98 *

RECOVERYLnUTS(39 - 96 )

OTE(S) :* Sunsptewyei outdewed ewurl Kinks

Kesiks a repordmg Fu hve kem i baZW fOr b WhL


6C Seaivolatiles

Lot-Sample 0...:Date Sampled...:Prep Date ......:Prep Batch #...:Dilution Factor:

D4D030176-00804/01/04 14:4004/08/0440985531

Work Order C...:Date Received..:Analysi Date.. :Analysis Time..:

GDHQ51AF04/03/0404/14/0401:15

Matrix ...... : SOLID

Method . . SW846 8151A

PARAMEIER2,4-D2,4-DB2,4,5-T2,4,5-TP (Silvex)DalaponDicambaDichlorpropDinosebMCPAMCPP

RESU[TNDNDNDNDNDND

* ND

NDNDED


8112

81008100

UNITSug/kgug/kgug/kgug/kgug/kg


SURROGATEPERCENTRECOVERY

95

RECOVERY

LIMITS(39 - 96 )

mOTE (S):Rauft a rqwof Emits have be= ausW fo dry wegr.

LO OD GREMEM

Client Sample ID: &S-2

TOERL Metals

lot-SaMple 6...: D4D030176-001Date Sampled...: 04/01/04 12:30 Date Received..: 04/03/04

REPORTINGPARAMETER RESULT LIMIT UNITS METHOD

Prep Batch 1.s:4096254Mercury RD 34 ug/kg 8W846 7471A

Hatr, ....... :

PREPARATICN-ANALYSIS DATE

SOLID

WORKORDER #

_ _ _ _ _ _ _ _ _ _ _ _ _

04/13-04/14/04 GDHQL1AL

Dilutio Factor: 1 Analysis Time..: 11:S4

Prep Batch ... : 4097647Arsenic 0.76 B 2

Diii

Lead 2.8 0Dii

Selenium kD 1Dill

marium 22 1Diii

Cadmium ND 0Dill

Chrolium 5.9 1Dili

silver 0.099 B 1

WOM (S):Rasuk am! qrepdnh lbars km beeu adjuned far dry wei1A.B Eawd euk. less k 9s RL

L. 0 mg/kgaLtion Factor: 1

O.81 mg/kgtioe Factors 1

1.3 mg/kgLtion Factor: 1

.a mg/kgrtion Factor: 1

,.S1 mg/kgLtion Factor: 1

1.0 mg/kgitiax Factors 1

.0 gl/kgItian Factor: 2

5W846 6010BAnalysis Time..: 01.S6

8H846 6010BAnalysis Time.-. 01:56

SW846 6010BAnalysis Time..: 01:56

8W846 6010BAnalysis Time.. : 01256

SW846 6010BAnalysis Time. .: 01:5C

E1846 6010B

Analysis Time..s 01:56

S1846 6010BAnalysis Time..: 01:56

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

GMHQLIkP

GMQLrAQ

GDHQL1AR

GDHQL1AN

aEQLUJ

GDHQLIAK

LEOD GREW

Client Sanple IDs 8S-6

* TOL Metal;

Lot-SamPle 8....: D4D030176-002Date Sampled....: 04/01/04 10:40 Date Received..: 04/03/04

REPORTINGPARAMETER RESULT LIMIT UNITS MTOD

Prep Batch 8...: 4096254Mercury ED 33 ug/kg SW846 7471A

Dilution Pactor: 1 Analysis Time..s 12:00

Matrix ......

PREPARATION-ANALYSIS DATE

04/13-04/14/04

SOLID

WORKORDER #

GDHQXlAL

Prep Batch 1... 4097647Arsenic 0.76 B 1.0 mg/kg

Dilution Factors I

Lead 2.2 0.81 mg/kgDilution Factors I

Selenium 1D 1.3 mg/kgDilution Factors 1

Barium 15 1.0 mg/kgDilution Factor: 1

Cadmium ED 0.51 mg/kgDilution Factor: 1

Chrcuium 3.1 1.0 mg/kgDilution Tactors 1

silver 0.10 B 1.0 mg/kg

Dilution Factor: 1

NMTE(S):RIesmulamn epoxg Ims have been 4usd for dry Lw

B EmaiendL Reft bkkm d= RL

8R846 6010BAnalysis Time..x

18(46 6010BAnalysis Time..l

8W846 6010BAnalysis Time..

8H846 6010BAnalysis Time..:

8W846 6010BAnalysis Time..:

81946 6010BAnalysis Time..s

8N846 6010BAnalysis Time..

02:01

02:01

02:01

02:01

02:01

02:01

02:01

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

Gnnox2P

GD8Q=2A

GDHQX1AR

eHOX2AG

GDHQXlAH

6HQX1A6

G3HOX3AK

0OHOOD GREEN


SL metals

Lot-Sample I...: D4D030176-003Date Sampled...: 04/01/04 15:15 Date Received..: 04/03J

REPORTINGPARAMETER RESULT LIMIT UNITS METHC

Prep Batch #...t 4096254Mercury ED 33 ug/kg SW844

Dilution Factor: 1 nalysi

/04

[OD

6 7471AU Time..: 12:02

matrix.....:


04/13-04/14/04

SOLID

WORK

ORDER #

GDHQ01AL

Prep Batch I... 4097647Arsenic ND 1-

Tead 3.3 0.D lul

Selenium ED 1.Dilul

Barium 53 1.Dilui

Cadmium ND 0.Dilul

Chromium 3.4 1.Dulut

silver 0.085 B 1.Dilul

WNr(S):Reks and rpznhg Wmkhe been adjsed for dry w*elgB Enmacd Reu ites ItssdI than RL

.0 mg/kgLion Factors 1

.81 mg/kgtion Vactors 1

.3 mg/kgtion Factors 2

.Q mg/kgtlion Factors 1

.51 mg/kgtion Factors .

.0 mg/kgdton Factor: 1

.0 mg/kgoti Factors I

8W846 6010BAnalyix Time..: 02s:05

S6846 6010BhAalyxis Time.. 02:05

5W846 6010BAnalysic Time..: 02:05

11846 6010BAnalysin Tise..: 02:05

SW846 6010BAnalysis Time..s 02:05

5846 6010BAnalysis Time.., 02:05

53846 60101Analyxis Time..: 02:05

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

GDEQOlAP

GDHOOQIA

GDRQO1AR

GDEHOAG

GDEQO1AM

GDED01W

GDQ0OI

LW GRM

Client Sample ID:

TO7hL Ketals

Lot-SaMple t...s D4D030176-004Date Sampled...: 04/01/04 10:00 Date Received..: c

REPORTINGPARAMETER RESULT LIMIT UNITS

Prep Batch .. : 4096254Mercury ED 33 ug/kg

04/03/04

METHOD

matrix ...

PREPARJMIOt-ANALYSIS DATE

04/13-04/14/04

SOLID

WORKORDER #

GDIQUlALSW646 7471Azalysis Tie.. s 12:04Dilutioa Factor: 1 A

Prep Batch ... : 4097647Arsenic 0.89 B I

Lead 2.8 CDilh

Selenilum ED IDlli

Barium 19 1Dill

Cadmium ND a

Dill

cranium 3.4 1Dill

Silver 0.11 B 1Dll

3auss and epwtDg Kmits bave be adaged for dLy wigt

3 Esimted rekd& Ii eW tan RL

.0 mg/kglution Factors 1

0.81 mg/kgatlon Factor: 1

.3 mg/kgatias Factors 1

.0 mg/kgatloa Factors 1

D.51 mg/kgLitla Factor: 1

.0 Mg/kgtiaon Factors 1

1.0 Mg/kgLtlas Factor. 1

91(846 601QBAnalysis Time..s

51(846 6010BAnalysis Time.-:

5W846 6010Banalysis Time.. 3

8846 6010BAnalysix Time..;

8W846 6010BAnalysi Time. .

61846 6010BAalysiu Time.. t

81846 6010BAnalysis Time.:

02:19

02 :19

02:19

02:19

02:19

02:19

02:19

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

GMEQ11AP

WDWQ11

GDEQ11AR

GDHQ1IW

GDEQUlAR

GEH11A

GDHWilAi


TOTAL Het ls

Lot-Sauple 4...: D4D030176-005Date Sampled...: 04/01/04 15:40 Date Received..: 04/03/04

REPORTINGPARAMETER RESUILT LIMIT UNITS METHOD

Prep Batch 4...: 4096254Mercury ND. 34 ug/kg 6W846 7471A

Dilution Factor: 1 Analysis Time..: 12:06

Matrix .... :

PREPARATION-ANLYSEIS DATE

04/13-04/14/04

SOLID

WOREORDER #

GDHQ21AL

Prep Batch 4097647Arsenic 0.77 B 1.0 mg/kg

Dilution Factor. I

Lean 2.7 0.81 mg/kgDilution Factor: 1

Selenium ID 1.3 mg/kgDilution Factors 1

Barium 19 1.0 mg/kgDilution Factors 1

Cadmium ND 0.51 mg/kgDilution Factor: 1

Crcmitniu 3.5 1.0 mg/kgDilution Factor: 1

Silver 0.10 B 1.0 ng/kgDilution Factor: 1

ZKY (S) gRme bs and epoung Iinhs e km been swtd fbr dry wdghL

B EsiWd resut. Remik k ms dan DL

8N846 6010BAnalysis Time..: 02:24

81846 6010BAnalysis Time..: 02U24

B8146 6010BAnalysis Time. . 02:21

611846 6010BAnalysis Time..: 02:24

8W846 6010BAnalysis Time..: 02:24

S3846 6010BAnalysis Time..i 02M24

83946 6010BAnalysis Tize..t 02:24

04/09-04/17/04 DEHQ22AP

04/09-04/17/04 GDEQ21AQ

04/09-04/17/04 GDHQ21AR

04/09-04/17/04 GD9Q21AG

04/09-04/17/04 GDEQ21AH

04/09-04/17/04 GDQ21M

04/09-04/17/04 G6DQ2IAM

WLCE1O0D GREENE

Client Sample XD: BS-13i

TO= Hetala

Let-Sanple f...s D4D030176-006Date Sampled, ... : 04/01/04 16:10 Date Received..s 04/03/04

REPORTINGPARAMETER RESULT LIMIT UNITS MTOD

Prep Batch 1.: 4096254Mercury wD 33 ug/kg SW846 7471A

Matrix ...... :


04/13-04/14/04

SOLID

WORKORDER #

GDHQ31ALDilution Factort 1 Analysis Time. . 2:08

Prep Batch 1.s:4097647Arsenic 1D I

Dil

Lead 2.6 CDil,

Selenium ED IDill

Barium 16 1Dill

Cadmium ED CDill

Chtmrium 3.0 2

Silver ND 1

Dill

wmO S):ekfh md zqxuwg lts km bhese ajustd to weht.

.. O nmg/kguticn Factor: 1

).81 ug/kgutien Factor: 1

1.3 Mg/kgutioa Factor: 1

I.0 mg/kgution Factor: 1

O. 51 mg/kglution Factor: 1

1.0 mg/kgution FactorS I

.0O mg/kgLtlen Factor: 1

SW846 6010BAnalysis Time-.

01846 6010B1nalysis Time.:

SW846 6010BAnalysis Time..:

511846 6010BMalysis Time..:

SW846 6010BAnalysis Time..t

53846 6010BAnalysis Time..:

SW846 60109Amalymis Time..:

02:28

02:28

02:28

02U28

02:28

02:28

02:28

04/09 -04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

GDHQ3lAP

GMMi31AO

GDHQ31AR

GUQ31AG

GDHQ31AN

GDH~3AJ

GDHQ32.AR

WOCD

Client Sample ID: ES-15

TOTAL Metals

Lot-Sanple #...: D4D030176-007Date Sampled...: 04/01/04 13:10 Date Received..: 04/03/04

MatriX .... : SOLID

REPORTING PREPARATION-ANALYSIS DATE

____

PARAMETER

Prep Batch

Mercury

_ RESULT

1...: 4096254ND

_ LIMIT UNITS

33 ug/kgDilution Factors 1

; METHODWORKORDER #

GDiQ41AL8W846 7471AAnalysiu Time..t 12:10

04/13-04/14/04

Prep Batch ... : 4097647Arsenic ND 1.0 mg/kg

Dilution Factors 1

Lead 2.5 0.81 mg/kgDilution Factors I

Selenium ND 1.3 mg/kgDilution factor: 1

Barium 17 1.0 mg/kgDilution Factora 1

Cadmium ND 0.51 mg/kgDilution Factor: 1

chrmium 3.1 1.0 mg/kgDilution Factor: 1

Silver 0.10 B 1.0 mg/kgDilution Factor. 1

BOTE(S):Reas wd repontb Kwim have been 4and ft day weh.

B Esdiued tre. Resul is Uazn RL.

BW846 6010B3na9lysi Time..1 02:33

SW846 6010BAnalyai. rime.. s02:33

83W846 6010BAnalysis Time.,. a02:33

S1846 6010BAnalysis Time.-a 02:33

S3846 6010Banalysis Time.. i 02:33

8H846 6010BIealyuia TiMe..9 02233

51846 6010 31nalyui Time..: 02:33

04/09-04/17/04

04/09-C4/17/04

04/09-04/17/04

04/09-04/17/04

04/09-04/17/04

C4/09-04/17/04

04/09-04/17/04

GDHQ4lAP

GDEQ41AQ

GDHQ41AR

GD041AG

GDHQ41A

GDR41AJ

GDEHQ41A

Client Sample ID: E8-16

TOTAL Metals

Lot-Sample z...: D4D030176-008Date Sampled...: 04/01/04 14:40 Date Received..: 04/03/1

REPORTINGPARAMETER RESULM LIMIT UNITS METRO]

Prep Batch 0...: 4096254Mercury ID 33 ug/kg 8W846

Dilution Factors 1 Analysis

'0

D

Matrix ..... :


04/13-04/14/04

SOLID

WORKORDER #

GDHQ5lAL7471A

Time..: 12U12

Prep Batch .. : 4097647Arsenic 0.96 B 1.0 mg/g

Dilution Factors 1

Lead 2.9 0.B1 mg/kgDilution Factor: I

Selenium ED 1.3 mg/kgDilution Factor, 1

Barium 24 1.0 mg/kgDilution Factor: 1

Cadmium ED O.50 mg/kgDilution Factors I

Chbrcuum 3.7 1.0 =g/kgDilution Factor: 1

Silver 0.11 B 1.0 mg/kgDilution Factor: 1

MOTE(S):Re uad rqt bngs have beem s#usted for dry weihL3 Esnme resuk Resk k ss duan RL

8R846 6010BAnalysis Time..

81846 6010BAnalysis Time..:

SW846 6010BAnalysis Time.. a

8W846 6010BAnalysis Time..:

SW846 6010Banalysis Time..:

811846 6010BAnalysis Time.. :

51846 6010BAnalysis Time. . s

02:37

02a37

02:37

02:37

02:37

02:37

02s37

04/09-04/17/04 GEO51AP

04/09-04/17/04 GEQ51AQ

04/09-04/17/04 GDRQ5lAR

04/09-04/17/04 GD5IAG

04/09-04/17/04 GDH0QS1A

04/09-04/17/04 GDMQSthJ

04/09-04/17/04 GDEQ51AK

I GOD -

Client Sauple ID: 8S-2

General Cbemi try

Lot-Sample #...s D4D030176-001 Work Order #...: GDHQL

Date SaMipled...: 04/01/04 12:30 Date Received..: 04/03/04Matrix........ : SOLI

PARAMETEIFluoride

z RESULT RL UNITS

ED 10 ~ mg/kg

Dilution Factors 1

MEHOD83846 9056valysixs Time..: :53

PREPARITION- PREPANALYSIS DATE BATCH #04/15/04 4107487

Percent moisture 1.6 0.10 tDilution Factors 1

ICMM 160.3 MD 04/19/04nalyuin Time.. 17:3S

4110593

IWOTE(S) :RL Rqofftg Limk

Imks Wz roftd Hfmit lave beem I d forry weight.

Lot-SaMPle t...: D4D030176-002Date SanPled... : 04/01/04 10:40

PARAMETER RESULT

Fluoride SDDilu

Percent Moisture 1.3Dilu

IWO= CS):RL Reporftg Lhk

Resauh wh ft links have kme Imed mr LT .gbt

.CKWOOD -

Client Sauple Th: SS-6

General Cemistry

Work Order 1... : GDHQX HaiDate Received..: 04/03/04

RI; UNITS METHOD

10 mg/kg SW846 9056tion Factors 1 Analyuli Time.. , 16127

0.10 t HMCW 160.3 MODlt4i lactor: 1 Analyst. Time..: 17:35

.ri .... .SOLID

PREPARATION- PREPANALYSIS DATE BATCH #

04/15/04 4107487

04/19/04 4110593

Client Sample ID: CS-9

General Meml try

Lot-Sample #...: D4D030176-003 Work Order q...: GDHQ0

Date Sampled...: 04/01/04 15:15 Date Received..: 04/03/04

HatriX ..... : SOLID

PREPARATION- PREP

ANALYSIS DATE BATCH #PARAMEMT RESULT RL UNITS METHOD

Fluoride 1.0 B 10 09/kgDilution Factors 1

3846 9056Analysix Time. . 16,38

04/15/04 4107487

Percent Noisture 1.2 0.10 %Dilutimn Factors 1

MKMN 160.3 HU 04/19/04Analysi Time.., 17:35

4110593

NME (S):RL Rleponhg Lk

Res deportng bikhav¢eo kJWedfordry wdpL

B Eye; lst k ResSUWth ku OmRL

mD GRAMB


Geoxal Chemistry

Lot-SaWple I... : D4D030176-004 Work Order t...: GDHQ1Date Sanpled...: 04/01/04 10:00 Date Received..: 04/03/04

Matrix.........: SOLID

PARAMETER

Mluoride

RESULT

1.2 B

RL UNITS

10 mg/kgDilution Factor: 1

0.10 tDilution Factors 1

PREPARATION- PREP- METHOD ANALYSIS DATE BATCH #

S8E46 9056 04/15/04 4107487anyaly Time..o 1H5O '

MCAUW 160.3 MM 04/19/04 4110593Analyusi Time... 17s35

Percent Moisture 1.3

l0T () v.RL Rupotdng Uhit

Remsui mx! reptifg Nazs live beestdgsped ft dry *bLt.

B sed;Vt Resul Is les Iu DL

LOCo0D. GREEHH

Client Sample IDs SS-12

erl bPM try

Lot-Sample #...s D4D030176-005 Work Order I...s GDHQ2Date Sampled...: 04/01/04 15:40 Date Received..s 04/03/04

HatriX ... .: SOLID

PREPARATPARAMETER

Fluoride

Percent Moisture

RESULT RL UWITS

]w 10 mg/kgDilution Factor: I

1.5 0.10 t

Dilution Factort 1

METHOD ANALYSIS

8W846 9056 04/15/04Analysia Time..: 17t01

HCRNW 160.3 MM 04/19/04Aaly~is TiMe..: 17:35

XON- PREPDATE BATCH #

4107487

4110593

KTH (S) SRL Reponig LUit

ts S rpwft Emhs mh bce Oaen 4ustd frdzy wdgbL

Lot-Sanple I...: D4D030176-006Date SaMpled...: 04/01/04 16:10

PARAMETER RESULT

Fluoride EDDilul

Percent Moioture 1.1Dilul

NOTBW8 sRL Repofiog LhakRe v*s fepotng b kve beaJeld rdry htL

lwCD GR-0 .

Client Sample ID: ss-13

General Chemi try

Work order #...: GDHQ3 MatDate Received..: 04/03/04

RL UNVTS METHOD

10 mg/kg SW846 9056tion Factor: I analysis Time. .3 17:35

0.10 t HKMfW 160.3 MMsti Factors I Analysis TiLe..: 2.7:35

=- ��

niX ... . : SOLID

PREPARATION- PREPANMLYSIS DATE BATCH #

04/15/04 4107487

04/19/04 4110593

IDCKKO -Ra


General Clemistry

Lot-Sample #...: D4D030176-007 Work Order 8...: GDHQ4Date SamPled ... : 04/01/04 13:10 Date Received..: 04/03/04

MatriZ ...... SOLID

PREPARATION- PREPANALYSIS DATE BATCH #Ilz.qTff.'r 10T. TThrrorg mfTEOn

Fluoride 1.0 B 10 mg/IgDilution Vactowi I

51(46 9056natycs TiSm..: 17346

04/15/04 4107487

Percent moisture 1.2 0.10 "Dilution Factort 1

HCMa 160.3 ED 0411914anlysiff Time..: 17:35

43a0593

la= (S) :DL Reporting Unitc

Resutts md reportics limis ham been aCfusted bu dy weighta9 Estlmated result Ranhk I kms gmn RL

OD -E

Client Sample ID: S3-16

General Chemistry

Lot-Swaple t...: D4D030176-008 Work Order #...: GDHO5 Natrix ......... ,: SOLID

Date Sampled...: 04/01/04 14:40 Date Received..: 04/03/04

PREPARATION- PREP

PARAMUETER RESULT RL UNITS METHOD ARJMYSIS DATE BATCH P

Fluoride ND 10 mg/kg 8W846 9056 04/15/04 4107487

Dilution Factors 1 Analyxis Time-: 17:s7

Percent Moisture 0.81 0.10 t !4CAW 160.3 MOD 04/20/04 4111603

Dilutio Jactor 1 Malysis Time : 17:15

RL Repordag LUnitReuIs and rpon 1Mks hke beea a4*e Ibr dry wdghL

QC DATA ASSOCIATION SUMMARY

D4D030176

Sample Preparation and Analysis Control NUmbers

ANALYTICAL LEACH PREPSAMPLE# MATRIX METHOD BEATCH # BATCH # HS RVN#

001 SOLID SW846 9056 4107487 4107237SOLID SW846 7471A 4096254 4096141SOLID 5W846 8141A 4095125 4095022SOLID 8W846 8081A 4096552 4114264SOLID gW846 6260B 4104274 4104174SOLID 8W846 6270C 4097621 4097303SOLID SW846 6010B 4097647 4097320SOLID SW846 8151A 4098553 4099301SOLID MCAW 160.3 ROD 4110593 4111080

002 SOLID SW846 9056 4107487 4107237SOLID SW846 7471A 4096254 4096141SOLID SW846 8141A 4095125 4095022SOLID SW846 8081A 4096552 4114264SOLID 8W846 62609 4104274 4104174SOLID SW846 8270C 4097621 4097303SOLID 8W846 6010B 4097647 4097320SOLID W8W46 8151A 4098553 4098301SOLID MCAKW 160.3 MOD 4110593 4111080

003 SOLID mW846 9056 4107487 4107237SOLID SW846 7471A 4096254 4096141SOLID 6W846 8141A 4095125 4095022SOLID SW846 8081. 4096552 4114264SOLID SW846 8260B 4104274 4104174SOLID SW846 8270C 4097621 4097303SOLID 8W846 6010B 4097647 4097320SOLID 8W846 81511 4098553 4098301SOLID MCAWW 160.3 MOD 4110593 4111080

004 SOLID SW846 9056 4107487 4107237SOLID 8W846 7471. 4096254 4096141SOLID SW846 81412 4095125 4095022SOLID 6W846 80811 4096552 4114264SOLID 8W846 8260B 4104274 4104174SOLID EWS46 8270C 4097621 4097303SOLID 8W846 6010B 4097647 4097320SOLID EW846 8151A 40985S3 4098301SOLID MCAWW 160.3 MOD 4110593 4111080

005 SOLID SW846 9056 4107487 4107237SOLID 6W846 7471A 4096254 4096141SOLID SW846 8141A 4095125 4095022


QC DATA ASSOCATION SUMMARY

IYD030176

Sample Preparation and Analysil.Control NZumbers

ANALYTICAL LEACH PREP

SAMPLE# MRIX METHOD BATCH BATCH * MS R'UN

005 SOLID 8W846 8081A, 4096552 4114264

SOLID 8W846 8260B 4104274 4104174

SOLID 8N846 8270C 4097621 4097303

SOLID SW846 6010B 4097647 4097320

SOLID W8N46 8152A 4098553 4098301

SOLID MCAWW 160.3 MOD 4110593 4111080

006 SOLID 8W846 9056 4107487 4107237

SOLID 8W846 7471A 4096254 4096141

SOLID 8W846 8141A 4095125 4095022

SOLID 8W846 8012A 4096552 4114264

SOLID 6W846 8260B 4104274 4104174

SOLID 8W846 8270C 4097621 4097303

SOLID SW846 6010B 4097647 4097320

SOLID 8W846 8151A 4098553 4098301

SOLID MCAWW 160.3 MOD 4110593 4111080

007 SOLID 6W846 9056 4107487 4107237

SOLID 8W846 7471A 4096254 4096141

SOLID 6W846 8141A 4095125 4095022

SOLID SW846 80811. 4096552 4114264

SOLID S91846 82605 4104274 4104174

SOLID 6W846 8270C 4097621 4097303

SOLID SW846 6010B 4097647 A097320

SOLID SW846 81511. 4098553 4098301

SOLID MCAWW 160.3 MOD 4110593 4111080

008 SOLID 8W846 9056 4107487 4107237

SOLID S8146 74711 4096254 4096141

SOLID 8W846 81411. 4095125 4095022

SOLID SW846 8081. 4096552 4114264

SOLID SW846 8260B 4104274 4104174

SOLID 6W846 8270C 4097621 4097303

SOLID 8W846 60103 4097647 4097320

SOLID SW846 81511 4098553 4098301

SOLID MCANW 160.3 MOD 4111603 4112076

m DE B REPaRT

GC/MS Volatiles

Client Lot #...: D4D030176NB Lot-Sample #: D4D130000-274

Analysis Date..s 04/12/04

Dilution Factor: 1

Work Order #...: GD3FW1AA

Prep Date ...... : 04/12/04

Prep Bateh I... : 4104274

Matrix ......... g SOLID


PARAMETERAcetoneBenzeneBromodichloromethaneBromofonrmBromomethane2-Butanone (MEN)Carbon tetrachlorideChlorobenzeneChloroethaneChloroformcbioromethaneDibromomethane1,2-Dibromoethane (EDB)1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroetbane1,2-Dichloroethane1,1-Dichloroethenei.2-Dichloroethene

(total)ciE-, 12-Dichloroethenetrans-1,2-Dich1oroethene1,2-Dichloropropanecis-1,3-Dichloropropenetrans-1,3-DichloropropeneEthylbenzene2-RexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1,1,1,2-Tetrachloroethane1,1,2.2-TetrachloroethaneTetrachloroetheneToluene

1,2,4-Trichloro-benzene

1,1,1-Trichloroetbane1,1,2-TrichloroethaneTrichloroethene

RESULT3.8 JNDNDNDNDNDND

NDNDNDNDNDNDNDhDNDNDNDNDND

ND

ND

EDNDNDNDllDNDNDNDNDND

ND

ND

NDND

ND

TLIMIT

205.05.05.010205.05.01010105.05.05.05.05.0105.05.05.05.0

2.52.55.05.05.05.0205.0205.05.05.05.05.05.0

5.0 I5.0 15.0 I

UNITS

uglkgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgag/kgug/kgUg/kgug/kgug/kgug/kgug/kgug/kg


ug/kgug/kg

ug/kgUg/kg

ug/kg

METHOD6N846 8260BS6846 8260B6W846 82.60BSW846 8260B6WE46 8260B6W846 826038W846 8260BSW846 8260B8W846 82603SW846 8260B8w846 8260BSW846 8260B8w846 8260BSW846 8260B

5W846 8260B5W846 8260B5W846 8260B8W846 8260B8W846 8260B8W846 8260B81846 8260B

8W846 8260B8W846 8260B8W846 82608

S8K46 8260BSW846 8260B8W846 8260BSW846 8260B

8W846 8260BSW846 8260B8W846 8260B

8w846 8260B8W846 8260B

8W846 8260B

6R846 82603

8W846 8260B

8w846 8260B

6w846 8260B8W846 8260B


METOD ELAN RDPORT

GCCkS Volatiles

Client Lot #...: D4D030176 Work Order #...: GD3FW1MA Katr .... : SOLID

PARAMETER

Trichlorofluoromethane1,2,3-TrichloropropaneVinyl chlorideXylenes (total)n-Butylbenzenesec-ButylbenzeneIsopropylbenzene1,2,4-Trimethylbenzene1,3,5-TriMethylbenzenen-Propylbenzenetert-ButylbenzeneDibromochloromethane2-Chlorotoluene4-Chlorotoluene1,2-Dibromo-3-

chloropropane (DBCP)1,3-Dichloropropane2,2-Dichloropropane1,1-DichloropropeneHexcadhlorobutadiene4-IsopropyltolueneMethyl tert-butyl ether1,2,3-Trichlorobenzenem-Xylene & p-Xyleneo-KyleneBromobenzeneEromochloromethane

RESULTED

DEDRDNDNDVDEDNDEDNDNDVDNDND

NDEDIDNDNDNDNDNDMDNDND0.58 J

REPORTINGLIMIT105.05.05.05.05.05.05.05.05.05.05.05.05.010

5.05.05.0

5.05.0205.02.52.55.05.05.0

UNITSug/kg


ug/kgug/kgug/kg


ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/i

FETHODSW846 8260B8W846 8260B68)46 8260BSW846 8260B68W46 8260BSW846 826088W846 8260B8IW846 8260BSW846 8260B8W846 8260BSW846 8260B

S8)46 8260B8W846 8260B8W846 8260B8W846 8260B

SW846SW8468W846S8)468W846SW8468W846SW846SW846SW8466W8468(846

8260B8260B826088260B8260B8260B8260B8260B826088260B8260B8260B

SURROGATEDibromofluoromethane1,2-Dichloroethane-d44-BromofluorobenzeneToluene-dS


RECOVERYLTTS(71 - 136)(67 - 131)(71 - 124)(77 - 129)

cdmd-m am pe-omad b-bm mding aowid simd-offm s a n ca holrd ks

J EsdmB d esuX 1mh k kss d= RL

XiWORATORY CONTROL SAMPLE B7AL1AT( REPORT

GC/mS Volatiles

CliCnt Lot #...: D4D030176LCS Lot-Saiplet: D4D130000-274Prep Date...... : 04/12/04Prep Batch 0....: 4104274Dilution Factor: 1

Work Order #... . GD3FWIAC-LCS atriSx ........ SOLIDGD3FWlhD-LCSD

Analysis Date..: 04/12/04Analysis Time..: 11:40

PARAMETERSenzene,

0Blroene

1, l-Diamroethene

Toluene

Tricbloroethen

PERCENT

RECOVERY9210890105911039310385101

RECOVERYLIMITS

(72 - 121)(72 - 121)(75 - 115)(75 - 115)(60 - 133)(60 - 133)(71 - 117)(71 - 117)(70 - 125)(70 - 125)

BPDRED LIMITS

16

15

13

10

17

METHOD01846 8260B

(0-25) 01846 8260B81846 8260B

(0-25) 8H846 8260B8H846 8260B

(0-25) 61846 8260B61846 8260B

(0-25) 8h846.8260B6H(46 8260B

(0-25) 68146 8260B

SURROGATEDibromofluoromethane

1,2 -Dichloroethane-d4


RECOVERYLIMITS(78 - 118)(78 - 118)(72 - 120)(72 - 120)(76 - 127)(76 - 127)(75 - 120)(75 - 120)

4 -Bromofluorobenzene

Toluene-dS

NOTE (S):Caiwlctlo are pcgmad boe swunfdio kvoi awd-ff hi calmulaW es

, am Fft dwiws bc=n parame

IABORRTORY cNTROLa SAMPL D a= REWOR

GC/HM Volatiles

Clieut Lot #...: D4D030176ICS Lot-Samplet: D4D130000-274Prep Date ...... s 04/12/04Prep Batch #... s 4104274Dilution Pactor: 1

Work Order 6...: GD3FW1AC-LCS Hatri ... . : SOLIDGD3FWlAD-LCSD


SPIKE MEASURED

Benzene

1,1-Difbloroethene

Toluene

Triooe 33en

AMOUNT50.050.0

SO.050.0

50.0

50.0

50.050.0

50.050.0

AMOUNT46.053.845.152.645.351.646.551.442.750.4

UNITSugfkg

ag/kgug/kg

uglkgug/kguglkgug/kguglkg


RPD ETWOD

5846 B260B16 8W846 8260B

8W846 8260B15 81146 8260B

68146 8260B13 O8146 8260B

5846 8260B10 S8146 8260B

S8146 8260B17 81846 8260B

SURROGATE

Dibromoflluorometbane

1,2-Dicbloroethane-dt

4-Bromofluorobenzene

Toluene-dS


RECOVERYLIMITS

(7B - 118)(78 - 118)(72 - 120)(72 - 120)(76 - 127)(76 - 127)(75 - 120)(75 - 120)

Wm (a) ):

hmf ame psened bdome oamnf io o3i towd-off am hb ubted esuk

Boxd pwh 4am awRu d prau

MATRIX SPI SAMPUE3 EVZU9I0Uf REPORT

GC/MS Volatiles

client Lot C...:MS Lot-Sanple #:Date Sampled...:Prep Date ...... s

D4D030176D4D050247-00204/01/04 13:5004/12/04

Work Order C..: GDKHM1-KMSGDKHM1AO-MSD

Date Received..: 04/05/04Analysis Date..: 04/12/04Analysis Time..: 21:10

Matrix .... : SOLID

Prep Batch #...: 4104274Dilution Factor: 1

PARAMETERBekzfene

ctemsnz

1 ,-Dic bloroethene

Toluene

Trichioroethene


RECOVERYLIMITS(51 - 133)(51 - 133)(28 - 137)(28 - 137)(49 - 134)(49 - 134)(33 - 140)(33 - 140)(46 - 135)(46 - 135)

RPDRPD LIMITS METHOD

SW8463.4 (0-40) 51(46

SK8460.70 (0-40) S846

388469.6 (0-40) 53846

5384612 (0-40) 53846

5K8461.7 (0-40) 5N846

8260B8260B8260B8260B8260B8260B8260B8260B8260B8260B

SURROGATEDibromfluoromethane

1,2-Dichloroethane-d4

4-Bromofluorobenzene

Toluene-dB


RECOVERYLIMITS(71 - 136)(71 - 136)(67 - 131)(67 - 131)(71 - 124)(71 - 124)(77 - 129)(77 - 129)

NOTE(S)

BolWd Vit dewtes conurol ptratmot

MM=RZ SPIKE SANPLE DAM REPORT

GC/MS Volatiles

Client Lot S...:MS Lot-Sample I:Date Sampled...sPrep Date ...... :Prep Batch I...sDilution Factor:

D4D030176D4D050247-00204/01/04 13:5004/12/044104274

Work Order I...: GDKHM1X-MSGDEHMlAO--SD

Date Received..: 04/05/04Analysis Date..: 04/12/04Analysis Time..: 21:10


PARAMETRBenzene

chlorcbenzene

1, 1-Dchloroethene

Toluene

Trichloroethene

SAmLE SP=IEAMOUNT AMT

lD 50.0ED 50.0

ED 50.0ND 50.0ND 50.0ND 50.00.23 50.00.23 50.0ND 50.0ND 50.0

HEASRD

AMOUNT35.036.226.626.839.342.835.640.329.028.5

PERCTUNITS RECVRYug/kg 70ug/kg 72ug/kg 53uglkg 54ug/kg 79ug/kg 86ug/kg 71ug/kg 80uglkg 58mg/kg 57

RPD METHOD0N846 8260B

3.4 01846 8260B38M46 8260B

0.70 SN846 8260B01146 826QB

8.6 S0846 8260BS1846 8260B

12 S0846 8260B38946 8260B

1.7 SN846 8260B

SURROGATEDibromofluoromethane-

1,2 -Dichloroethane-d4

4 -Bromofluorobenzene


RECOVERYLIMITS(71 - 136)(71 - 136)(67 - 131)(67 - 131)(71 - 124)(71 - 124)(77 - 129)(77 - 129)

Toluene-de

NxYR f 1 r

Boulpinons am Wefned kfore zwulinc m id rond-off err k cacud gesuk.

Bold Piii denowcs coamrl varmmc

METOD SIAM REPORT

GCINS Seiotle

Client Lot C..: D4D030176

MB Lot-Sanple 4: D4D060000-621

analy5is Date..: 04/22/04Diluticn Factor: 1

Work order .... : GDM57LAA

Prep Date ...... : 04/07/04Prep Batdh 1...s 4097621



PAR)METERAcenaphtheneAcenaphthyleneAcetophenone2-Acetylaminofluorene4-AminobiphenylAnilineAnthraceneAramiteBenzo(a)nathraceneBenzo(b)fluorantheneBenzo(k)fluorantheneBenzo(ghi)peryleneBenzo(a)pyreneBenzyl alcoholbiB(2-Chloroethoxy)


etherbis (2-Ethylhexyl)


etherButyl benzyl phthalate4-ChloroanilineChlorobenzilate4-Chloro-3-methylphenol2-Chloronaphthalene2-chlorophenol4-Chlorophenyl phenyl

etherChryseneDiallateDibenz(a,h)anthraceneDibenzofuranDi-n-butyl phthalate

1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-Dichlorobenzene3,3'-Dichlorobenzidine2,4-Dichlorophenol

2,6-Dichlorophenol

RESULTNDNDNDNDNDND

NDNDNDDD

NDNDNDND

ED

REPORTINGLIMIT33033033033001600330330660330330330330330330

330

330

ND 330

UNITS

ug/kgu9/kgug/kgug/kgug/kgug/kg


ug/kg

ug/kg

ug/kg


ug/kgug/kgug/kg


METHODSW846 8270C

W8)46 8270C8w846 8270C81846 8270C8W846 8270C81846 8270C8W846 8270CSW846 8270C

SW846 8270C6w846 8270C6W846 8270C8w846 8270CSW846 8270CSW846 8270C

6W846 8270C

SW846 8270C

6W846 8270C

6w846 8270C330

NDNDNDNDNDNDND

330330330330330330330

NDNDNDNDNDNDNDNDNDNDND

33066033.03303303303303301600330330

SW8468W8468W846SW846SW846

SW846

8w846

8W8468w846S8846Sw8468w8468W8468W846

8W846

8W846SW846SW846

8270C8270C8270C8270C

8270C8270C

8270C

8270C8270C8270Ce270C8270C8270C8270C8270C

827QC8270C

8270C


I4ETEOD BUMNK REPORT

6CC/s Bemivolatiles

Client Lot I...: D4D030176 Work Order #...: GDM571AA Hatrix .... : SOLID

PARAMETER

Dietbyl phthalateDimethoate7,12-Dimethylbezz(a)-

antbracene3,3'-Dimetbylbenzidine2,4-DimethylphenolDinethyl phthalate1,3-Dinitrobenzene4,6-Dinitro-

2-niethylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DnintrotolueneDi-n-octyl phthalateDiphenylamineDisulfotonEthyl methanesulfonateFluorantheneFluoreneHexachlorebenzeneHexachlorobutadieneHexachlorocyclopenta-

dieneNexachloroethaneHexachloropropeneIndeno(1,2,3-cd)pyreneIsodrinIsophoroneIsosafroleMethapyrilene3-MethylcholanthreneMethyl methanesulfonate2-MethylnaphtbaleneMethyl parathion2-Methylphenol3-Methylphenol &

4-MethylphenolNaphthalene1,4-Naphthoquinone1-Naphthylamine2-Naphthylamine2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene

RESULTNDNDED

REPORTINILIMIT660660660

NDNDNDNDND

6603303303301600

IDEDNDNDEDEDEDEDIDNDUDND

160033033033033016003303303303303301600

UNITSug/kgug/kgug/kg




uglkgug/kg

ug/kgug/kgugfkgug/kgug/kgug/kgug/kgug/kg

SW846SW846SW8468W8468W846

SW846SW846SW846SN146SW8466W8468W846681468W8468W84681W8461SW846

METHODSW846 8270CSW846 8270C

8W846 8270C

8270C8270C8270C8270C8270C

8270C8270C8270C8270C8270C8270C8270C8270C8270C

8270C8270C8270C

NDNDlDVDND

NDNDNDNDNDNDNDND

330330033033033066016006603303301600330330

8W846 8270C

SW846 8270C8W846-8270CSW846 8270CSW846 8270C

6N846 8270C

6W846 8270C8W846 8270C

8W846 8270C8W846 8270C

SW846 8270C8W846 8270C

SW846 8270C

NDlDNDNDEDNDEDND

3301600

330330160016001600330

SW846SW8466W846

SW846SW84688466W8468W846

8270C8270C8270C8270C8270C

8270C8270C

8270C


HEMOD BINK REPORT

GC/MS Bemivolatiles

Client Lot I...: D4D030176 Work Order #...: GDMS71AA. matrix .... : SOLID

PARAMETER2-Nitrophenol4-Nitrophenol4-Nitroquinoline-

1-oxideN-Nitrosodi-n-butylamineN--Nitrosodietb1yamineN-NitrosodimethylamineN-NitrosodiphenylamineN-Nitrosodi-n-propyl-

amineN-BitrosomethyletbylamineN-NitrosomorpholineN-Nitrosopiper&dineN-Nitrosopyrrolidine5-Nitro-o-toluidineParathionPentachlorobenzenePentachloroethanePentachloronitrobenzenePentachlorophenolPhenacetinPhenanthrenePhenolPhorate2-PicolicePronamidePyrenePyridine1,2,4,5-Tetrachloro-benzene

2,3,4,6-TetrachlorophenolThionazino-Toluidine1,2,4-Trichloro-

benzene2,4,5-Trichloro-phenol

2,4,6-Trichloro-phenol

0,0,0-Triethylphosphoro-thioate


RESULTRDNDND

REPORTIMLIMIT33016003300

IDNDEDNDND

330330330330330

IDEDNDNDNDNDNDNDNDNDlDNDNDED2DNDEDNDND

33033033033066016003301600160016006603303301600660660330660330

ug/kgug/kguzgtkg


ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kgug/kgug/kg


ug/kcg

ugtkg

ug/kg

ug/kg

8W846 8270C

SW846 8270CSW846 8270CSW846 8270C

EW846 8270C

8W846 8270CSW846 8270C

EW846 8270CSW846 8270C8W846 8270CSW846 8270C8W846 8270C

8W846 8270C8W846 8270CSW846 8270CSW846 8270CSN846 8270C

8N846 8270CSW846 8270C8W846 8270C8W846 8270C

8W846 8270CSW846 8270C8W846 8270C

8W846 8270C

8W846 8270C8W846 8270C

68846 8270C

-METHODS9846 8270CBW846 8270C

5W846 8270C

EDNDNDND

16001600660330

ND 330

ND 330

5W846 8270C

8W846 8270C

SW846 8270C

8W846 8270C

ND 1600

ND 1600


HIMOD BLMO REPO

GC/S Semaivolatiles

Client Lot #...: D4D030176 Work Order I...: GtM571AA, trix.........: SOLID

REPORTINGT.LTrrq MQTqI MpqweUnn

ADULTS~r- czar--v~

SURROATE2-FluorophenolPhenol-dSNitrobenzene-dS2 -Fluorobiphenyl2,4, 6-TribromophenolTerphenyl-dM4


RECOVERYLEITS(28 - 95)(35 - 90)(39 - 89)(35 - 86)(11 - 111)(30 - 98)

W0TE(S):CIadatios awe periformd before rcwfig io avoid mdO-ff arm k mi hed cmhLb

LAEORATRY aoNTROi SK14PLE Ey WiT=IO REPORT

GC/MS Sezmvolatiles

Client Lot I...: D4D030176LCS Lot-Sample#: D4D060000-621Prep Date ...... :t 04/07/04Prep Batch 1...s 4097621Dilution Factort 1

Work Order C...: GDM571AC Matrix .... : SOLID

Analysis

Analysis

Date..s 04/22/04Time..: 14:09

PARAMETERAeaephtehne4-Whoro-3-setbylphiendl2- loraphenol1,4-Dichlordbeznzene2,4-Dinitrotoluene4-UitrophenolN-Nitrosodi-n-propyl-

aminePentachlorophenolPhenolPyrene1,2,4-TriChloro-benzene

PERCENTRECOVERY75

797974

797575

RECOVERYLIMITS(49 - 89)(53 - 93)(52 - 92)

(47 - 87)(51 - 98)(37 - 103)(46 - 90)

METHODS8846 8270CSN846 8270C53846 8270C5846 8270CM846 8270CS846 8270CSn846 8270C

77797876

(37 -(52 -(46 -(49 -

96)92)95)89)

SW846SW8468W846R9S46

8270C8270C8270C

8270C

SURROGATE2-FluorophenolPhenol-d5Nitrobenzene-dS2-Fluorobiphenyl2,4,6-TribromophenolTerphenyl-dl4

PERCENTRECOVERY7677

76 .717S81

RECOVERYLIMITS(52 - 92)(52 - 92)(51 - 91)(47 - 88)(48 - 94)(50 - 103)

BOTE(S):Cdlazim oe pfnmed before fomdl w void rmducffamn hI ailated nea1Ls.

BMd pri deotu oz lpume

ZEORATORY CXTROL SAMPLE nac REPORT

GC/MS Semivolatiles

Client Iot 0...: D4D030176IC Lot-Sample#: D4D060000-621Prep Date ...... s 04/07/04Prep Batch 1... : 4097621Dilution Factor: 1

work Order ... : GDM571AC

Znalysis Date..: 04/22/04Analysis Time..: 14:08

Matrix ...... : SOLID

Acenapih en4-Chloro-3-methylphenol2-chiorophenol1, 4-Dibo ez2, 4-Dinitrotoluene4-NitrophienolN-Nitrosodi-n-propyl-

amine

Phenol

Pyrene1,2,4-TriduLoro-

benzene

SPIKEAMOUNT3300495049503300330049503300

4950495033003300

MEASUREDAMOUNT2470393039202450262037202490

3830392025902520

UNITSug/kguglkgugftug/kgug/kgug/kgug/kg

ug/kgug kgugWug/kg


METHODSN846 8270C9N846 8270C8(846 8270C8W846 8270C81(46 8270CSH846 8270C81846 8270C

77797876

81(94681(94681(84681(846

8270C8270C8270C8270C

SURROGATE

2-FluorophenolPhenol-d5Nitrobenzene-d52-Fluorobiphenyl2,4,6-TribromophenolTerphenyl-d14

PERCENTRECOVERY7677767175at

RECOVERYLIMITS

(52 - 92)(52 - 92)(51 - 91)(47 - 98)(48 - 94)(50 - 103)

NOTE(S):Ckunih= am perfmed kebforoxmug so ate smmdoff scm In hk ualW rcfs}old pAU d&wW atrl param

MATRa Spin 8W EVLXIO1 RFPRT

GC/MS Semivolatiles

Client Lot 0... sD4D030176MS Lot-Sanple tt D4D020177-001Date Sampled...: 04/01/04 09:4Prep Date ...... s04/07/04Prep Batch #...s 4097621Dilution Factor: 5

Work Order C...:

5 Date Received..:Analysis Date..:Pnalysis Time..

GDE20 LhX-MSGDE201A0 -MSD04/02/0404/22/0420:45

atri...... ... SOLID

Acenaphthene

4-Chloro-3-gethylpbenol

2- hlophrznol

1, 4-Dicblorobenzene

2,4-Diflitrotoluene

4-Nitrxphenol

N-Nitrosodi-n-prxpyl-amine

PERCENTRECOVERYMCDILNCDILNCDILNCDILDC,DILNC,DIhDC,DILNC,DILNC,DrLNC,DILNC,DILNC DILNCDXL

HCDIL

RECOVERYLIMITS(25 - 101)(25 - 101)(32 - 97)(32 - 97)(29 - 95)(29 - 95)(34 - 81)(34 - 81)(31 - 105)(31 - 105)(10 - 128)(10 - 128)(33 - 91)

RPDRPDLIMITS METHOD

0N846 8270C(0-40) 81846 8270C

S8846 8270C(0-40) 8N846 8270C

S1846 8270C(0-40) m846 8270C

E8146 8270C(0-40) 61846 8270C

61846 0270C(0-40) SW846 9270C

E8846 8270C(0-40) S8846 8270C

81846 8270C

(33 - 91) (0-40) S146 8270C

Pentachloropbenol

Phenol

Pyrene

1,2,4-Trichloro-benzene

HCDIDLWC, DILNC, DXLNC, DILKCIDILNCUDILNC. DIL

(10(10(34(34(13(13(33

- 101)

- 101)- 93)

- 93)

- 105)

- 105)

- 88)

S1846(0-40) 5846

51846(0-40) S5946

S1146(0-40) SR846

81(46

8270C8270C8270C8270C8270C8270C8270C

NC,DIL (33 - 88) (0-40) S8846 8270C

SURROGATE2-Fluorophenol

Phenol-dS

Nitrobenzene-ds

2-Fluorobiphenyl

2,4,6-Tribromophenol

PERCENTRECOVERYNC,DILNC, DILNC,DILNCDILNC,DILNC, DLNC, DILNC,DILNC,DILNCDIL

RECOVERYLIMITS(28 - 95)(28 - 95)(35 - 90)(35 - 90)(39 - 89)(39 - 89)(35 - 86)(35 - 86)(11 - 111)(11 - 111)


MATRIX SPIKE SAMPLE EVAWAITICO REPORT

GC/KS Semivolatiles

Client Lot I.,.: D4D030176MS Lot-Sample #: D4D020177-001

Work Order * ... : GDE201AX-MSGDE201AO-MSD

Matrix.........: SOLID

PERCENTSURROGATE RECOVERY

RECOVERYLIMITS

Terphenyl-dl4 KC,DILRC, DIL

(30 - 98)(30 - 98)

OTE (S):

calulaons am perboed borte nuaDt s0 to avoid md-off a b causatd madtL

Dom pdzt 4amoes reuro param m~NC The ncoveuy uIor RPD sm not calcslad.DIL Te coie"atnion h estimated or rti reporsed due to dilution or dfe prese of bmfatSh ayes

}ATRIK m SAMPLE DATA REPORT

GC/MS Semivolatiles

Clielt Lot #...:

uS Lot-Sample #:Date Sampled...:Prep Date .. :...

D4DC30176 Work Order #... :D4D020177-001

04/01/04 09:45 Date Received..:04/07/04 Analysis Date.. s

GDE201AX-MSGDE201AO -MSD04/02/0404/22/04

matrix ......... : SOLID

Prep Batch 1...: 4097621Dilution Factor: 5

Analysis Time.. : 20:45

PARAMETERA hene

4-hloro-3-methylphenol

2-Chlorophenol

1,4-Dichlorobenzene

2,4-Dinitrotoluene

4-Hitrophenol

N-Nitrosodi-n-propyl-amine

SAMPLE SPIKE MEASRD

AMOUNT AIT AMOUNTND 0.0RD 0.0

ND 0.0RD 0.0RD 0.0ID 0.0ND 0.0RD 0.0RD 0.0ED 0.0ID 0.0WD 0.0RD 0.0

UNITS

Uw/gug/kgug9/kuglkgug/ksug9/kugl/guglkgug/kgug/kgug9/kug/kgUg/kg

PERCETRECVRYNCD3hNCUDILNCEDIhNCDILNCDILNC,DILIDICMDLNCDILNCDILXC,DILNCDILNC,DIL

NICDIK

NC,DIL

RPD METHOD51146 8270C8H846 8270C51146 8270CS5846 8270C68W46 8270CS1846 8270C81146 8270C51846 8270CSW846 8270C5846 8270CS5846 8270CS8146 8270CS1846 8270C

5846 8270CWD 0.0

Pentadblorophenol

Phenol

NDEDNDND

ImJNDNM

ND

0.00.00.00.00.00.00.0

0.0

ug/kg


uglkgug/kg

ug/kg

NC.DILNCDILNCDILXCDILHCDILNC,DI3LNC,DIL

NC,DXL

5W846SW1468H846S884681146S8146

81846

8270C8270C8270C8270C8270C8270C8270C1,2,4-Trichioro-

benzeneS81146 8270C

SURROGATE2-Fluorophenol

Phenol-d5

Nitrobenzene-d5

2-Fluorobiphenyl

2,4*6-Tribromophenol

PERCENTRECOVERYNC.DILNCDIL

NC,DILNCDILNC, DILNC,DIL

NC.DILNCDILNC,DIL

KC,DIL

RECOVERY

LIMITS(28 - 95)(28 - 95)(35 - 90)

(35 - 90)(39 - 89)(39 - 89)(35 - 86)(35 - 86)(11 - 111)

(11 - 111)


NATRZK m SAME Dfl REPOtT

CC/M Semivolatiles

Client Lot #...: D4D030176HS Lot-Sample #: D4D020177-001

Work Order ... : GDE201AX-MSODE201AO-MSD

atriX......... SOLID

PERCTETRECOVERYv_

RECOVERYLIMITS

(30 - 98)(30 - 98)

Terphenyl-dl4 CCDILNC,DIL

NOTE(S) :C<muda am pafd befoe zmmuing so miod bind-off arm hi alaced seftBold Viml denote cantrol param terNC The cvery mdor PD we mot Idud.DIL The co ccradon Es asmud or ut rpoeed due oiDd or dAe-p of iterfeting alycm

ETHO B REPORT

GC semivolatiles

Client Lot ... : WDD030176HB Lot-Sample 0: D4D050000-552

Alnalysis Date..: 04/28/04Dilutimn Factor: 1

Work Order # ... s GDJSX1AA

Prep Date ..... : 04/06/04Prep Batch 1...t 4096552


Analysis Tioe..: 13:34

PARAMETER

Aldrin

alpba-BHC

beta-EHC

delta-BEC

gamia-EXC (Lindane)

Chlordane (technical)

4,4 -DDD

4,4'-DDE

4,4'-DDT

Dieldrin

Endrin

Endrin aldehyde

Endosulfan I

Endosulfan II

Endosulfan sulfate

Heptachlor

Heptachlor epoxide

Methoxychlor

Toxaphene

RESULTND

NDNDNDNDNDNDNDNDEDNDND2EDNDNDND

ND

REPORTINGLIaT1.71.71.71.71.7171.71.71.71.71.71.71.71.71.71.71.73.3170

UNITS

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgu/kg

ME=TOD8W846 8081ASW846 B08SASW846 8081A8W846 8081ASW846 808616W846 80BlASW846 8082A5W846 8081A8W846 8081A8W846 8081ASW846 8081A

E8846 8081ASW846 8081A8W846 8081ASW846 8081ASW846 8081ASW846.80812EW846 8081ASw846 80812A



RECOVERYLMaTS(41 - 142)(50 - 127)

NOTE(S):

LABOPAUY ONTROL SaMPE EVABWLTIO REPORT

GC Semivolatiles

Client Lot t...: D4D030176WCS Lot-Sauplet: D4D050000-552Prep Date ...... s 04/06/04Prep Batch 1...: 4096552Dilution Factor: 2

PARAMETERAldringamna-DMC (Idndane)4,4 -DDTDieldrinEndrinHetahl or

Work Order t... : GDJ8X1AC MatriX ......... SOLID

Analysia Date..: 04/24/04Analysis Tim..: 02:12


RECOVERY

LIMITS(72 - 113)(71- 112)(66 - 125)(76 - 115)(73 - 124)(68 - 123)

METHOD51(84651(84651(84691(4651(4651(846

9081A~8082ASOSlA.SO81.A80811

08B1&

DecachlorobiphenylTetracbloro-mn-xylene


RECOVERYLIMITS(66 - 128)

(65 - 119)

07E (S):caiaii2dow ar performed More rocaUnDg to xavod udoff aosn h lcubed resuaslsold prv denomes couM par s

IABORATMY CONTROL - DATA REPORT

GC semivalatiles

Client Lot #... a D4D030176LCS Lot-Sample#: D4D050000-S52Prep Date ...... : 04/06/04Prep Batch 0...' :4096552Diluticu Factor: 1

Work Order 0...: GDJ8X1AC Matrix .... : SOLID

Analysis Date..: 04/24/04Analysiz Time..: 02:12

PARAMETERWAri

gama-BEC (T.4nan )4, 4 ' -DDTDieldrinEndrin

IHeptacbor

SPIKEAMOWNT

16.716.716.716.716.7

16.7

MEASUREDAMOUNT16.8

16.3

17.817.720.216.9

UNITSug/kguglkgugIkgugkcgug/kgug/kg

PERCENT

RECOVERY10198107106121101

METHOD8W846 808ka8W846 8081281846 8081AS8146 8081A81846 808125846 8081A

SURROGATEDecachlorobiphenyl

Tetrachloro-m-xylene


RECOVERY

(66 - 128)

(65 - 119)

NOTE(S) :hdk =ons we pernwed befote frdh 10 aoid =nd-off h .b ah renft.

Bod pt denoes a8mw pzirma

HATI m SAMPL EVAXADMON RE'ORT

GC Semivolatiles

Client Lot 0...: D4D030176NS Lot-SamPle #: D4D010150-002Date Sampled ... : 03/29/04 08:04Prep Date ...... : 04/06/04

Prep Batch C..: 4096552Dilution Factor: 1

Work Order 0...:

Date Received..:analysis Date..:Analysis Time..:

GET271AD-HSGET271AE-MSD03/30/0404/24/0403:09

KatriX .... : SOLID

PARAMETERAldrin

gama-BUC (Lindane)

4,4'-DDT

Dieldrin

Endrin

Eleptachior

PERCENTRECOVERYNCDILNC,DILNC,DILNC,DILHC,DILNC,DILNC,DILNC,DILnc,nxr

JC, DNC,DImNCDIL

RECOVERYLIMITS156 - 117)

(56 - 117)

(55 - 122)

(55 - 122)(47 - 132)

(47 - 132)

(57 - 117)(57 - 117)

(56 - 130)

(56 - 130)(41 - 134)

(41 - 134)

RPDRPDLIMITS METHOD

S6846 1(0-30) 61146 1

8W846 I(0-30) 8N146 1

81846 1(0-30) 81846 I

S6846 I(0-30) 8N846 1

51846 I(0-30) 6R846 I

81146 1(0-30) 61846 1

8081A8081A0 8IA

3081A3081A3081A8081A3082k3081A3081A3081A3081A



PERCENTRECOVERYNC,DIL

NCDILNC,DILSC,DIL

RECOVERYLIMITS(41 - 142)(41 - 142)(50 - 127)

(50 - 127)

NOTEs) :C& u a-e pefmed btefort ounding W aiod mound-offerwrs i aa ned mblc

BoUl pft denoes corol paraemmNC De cay nd/or RPD ah. mm acuW.DIL The kwnaW= b adiued or Wot repoeW due to diklon or bc preseof ofberfing xrmyos

GC semivolatiles

Client Lot # ... s D4D030176MS Lot-Sawple #: D4D010150-002Date Saqpled ... : 03/29/04 08s04Prep Date ...... : 04/06/04Prep Batch 1 ... : 4096552Dilution Factor: 1

Work Order # ... :

Date Received..:Analysis Date..sAnalysis Time..

GET271AD-MSGET271AE-MSD03/30/0404/24/0403:09

Matrix......... : SOLID

PARAMETERAldrin

gamma-BBC (Lindane)

4,4 ' -DT

Dieldrin

Eadrin

SAMPLE SPIKE MEASRDAMOUNT AMT AMOUNT

MDMDND1DNDRD

NDJlDRD

ND

t1NITS

ug/kguglkg

ug/kgng/kgw9/k9ug/kguglkgug/kugfkguglkgug/kg

PERCNTRECVRYNC,DnLNC,DILNC,DILNC,DILNCDILNC,DILXC,DILNC,DMNC,DILXC, DELNCDILNC,DIL

RPD METHODS8846 8081k81146 0081A81846 8081A81846 8081A5816 083LA

M846 8081O81846 80lA

6W846 808LaS1846 8081k8W846 8081L81846 B081hSH846 8081A



PERCOEfTRECOVERYNC,DILNC,DILNCDILNC,DIL

RECOVERYLIMITS(41 - 142)(41 - 142)(50 - 127)(50 - 127)

NOTE (S):

Bol pdt deote swcor pmers

NC lie enray aydeor RPD were e cakulntc

DIL The ceauzd= hadmaed or = rqwnad due w dlldo atr pere o f efd ng valyt

METHOD IRTUK REPORT

GC Semivolatiles

Client Lot C...: D4D030176

HB Lot-Sample #: D4D040000-125

Analysis Date..: .04/12/04

Dilution Factor: 1

PARAMETERAziDphos-methylBolstarChlorpyrifosCoumaphosDemeton (total)DiazinonDichlorvosDimethoate

DisulfotonEthopropEthyl parathionFamphurFensulfothionFenthionMalathionMerphosMethyl parathion

14evinphosNaled00, 0-Triethylphosphoro-

thioatePhorateRonnelSulfoteppThionazinTokuthionTrichloronateEPNDemeton-ODemeton-STetrachlorvinphos (Stirop

Work Order #...: GDHT41kA

Prep Date ...... : 04/04/04Prep Batch ... : 4095125

Matrix .... : SOLID


RESULTNDNDNDIDNDNDNDNDND

NDNDNDNDNDNDNDNDNDNDND

REPORTINGLDMIT1313131313131313

131313131313131313133313

UNITS

ug/kgug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kgug/kgug/kg,ug/kgug/kgug/kgug/kgug/kg.ug/kgug/kgug/kgug/kg


METHODSW846 I8W846 I

8W846 ISW846 I

8W846 ISW846 ISW846 I

8W846 1

SW846 1

8W846 ISW846 I

8W846 18W846 1SW846 1

8W846 18W846 1SW846 I

SW846 i8W846 1

8W846 9

SW846 15846 I

8W846 18W846 1

8W846 18W846 I

8W846 E

8W846 ISW846 I

SW846 8

B141AB141h8141A8141A8141A3141k3141A314LA

3141A8141A3141A8141A8141A8141A8141A8141A8141A8141A1141A1141A

1141h1141A1141A1141k1141A8141A8141A8141AB141A141A

NDND

ND

ND

ND

ND

ND

ND

ND

ND

13671313131313131313

SURROGATEEthyl Pirimifoschlormefos

PERCENrRECOVERY7076


NM re(s)Cdcaahwoo ame pero=We beore rowdlg o avoid rood-off mrom In clulatda Ecufta.

1ABORATORY CORJROL SAMPLE EVALUATION REPORT

GC semivolatiles

Client Lot C..: D4D030176

LCS Lot-Sauple#: D4D040000-125Prep Date ........ 04/04/04Prep Batch #...: 4095125Dilution Factor: I

Work Order C...: GDHT41AC-LCS Matrix ..... : SOLIDGDHT41AD-LCSD

Analysis Date-.: 04/12/04Analysis Time..: 07:35

PARAMETERDemta (total)

Diazinan

Etbyl parathion

Halathion

Methyl parathion

Pborate

PERCENTRECOVERY

116 a32 p175 a180 a138 a166 a168 a165 a151 a171 a160 a135 a

RECOVERYLIMITS

(27 - 104)(27 - 104)(60 - 13S)(60 - 135)(74 - 127)(74 - 127)(64 - 138)(64 - 138)(72 - 108)(72 - 108)(58 - 106)(58 - 106)


51846113 (0-40) C8146

5118463.0 (0-40) 81846

C814619 (0-40) CR846

681461.5 (0-40) 81846

8184612 (0-40) R8846

R884617 (0-401 C8846

8141A8141A814118141A8142A8141A8141A8141k8141k8141A8141k8141k

SURROGATE

Ethyl Pirimifos

Chlormefos

PERCENTRECOVERY

88763E4

RECOVERYLIMITS(36 - 118)(36 - 118)(59 - 112)(59 - 112)

NOTE(S) sCdlaldo are perfolud before moift ao d rund-offerroIn cd ulated resufr .

3ld ;dnf denoe Gooftot punmers

p RlWve pere dIfferarce GRPD) k emswde nated cntl Wm

t Spiked uyce scoovery h eutaide awed cowtol limits.

LABORATORY aCITTOL SMLE DATA REPORT

GC Siivlti

Client Lot f...:WCS Lot-Sanplet:Prep Date ...... sPrep Batch I... :Dilution Factor:

D4D030176D4D040000-125

04/04/0440951251

Work Order Y... : GDHT41AC-LCS Matrix ......... 2: SOLIDGDHT41AD-LCSD

AnalySiS Date..: 04/12/04knalyuis Time..: 07:35

SPIKE =EAZUREDPARAMETERDemeton (total)

Diazzmen

Ethyl parathion

Malathion

Methyl parathion

Ehorate

AM6666.766.766.766.766.766.766.766.766.766.766.766.7

AMOUNT77.2 a21.6 p116 a120 a91.9 a111 a112 a110 a101 a114 a106 a90.1 a

UNITS

Wlkgug/kgugkgUI/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg


RPD METHOD81846 8141A

113 21846 8141A2W846 8141A

3.0 61846 8141A61146 8141A

19 6N846 8141-A2W846 8141A

1.5 6W846 8141A6w846 8141A

12 S2846 8141AS8146 8141-A

17 81846 8141A

Ethyl Pirimifos

Chlormefos


RECOVERYLIMITS(36 - 118)(36 - 118)(59 - 112)(59 - 112)

NOTE(CS) :Caitmo ae perbfod before wning lo avoid round-off ero hin alaculed 1mdis

Bold pFrmt des cocro pameter

p Relstive pee dffeco (D) E oumside aaed cootrol ihmis.

a Spiked aIMly cimoveij k outside azwed enabunlimi

MRTRZ SPTIKESMPLE EVALU&TION REPORT

GC Semivolatiles

Client Lot C...: DtKS Lot-Sample 6: DDate Sampled...: Os'Prep Date ...... s04Prep Batch 6...: 4sDilution Factor: 1

1D0301761C230295-008

Work Order C..:

1/22/041/04/04O95125

09:45 Date Received..:Analysis Date..:Analysis Time..s

GCQ2E1DC-MSGCQ2ElDD-HSD03/23/0404/12/0409:47

Matrix .... . s OLID

PARAMETER

Demeton (total)

Dniznion

Ethyl parathion

Malathion

Methyl parathion

Phorate

PERCENTRECOVERY227 a207 a228 a214 a170170184 a186 a177 a179 a201 a193 a

RECOVERYLIMTS(33 - 131)(33 - 131)(20 - 168)(20 - 168)(20 - 175)(20 - 175)(42 - 148)(42 - 148)(35 - 129)(35 - 129)(20 - 145)(20 - 145)

RPDRPD LIMITS HETHOD

81(469.3 (0-40) 81(846

S18466.4 (0-40) 61846

8W8460.26 (0-40) 61846

91(461.3 (0-40) 51846

9W8461.0 (0-40) 6W(846

818464.0 (0-40) S;8146

8142A8141A8141A8141A8141A8141A8141A8141A8141k8141h8141A8141A


Chlormefos


RECOVERYLIMITS(11 - 137)(1t - 137)(37 - 124)(37 - 124)

NOTE(S)):Caladam amc pomed befrouendig so awd wund-off a in eakulatd ets.ld prA dees coned panmems

a SpIked anyed ecv= keulut aced ceaml limbs.

Re hs an qoti i hasve bee u W or dry we

ATRIX 8P SAMPLE DA.A REPORT

GC Semivolatiles

Client Lot I ... :MS [ct-Sample #sDate Saxpled...:Prep Date ...... :Prep Batch U ... :Dilutioa Factor:

D4D030176D4C230295-00803/22/04 09:4504/04/0440951251

Work Order #...:

Date Received..:Analysis Date..:Analysis Time..:

GCQ2E1DC-MSGCQ2E1DD-MSD03/23/0404/12/0409:47

Matrix .... : SOLID

PARAMETERDeMeton (total)

Diaziflon

Ethyl parathio

Halathion

Hethyl parathio

Phorate

SAMPLEAMOUNTEDIDND

DD

NDNDEDND

llDN9DED

SPIKEAMT93.093.093.093.093.093.093.093.093.093.093.093.0

MEASRDAMOUNT UNITS

211 ug/kg192 ug/kg212 ug/kt199 ug/kg158 ug/kg158 ug/kg171 Ug/kg173 ug/kg164 ug/kg166 ug/kg187 ug/kg180 ug/kg

PERCUTRECURY RPD METHOD227 a 51846 8141A207 a 9.3 81846 8141A228 a SW846 8141A214 a 6.4 51846 81412170 S5846 8142k170 0.26 5S146 8141A184 a SR846 8l41A186 a 1.3 51146 81412177 a 5N846 8141A179 a 1.0 5846 8141a201 a Sn846 8141A193 a 4.0 511846 8141A


Chlormefos


RECOVERYLIMITS(11 - 137)(11 - 137)(37 - 124)(37 - 124)

NOT(Ss):Cd cuim ave peformed before mut w mid round-4ff hi cacuted r!wBold primdenoe co=o parmee

a Spiked yte emovay k de = Ued contol Wmhs.Resks cmd odg i ends hr bftn aduised dry we!&.

MTED SLIM REPRT

GC Semivolatiles

Client Lot I...: D4D030176HB Lot-Sample f. D4D070000-553

Analysis Date..: 04/13/04

Dilution Factor: 1

Work Order ... :DQR1AA

Prep Date ...... : 04/08/04Prep Batch U ... : 4098553

Matrix .... D : SOLI

Analysis TiMe..t 17:39

PARAMETER2,4-D2,4-DB2,4,5-T2,4,5-TP (Silvex)DalaponDicambaDichlorprop

DinosebMCPAMKPP

RESULTEDNDNDNDNDNDND

NDNDND

REPORTINGLIMIT80

2020204040801280008000

UNITS

ug/kgug/kgug/kgVg/kg


METHODS8146 8151A8W846 8151A

SW846 8151A8W846 8151A

81846 815LASW846 8151A8W846 8151ASN846 8151ASW846 8151ASW846 8151A

SURROGATEDCAA

PERCENTRECOVERY

96

RECOVERYTL TS

(39 - 96)

NOTE (S):

Cakuafig- am Paned bfore MiUing I uoid rou-Off C= in Chk ta rMU.

IUBORAT= CcETROL SMPWL EVLUMICN REPORT

GC Semivolatiles

Client Lot ... : D4D030176WS Lot-Sanpleft D4D070000-553Prep Date ...... : 04/08/04Prep Batch 1...: 4098553Dilution Factor: 1

Work Order #... : GDQMRLAC-LCS Matrix......... : SOLIDGDQNRIAD-LCSD


PARAMETER2,4-D

2,4,5-T

2,4,5-TP (Silvez)

PERCENTRECOVERY93 a89111108112110

RECOVERYLIMITS

(26 - 92)(26 - 92)(26 - 115)(26 - 115)(31 - 114)(31 - 114)


5N846 M152A5.1 (0-40) SH846 8151A

SW846 8151A2.6 (0-40) 5W846 8151A

SW846 8151A2.1 (0-40) BW846 8151A

SURROGATEDCAA

PERCENTRECOVERY102 *

95


OTE (S):Omdadons are pertmed before gmdhg to void rowd-ofrfavrs in cabAmed maUL

BNO pft dene p== Imtm

a Spikd oye mvay bmide d sonirolmi

* Surwgpe recoveay iontfde aed ano vmhL

aCOROL SAMPLE DA REPORT

GC Semivolatiles

Client LOt #.. .: D4D030176

LCS Lot-Samle$: D4D070000-553Prep Date ...... z 04/08/04Prep Batch 1... : 4098553Dilution Factor: 1

Work Order #...s GDQNRAC-LCS Matrix .... : SOLID

GDQNR1AD-LCSDAnalysis Date..: 04/13/04Analysis Time..: 16:20

SPIKE MEASMUR PERCENTPARAMETER2,4-D

2,4,5-T

2,'I5-TP (Silvex)

AMo=64.064 .16. 016.016.016.0

AMOUNT59.8 a56.817.717.318.017.6

MITS RECOVERY

Ug/g 93ug/kg 89ug/kg 111

g/kg 108ug/kg 112ug/kg 110

RPD METWODS8846 8151k

5.1 51846 8151A81846 8151A

2.6 91(846 8151A61(846 8151k

2.1 SR846 8151k

SURROSATEDCAA

PERCENTRECOVERY102 *95


NOTE (S) :azuais wre pufamd bfort toung D avoid mmd offem In icatmiat re

Bd prm dems contro l pam

a S4&d msIyte evey I oude sae mo imit.

* Suwmgae ery k ouie atwd Wvtt lins

3: BP= MPW EVMALU=TI REPORT

GC Semivolatiles

Client Lot E...: D4D030176NS Lot-Sample t: D4D070249-001Date SaMpled ... : 04/05/04Prep Date ...... : 04/08/04Prep Batch 0 ... : 4098553Dilution Factor: -I

Work Order #...:

Date Received..sAnalysis Date..:Analysis Time. .:

GDPJ4LhJ-MSGDPJ41hX-MSD04/07/0404/14/0402:38

matrix ... .: SOLID

2,4-D

2,4,5-T

2,4,5-TP (Silver)

PERCENTRECOVERY103 a81121 a103120 a101

RECOVERYIMIS(26 - 92)(26 - 92)

(26 - 115)(26 - 115)(31 - 114)(31 - 114)

RPDRPD LIMITS _ METHOD

8K84623 (0-40) EW846

884616 (0-40) 81(846

8W84617 (0-40) 8846

815LASISlA8LMIA8152A8151A8152A

SURROGATEDCRA

PERCENTRECOVERY103 *88

RECOVERYLIMTS(39 - 96)(39 - 96)

NOTE(8):Cdca ire am pefxed efore ,imdi to m smd-off aors IamW ed ruft

aom pd 4e ames con pummm

a Sp&ed mnslym memM k oteide Ktd corl lmft.

Lurropte movay Iks ou e mat contol Slts

MATRIX S SANPLE DN REPORT

GC Semivolatiles

Client Lot # ... I D4D030176 Work Order C...:NS lot-Sample #: D4D070249-001Date Sampled ... : 04/05/04 . Date Received..:Prep Date ...... : 04/08/04 tAnalysis Date..:Prep Batch # ... : 4098553 Analysis Time..Dilution Factor: 1

GDPJ41AJ-MSGDPJ41AK-4SD04/07/0404/14/0402:38

Matrix......... : SOLID.

2,4-D

2,4,5-T

2,4, 5-TP (Silvex)

SAMPLE SPIKEAMOUNT ANTED 64.0RD 64.0MD 16.0MD 16.0MD 16.0WD 16.0

MEASRDAMOT65.652.119.416.519.216.2

UNITSug9/kug/kgug/kgug/kgugl/guglkg

PERCNTRECVRY103 a81121 a103120 a101

RPD METHODSnB46 1

23 8W846 I8WB46 1

16 5846 I5W846 1

17 0S846 I

MLIABISIA815IAB15LABiSIA8151A

SURROGATEDCAA

PERCENTRECOVERY103 *

se


BME(S):Chwuhfio we perfomed before oundl lo avoid mnd-offom h calmlated emsults.ld prim dauen trol prametrs

a Spiked NWe recovezy is outside oaed r ntrol I Wm* Surroe rcovay I Suidted conro EM

=MTD BLANK REPORr

TOTAL metals

Client Lot # ... : D4D030176 H atri r .S....... s SOLID

REPORTINGLIMIT

PREPARATION- WORKMETHOD ANALYSIS DATE ORDER IPAIZMrDTER PRASTTU UNIqiS

HB Lot-SampleMercury

#: D4DOS0000-254 Prep Batch 0...:ND 33 ug/kg

Dilutio Factor: 1Analysus Time. . 11:44

4096254SW846 7471A 04/13-04/14/04 GDH7J1AP

BB Lot-SanpleArsenic

4: D4D060000-647 Prep Batch ...: 4097647ND 1.0 mg/kg SW846 6010B

Dilution Factor: 1Analysis Time..s 01:24

04/09-04/17/04 GDM8G1AC

Lead ND 0.80 mg/kgDilution Factor: 1Analysis Time..: 01:24

6W846 6010B

EW846 6010B

04/09-04/17/04 GDMSG180

04/09-04/17/04 GDM8G1ANSelenium 1.3DilutionAnalysis

mg/kgFactor: 1Tize. .s 01s24

Barium ND 1.0DilutionAnalysis

Mg/kgractort 1Time..: 01:24

SW846 6010B 04/09-04/17/04 GDMsQlAD

Cadmium

Chromium

Silver

ED 0.50 mg/kgDilution Factors 1Aalyssl Time..2 01:24

1.0 mg/kgDilution Factor: 1Analysis Time.. 01s24

1.0 mg/kgDilution Factor: 1Analysis Time..s 01:24

SW846 6010B

SW846 6010B

SW846 6010B

04/09-04/17/04 GDM$GLAF

04/09-04/17/04 GDM8G1AG

04/09-04/17/04 GDM3GlAPND

NOS(S) :Caeuadows ae perforted before rodng t0 avod rond-off em In calhm msus.

LASORATORY CONTROL SMPLE EVALMWIO RE ORT

TOTAL Metals

Client Lot 6-..: D4D030176

PERCENT RECOVERYPARAMETER RECOVERY LIMITS METHOD

WS Lot-Samplef: D4D050000-254 Prep Batch #...: 4096254Mercury 90 (82 - 113) SW846 7471A

Dilution Factor: 1 Analysis

LCS Lot-Sanple#: D4DO60000-647 Prep Batch #...t 4097647Arsenic 89 (80 - 111) SW846 6010B

Dilution Factors I Analysis

Lead 91 (80 - 116) SW846 6010BDilution Factors I Analysis

Selenium 88 (80 - 112) SW846 6010BDilution Factors 1. Analysis

Barium 97 (80 - 117) SW846 6010BDilution Factors 1 Analysis

Cadmium 88 (80 - 119) SW846 6010BDilution Factor: 1 Analysis

Chromium 94 (80 - 120) 8W846 6010BDilution Factor: 1 Analysis

Silver 93 (80 - 109) SW846 6010BDilustion Factor: 1 Analysis

NOTE(S) IlcaUos am padmed bcore rounding l *void vound-off ans In cadIand asulm

Matrix . .3: SOLID

PREPARATION-ANALYSIS DATE WORK ORDER #

04/13-04/14/04 GDH7J1AC

Time..: 11s46

04/09-04/17/04 GDHSO1AVTime..s 01229

04/09-04/17/04 GDM8G1A4Time..: 01s29

04/09-04/17/04 GDM8GLA7Time.. s 01s29

04/09-04/17/04 GDM8GlAWTime. . 01m29

04/09-04/17/04 GDMSGlAOTise..: 01:29

04/09-04/17/04 GDMSGlAlTime.. 3 01:29

04/09-04/17/04 GDMtGlABTime.. a Gls29

LABORATORY OaOaT , SLIE DATh REPORT

TOTAL metals

Client Lot C....: D4D030176 Hatris .... D.... : SOLID

SPIKE MEASURED PERCNT PRBPARATION- WORKPARAMETER AMOUNT AMOUNT UNITS RECVRY METHOD ANALYSIS DATE ORDER #

LCS Lot-Saxzplef: D4DO50000-254 Prep Batch 4...: 4096254Mercury 833 750 ug/kg 90 SW846 7471A 04/13-04/14/04 GDH7J1AC

Dilution Factor: 1 Analysis Time. . s 1s46

LCS Lot-Sample#: D4D060000-647 Prep Batch C..: 4097647Arsenic 200 177 mglkg 89 8W846 6010B 04/09-04/17/04 GDM8G1AV

Dilution Factors 1 Analysls Time..: 01s29

Lead 50.0 45.6 mg/kg 91 BW846 6010B 04/09-04/17/04 GDM8GlA4Dilution Factor: 1 Analysis TLe...s 01:29

Selenium 200 177 mg/kg 88 SW846 6010B 04/09-04/17/04 GDM8G1A7

Dilution Factor: I Analysis Time..: 0M29

Barium 200 193 mg/kg 97 EW846 6010B 04/09-04/17/04 GDM8G1AWDilution Factor: 1 Analysis Time..: 01:29

Cadmium 5.00 4.40 mg/kg 88 £W846 6010B 04/09-04/17/04 GDM8G1A0

Dilution Factor: 1 Analysis Time : 01:29

Chromium 20.0 19.7 mg/kg 94 6W846 6010B 04/09-04/17/04 GDM8G1A1Dilution Factors 1 Analysis Time..S 01:29

Silver 5.00 4.65 mg/kg 93 8846 6010B 04/09-04/17/04 GDM8G1ASDilution Factors 1 Analysis Tine. s 01:29

Cah0A;1ns at purkmed betor :ouing to 1od lwudoffawn b culamd remkl

KA7TR BP SAMPLE EVMDhUlION REPORT

TOTAL metals

Client Lot #...z D4D030176Date Sampled...: 03/29/04

Matrix ..... : SOLIDDate Received..: 03/30/04

PERCENT RECOVERY RPD

PARAMETER RECOVERY LIMITS RPD LIMITS METHODPREPARATION- WORKANALYSIS DATE ORDER #

US Lot-Sample #:Mercury 104

93

D4C300294-001 Prep Batch #...: 4096254(82 - 113) SW846 7471A

(82 - 113) 10 (0-20) SW846 7471ADilution Factort 1.Analyuis Tim. .i lSO*0

04/13-04/14/04 GC7TP1CE04/13-04/14/04 GC7TP1CF

NMO(S):cao am prfofmeld berore mmdlgs loD r found-offmon in ccW zesusb

Resits and apoxdn Imhs bs been aeumd for dry weg&.

MQdTRIX SPIKE SAMPLE DA32L REPORT

TOTAL Metals

Client Lot #... : D4D030176Date Sampled...: 03/29/04

HatriX .. O...... : SOLIDDate Received..: 03/30/04

SAMPLE SPIKE MEASRD PERCHTPARPAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD

PREPARATIORq-ANALYSIS DMTR

WORKORDER #

4S Lot-Sanple #: D4C300294-001 Prep Batch C...: 4096254Mercury

44 96644 966

1050 ug/kg 104945 ug/kg 93

Dilution Factors 1Analysis Time.- llt50

8W846 7471A10 5W846 7471A

04/13-04/14/04 GC7TP1CE04/13-04/14/04 GC7TP1CF

NOTE S) sCdadatms am parfowat before bauad tI &vol mid-cIT uors In Caad rwkLcs.

Reisuht wxd rwqg labw have ben bd r dI y wdgbL

M19TRIX SPI SAPLE EVULUWIM RE 'T

TOTL Metals

Client Lot t...: D4D030176Date Sampled...: 04/01/04 09:45 Date Received..: 04/02/04

PERCENT RECOVERY RPDPARAM4ETER RECOVERY LIMITS RPD LIMITS METHOD



WORKORDER #

FS lot-Sample #: D4D020177-001 Prep Batch 1...: 4097647

Arsenic 44 N76 *

Lead 44 N79 *

Selenium

Barium

Cadmium

46 N77 *

52112 *

4072 *

(76 - 111) 6W846 6010B(76 - 111) 52 (0-30) 8W846 60103

Dilution Factor: 1uaalyzis Time..-: 0142

(70 - 200) SW846 6010B(70 - 200) 54 (0-40) SW846 6010B

Dilution factor: 1Analysis Tie..: 01:42

(76 - 104) 5W846 6010B(76 - 104) 51 (0-30) SW846 6010B

Dilution Factor: 1


(52 - 159) 8W846 6010B(52 - 159) 53 (0-30) 8W846 6010B

Dilution Factor: 1Analysiu Time..s 01:42

(40 - 130) EW846 6010B(40 - 130) 56 (0-30) SW846 6010B

Dilution Factor: 1Analysis Time..: 01:42

(70 - 200) 5W846 6010B(70 - 200) 8.6 (0-40) SW846 6010B

Dilution Factor: 1

Asalydsi Time..s O:sU

04/09-04/17/04 GDE201A3

04/09-04/17/04 GDE201A4

04/09-04/17/04 GDE201CJ

04/09-04/17/04 GDE201CK

04/09-04/17/04 GDE201CO

04/09-04/17/04 GDB201CR

04/09-04/17/04 GDB201AS04/09-04/17/04 GDE201A6

04/09-04/17/04 GDE2O1A904/09-04/17/04 GDE201CA

04/09-04/17/04 GDE201CC04/09-04/17/04 GDE201CD

Cbromium 136119

silver 45 N79 *

(75(75

- 141)

- 141) 51 (0-30)Dilution Factor: 1

Analysis Time..s :1:42

S1846 601GB8W846 6010B

04/09-04/17/04 GDE201CTP4/09-04/17/04 GDE201CU

OTE8(s):Caiahdo at paftmed befot =oimdk So aoi wmd-offcomn In c tdaed smu.N Spikd acyfe ioery k oude aculed 1am EmRb -d repordg Hmmt be beenl a e for dry wdL

* Rd-ve peceat diffnce (M1D) Is oi cud co im

HLTRIX SPUR SAMPLE DATA REP(RT

TOTAL Metals

Client Lot t...:Date Slampled'.'.:.2

D4D03017604/01/04 09:45 Date Received..: 04/02/04

Matrix ..... ,.2 SOLID

SAMPLE SPIKE HEASRD PERCNTPARAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD

PREPARATION- WORKAULLYSIS DATE ORDER #

MS Lot-SampleArsenic

t: D4D020177-001 Prep Batch C...: 4097647

1.7 2071.7 207

92.6 N Mg/kg 44158 * Mg/kg 76

Dilution Factor: 1Azalysiu Tie. .: 01:42

S1W846 6010B52 SW846 6010B

04/09-04/17/04 GDE201A304/09-04/17/04 GDE2O1A4

Lead2.12.1

51.7 25.0 N mg/kg51.7 43.2 * mg/kg

Dilution Factor: 1

4479

SW846 6010B54 SW846 6010B

04/09-04/17/04 GDE201CJ04/09-04/17/04 GDE201CK

Analysis Time..s 01:42

SeleniumRD 207ND 207

94.9 N Mg/kg160 * Mg/kg

Dilution Factort 1

4677

SW846 6010B51 SW846 6010B

04/09-04/17/04 GDE2O1oQ04/09-04/17/04 GDE201CR

Analynis Time..1 01342

Barium67 20767 207

173 mg/kg 52298 * mg/kg 112

Dilution Factor: 1


8W846 6010B53 SW846 6010B

04/09-04/17/04 GDE201A504/09-04/17/04 (WE201A6

Cadmium

ND 5.17 2.09 mg/kgND 5.17 3.73 * mg/kg

Dilution Factor: 1.

4072

8w846 6010B56 SW846 6010B

04/09-04/17/04 GDE201A904/09-04/17/04 GDE201CZ


chromium

Silver

13 20.7 40.8 mg/kg 13613 20.7 37.5 mg/kg 119

Dilution Factors 1Analysis Time..S 01i42

SW846 6010B8.6 8W846 6010B

8W846 6010B51 SW846 6010B

04/09-04/17/04 GDE201CC04/09-04/17/04 GDE201CD

04/09-04/17/04 GDE201CT04/09-04/17/04 GDE201CU

0.18 5.17 2.53 N mg/kg0.18 5.17 4.24 * Mg/kg

Dilution Factors I

4579



1 SPIKE SAMPLE Do REPORT

TOTAL Msetals

Client Lot t... : D4D030176Date Sampled...: 04/01/04 09:45 Date Received..: 04/02/04

Matrix......... SOLID

NOB (S) :Cadatim art pformed beoe rodiaI lo amid Timuoffsenm In Alcuned n k.

N Spiked ayte Scowy k outse d cowoAll EAits.Resu and epordag Et he bma rend for dry wAti.

* kebaw parw diffau= IR) I oumd iwezd cowuL imis.

BA A So REPOR

General cht try

Client Lot f...: D4D030176 Matrix.........: SOLnM

PARAMETER

Fluoride.

REPORTING PREPARATION- PREP

RESULT LIAIT UNITS METHOD ANALYSIS DATE BATCH #Work Order #: GECK61MA MB Lot-Sample #: D4D160000-487

ED 10 mg/kg SW846 9056 04/15/04 4107487Dilutiml Factors 1Analysis TLme. . s 15:42

IO=E(S):Cakuladous eperfd before ouiog o ovoi toed-off erws b caadawdwekt

IJOaTaOr CONTOL SAIE EVALUAI REPORT

General Malitry

Lot-Sample I...: D4D030176 Matrix.........: SOLID

PARAMETERFluoride

PERCENT RECOVERY RPD PREPARATION- PREPRECOVERY LIMITS RPD LIMITS METhOD AIMLYSIS DATE BATCE #

WO#:GECM61AC-LCS/GECK61AD-LCSD LCS Lot-Sample#: D4D160000-48798 (90 - 110) 5W846 9056 04/15/04 4107487100 (90 - 110) 1.9 (0-10) SW846 9056 04/15/04 4107487

Diltutl Factors 1 Analysis Jime..t 15:20

NOTE (S):uCkkdudarPafrmgefbr tounag u avoid wrawudsoffan kcalcuIated rut.

LBEnRAT= WRWL SAMPLE DL REPORT

General Chemistry

Lot-Sample if...: D4D030176 Matrix......... SOLID

PARAMETERFluoride

SPIKE MEASURED PERCNTAMOUNT AMOUNT UNITS RECVRY RPD METHOD

WO#:GECM61AC-LCS/GECM61=D-LCSD40.0 39.3 mg/kg 98 SW846 !40.0 40.0 mg/kg 100 1.9 SW846 !

Dilution Factors I Analysis I

LCS?0569056


Lot-Sample#: D4D160000-48704/15/04 4107i8704/15/04 4107487

rize..% 15X20

NOT ES):CaIcU ns we petfrmed befare rounding o avoid Iund-of a. In =haih rena.

MhTRIX SPIKE SAMPLE EVJXCLK1IN REPORT

General Cintry

Client Lot #...: D4D030176Date Sampled...: 04/01/04 12:30 Date Received..: 04/03/04

MatriX .... : SOLID

PARAMETERFluoride

PERCENT RECOVERY RPDRECOVERY LIMITS RPD LIMITS METHOD

WO#: GDHQL1AV-MS/GDHQL1AW-MSD94 (80 - 120) SW846 905694 (90 - 120) 0.48 (0-10) SW846 9056

Dilution Factor: 1Analysis Time..: 16X05


MS Lot-Sample #s D4D030176-0o104/15/04 410748704/15/04 4107487

DO (S):Ca3toIs are pefoted before wudingso avoid owtd-off wos k cakuated mweks.

Rem ad epoialimbharebeeadustcdfrdzyweight

MAT=R SPK SATEW DM REPORT

eneral cbzMatry

Client Lot t...: D4D030176 SOLMatri.SIDDate Sampled ... : 04/01/04 12:30 Date Received..: 04/03/04

SAMPLE SPIKE MEASRD PERCNT PREPARATION- PREPPARAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD HMEHOD ANALYSIS DATE BATCH #Fluoride WO#: GDHQL1AV-KS/GDHQL1AW-MSD MS Lot-Sample #: D4D030176-001

ND 50.8 48.4 mg/kg 94 6W846 9056 04/15/04 4107487ND 50.8 48.6 mg/kg 94 0.48 SW846 9056 04/15/04 4107487

Dilution aCtor: IAnalysis Time..: 16s05

OTR (S):Ckbtiow arm perfbmed before rutmdhl a S id ,amd-off am in mab-ed rm*s

SAMPLE DUPLICTE EVAItIOK ZKPORT

General CeMistry

Client Lot # ... : D4D030176 Work Order @... : GD51-SMP HatriGD518-DUP

Date Sampled ... : 04/12/04 14:30 Date Received..: 04/14/04% Misture ..... : 20

DUPLICATE RPDPARAM RESULT RESULT UWITS RPD LIMIT METHODPercent Moisture SD Lot-Sample $ I

20 19 t 8.6 (0-20) MCMA 160.3 MOD

.x : SOLID

PREPARATION-ANALYSIS DATEW D140295-00104/19/04

PREPBATCH #

4110593Dilutin Facort 1 AnalyuiE TieW..3 17t3S

NO (S):Wzlaiu am pmfonwd tetbre wcumh ID avoid md-off ros hI akcad mike

Rmz ad a ouig linihs hame bcen a4uted fr dry wekhL

vFJPTE D CPLrc2M EALARi REPORT

General mistry

Client Lot #...: D4D030176 Work Order I...: GDSHQ-SMP matrix .....: SOLIDD8IHQ-DUP

Date Sampled...: 04/09/04 12:15 Date Received..: 04/15/04t Hoisture ..... : 21

DUPLICATE RPD PREPARATION- PREPPARPM RESULT RESULT UNITS RPD LIMIT METHOD 1NPLYSIS DATE BATCH #Percent Moisture SD Lot-Sample #: D4DD50302-001

21 19 t 9.9 (0-20) MCAKW 160.3 MOD 04/20/04 4111603Dilutian Factor: 1 Analysis Time..1 17:15

SAMPLE DUPLCA EVAUTX REPORr

Geoa <aiemiSt

Client lot I...: D4D030176 Work Order I...: GEFXS-MP Hatri ....... : SOLIDGEFXS-DUP

Date Sapled... : 04/14/04 13:20 Date Received..: 04/19/04t Moisture.....: 14

DUPLICATE RPD PREPARATION- PREPPARAM RESULT RESULT UNITS RPD LIMIT METHOD ANALYSIS DATE BATCH $Percent Moisture SD Lot-Sample #: D4D190181-013

14 15 t 6.5 (0-20) KCAWW 160.3 MOD 04/20/04 4111603Dilutti Factor: 1 Analysi sTe. T s 17315

:haln of:ustody Record

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