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Annex to the accreditation certificate Bijlage bij accreditatie-certificaat Annexe au certificat d'accréditation Beilage zur Akkreditierungszertifikat EN ISO/IEC 17043:2010 Version / Versie / Version / Fassung 6/1 Validity / Geldigheidsperiode / Validité / Gültigkeitsdauer 2020-05-04 - 2022-10-27 Maureen Logghe Chair of the Accreditation Board Voorzitster van het Accreditatiebureau La Présidente du Bureau d'Accréditation Vorsitzende des Akkreditierungsbüro Retieseweg 111 2440 Geel Via Enrico Fermi 2749 21027 Ispra (VA) Italy Wetstraat 200 268-PT The accreditation is granted to / De accreditatie werd uitgereikt aan / L'accréditation est délivrée à /Die akkreditierung wurde erteilt für: European Commission 1040 Brussels Sites of activities / Activiteitencentra / Sites d'activités / Standorte mit aktivitäten: JOINT RESEARCH CENTRE (JRC) Directorate F, Unit F.5 - Geel site JOINT RESEARCH CENTRE (JRC) Directorate F, Unit F.5 - Ispra site

268-PT...1 elements Characterization of a non-operationally defined measurand using two or more methods of demonstrable accuracy in one or more competent laboratories 2 organic molecules

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Page 1: 268-PT...1 elements Characterization of a non-operationally defined measurand using two or more methods of demonstrable accuracy in one or more competent laboratories 2 organic molecules

Annex to the accreditation certificateBijlage bij accreditatie-certificaat

Annexe au certificat d'accréditationBeilage zur Akkreditierungszertifikat

EN ISO/IEC 17043:2010

Version / Versie / Version / Fassung 6/1

Validity / Geldigheidsperiode /

Validité / Gültigkeitsdauer2020-05-04 - 2022-10-27

Maureen Logghe

Chair of the Accreditation Board

Voorzitster van het Accreditatiebureau

La Présidente du Bureau d'Accréditation

Vorsitzende des Akkreditierungsbüro

Retieseweg 111

2440 Geel

Via Enrico Fermi 2749

21027 Ispra (VA)

Italy

Wetstraat 200

268-PT

The accreditation is granted to / De accreditatie werd uitgereikt aan /

L'accréditation est délivrée à /Die akkreditierung wurde erteilt für:

European Commission

1040 Brussels

Sites of activities / Activiteitencentra / Sites d'activités / Standorte mit aktivitäten:

JOINT RESEARCH CENTRE (JRC)

Directorate F, Unit F.5 - Geel site

JOINT RESEARCH CENTRE (JRC)

Directorate F, Unit F.5 - Ispra site

Werner.Christiaens
BELAC papier
Page 2: 268-PT...1 elements Characterization of a non-operationally defined measurand using two or more methods of demonstrable accuracy in one or more competent laboratories 2 organic molecules

Field Sample matrix categories Properties determinedType of proficiency testing scheme

(see ISO/IEC 17043, annex A)

Food and feed products FeedContent of element or inorganic species

Content of organic moleculeSimultaneous participation scheme

Field Sample matrix categories Properties determinedType of proficiency testing scheme

(see ISO/IEC 17043, annex A)

Food and feed products Food & Feed Genetically Modified content in % (m/m) and % (cp/cp) * Simultaneous participation scheme

Food and feed products FoodContent of element or inorganic species

Content of organic moleculeSimultaneous participation scheme

Food and feed products Food Contact MaterialsContent of element or inorganic species

Content of organic moleculeSimultaneous participation scheme

FLEXIBLE SCOPE - GEEL SITE

A more detailed version of this scope (addendum on the organisation of ILC's: compilation of past activities) is available upon request in the laboratory.

(*) m/m : mass to mass, cp/cp : copynumber to copynumber

FLEXIBLE SCOPE - ISPRA AND GEEL SITE

Bijlage/Annexe/Annex/Beilage BELAC 268-PT V. 6/1 - 2/2

Page 3: 268-PT...1 elements Characterization of a non-operationally defined measurand using two or more methods of demonstrable accuracy in one or more competent laboratories 2 organic molecules

Annex to the accreditation certificateBijlage bij accreditatiecertificaat

Annexe au certificat d'accréditationBeilage zur Akkreditierungszertifikat

EN ISO 17034:2016

Versie / Version / Version / Fassung 10/1

Geldigheidsperiode / Validité /

Validity / Gültigkeitsdauer2020-05-04 - 2022-10-27

Maureen Logghe

Chair of the Accreditation Board

Voorzitster van het Accreditatiebureau

La Présidente du Bureau d'Accréditation

Vorsitzende des Akkreditierungsbüro

1040 Brussels

Sites of activities / Activiteitencentra / Sites d'activités / Standorte mit aktivitäten:

JOINT RESEARCH CENTRE (JRC)

Directorate F, Unit F.6 - Geel site

268-RM

The accreditation is granted to / De accreditatie werd uitgereikt aan /

L'accréditation est délivrée à / Die akkreditierung wurde erteilt für:

European CommissionWetstraat 200

Retieseweg 111

2440 Geel

Werner.Christiaens
NO MLA
Page 4: 268-PT...1 elements Characterization of a non-operationally defined measurand using two or more methods of demonstrable accuracy in one or more competent laboratories 2 organic molecules

1 elements Characterization of a non-operationally defined measurand using two

or more methods of demonstrable accuracy in one or more competent

laboratories

2 organic molecules Characterisation of a non-operationally defined measurand using two

or more methods of demonstrable accuracy in one or more competent

laboratories

3 macromolecules including genetically modified

organisms (GMO)

Characterization of a non-operationally defined measurand using two

or more methods of demonstrable accuracy in one or more competent

laboratories

Characterization based on mass or volume of ingredients used in the

preparation of the RM

4 method defined properties Characterization of an operationally-defined measurand using a

network of laboratories

5 elements Characterization of a non-operationally defined measurand using two

or more methods of demonstrable accuracy in one or more competent

laboratories

6 organic molecules Characterization of a non-operationally defined measurand using two

or more methods of demonstrable accuracy in one or more competent

laboratories

7 macromolecules including genetically modified

organisms (GMO)

Characterization of a non-operationally defined measurand using two

or more methods of demonstrable accuracy in one or more competent

laboratories

Characterization based on mass or volume of ingredients used in the

preparation of the RM

8 method defined properties Characterization of an operationally-defined measurand using a

network of laboratories

Code Type of matrix Certified analytes/properties

FLEXIBLE SCOPE - GEEL SITE

Reference materials (certified) for chemical composition [(C)RM]

Solid biological material from plant or animal

matter including food

liquid biological material from plant or

animal/human matter including food

Characterization approach

Bijlage/Annexe/Annex/Beilage BELAC 268-RM V. 10/1 - 2/4

Page 5: 268-PT...1 elements Characterization of a non-operationally defined measurand using two or more methods of demonstrable accuracy in one or more competent laboratories 2 organic molecules

Code Type of matrix Certified analytes/properties Characterization approach

9 Solutions of pure substances Small organic molecules and nucleic acids Characterization using a single reference measurement procedure (as

defined in ISO/IEC Guide 99) in a single laboratory

Characterization based on mass or volume of ingredients used in the

preparation of the RM

10 Soils, sludges and sediments Elements, organic molecules Characterization of a non-operationally defined measurand using two

or more methods of demonstrable accuracy in one or more competent

laboratories

Characterization of an operationally-defined measurand using a

network of laboratories

11 Organic liquids Elements, method defines properties Characterization of a non-operationally defined measurand using two

or more methods of demonstrable accuracy in one or more competent

laboratories

Characterization of an operationally-defined measurand using a

network of laboratories

12 Waters Elements Characterization of a non-operationally defined measurand using two

or more methods of demonstrable accuracy in one or more competent

laboratories

Characterization of an operationally-defined measurand using a

network of laboratories

13 Solid industrial materials Elements Characterization of a non-operationally defined measurand using two

or more methods of demonstrable accuracy in one or more competent

laboratories

Characterization of an operationally-defined measurand using a

network of laboratories

Bijlage/Annexe/Annex/Beilage BELAC 268-RM V. 10/1 - 3/4

Page 6: 268-PT...1 elements Characterization of a non-operationally defined measurand using two or more methods of demonstrable accuracy in one or more competent laboratories 2 organic molecules

Code Type of matrix Certified analytes/properties Characterization approach

14 Pure suspensions Size and electrochemical properties of nanoparticles Characterization of a non-operationally defined measurand using two

or more methods of demonstrable accuracy in one or more competent

laboratories

Characterization of an operationally-defined measurand using a

network of laboratories

15 steel Absorbed energy (KV) according to ISO 148 (Impact

toughness)

Characterization of an operationally-defined measurand using a

network of laboratories

Value transfer from an RM to a closely matched candidate RM

performed using a single measurement procedure performed by one

laboratory

A detailed list of the reference materials covered under accreditation, including the characterization approach for these reference materials is maintained by, and available upon request from,

the reference material producer.

Reference materials (certified) for physical/electro-chemical properties [(C)RM]

Bijlage/Annexe/Annex/Beilage BELAC 268-RM V. 10/1 - 4/4

Page 7: 268-PT...1 elements Characterization of a non-operationally defined measurand using two or more methods of demonstrable accuracy in one or more competent laboratories 2 organic molecules

Annex to the accreditation certificateBijlage bij accreditatiecertificaat

Annexe au certificat d'accréditationBeilage zur Akkreditierungszertifikat

EN ISO/IEC 17025:2017

Version / Versie / Version / Fassung 19

Validity / Geldigheidsperiode /

Validité / Gültigkeitsdauer2020-05-04 - 2022-10-27

Maureen Logghe

Chair of the Accreditation Board

Voorzitster van het Accreditatiebureau

La Présidente du Bureau d'Accréditation

Vorsitzende des Akkreditierungsbüro

Wetstraat 200

268-TEST

The accreditation is granted to / De accreditatie werd uitgereikt aan /

L'accréditation est délivrée à / Die akkreditierung wurde erteilt für:

European Commission

1040 Brussels

Sites of activities / Activiteitencentra / Sites d'activités / Standorte mit aktivitäten:

JOINT RESEARCH CENTRE (JRC)

Directorate F, Unit F.4, Unit F.5 & Unit F.6 - Geel site

JOINT RESEARCH CENTRE (JRC)

Directorate F, Unit F.4, Unit F.5 & Unit F.6 - Ispra site

Retieseweg 111

2440 Geel

Via Enrico Fermi 2749

21027 Ispra (VA)

Italy

Werner.Christiaens
BELAC papier
Page 8: 268-PT...1 elements Characterization of a non-operationally defined measurand using two or more methods of demonstrable accuracy in one or more competent laboratories 2 organic molecules

LIST OF ABBREVIATIONS:

DNA Deoxyribonucleic acid

EA-IRMS Elemental Analyser - Isotope Ratio Mass Spectrometer

ET-AAS Electro-thermal Atomic Absorption Spectrometry

GC-MS Gas chromatography – Mass Spectrometry

HPLC High-Performance Liquid Chromatography

HPLC-DAD High-Performance Liquid Chromatography with Diode-Array Detection.

HPLC-FLD High Performance Liquid Chromatography with Fluorescence Detection

HPLC-UV High-Performance Liquid Chromatography with UV Detector

ICP-MS Inductively Coupled Plasma Mass Spectrometry

ICP-OES Inductively Coupled Plasma Optical Emission Spectrometry

IRMS Isotope-Ratio Mass Spectrometer

LC-MS Liquid Chromatography - Mass Spectrometry

OIV International Organisation of Vine and Wine

PCR Polymerase Chain Reaction

SNIF-NMR Site Specific Natural Isotope Fractionation studied by Nuclear Magnetic Resonance

UPLC-MS/MS Ultra Performance Liquid Chromatography - Tandem Mass Spectrometer

Bijlage/Annexe/Annex/Beilage BELAC 268-TEST V. 19 - 2/4

Page 9: 268-PT...1 elements Characterization of a non-operationally defined measurand using two or more methods of demonstrable accuracy in one or more competent laboratories 2 organic molecules

Fat soluble vitamins and pro-vitamins Feed Reverse-phase HPLC with UV and fluorescence detection

Coccidiostats Feed HPLC coupled to optical or mass spectrometry detectors

Polycyclic Aromatic Hydrocarbons Food and feed GC-MS

Genetically Modified content in % (m/m) and % (cp/cp) ** Food and Feed DNA extraction, DNA identification and Real-time PCR

Genetically Modified content in % (cp/cp) ** Food and Feed DNA extraction and digital PCR

DNA copy number pure DNA solutions digital PCR

Elements Food and related materials (*) ICP-OES, ICP-MS, ET-AAS

Pesticides Food and Feed GC-MS(/MS), (UP)LC-MS/MS

Water content Biological and environmental matrices Volumetric Karl-Fischer titration

Migrated substances from materials in contact with food Plastics and plastic coated metal food contact materials In house method according to Regulation (EU) No 10/2011, HPLC-UV/FLD

Genetically Modified content in % (cp/cp) ** Food and Feed DNA extraction and digital PCR

Genetically Modified content in % (m/m) and % (cp/cp) ** Food and Feed DNA extraction, DNA identification and Real-time PCR

FLEXIBLE SCOPE - GEEL SITE

This is a flexible scope: in the framework of its accreditation, the laboratory is authorized to determine all analytes belonging to the group of analytes mentioned in the first column for all matrices belonging to the group of matrices mentioned in the second column.

This authorization is given, provided that an appropriate validation is performed according to the general validation concept as set out in the laboratory’s quality system. The laboratory keeps a detailed list of the analytes and matrices, belonging to the above

mentioned groups, up-to-date for anyone involved.

(*) Testing is performed in the context of reference material production rather than on routine samples. Measurement uncertainties of the results are reflected in the certified uncertainties and studies can be adapted to achieve the target uncertainty of certified

values for a given measurement uncertainty.

(**) m/m : mass to mass, cp/cp : copynumber to copynumber

Technique used

FLEXIBLE SCOPE - ISPRA SITE

MatrixAnalyte

Bijlage/Annexe/Annex/Beilage BELAC 268-TEST V. 19 - 3/4

Page 10: 268-PT...1 elements Characterization of a non-operationally defined measurand using two or more methods of demonstrable accuracy in one or more competent laboratories 2 organic molecules

WI-D-00138 Biological matrices Water contentCoulometric Karl-Fischer titration

In house method

WI-D-00042 Biological, environmental and industrial matrices Particle size distributionLaser light diffraction

In house method

WI-D-00170 Metals and alloys Absorbed energy (KV) Impact toughness ISO 148

WI-D-00561Differential Centrifugal Sedimentation (method 2 only for precision testing)

In house method

WI-D-00334Dynamic Light Scattering

In house method

WI-D-00728Particle Tracking Analysis

In house method

WI-D-00507 Samples with low water content (e.g. Serum, Amino acids: valine proline, Leucine etc.). Water content determinationVaporisation coulometric Karl Fischer titration

In house method

WI-D-00771 Wines Deuterium isotope ratios D/HSNIF-NMR

OIV-MA-AS311-05

WI-D-00959 Wines 18O / 16O isotopic ratio of water wineGas Bench - IRMS

OIV-MA-AS2-12

WI-D-00947 Wines 13C / 12C isotopic ratio of wine ethanolEA-IRMS

OIV-MA-AS312-06

WI-D-00602 Sub-micrometre particles Zeta potentialElectrophoretic Light Scattering

In house method

WI-D-00766 Organic solvent 2,4,6-trinitrotoluene (TNT)HPLC-DAD

In house method

WI-D-00971 Cookies Total cow's milk proteinLC-MS

In house method

JRC.F5.FCM.

PRO.102 Water/alcohol 50:50 % Content of Bisphenol A

HPLC-FLD

In house method

JRC.F5.FCM.

PRO.101 Oil food simulant Content of Bisphenol A

HPLC-FLD

In house method

FIXED SCOPE - ISPRA SITE

FIXED SCOPE - GEEL SITE

Testcode Type of samples Measured property Method / Technique used

Nanoparticles Characteristic parameters of particle size distributions

Bijlage/Annexe/Annex/Beilage BELAC 268-TEST V. 19 - 4/4