inactive.cityoffortwayne.org · 2017-12-01 · Project. 07-791. Environmental Science and Engineering. 508 Incentive Drive, Fort Wayne, IN 46825 (260) 497-9620 Fax: (260) 497-9720

Project

07-791

Environmental Science and Engineering

508 Incentive Drive, Fort Wayne, IN 46825

(260) 497-9620 Fax: (260) 497-9720

Task

20 ASize

9/4/07Date

TITLE

CLIENT

Figure 1 - Site Location MapOmniSource Corporation1610 N. Calhoun StreetFort Wayne, Indiana

City of Fort Wayne

SOURCE: FORT WAYNE WEST, INDIANA, USGS TOPOGRAPHIC QUADRANGLE MAP, 1963, REVISED 1981

SCALE: 1 INCH = 2,000 FTN

OR

TH

FORT WAYNE EAST, INDIANA, USGS TOPOGRAPHIC QUADRANGLE MAP, 1963, REVISED 1981

SITE

ENVision Laboratories, Inc. 1439 Sadlier Circle West Drive

Indianapolis, IN 46239 Tel: 317.351.8632 Fax: 317.351.8639

www.envisionlaboratories.com

Your Projects. Our Passion.

ENVISION

Mr. Mark LeMay Avant Group 508 Incentive Drive Fort Wayne, IN 46825 August 28, 2007 ENVision Project Number: 2007-1608 Client Project Name: Omni Source Dear Mr. LeMay, Please find the attached analytical report for the samples received August 4, 2007. All test methods performed were fully compliant with local, state, and federal EPA methods unless otherwise noted. The project was analyzed as requested on the enclosed chain of custody record. Please review the comments section for additional information about your results or Quality Control data. Metals analysis is not included in NELAC certification. Feel free to contact me if you have any questions or comments regarding your analytical report or service. Thank you for your business. ENVision Laboratories looks forward to working with you on your next project. Yours Sincerely, Cheryl A. Crum Director of Project Management ENVision Laboratories, Inc. IL ELAP / NELAC Accreditation # 100454

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Client Name: Avant Group

Project ID: Omni Source

Client Project Manager: Mark Lemay

ENVision Project Number: 2007-1608

Analytical Method: 8260Prep Method: 5035Analytical Batch: 081407VS

Client Sample ID: B-1 Sample Collection Date/Time: 8/3/07 8:38Envision Sample Number: 7-10384 Sample Received Date/Time: 8/4/07 12:00Sample Matrix: soil

Compounds Sample Results (mg/kg) Reporting Limit (mg/kg) FlagsBenzene < 0.005 0.005Toluene < 0.005 0.005Ethylbenzene < 0.005 0.005Xylene, M&P 0.0151 0.005Xylene, 0rtho < 0.005 0.005Xylenes, Total 0.0151 0.011Methyl-tert-butyl-ether < 0.005 0.005

Dibromofluoromethane (surrogate) 113%1,2-Dichloroethane-d4 (surrogate) 95%Toluene-d8 (surrogate) 96%4-bromofluorobenzene (surrogate) 108%Analysis Date/Time: 08-14-07/16:54Analyst Initials tjg

Percent Solids: 95%

Results reported on dry weight basis.

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Analytical Method: 8015 TPH Gasoline RangePrep Method: 5035Analytical Batch: 080907GS


Compounds Sample Results (mg/kg) Reporting Limit (mg/kg) FlagsTPH-Gasoline < 16 164-bromofluorobenzene (surrogate) 119%Analysis Date/Time: 08/09/07/12:53Analyst Initials tjg

Percent Solids 95%

All results reported on dry weight basis.

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Analyte Sample Results Flags Method Percent Moisture 5.0% 1684Percent Solids 95.0% 1684Analysis Date: 8/14/07Analyst Initials zrc

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Compounds Sample Results (mg/kg) Reporting Limit (mg/kg) FlagsBenzene < 0.005 0.005Toluene < 0.005 0.005Ethylbenzene < 0.005 0.005Xylene, M&P < 0.005 0.005Xylene, 0rtho < 0.005 0.005Xylenes, Total < 0.011 0.011Methyl-tert-butyl-ether < 0.005 0.005


Percent Solids: 94%


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Percent Solids 94%


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Percent Solids: 85%


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Percent Solids 85%


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Percent Solids: 95%


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Percent Solids 95%


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Analytical Method: 8015 TPH Extended C8-C36Prep Method: 3550BAnalytical Batch: 082307E

Client Sample ID: B-5 (0-0.5) Sample Collection Date/Time: 8/3/07 11:25Envision Sample Number: 7-10388 Sample Received Date/Time: 8/4/07 12:00Sample Matrix: soil

Compounds Sample Results (mg/kg) Reporting Limit (mg/kg) FlagsTPH--Extended C8-C36 351 22o-Terphenyl (surrogate) 134%Analysis Date/Time: 8/23/2007 22:45Analyst Initials: gjdDate Extracted: 8/13/2007Initial Sample Weight: 30.0 gFinal Volume: 3.0 mL

Percent Solids 91%


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Compounds Sample Results (mg/kg) Reporting Limit (mg/kg) FlagsTPH--Extended C8-C36 < 21 21o-Terphenyl (surrogate) 76%Analysis Date/Time: 8/23/2007 23:16Analyst Initials: gjdDate Extracted: 8/13/2007Initial Sample Weight: 30.0 gFinal Volume: 3.0 mL

Percent Solids 94%


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Compounds Sample Results (mg/kg) Reporting Limit (mg/kg) FlagsTPH--Extended C8-C36 5900 220 2o-Terphenyl (surrogate) 338% 3Analysis Date/Time: 8/23/2007 23:48Analyst Initials: gjdDate Extracted: 8/13/2007Initial Sample Weight: 30.0 gFinal Volume: 3.0 mL

Percent Solids 92%


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Percent Solids 91%


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Percent Solids 95%


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Compounds Sample Results (mg/kg) Reporting Limit (mg/kg) FlagsTPH--Extended C8-C36 4940 220 2o-Terphenyl (surrogate) 111%Analysis Date/Time: 8/23/2007 23:48Analyst Initials: gjdDate Extracted: 8/13/2007Initial Sample Weight: 30.0 gFinal Volume: 3.0 mL

Percent Solids 93%


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Percent Solids 84%


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Client Sample ID: B-8 (3-4) Sample Collection Date/Time: 8/3/07 11:39Envision Sample Number: 7-10396 Sample Received Date/Time: 8/4/07 12:00Sample Matrix: soil

Acetone < 0.119 0.119Acrolein < 0.119 0.119Acrylonitrile < 0.119 0.119Benzene < 0.006 0.006Bromobenzene < 0.006 0.006Bromochloromethane < 0.006 0.006Bromodichloromethane < 0.006 0.006Bromoform < 0.006 0.006Bromomethane < 0.006 0.006n-Butanol < 0.060 0.0602-Butanone (MEK) < 0.012 0.012n-Butylbenzene < 0.006 0.006sec-Butylbenzene < 0.006 0.006tert-Butylbenzene < 0.006 0.006Carbon Disulfide < 0.006 0.006Carbon Tetrachloride < 0.006 0.006Chlorobenzene < 0.006 0.006Chloroethane < 0.006 0.0062-Chloroethylvinylether < 0.060 0.060Chloroform < 0.006 0.006Chloromethane < 0.006 0.0062-Chlorotoluene < 0.006 0.0064-Chlorotoluene < 0.006 0.0061,2-Dibromo-3-chloropropane < 0.006 0.006Dibromochloromethane < 0.006 0.0061,2-Dibromoethane (EDB) < 0.006 0.006Dibromomethane < 0.006 0.0061,2-Dichlorobenzene < 0.006 0.0061,3-Dichlorobenzene < 0.006 0.0061,4-Dichlorobenzene < 0.006 0.006trans-1,4-Dichloro-2-butene < 0.119 0.119Dichlorodifluoromethane < 0.006 0.0061,1-Dichloroethane < 0.006 0.0061,2-Dichloroethane < 0.006 0.0061,1-Dichloroethene < 0.006 0.006

Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags

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8260 continued…

cis-1,2-Dichloroethene < 0.006 0.006trans-1,2-Dichloroethene < 0.006 0.0061,2-Dichloropropane < 0.006 0.0061,3-Dichloropropane < 0.006 0.0062,2-Dichloropropane < 0.006 0.0061,1-Dichloropropene < 0.006 0.006cis-1,3-Dichloropropene < 0.006 0.006trans-1,3-Dichloropropene < 0.006 0.006Ethylbenzene < 0.006 0.006Ethyl methacrylate < 0.119 0.119Hexachloro-1,3-butadiene < 0.006 0.006n-Hexane < 0.012 0.0122-Hexanone < 0.012 0.012Iodomethane < 0.012 0.012Isopropylbenzene (Cumene) < 0.006 0.006p-Isopropyltoluene < 0.006 0.006Methylene chloride < 0.024 0.0244-Methyl-2-pentanone (MIBK) < 0.012 0.012Methyl-tert-butyl-ether < 0.006 0.006Naphthalene < 0.006 0.006n-Propylbenzene < 0.006 0.006Styrene < 0.006 0.0061,1,1,2-Tetrachloroethane < 0.006 0.0061,1,2,2-Tetrachloroethane < 0.006 0.006Tetrachloroethene < 0.006 0.006Toluene < 0.006 0.0061,2,3-Trichlorobenzene < 0.006 0.0061,2,4-Trichlorobenzene < 0.006 0.0061,1,1-Trichloroethane < 0.006 0.0061,1,2-Trichloroethane < 0.006 0.006Trichloroethene < 0.006 0.006Trichlorofluoromethane < 0.006 0.0061,2,3-Trichloropropane < 0.006 0.0061,2,4-Trimethylbenzene < 0.006 0.0061,3,5-Trimethylbenzene < 0.006 0.006Vinyl acetate < 0.012 0.012Vinyl chloride < 0.002 0.002Xylene, M&P < 0.006 0.006Xylene, 0rtho < 0.006 0.006Xylene, Total < 0.012 0.012Dibromofluoromethane (surrogate) 53.4 107%1,2-Dichloroethane-d4 (surrogate) 46.2 92%Toluene-d8 (surrogate) 50.9 102%4-bromofluorobenzene (surrogate) 54.3 109%Analysis Date/Time: 08-14-07/05:40Analyst Initials tjg

Percent Solids: 84%All results reported on dry weight basis.

Compounds Sample Results (mg/kg) Rep. Limit (mg/kg) Flags

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Client Sample ID: B-8 (3-4) Sample Collection Date/Time: 8/3/07 11:39Envision Sample Number: 7-10396 Sample Received Date/Time: 8/4/07 12:00Sample Matrix: soil


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Percent Solids 86%


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Percent Solids 91%


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Analytical Method: Metals 6010B/7471APrep Method: 3050B


Compounds Sample Results (mg/kg) Reporting Limit (mg/kg) FlagsArsenic 3.1 2Barium 81 2Cadmium 4.6 2Chromium 125 2Lead 295 2Mercury < 1 1Selenium < 2 2Silver < 2 2

Percent Solids 90%

Analysis Date/Time: 8/11/2007 10:10 Hg Analysis Date/Time: 8/18/2007 10:30Analyst Initials: gjd Hg Analyst Initials: gjdDate Digested: 8/10/2007 Date Digested: 8/17/2007Initial Sample Weight: 1.0 g Initial Sample Weight: 0.6 gFinal Volume: 50 mL Final Volume: 50 mLAnalytical Batch: 081007icp Analytical Batch: 081807hgs


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Compounds Sample Results (mg/kg) Reporting Limit (mg/kg) FlagsArsenic 6.2 2Barium 562 2Cadmium 54 2Chromium 456 2Lead 1933 2Mercury 9.6 6 1Selenium < 2 2Silver < 2 2

Percent Solids 88%



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Analytical Method: TCLP Metals 6010B/7471APrep Method: 1311


Compounds Sample Results (mg/l) Reporting Limit (mg/l) FlagsLead 0.28 0.01

Analysis Date/Time: 8/27/2007 15:16Analyst Initials: gjdDate Digested: 8/25/2007Initial Sample Volume: 50 mlFinal Volume: 50 mlAnalytical Batch: 082707icp

Results reported on wet weight basis.

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Compounds Sample Results (mg/kg) Reporting Limit (mg/kg) FlagsArsenic 7.6 2Barium 603 2Cadmium 11 2Chromium 264 2Lead 1410 2Mercury 2.3 1Selenium < 2 2Silver < 2 2

Percent Solids 96%



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Compounds Sample Results (mg/kg) Reporting Limit (mg/kg) FlagsArsenic 3.5 2Barium 698 2Cadmium 5.8 2Chromium 29 2Lead 3081 2Mercury < 1 1Selenium < 2 2Silver < 2 2

Percent Solids 92%



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Compounds Sample Results (mg/kg) Reporting Limit (mg/kg) FlagsArsenic < 2 2Barium 109 2Cadmium 4.2 2Chromium 125 2Lead 721 2Mercury 1.6 1Selenium < 2 2Silver < 2 2

Percent Solids 96%



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Analytical Method: 8015 GROPrep Method: 5030Analytical Batch: 081107GW

Client Sample ID: B-1 Sample Collection Date/Time: 8/3/07 10:00Envision Sample Number: 7-10404 Sample Received Date/Time: 8/4/07 12:00Sample Matrix: water

Compounds Sample Results (mg/L) Reporting Limit (mg/L) FlagsTPH-Gasoline < 0.22 0.22

4-bromofluorobenzene (surrogate) 82% Analysis Date/Time: 08/11/07/12:20Analyst Initials tjg

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Analytical Method: 8260Prep Method: 5030BAnalytical Batch: 081207VW


Compounds Sample Results (mg/L) Reporting Limit (mg/l) FlagsBenzene < 0.005 0.005Toluene < 0.005 0.005Ethylbenzene < 0.005 0.005Xylene, M&P < 0.005 0.005Xylene, 0rtho < 0.005 0.005Xylenes, Total < 0.01 0.01Methyl-tert-butyl-ether < 0.005 0.005Dibromofluoromethane (surrogate) 48.9 98%1,2-Dichloroethane-d4 (surrogate) 53.2 106%Toluene-d8 (surrogate) 51.1 102%4-bromofluorobenzene (surrogate) 44.3 89%Analysis Date/Time: 08-12-07/06:27Analyst Initials tjg

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Analytical Method: 8015 GROPrep Method: 5030Analytical Batch: 081107GW


Compounds Sample Results (mg/L) Reporting Limit (mg/L) FlagsTPH-Gasoline < 0.22 0.22

4-bromofluorobenzene (surrogate) 96% Analysis Date/Time: 08/11/07/12:40Analyst Initials tjg

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Analytical Method: 8260Prep Method: 5030BAnalytical Batch: 081307VS


Compounds Sample Results (mg/L) Reporting Limit (mg/l) FlagsBenzene < 0.005 0.005Toluene < 0.005 0.005Ethylbenzene < 0.005 0.005Xylene, M&P < 0.005 0.005Xylene, 0rtho < 0.005 0.005Xylenes, Total < 0.01 0.01Methyl-tert-butyl-ether < 0.005 0.005Dibromofluoromethane (surrogate) 64.4 129%1,2-Dichloroethane-d4 (surrogate) 53.2 106%Toluene-d8 (surrogate) 52 104%4-bromofluorobenzene (surrogate) 58.2 116%Analysis Date/Time: 08-13-07/09:05Analyst Initials tjg

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8260 Quality Control Data

ENVision Batch Number: 081607VS

Method Blank (MB): MB Results (ug/kg) Rep Lim (ug/kg) FlagMethyl-tert-butyl-ether < 5 5

Benzene < 5 5Toluene < 5 5

Ethylbenzene < 5 5Xylene, M&P < 5 5Xylene, 0rtho < 5 5Xylenes, Total <10 10

Dibromofluoromethane (surrogate) 89%1,2-Dichloroethane-d4 (surrogate) 96%

Toluene-d8 (surrogate) 100%4-bromofluorobenzene (surrogate) 101%

Analysis Date/Time: 08-16-07/15:29Analyst Initials tjg

Laboratory Control Standard (LCS): LCS Results (ug/kg) LCS Conc (ug/kg) % Rec FlagMethyl-tert-butyl-ether 54.9 50 110%

Benzene 50.5 50 101%Toluene 45.7 50 91%

Ethylbenzene 51.7 50 103%Xylene, M&P 108 100 108%Xylene, 0rtho 54.5 50 109%




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ENVision Batch Number: 081407VS

Method Blank (MB): MB Results (ug/kg) Rep Lim (ug/kg) FlagAcetone < 100 100Acrolein < 100 100

Acrylonitrile < 100 100Benzene < 5 5

Bromobenzene < 5 5Bromochloromethane < 5 5

Bromodichloromethane < 5 5Bromoform < 5 5

Bromomethane < 5 5n-Butanol < 50 50

2-Butanone (MEK) < 10 10n-Butylbenzene < 5 5

sec-Butylbenzene < 5 5tert-Butylbenzene < 5 5Carbon Disulfide < 5 5

Carbon Tetrachloride < 5 5Chlorobenzene < 5 5Chloroethane < 5 5

2-Chloroethylvinylether < 50 50Chloroform < 5 5

Chloromethane < 5 52-Chlorotoluene < 5 54-Chlorotoluene < 5 5

1,2-Dibromo-3-chloropropane < 5 5Dibromochloromethane < 5 5

1,2-Dibromoethane (EDB) < 5 5Dibromomethane < 5 5

1,2-Dichlorobenzene < 5 51,3-Dichlorobenzene < 5 51,4-Dichlorobenzene < 5 5

trans-1,4-Dichloro-2-butene < 100 100Dichlorodifluoromethane < 5 5

1,1-Dichloroethane < 5 51,2-Dichloroethane < 5 51,1-Dichloroethene < 5 5

cis-1,2-Dichloroethene < 5 5trans-1,2-Dichloroethene < 5 5

1,2-Dichloropropane < 5 51,3-Dichloropropane < 5 52,2-Dichloropropane < 5 51,1-Dichloropropene < 5 5

cis-1,3-Dichloropropene < 5 5trans-1,3-Dichloropropene < 5 5

Ethylbenzene < 5 5Ethyl methacrylate < 100 100

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8260 QC Continued…

MB Results (ug/kg) Rep Lim (ug/kg) FlagHexachloro-1,3-butadiene < 5 5

2-Hexanone < 10 10n-Hexane < 10 10

Iodomethane < 10 10Isopropylbenzene (Cumene) < 5 5

p-Isopropyltoluene < 5 5Methylene chloride < 5 5

4-Methyl-2-pentanone (MIBK) < 10 10Methyl-tert-butyl-ether < 5 5

Naphthalene < 5 5n-Propylbenzene < 5 5

Styrene < 5 51,1,1,2-Tetrachloroethane < 5 51,1,2,2-Tetrachloroethane < 5 5

Tetrachloroethene < 5 5Toluene < 5 5

1,2,3-Trichlorobenzene < 5 51,2,4-Trichlorobenzene < 5 51,1,1-Trichloroethane < 5 51,1,2-Trichloroethane < 5 5

Trichloroethene < 5 5Trichlorofluoromethane < 5 51,2,3-Trichloropropane < 5 51,2,4-Trimethylbenzene < 5 51,3,5-Trimethylbenzene < 5 5

Vinyl acetate < 10 10Vinyl chloride < 2 2Xylene, M&P < 5 5Xylene, 0rtho < 5 5Xylenes, Total <10 10




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8260 QC Continued…

Laboratory Control Standard (LCS): LCS Results (ug/kg) LCS Conc(ug/kg) % Rec Flag1,1-Dichloroethene 55.3 50 111%

Benzene 51.9 50 104%Trichloroethene 50.7 50 101%

Toluene 50.9 50 102%Chlorobenzene 50.3 50 101%




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8015 TPH-Extended Range Quality Control Data

ENVision Batch Number: 081307DS

Method Blank (MB):MB Results

(mg/kg)Reporting Limit

(mg/kg) FlagTPH-Extended Range < 20 20

o-Terphenyl (surrogate) 63%Analysis Date/Time: 08-15-07/09:02

Analyst Initials: bdsDate Extracted: 8/13/2007

Initial Sample Weight: 30.0 gFinal Volume: 3.0 mL

LCS/LCSDLCS Result

(mg/kg)LCS/LCSD Conc.

(mg/kg)LCSD Result

(mg/kg)LCS Rec.

LCSD Rec. RPD Flag

TPH-Extended Range 80.26 100 92.07 80.3% 92.1% 13.7%o-Terphenyl (surrogate) 75% 86%

Analysis Date/Time: 08-15-07/09:31 08-15-07/10:01Analyst Initials: bds bdsDate Extracted: 8/13/2007 8/13/2007

Initial Sample Weight: 30.0 g 30.0 gFinal Volume: 3.0 mL 3.0 mL

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8015 TPH-Gasoline Quality Control Data

ENVision Batch Number: 080907GS

Method Blank (MB): MB Results (mg/kg)Rep Lim (mg/kg) Flag

TPH-Gasoline < 15 154-bromofluorobenzene (surrogate) 112%

Analysis Date/Time: 08/09/07/05:27Analyst Initials: tjg

LCS/LCSD LCS Results (mg/kg)LCS/LCSD

Conc. (mg/kg)LCSD Result

(mg/kg)LCS Rec.

LCSD Rec. RPD Flag

TPH-Gasoline 9.45 10 9.49 95% 95% 0.4%4-bromofluorobenzene (surrogate) 100% 102%

Analysis Date/Time: 08/09/07/04:47 08/09/07/16:32Analyst Initials tjg tjg

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6010B/7471A Metals Quality Control Data

ENVision Batch Number: 081007icp / 081807hgs

Method Blank (MB): MB Results (mg/kg) Rep Lim (mg/kg) FlagArsenic < 2 2Barium < 2 2

Cadmium < 2 2Chromium < 2 2

Lead < 2 2Mercury < 1 1

Selenium < 2 2Silver < 2 2

Analysis Date/Time: 8/10/07 15:09icp / 8/18/07 10:09hgAnalyst Initials: gjd

Laboratory Control Standard: LCS Results(ppm) LCS Conc(ppm) % Rec FlagArsenic 0.55 0.50 110%Barium 0.48 0.50 96%

Cadmium 0.49 0.50 98%Chromium 0.51 0.50 102%

Lead 0.48 0.50 96%Mercury 0.0098 0.01 98%

Selenium 0.55 0.50 110%Silver 0.48 0.50 96%

Analysis Date/Time: 8/10/07 15:16icp / 8/18/07 10:12hgAnalyst Initials: gjd

Matrix Spike/Matrix Spike Dup: Smpl Results(ppm) MS Res(ppm) MSD Res(ppm) Spk Conc(ppm) MS Rec MSD Rec % D FlagArsenic 0 0.49 0.46 0.50 98% 92% 6.316Barium 0.44 1.02 1.01 0.50 116% 114% 1.739

Cadmium 0 0.44 0.44 0.50 88% 88% 0Chromium 0.09 0.59 0.57 0.50 100% 96% 4.082

Lead 0.27 0.73 0.74 0.50 92% 94% 2.151Mercury 0.0037 0.0061 0.0051 0.0025 96% 56% 52.63 3

Selenium 0 0.43 0.41 0.50 86% 82% 4.762Silver 0 0.33 0.3 0.50 66% 60% 9.524

Original Sample Number Spiked: 7-10593icp / 7-10399hgAnalysis Date/Time: 8/11/07 10:26icp / 8/18/07 10:32hg

Analyst Initials: gjd

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6010B TCLP Metals Quality Control Data

ENVision Batch Number: 082707icp

Method Blank (MB): MB Results (mg/L) Rep Lim (mg/L) FlagLead < 0.01 0.01

Analysis Date/Time: 8/27/2007 15:09Analyst Initials: gjd

Laboratory Control Standard (LCS): LCS Results(mg/L) LCS Conc(mg/L) % Rec FlagLead 0.54 0.5 108

Analysis Date/Time: 8/27/2007 15:09Analyst Initials: gjd

Matrix Spike/Matrix Spike Dup (MS/MSD) Sample Results (mg/L) MS Res(mg/L) MSD ResSpike CMS Rec MSD Rec % D FlagLead 0.21 0.67 0.66 0.5 92% 90% 2.198

Originial Sample Number Spiked: 7-1401Analysis Date/Time: 8/27/2007 15:09

Analyst Initials: gjd

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ENVision Batch Number: 081307VW

Method Blank (MB): MB Results (ug/L) Rep Lim (ug/L) FlagMethyl-tert-butyl-ether < 5 5






Laboratory Control Standard (LCS): LCS Results (ug/L) LCS Conc (ug/L) % Rec FlagMethyl-tert-butyl-ether 57.7 50 115%

Benzene 56.9 50 114%Toluene 50.4 50 101%

Ethylbenzene 56.9 50 114%Xylene, M&P 115 100 115%Xylene, 0rtho 52.5 50 105%




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ENVision Batch Number: 081207VW

Method Blank (MB): MB Results (ug/L) Rep Lim (ug/L) FlagMethyl-tert-butyl-ether < 5 5






LCS/LCSD LCS Results (ug/l)LCS/LCSD Conc.

(ug/l)LCSD Result

(ug/l)LCS Rec.

LCSD Rec. RPD Flag

Methyl-tert-butyl-ether 51.1 50 49.1 102% 98% 4.0%Benzene 56.3 50 52.9 113% 106% 6.2%Toluene 51.7 50 49.7 103% 99% 3.9%

Ethylbenzene 56.3 50 51.7 113% 103% 8.5%Xylene, M&P 110 100 103 110% 103% 6.6%Xylene, 0rtho 53.6 50 51.2 107% 102% 4.6%

Dibromofluoromethane (surrogate) 79% 92%1,2-Dichloroethane-d4 (surrogate) 101% 103%

Toluene-d8 (surrogate) 97% 101%4-bromofluorobenzene (surrogate) 101% 105%

Analysis Date/Time: 08-12-07/00:35 08-12-07/00:12Analyst Initials tjg tjg

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8015 TPH-Gasoline Quality Control Data

ENVision Batch Number: 081107GW

Method Blank (MB): MB Results (mg/L)Rep Lim (mg/kg) Flag

TPH-Gasoline < 15 154-bromofluorobenzene (surrogate) 112%

Analysis Date/Time: 08/11/07/05:36Analyst Initials: tjg

LCS/LCSD LCS Results (mg/L)LCS/LCSD

Conc. (mg/kg)LCSD Result

(mg/L)LCS Rec.

LCSD Rec. RPD Flag

TPH-Gasoline 9.83 10 8.67 98% 87% 12.544-bromofluorobenzene (surrogate) 100% 102%

Analysis Date/Time: 08/11/07/04:57 08/11/07/09:39Analyst Initials tjg tjg

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ENVISION

Flag Number Comments

1 Reported value is from a 6x dilution. GJD 08-18-072 Reported value is from a 10x dilution. GJD 08-18-073 Matrix Interference caused the % Recovery to be outside the

established limits. All other QC is in control. GJD 08-25-07

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