semspub.epa.gov · 2017. 1. 12. · CONESTOGA-ROVERS & ASSOCIATES 14496 Sheldon Road, Suite #200 Plymouth, Michigan 48170 Telephone: (734)453-5123 Fax: (734)453-5201 …

CONESTOGA-ROVERS & ASSOCIATES

14496 Sheldon Road, Suite #200 Plymouth, Michigan 48170 Telephone: (734)453-5123 Fax: (734)453-5201 www.CRAworid.com

TRANSMITTAL

DATE: September 12,2003

TO: Ms. Lorie Hong

Weston

300 River Place, Suite 2800

Detroit, MI 48207

REFERENCE NO.:

PROJECT NAME:

32664-40

Sybi^JUngw^ r-

•fcwi-5£P 2 3 200^

Weston Solutions of Michigan, Inc.

Please find enclosed: Q Draft r~l Originals • Prints

Sent via: 1^ Mail • Overnight Courier

^ Final r~l Other

r~l Same Day Courier r~l Other

QUANTITY DESCRIPTION 1 Set of Container Inspection Records (through TK-103)

• As Requested

1^ For Your Use

COMMENTS:

• For Review and Comment

• •

us i:i>A RECORDS CENTER REOION 5

497026

Copy to;

Completed by: Liz Paler [Please Print]

Filing: Correspondence File

EQUAL EMPLOYMENT OPPORTUNirY EMPLOYER

Signed: V 4

HtGHTEHED COHPAMT FOR

ISO 9001 ENGINEERING DESIGN

Mm RA/NAL Project Number:

2664/ ' DOTHAZ UN/NA Code

Project Name/Location: Sybil), Inc. Site/Petriot, Michigan MFC Name

Container Inventory Num r Inventory Nu

Chemical Name

Container Typ<

£ Container Size Container Conten^(l/4,1/2,3/4,full)

Loggers Name. jj2. Paler

VeU I I'KCK Samplers Name

Gfg>M\ [ f PC^ Additional Infoirnation

No. of Containers Q CONTENTS DESCRIPTION

Top (A) Middle (B) Bottom (C) Layer

CONTENTS DESCRIPTION

Top (A) Middle (B) Bottom (C)

Sainple ID

Physical State

Color

Clarity

Thickness

FID (ppm)

Radiation

igiologicais m ABORATORY TESTS Top (A) . Middle (B) Bottom (C)

Laboratory ID:

Analyses Date:

Reactivity (Yes or No)

Air: Water:

Solubility (S/PS/I) Water: Solvent

Density LorH

pH:

Peroxide Test posorneg

Oxidizer Test pos or neg

Halogens pos or neg

Flame Color:

Sulfide pos or neg.

Confirmation Yes/No

Cyanide . pos orheg

Confirmation Yes/No

Flashpoint pos or neg

HO'F I's >10or<10ppm

Signature

Relinquished By:

Date Time

-Li-03- '1^30 Name and Affiliation

Received By:

rp 6 vie

CONTAINER INSPECTION RECORD iF :RA/NAL Project Number:

32664/ DOTHAZ UN/NA Code

Project Name/Location: Sybilh Inc; Site/Detriot, Michigan MFC Name kj gyu

Cdntalner Inventory lumber _

Chemical Name

Container Type , ^ ^ C'

ite W / Tlme^ ^ I.<

lontainer Size Container Content (1/4,1/2J/4,full)

Additional Imormation 131.

Loggers Name Samplers Nai

Cinch No. of Containers CONTENTS DESCRIPTION /


CONTENTS DESCRIPTION /


Sample ID

Physical State

Color

Clarity

Thickness

PID (ppm)

Radiation

lîologicals

^BORATORY TESTS Top (A) Middle (B) Bottom (C)

Laboratory ID:

Analyses Date:

Reactivity' (Yes or No)

Air: Water:

Solubility (S/PS/I) Water: Solvent:

iDensity LorH

pH:

Peroxide Test pos or neg

Oxidizer Test pes or neg

Halogens pos or neg

Flame Color:

Sulfide pos or neg

Confirmation Yes/No

Cyanide pos or neg

Confirmation Yes/No

m Flashpoint. pos or neg

HOT "B's ^10or<10ppm

Signature

Relinquished By:

Date Time Name and Affiliation

,C/Uuv- CM. Received By:

08/20/2003 10:41 61B9273411 NEW AGE LANDMARK PAGE 02

CONTAISER INSPECTION RECORD |CRA/NAL Frojiect Number; 12664/ DOTUAZ UN/NA Code

Project Naine/LocatioD: Sybill, Inci Site/DetrioL Michigan MFC Name

Container Inventory Nmnber ^

Chemical N

Container Type

pate _ / / Time . J

Container Size >. SSaoie

Time . Sgeyig

Loggers ibnue . TAT. Ftfiies

Samplers Name

Additional Infomiation

(o\e4Lri

No. of Containers (

Layer Top ( A) ^{j^^-etSSnrENTS DESCRIPTION

Middle fB) Bottom (C) Sample ID

Physical Staie

Color

Clarity • CtcaA S6^ wtZ Thickness

PID (ppm)

Eladiaiion

Biologicals

1 Laboratory ID: 03 C>S"i - ^1 \ Analyses Dau: \ Reactivity (Yes or No)

Air: h>0 Reactivity (Yes or No) Water: lav X Solubility (S/PS/I) Water S \ Solubility (S/PS/I)

Solvent: -JT \

Density L or H

pH: Cs.ni k Peroxide Test posorneg

îdizcrTcst posorneg

^logons pos or neg

Flame Color yj<56 ,

\ Sulfide pos or neg

Confirmation Yô \ Cyanide poc or neg

Coniiimation Ycs/No luetSr-

\ Flashpoint pos or neg

0140'F \ PCB^s >l0ar<10ppyf/I ' J

iinquishcd By:

Received By: ^

CRA32661Cimi>iner

Date Time

nrsB I3H0

_ Name and Aiiiliation

N*VL

08/20/2003. 10:41 6189273411 NEW AGE LANDMARK PAGE 03

CRA/NAL Project Number; ^2664/.,' DOTHAZ UN/NACode

Project Name/Locotion; Sybill, bic. Site/Debiot. Michi;^ MFG Name

MtnuL

Contaioerla

Cbemical Name

CoQtaiaer Type i Container Sine.

Loggers Na;

:iji i? WA/T

Con^^^n^rt

Samplers Nai

Content (1/4,1/:

Additional Information

-5le^/Qw>. Q-h

I No. of Containers

tiOS. T°P<A2 CONTENTS DESCRIPTION

Middle (B)

Laboratoty ID:

Analyses Date: -


Air: ^30 Reactivity (Yes or No) Water AJO

Solubility (S/PS/lj Wata: SL Solubility (S/PS/lj Solvent: s

Density L or H L pH: rs Peroxide Test posorncg . iiSC^

Oxidizer Test posorncg • Halogens pos tn- neg

Rame Color:

Sulfide pos or neg

Confimnation Yts/No me&r

Cyanide pos or neg

Confirmation Yas«o

Flastvpoint pos or neg

& UO'V Hee. PCB's > 10 or < 10 ppm

a ^ •5^"

9L Signature

linqulshed By:

Received By:

OU 32S6«;oiitoino liapeetiDn JbtcoRLxb

Time

J2£.

Name and Affiliation

m<a^ CRA

faar'A>-fce- /ufe_

CONTAINER INSPECTION RECORD

LABORATORY TESTS Top (A) Middle (B) Bottom (C)

Laboratory ID:

Analyses Date:


Air: Reactivity (Yes or No) Water:

Solubility (S/PS/I) Water: Solubility (S/PS/I) Solvent:

Density L or H

pH:

Peroxide Test pos orneg


Halogens pos or neg

Flame Color:

Sulfide pos or neg

Confirmation Yes/No

Cyanide pos or neg

Confirmation Yes/No


@ HO-F

jpCB's > 10 or < 10 ppm

Signature

Relinquished By:

Received By:


B-11-03 \tl,0L

IRA/NAL Project Number: ^32664/

Project Name/Location: Sybill, Inc. Site/Detriotj Michigan

Container Inventoj

DOTHAZ MFGName Chemical Name UN/NA Code Container Type , .

w/ bate _ I' Time ' Time

Container Size .•yjqa/

i:faj4ame T rJ?, Palgv'

Logged Samplers Name


NOi of Containers CONTENTS DESCRIPTION




Sample ID

Physical State

Color

Clarity

TTiicloiess

FID (ppm)

Radiation

îologicals

" LA ^BORATORY TESTS Top (A) Middle (B) Bottom (C)

Laboratory ID:

Analyses Date:


Air:

Water:

Solubility (S/PS/I) Water: . Solvent:

Density LorH

pH:



Halogens pos or neg

Flame Color:

Sulfide pos or neg

Confirmation Yes/No

Cyanide pos or neg

Confirmation Ves/No

m Flashpoint pos or neg

@ 140°F

CB'S > 10 or< 10 ppm

Signature i

:: rci • Relinquished By;

Received By:


c?J.

08/20/2003 10:41 6169273411 NEW AGE LANDMARK PAGE 04


UboratotylD;. ^3t^-003-^ asoSS-cfiA Analyses Date:


Air: U w Reactivity (Yes or No) Water: AI n ••

Solubility (S/PS/I) Water; wo -U- YtS Solubility (S/PS/I) Solvent: • Ho WO

Density L or H a •K(pi

pH: 5". s:')/ Peroxide Test pes or ncg toeo »OeCr Oxidizer Test pos or ncg

Halogens pos or neg

Flame Color:

Sulfide .posornpg

Confimiation Vei/No Cyanide pos ortieg

Coiifirmanbn Yes/No .


@ MCF _ He A A/Ad-PCB's >10orC10>^tjl 1

linquished By:

Recdved By:

CRA 32«Mani»liMr j^ftpec^n )tKori.xl(

Date Name and A ffiliation


CRA/NAL Frojeet Number: 32664/ DOTHAZ IIN/NA Code

Project Name/Locstfoii; Sybil], lac. Site/PetrioL Michigan MFG Name

w/. .rLtime L LoajersName ' Date

Chcmieal Name

ComaiberjCoi l/4.ia,3/a,ftiii)

Additional Infonnation

SamplersVame . -Gfeiuil&ti'a^ (iUlPC.

^0. of Coiitainera

Layer

Sample ID

Physical State

Color

Clarity

Thickness

PID (ppm)

.1 •

CONTENTSDESC

Middle {B1 Bottom (C)

y ^

Radiation

Biolbgicals £jffM

4'

flr LABORATORY TESTS Middle (B) Bottom (C)

iboratory ID:

Analyses Date:

Reactivity (Yea or No)

H Water: a h Solubility (S/PS/I) Water; Solvent:

Density LorH

RH: peroxide Test pos or neg

Oxidizer Test posorneg

Halogens pos or neg

Flarnc Color: ^

Sulfide poa or neg

Confirmation YO/NQ

Cyanide poa or neg

COnfinnation Ycs/No

A/^Gr-

A-jgiSr

:|aahpoint @140»F

posorneg

PCB's >10 or <10

iinquished By:

Received By:

CSA SZSMOuiiQintr bupeeiiiiii Reeordjci*

Date Time

It

Name and ABiliation

ORfl-

^ I25& -jisirmu.

08/20/2003 10141 6169273411 NEM AGE LAI^MARK PAGE 06

CONTAINER INSPECTION RECORD CRA/NAL Project Nnmber; 32664/ )OTHAZ

UW/WACode

Project Nsme/Locatioa: Sybili, fac, Site/Detriot, MieliiffaTi MFG Name Chemical Name

Container TVpe , ii Container Sine - - j mt/hfork /iWiMirt, w7 sfe f

/ I . Loggers ISame O ap/Q?)-! /dtp I Lfefii/c^

Container Content /i/4,r/3^/4,niii)

Samplers N

Additional Information jUksL oaAJbpn ^//•/•gy iuiCwM:

No. of Containers (

Layer Top (A)


Middle (B1 Botto 10(C)

Sample ID

Physical State

Color

Clarity

Thickness

¥ Pip(ppni)

Radiation

i Biolqgicals

LaboratoiylD:

Analyses Date:

Resctiyity (Yes or No)

Air: Resctiyity (Yes or No) Water: h Solubility (S/PS/I) Water: a: Solubility (S/PS/I)

Solvent:

Density L or H

pH:

Peroxide Test pos or ncg Jt/£&r Oxidizer Test posorneg

Halogens pos or neg

Flame Color:

Sulfide posorneg

Confiimation Yes/No uea

Cyanide pos or neg

ConfimuitiQn Yes/No Flashpoint pos or neg

(31140'F '

FOB'S >10or< lOppqfi'y

•m. iinquishcd By;

Received By;

CRA33«<4CO


B-U-Q-^ V%T<S CfeA

IEM IMI LntL

08/20/2003 10:41 6189273411 MEW AGE LANDMARK PAGE 0/'

ti |GRA/NAL Proj^ Ntiniber: 2664/ lOTHAZ

Project Nune/Loc«tion: Sybil], Inc. Site/Detriot, MichiBan MPGName

UN/NACode

Co]i'taiiiiÎnvantotY:Nu]iiber

Chemical Name

Container Size « Container C ConfenUl/f

Additional InfoTnution

No. of Cootainera

Layer Sample ID

Physical State

Color

Clarity

CONTENTS DES

Middle

Igâc^

JO Bottom fC)

thidoiess

FID (ppm) Û'Ch

t3M tt lUdiaticm MM

Bioiogicals

§ * Laboratory ID: a5i>^'Ss>L^ Analyses Date: -


Air A/ A/ Reactivity (Yes or No) Water Ay A/ Solubility (S/PSA) Water; Solubility (S/PSA)

Solvent: "P^ Densiv L or H m L. pa-Peroxide teat posorneg N&B.


Halogens. pos or ncg

Flame Color; UQL Sulfide pos or neg

Confinnatian Yn/No NHL Cyanide pos or neg

Confirmation Ysf/No

Flashpoint pos or nog @140°F

PCB's • > 10or< lOppti/'; , ' -€ linquished By;

Received By:

CKA SasSlCMictina Inspactiini Kucaidgds

Date

-03^ Time Name and Affiliation

' Ct-A-

CRA/NAL Project Number: 32664/ BOTHAZ UN/NACode

Praject Namc/Location; Sybill, he. Site/Dehiot, Michigan MPG Name

CoBtuinerJt j^t^ Nu^ber

Cbeznicai Name

Contaioer Siae. Cojitainer >^^1/24/4,AiU)

Loggers Nam L-^ Samplers Name


liST/ftY/a*. oujPc^

No. of Containers I Layy., TonfAl

CONTENTS DESCRIPTION Middle fJB) Bottom (Q

Sample ID

Physical State 5 (I Color

Garity

XKVt AMH^ 0.0

Thickness

»ID(ppm)

Radiation

Biologicals

âboiatoiy ID:

iRnalyses Date;

Reactivity, , (Yes or No)

Air: u • Reactivity, , (Yes or No) Water-

SplubiHty (S/PS/IJ Water: SplubiHty (S/PS/IJ Solvent:

Density L or H h{ pH: - ,

Peroxide Test pos or ncg ^teCsr Oxidizer Test posorneg

HalogenB pos or ncg

Flame Color:

Sulfide pos or neg

Confirmation YU/NO

/v/^4-

Cyanide posorneg

Ccmfinnatian Yas/Mo


M 140"F PCB's > 10or<10ppi3O

ir linquished By:

Received By:

OUaatSlCoiuaaiar

Date Time

r$.-^ Name and Afhliation

1^^%/st)ALL KMi.

biby^/'jaai NEW AQE LANDMARK PAQE m

CRA/NAL Project Number: 32664;

Project Name/Locadon; Sybil], Inc. Site/Detnot, NfichiKan

' DOT HAZ MFG Name Chemical Name UN/NACode

MFG Name Chemical Name

Container Type rkMu/in

Container Contc^^;^/Zj3|<.ft>ii)^ J

"tlsh Time

IQ2> 3

1 Laboratory ID:

Analyses Date:


Air: hi Reactivity (Yes or No) Water u Solubility (S/PS/I) Water; Solubility (S/PS/I)

Solvent: •r. Density L or H m-pH: 2-44 Peroxide Teat posorneg Me-Cs-Oxidizer Test pes or neg

Halogens pos or neg

Flame Color:

Sulfide posorneg

Cqnfinmtion Ya/No

Cyanide posorneg

Confirmation y«i/Na

Flashpoint posorneg

@140'T FOB'S > 10 or< lOppjT)

ilinquishcd By;

Received By:

CSA aaeUContamU'llivcciion Beeeid.xl!i

Time Name and A fCilintion

CkA

mh m' âsrr^^ iJh

08/20/2003 10:41 8189273411 NEW' AGE LANDMARK PAGE 10

CRA/NAL Project Number: 32664/

Frojetlt Naioc/Locatiou: iSybin. Inc. Site/Petrioti Michigan

Cbutalner I

DOTHAZ MFG Name Chemical Name ON/NA Code

No. of Coniaincia

Layer

7^ CONTENTS DESC

Middle (B) Bottom (O Sample ID

Physical State

Color mssmivjmm Clarity

Thickness

^cdt^CbiX JJSQJJL

FiDOn>'") D; Eradiation

iologicals

* Laboratory DO; 053-00^ 6 Analyses Date:


Air: hJ %J Reactivity (Yes or No) Water: Nt Solubility (S/PS/I) Water: x: < Solubility (S/PS/I)

Solvent: . n

Density LorH tt m pH;

peroxide Test posor neg A^G-Oxidizer Test posorneg

Halogens pes or neg

Flame Color:

SulBde pas or neg

CanHrmatlon YO/NB Cyanide posorneg

Confinnatian Ye«/No


caI40'F uu PCB's >10or< lOppip^ m .elinquishcd By:

Received By:

CKA SZSfilContalhiif tapbciion RKOcd-xk

Date Time

Hb2> Name and Afdliacion

m CONTAINIR INSPECTION RECORD RA/NAL Project Number:

32664/ Project Name/Location: Sybil), Inc. Site/Detriot, Michigan

Container Inve: :ntoi7 Nuniber, , /

1b"T)/Y A I POTHAZ MFC Name Chemical Name

UN/NA Code Container Type

swacfc-Time. _

Container Size Container Content (i/4;i/2,3/Wuii

(03f) Loggers Nami Samplers Name


No. of Containers

Layer Top (A)


Middle (B) Bottom (C)

Sample ID

Physical State

Color

Clarity

Thickness

PID (ppm)

Radiation

iologicals


Laboratory ID:

Analyses Date:




Density L or H

pH:

Peroxide Test pes or neg


Halogens pes or neg

Flame Color: -

Sulfide pos or neg

Confirmation Yes/No

Cyanide pos or neg

Confirttiation Yes/No

iPlashpoint pos or neg

^140"? |peB's > iO or < 10 ppm

Signature ,

Relinquished By: ' /


Received By:

0B/20/2003 1M:41 6163273411 NEW AGE LANDMARK PAGE 11

Laboratoiy ID:

Analyses Date: •??////« Eleactivity (Yes or No)

Air /y Eleactivity (Yes or No) Water A/ Solubility (S/PS/I) Water: 5 Solubility (S/PS/I)

Solvent: ZL. Density L or H

PH:

Peroxide JTest pes or neg

Oxidizer Test posorneg Kf5A . :

IHalOgens pos or neg

Flmc Color. A/^

Sulfide pos or neg

Confirmation Yei/No

Cyanide pos or neg

Confinnation Yas/No

Flashpoint posorneg

.ffl 140'F PCB's >10or<I0pp(t^.'

.quished'By;

Received By:

CRASaSMCanaiiiu

. Date Time

\'S-S6' Name and Affiliation

thM. kUL

08/20/2003 1:0:41 6169273411 NEW AGE LANDMARK PAGE 12

CRA/NAL Project Number: 32664/. DOTHAZ tnSf/NA Code

Frtijert Name/Location: Sybill, Inc. Site/Dctript, Michigan MFC Name Cbemical Name

GoAtainer Invento^ NmB|>^

Container"N.

•'* To'i'i Dai

Giantai a Additional Infonnation

Container Content a/4,i/z^/4iii^|i>i

3^^ d/«tAr\-' €uph^ No. of Containers

Layer TopfA) CONTENTS DESCRIPTION

Middle (B1 Bottom (C) Sample ID

Physical State

Color

Clarity

JtkMD Thickness

FID (ppm)

Radiation 1 Biologicals

Laboratory ID:

Analyses Date:

Reactiviiy (Yes or No)

Air: N Reactiviiy (Yes or No) Water: N Solubility (S/PSA) Water Solubility (S/PSA)

Solvent: 7>5 Density L or H L pH: a.u Peroxide Test posorneg

Oxidizer Test. pos orneg

Halogens poa or neg

Flame Color:

•

Sulfide pos or ncg

Confirmation Ye»/No

Cyanide pos orneg

Confirmation Yes/No


® 140'F PCB's > 10 or < 10 ppm ^

« illnqiiished By:

Received By;

CXA 326MQ>ncamer Inipcclion n«oidiXli


g'U-Qi r^-ê> CR/U

is CONTAINER INSPECTION RECORD

:RA/NAL Project Number: 32664/

Project Name/Location: Sybil), Inc. Site/Detriot, Michigan

Container Inventory Number

>0R DOTHAZ MEG Name Chemical Name

UN/NA Code Contai

ime _

1£!31

Container Siz^ ^ Container Content (l/4,l/2,3/4,full)

Logg^^î


' C Samplers Name

No. of Containers H Layer Top (A)



Sample ID

Physical State

Color

Clarity

Thickness

PID (ppm)

Radiation

iologicals


Laboratory ID:

Analyses Date:


Air:

Water:


Density LorH

pH:


Oxidizer Test pos Or neg

Halogens pos or neg

Flame Color:

Sulfide pos or neg

Confirmation Yes/No

Cyanide pos or neg

Confirmation Yes/No

*


140°F

CB's >10 or <10 ppm

Relinquished By:

Signature j ^ Date Time ^ Name and Affiliation

: U'O"^ — CR,/

Received By:

HB/20/2003 10:41 5159273411 NEW AGE LANDMARK PAGE 13

CRA/NAL Project Number: 32664/ DOTHAZ

Project Name/Locatfas: Sybill, Inc. Site/Detriot, Micli MFG Name

PN/NA Code

CoiltaiBerl:

Chemical Name

'uveBteiy

Con

Date


Coatainer Content i

SainplersName rs Name • ^ ^

No. of Container

Layer

Sample ID.


APdtBrTBT^

%yaical State

Color

Clarity

Tbicknesa

PID (ppm)

Radiation

Bioiogicals

IRATORY TESTS

rID: T»PW „ Middle (B) Bottom (C)

Analyses Date:


Solubility (S/PS/I)

- /2A

Air; ' Water; Water; Solvent:

Density -LorH

Peroxide Te^ posorncg

OxidiaerTest posorneg

Halogens posorneg

Flame Color;

Sulfide pos or neg

Confinnation Ycs/No

Cyanide pos or ncg

Confirmation Y«s/No

Flashpoint pos or neg @1^0°F

PCB's" >10 or <10

AJCS-

quished By;

Received By;

CKASaSUCnitainer

N^ and Affiliation

iM!

Time

08/20/2003 10:41 61B9273411. NEW AGE LANDHARK PAGE 14

|CRA/NAL Project Number; 12664/

Project Name/Location: Sybil], Inc. Site/Betriot, Michigan

Coiitdiier lovgjitory Numb

DOTHAZ MFC Name A Code

ChemlcalName

HBtaiiier Type

Time m. Additional Infomiation

UlRdk>r

Container Coi

SamplersNimie ^

CleMm jBhia^n Cr^PC

No. of Comainas

..aycr CONTENTS DESCRIPTION

TopfAl Middle fB) Bottom (C) Sample ID

Physical State

Color

Clarity

Thiclmess

SSI PID{ppm)

Radiation

Siologicals

Laboratory ID:

Analyses Date:

R-eactivity (Yes or No)

Air: -fj R-eactivity (Yes or No) Water:

Solubility (S/PS/I) Wata: s Solubility (S/PS/I) Solvent; X

Density L or H M •• ' ' pH:


Oxidizer Test posorneg /L>^6c-Halogens pos or neg

Flame Color: m Sulfide pos or neg

Confirmation Ym/No

Cyanide pos or neg

Confirmation Yci/No

Flashpoint posoriicg

(S 140*F I PCB's > 10 or < 10 ppm

^Rlinqi |uishcdBy:

Received By;

CBA32664Cantatn«r


3hm. AteC /}M!_

08/20/2003 10:41 6189273411 NEW AGE LANDMARK PAlat 15

CRA/NAL Project Number: 32664/ DOTHAZ

Project Nune/Locutioa: Sybill. Inc. Site/Detriot, Miehigan MFGName

Cootaluer Inventory Number

Chemical Nunc UN/NA Code

Addirionfll InforniBtioii

No. of Coritmners j

Layer Top (A) CONTENTS DESCRIPTION

Middle (B) Bottom (Q

Sample ID OA Physical State

Color

Clarity

Thickness

PID (ppm)

Radiatioq

Biolosicals

•LaboTatary ID:

Analyses Date:


Air: Reactivity (Yes or No) Water

Solubility (S/PS/I) Water. Solubility (S/PS/I) Solvent:

Density L or H

pH;

Peroxide Test pas or neg Ueisr Oxidizer Test pos or neg

Halogens pos or neg

Flame Color: ,

Sulfide pos or neg

Confimiation Yes/No t^-Ziar ' • '

Cyanide pos or neg

Confirmation Yex/No . jL)6fe-


® 140°P /

FOB'S >10or<l0ppT/ /

illnquishcd

Received By:

CSAUSSlCamaiiie)'

Name and Afhliation

/^2V

Time

IpRA/NAL Project Number: 32664/

Project Name/Location: Sybilij Inc. Site/Detriot, Michigan

Contalnenlnveâ Number

DOT HAZ UN/NA Code

MFC Name Chemical Name

CoDtalner Type Container Size Container Content (l/4,l/2;3/4ifull)

"•"610/63 Tisa Samplers Name

Additional InfonnatiGn

No. of Containers CONTENTS DESCRIPTION




Sample ID • • Physical State

Color

Clarity

Thickness

PID (ppm) ..

Radiation

îologicals -

JORATORY TESTS T°P(A) Middle (B) Bottom (C)

Laboratory ID:

Analyses Date:


Air:

Water:

Solubility (S/PS/I) Water: -Solvent:

Density L.orH

pH:



Halogens pos or neg

Flame Color:

Sulfide pos or neg

Confirmation Yes/No

Cyanide pos pr neg

Confirmation Yes/No

m Flashpoint pos or neg

UO^F

;B'S >10or<I0ppm

Signature Date Time Name and Affiliation

Relinquished By:

Received By:

08/20/2003 10:: 41 6163273411 NEW ASE LANJJMHNN

CRA/NAL Project Nuniber: 32664/

BAZ UN/NACode

Project NaiDi^qcatiaB: Sybill, fac. SitE/Detriot. Nfichigm MFCNanie

Contaiiicr Ibvcntory

ChebticalMame

ConteijerType Container C:aatebt (i


No. of Containers

Layer Sample ID

TopfAl


Middle fB)

Physical State

Color

Clarity

Thickness

Bottom (C)

PB3.(ppni) HZ Radiatioq NJfifcf. Biologicals

Bboratdiy ID: • - S' ••....

âlyses Date:

Reactivity CYesorNo)

Air: ki Reactivity CYesorNo) Water: /7

Solubility (S/PSA) Water: 3 Solubility (S/PSA) Solveni; T.

Density L orH m pH:

Peroxide Test poftorneg

Oxidizer Test posor neg Deer Halogens posorneg

Plaome Color Sulfide posorneg

Cpnfinnaition Ya/No

Cyanide. pos or neg

CanSnnkiQn Yei/Ne Flashpoint pos or neg

aidCF -FGB'a >I0or<10ps(6/

^jjjûished By:

Received By:


aa/zH/ZHHd Id:«n NEW AGE LANDMARK PAGE 17

CRAmAL Project Nnmben 132664/

Project Nanie/Locatioii: Sybil]^ Inc. Slte/Demox. Michigan

Contaiiier Inventory Number

HAZ MFGName Cbemical Nome UN/NA Code Container type

Ral n-,r-cA,i„ Container Content (^4,i/2^/4,full)

Samplers Name

Additionar Infonnation fyuilH fck

No. of Containeis Layer TOP /A)

CONTENTS DESCRIPTION MiddlefB) Bottom fC)

Senile ID

Physical State

Color

Clarity

(Vi<,c;ovtO thickness

FID CPP")} Radiation

Biologicals

Moratory ID; 030^'oib' Analyses Date: \ Reactivity (Yes or No)

Air: u Reactivity (Yes or No) Water N Solubility (S/PS/I) Water; Solubility (S/PS/I)

Solvent: Density L or H L pH:

PerondeTest posorneg UOs Oxidizer Test posorneg

Halogens pos or neg

name Color:

Sulfide pos or neg

Confirmation Yes/No

Cyatiide pos or neg

Confirmation Yej/No

Flaahpoint pos or neg

@ 14P-F PCB's >10or<10pp5ir^

linquishcd By;

Received By:

CRA SZ66lCantiliMr InpiKUoii XeconLxlt

Name and ACftliation

08/20/2003 10:: 41 61&9273411 NEW AGE LANDMARK PAGE IB

CRA/NAL Project Nrnnbcr: 5^

Project Nfline/Locatiou: SyWil, Inc. Sitefl3etriot. Michigan MFGName

Contafaier Inventory Number

CbemiealName

Contaiber Size Container Content (i/'>^>3/4,ikiiQ

LnggersName

U2 Samplen Name

(jWf Additional Infoimation

No. of Containers

^yer

Sample IP J2B.

CONTENTS PESCRIPTIOJ

JtfWlllcCBl

Physical State

Color y^rM C-1-efL. Oarity Thickness

2:2 PID(p|im)

Radiation

Biologicals

^mbpraiorylD: f 1 » •

' Analyses Date:


Air: V yj Reactivity (Yes or No) Water: V •' • Solubility (S/PS/I). Water; Solubility (S/PS/I).

Solvent: •5 • Density L or H /- \ pH: •7,^ Peroxide Test posornes

Oxidizer Test posor neg ijesr Halogens s>osorn«g PlxmeKôlor. kJM, yBA Sulfide pos or neg

Conlinnation Yci/No A/esfe- A/€T2—

Cyanide pos or neg

Coiifhrnaiian Yai/No KJ^&-Flashpoint pos or neg

(S 140"? PCB's , >10ar<10pgffj

[uished By;

ItecBived By;

Time.

ws Name imd ASiliation

5/^ /iXiU, KM

08/20/200a 10: 41 6169273411 NEW AGE LANDMARK PAGE 37

rONTAlNER INSPECTION RECOM) JlipiAL rrideet Nambars FialaetNuiM/LwBttiMi:

Svm Ruk SileiAielriot Michipm 1>-AM ^«A-PV

DorrHAZ MVGNmo ChemiMlNue

Contaburiypo GanMlecr Couteirt (Ml/%3a,mil}

beie Time • IHOO

Loo^ I*""!'

IV. sJ s. - rtlrt A<0^

No. of Cenodnen \ coNTBrrns IHBSCBIPTION /A% Mhuiem Brtiwira

SunpielD ft- » L

Color C('«601

Cleric Ihiekmu

PlD<ppin) O.O • 0.(3

Biologicata -- .

jjSonnrylD: 3<P "B lAnBtysuDac: v9 0:3 iH'O-ji

(yeeorNe) Air; fUeCr

(yeeorNe) Wider: tyjr&

Solubility (S/PSO) Water: :r ^'S Solubility (S/PSO) jz:

Dtaaily LorH z_ pH: 2..S 7.D PinxideTest pocornes yue-sr OxkHwrToBt poiorneB IVict. 1 ivieii: Kalogeqa paeorneg Phmo Color. K/flis-

1 lUtTfe,

ISuifide poiorneg

jCodbinuion YOIAOO /ViE& . A^<Sr-

cyanide poaorneg

Cohftntflloii YaiMo

PlaafapOQit pas or neg ai-wp

PCB'g ilOar<10ppin iOr-G-

•hedBy;

Received By;

a-rs-oi rioo noo £

CRA

jCRAyNAL Project Number: m664/

Project Name/Location: ^bill. Inc. Site/Detriot, Michigan

Container Inventory Numbes^ ^ o-naT DOT HAZ UN/NA Code


Container Type *

Container Size Container Content (1/4,1/2^/4,full)

loggmN™. Samplers Name






Sample ID

Physical State

Color

Clarity •

Thicicness

PID (ppm)

Radiation

Biologicals

ORATORY TESTS Top (A) Middle (B) Bottom (C)

laboratory ID:

Analyses Date:


Air:

Water:


Density LorH

pH:



Halogens pos or neg

Flame Color:

Sulfide pos or neg

Confirination Ves/No

Cyanide pos or neg

Confirmation Yes/No


@ lAOT

(11^ I's >10or<10ppm

Signature

Relinquished By:

Received By;


|||OftA/NAL Project Number: •6647

Project Name/Location: Sybill, Inc. Site/DetrioL Michigan

Coiitaiher Inventory Number"*'^ /\ O /

DOT HAZ MFC Name Chemical Name UN/NA Code


Contains Type J eu&ifKkfJ?

Container Size Container Content (i/4,i/2^/4juli)

''"•ft/8/03 Samplers Name

Layer Top (A)

INTENTS DESGRimON


Sample ID

Physical State

Color

Clarity

Thickness

PID (ppm) .

Radiation

Siologicals

ORATORY TESTS Top (A) Middle (B) Bottom (C)

Laboratory ID:

Analyses Date:


Air:

Water:


Density LorH

pH:



Halogens pos or neg

Flame Color:

Sulfide pos or neg

Confimiation Yes/No

Cyanide pos or neg

Confirmation Ves/No

Flashpoint pos or neg @14Q°F

I's >10 or <10 ppm

Signature

Relinquished By:

Received By:

• Date Time Name and Affiliation

Coatoiiêr Inventory Nunibet- ' jk '"7 { .X s

A,-- y •

A/NAL "rojciit Nuiiiber;

325C4/

«

FrOjcci Name/Location: Sybin inj; Michigai:

•THAZ MKG Name Cben-ica! Nsns^;

^/NA Code CoTitamrT Typt Coatasasi' iiitM tbtntainer Comcnt itM,!/2,3/4,ru»l)

Date^l^ ITime.jLoggers Name i ^ Sanip!»r5 Nan:^ .

i' i ii iOTi i'Oi j

u^'7^:W—p/ J= :/j •r i •: • -V . ^ > -V > r-f .•*-.=- ••• •••«• . - r.-"

-M. 2:r2.rv4j •-S.

No. of Co-tainors

Layer

yamplc ID

f nysicai Staie

...

CONTKN-re DSSCKiPTION

M'ilule (B) fC)

PID fsnml

Raiiiatioii

jE'ioiogicais 7-. LW w .«•« naisa &.•« £ «•-. M k ->

f^|!aiOry IL>: 1 ^Riyscs Date; i

• Re:ic!!viiy Air:

ry?5c;rNo) 1 1 f

i i wwlua*111 «-_T tK*fX or 1 » 1

i Solvent: i 1 Density I, or H 1 1 pH: i i

•beroxide ! est pos or ncg 1 i esi pij-s or ncg •i

i iiiiOgeiiO pos or nftil i 1 • i • i

Sulfide 150-; or rvip !

ConSm-iaiiijIi Yes.'>io I ! ' ' I i >

CyaTiide p05 or iicg

C.(,i< 1 Citniaiion YTr'Mc

1 •, ! i 1

rIa:":h,pos -or n-sg j

fo 140"? • 1 .

.'CB's > J 0 or < ! 0 pptn i' .1 ,

SibTnature Ho i jiili'D. .'s : :

nsnr-if. M\/-

tecei ved By;

08/20/2003, 10:41 6169273411 NEW ASE LANDMARK PA6E 29

Received By.

03/20/2003 10:41 6169273411 NEW AGE LANDMARK THUC. OO

|||||MAL Fntlcct Nanlwrt jpraleet NamaiUratlou: SvbilL be. SHaffDoriot. hlldiiiBn T-COiiA

{DOTHAZ MfGMama ChamlcBl Nana

CoislalliwTypa m

ConblacrSllsB Contaliiar Coptont (VMO^MiAiii)

Dafa Tliae LoggarMtbum

AddittoDiU Infonnatian

ofContifaaw j coNTiam sBscauPTiorr HaWtotB) SSL

Sample ID

Physical State u Color

Qailty

thieknew

«P(PPM) (3.0 Radiatwn

Biologicah

Jjôiu^ .TORYTE5TS JtttiAL MhMtetm BottamfO ID:

Analyses Dale:

Reaoliviiy (VeaorNo)

Soliib«ity(S«SI/I>

Air; Watef;

DoMfty LorH

S-- IV 03 lurs-

IL/ITCS-

Jfl

///J

iWclikTeat posoriwa

OaidiaaiTeat pCacsneg

3-' ̂ KJOT&-

Halogens poaorneg Piama Colon

ilfide pesornes Con&iBBtton YMfffti

pyaDlda poa orneg Coolimwrion Yoitfiiii

peaorneg

>10ar<]0pp ppm

joesr

\0C&

Signature Date Time None and AfiSIiatiQn

Mk£53J2oO_


JCRA/NAL]

^ DOT HAZ

[CRA/NAL Project Namber; m/

im/NACode

jPraject Name/Location: SybiU, Inc. Site/Detriotj MichigM MFGNi

ContiiRer Inveacory Number.

Chemical Name

Time

i3li Loggers Name _ .

liZ

Container Content a/4,:

M. "V^/si'^rrVPc'^ Additional Infbnnation

No.ofCoiilaiiiaa

Layer Top(:

CONTENTS DESCSIPTION

Middle fB) Bottom (C)

Sample ID

Physical State

Color

Claiity

TTiickneas

PIDCppm}

Radiation

Biologicals

lubomoiy ID:

Analyses Date:


Ain W Reactivity (Yes or No) Wa»n H. Sblubil% (S/PS/I) Water h Sblubil% (S/PS/I)

Solvent Density L or H

pH:

PeroxideTest poeorneg

Oxidizer Test poeorneg

Halogens pos or neg.

Flame Color

- • Sulfide pos or neg

ConfmnBtiaii yo/Xo ILTfe-fe. . .

Cymide pos or neg

Confirmation Yai/No hJ€&r

Flashpoint posorneg 9o% PCB's >10or< lOppi/'^

m imquishcd By:

Received By:

Date Time

IM. Name arid A fSIialion

CML tm—

08/20/2003 10i:41 6169273411 iNEU AGE LANDMARK PAGE 20

[AL Project Number:

HAZ UN/NA Code

Project Name/Location: Syfaiii^ Inc. Site/Detoot, Michigm MFGName

Container Size 350 q' 6(J0 Ci JLbggersNa|M.^

Cbntaliier Ibventory Number

Chemical

Contalaj

Sao

laax '/aim( v^c)

UPoboratoty IP: -

(Analyses Date; -

Reactivity jfyesorNo]

Air: A/ Reactivity jfyesorNo] Water; A/ Solubility (S/PS/I) Water: rZT Solubility (S/PS/I)

.Densi^ LorH H pH: i Peroxide Test posorncg yjecr

Oxidizer Jest pos orneg t^QC^

Halogens posorneg Flame Coior: Meo-Sulfide posorneg

Conflnnation Yes/No iar<S-

Cyanide posorneg

Coiifiimstian Yei/No

. i


® IdOT PCB's >10or<10ppn^ 1

Date Time Name and Afniiation ylH—— grR-oi ms c^/i

j!t^ x/jt

BU/:^!B/IB: 41 bibyi:/fa4.ii NEW AGE LANDMARK •PAGE 21

[AL Projert Naaber: 2664/

Project Name/LocatlQo; SvfaiUi Inc. Site/Deiripti Mi«^"Ban

OTHAZ mEsgpiFiiira. Container Type Container Size

Logg**^ Name i ^

Wr

Ivjz. FkM

Container Inventory Nuinba'

(WTni/ Container Contei

Sampjurs Name \

Additional ihforniation

No. of Containen Layer

CONTJBNTS DESCRIPTION Middle (B) Bottom (C)

Sample ID

Phyeical State

Color Oarity

Thickness PTOCppin) Radiation Biolpgjcala

Phboratoiy ID: /}3SS^-dZQ

Analyses Dote: • Reactivity (Yes or No)

Air: u Reactivity (Yes or No) Water 7J Solubility (S/PS/I) Water 7>^ -Solubility (S/PS/I)

Solvent: 1$ 1 ^

Density LorH hi pH:

.... ,



Halogens posorneg

Plaine Color:

Sulfide posorneg

Coiifinnation Yes/No

*

Cyanide posorneg

Confirmation Yn/No jFIashpoint pos or ncg

iai40*F fTi tiln ô>

PCB!S >10or<10pi^^

Date Time

-ms Name and Affiliation

'"^kSb^ytcLea—



No. of Coniainers

Layer Top (A)

CONTENTS DESCWPTION Middle (B) Bottom (O

Sample ID

Physical State

Color

Garity Thickness

ftp jste.

TTTO TT^

PID'(ppin)

Radiation

Biologicals

il piboraioTy ED:

Analyses Date:


Air kjp Reactivity (Yes or No) Water: u Solubility (S/PS/t) Water Solubility (S/PS/t)

Solvent: -r Density LorH m-pH;

Peroxide Test poaorneg

Oxidizer Test pos orneg

Halogens posorneg Flame Color:

Sulfide posorneg

Confinnation Ves/No

Cyanide posorneg

Confirmation Y<uA4a

Flasbpoint pos or ncg

@140-F / PCB'c > lO orciOppr/y

A linqufshcd By;

Received By:


'3

CRA/NAL Project Number: mmi

Project Name/Location: Sybill, Inc. Site/Detriot, Michigan

Container Inventory Numjifir 0

DOT HAZ t/N/NA Code


Container Typ^ Container Size Container Content (i/4.i/2^/4,rull)

Time oas Loggers Name Samplers Name


No. of Containers ( ) CONTENTS DESCRIPTION

Layer Top(A) Middle (B) Bottom (C)

Sample ID

Physical State

Color

Clarity

Thickness

PID (ppm)

Radiation

Biologicals

iRATORY TESTS Top (A) Middle (B) Bottom (C) Laboratory ID:

Analyses Date:


Air: Water:


Density LorH

PH:



Halogens pos or neg

FlameColor:

Sulfide pos or neg

Confirmation Ves/No

Cyanide pos or neg

Confirmation Ye»/No


@ 1401?

I's >10or<10ppm


Relinquished By:

Received By:

08/20/2003 10:41 B163273411 NEW AGE LANDMARK PAGE 23

CONTAINER INSPECTION RECORD fAL Project Number:

HAZ DN/NA Code

Projett Nanie/LocatiDtt: Sybil]. Inc. Site/Petriot Michigao MFG'Nune

Container laventoi

Cbemical Name

InventoryNnmber < ^

A Container Type Container Sl» Container Content (i/4,i/2^4,bli)

Additional Inibmiation

^titter N«me

BiJbA. f

No. of Containcia

Layw Sample ID

Physical State

Color

Clarity

Thidoiess

//(5hL-/ycDY' o/ /J AAg(

Top (A)

3V /J


Middle ( [tddl^ iottom fC]

FTDCppm)

Radiation

Biologicals

IÔRATORY TESTS Top (A) Middle (B) Bottom (O ^boratoiy ID; /5'5d>55' 02.Z, ̂ Analyses Date:.

Reactivity Air: N N (Yes or No) Water: N /J -

Solubility (S/PS/I) Water: 5 Solubility (S/PS/I) Solvent; -r

Density L or H /4f pH:

Peroxide Test posoriieg WBS- AAcS- f


Halogens pos or ncg

Flame Color A/^Cr

Sulfide posorneg

Confiimatian Yes/No tJc3-

Cyanide posorneg

Confinnation Y«/Me •jrO^T^

Flashpoint pes or neg

& IdOT PCB's > 10cr< lOppm^

îiiquished By; -—

Siâtme k Date Time Name and AifiHatian

— S-H-03 cftA Received By:

m IRA/NAL Project Number: .664/

Project Name/Location: Sybil), inc. Siteêtriot, Michigan


DOT HAZ MFC Name Chemical Name

UN/NA Code Container Container Content (1/4,1/2,3/4,ftiii)


Layer Top (A) Middle (B) Bottom (C)

Sample ID

Physical State

Color

Clarity

Thickness

PID (ppm) .

Radiation

Biologicals

^BORATORY TESTS Top (A) Middle (B) Bottom (C)

Laboratory ID:

Analyses Date:


Air:

Water:


Density LorH

pH;



Halogens pos or neg

Flame Color:

Sulfide pos or neg

Confirmation Yes/No

Cyanide pos or peg

Confirmation Yes/No


@ 140'F

I's ' > 10 or < 10 ppm


Relinquished By:

Received By:

08/20/2003 10:41 61G9273411 NEW AGE LANDMARK PAGE 24

J.CRA/NAL ProjBct Nnmber;

™ DOTH

iProJeet Ngin«/LpeadDn: Sybill, foe, Site/Dietrioi. MiehlRm

Coataiuer Inv«tory Ngmber D-03^ 'HAZ MFG:Naiitic Chemical Name

Cbntainer Sizci

Additional Infotmation

fh t

Contalaer Conteot (lAi,l/3ÂfnU)

Samplers.Name

•u lufd OdP " 1^0. of Containcis CONTENTS DESCRIPTION

Middle m Bottem fO

Radiation MAI ̂ urn IT • ^Sg) -fegfe

Bioiogicala

\ Rboratoiy D>:

Analyses Dale:


Air: hJ Reactivity (Yes or No) Water: u Solubility (S/PS/i) Water Solubility (S/PS/i)

Solvent: Density L or H

PH: L.O Peroxide Test posorneg


I^logcns posorneg

Flame Color T^^(S- '

Sulfide pos or neg

Coniimiation Yes/No /J&Ss

Cyanide pos or neg

Confiimation Ycs44a fi/^& Flasbpoint pos or neg

®140"F fi/eCsr-

-

PCB's > 10 or < 10 ppm^

Date Time Name and Afliiiarion

/V5S' kti!


IjdRA/NAL project Nnmben

SKTHAZ

Frojeetftame/Loeation! Sybil!, fee. Site/Detriot. Michigan

Contaiqarlnventary Number

MFGName Cbemicul Name' UN/NACode Container tivpe • iGbntainerSte /7

• pfflBSr erterv-big , />a!/

Additional Infomiaticm 1*^1^1

Container Content (l/4,ia,s/4,flili}

Sauipleri Name c)

No. of Contamen

Layer Top (A) CONTENTS DESCRIPTION


PID (ppm)

Radiatibn

Bidlogicals

'Mli

^j^BOl^

* Rboratoiy

IRATORY TESTS T°P(A) ID: 0?rfX-O3tf

Middle fB) Bottom (C)

Annlyses Dam:


Solubility (S/PS/Q

Air: Water:

Water; Solvent

Density LorH Jt/L pH:

iâideTesi poeoriwg ftJtrSr Oxidizer Test pos m neg

Imogens pos brheg ininfiie Color ^

Sulitde, posorneg

CanSnnation YesMe

Qpude pos orneg ConfikmBtian'.YM/Na

poaoriieg

•jlSTT

Date Time Name and AfliKation

S-li-p rvis natL.

138/20/2003 10:41 B1B82/3411 NEW PJSE LANUMfiKK

,|QM/NAL,|yojMtiNuBil»«r:

Ji||g6£_ Wbini

Prajieet Nam/LooMira: SIPWB. Inc. gte(Debriot Mjchigiai

CdiitaiBer Imnrtdi^

-HAZ MFC Nam

ON/NA Code

IATP^

OumliialNi

Conlalner Cootairt

Sampien,

Addidonal Infonnation

dlA/PC

No. of CoiitauicTB

Layer SainplelD

TOPCA)

CONTENTS DESqaPTiON

MMdle(B) iSL

Physical State

Color

Clarity

Thickness

PiPO>pni}

RadiaikM to HSOfBW

Biologicala

^Boratoiy ID:

lâlyses Date:

Resco'vily (Yes or No)

Ah: V Resco'vily (Yes or No) Water

Solubility (S/PS/I) Water. ' Solubility (S/PS/I)

PRO! Density LorH jt/yf- *

pH: > V

Peroxide Test posorneg yj&f

Oxidizer Test posorneg A-'es- 1

Halogens pos orneg Flame Colon •

Suiiide posorneg

Confitmatiaa YttfNo fje& Cyanide poa orneg Confbmaeian YeiWa

• Flashpoint pos or neg

& 140"F PCffs >iaor<VOpp^ 1 » . r

lUislied By; . AiioiiH . x-yoijic Ofiu /IkiiJJlBUan

-^gfc>f7gL^ re.A-

m h. 5£sr jjtL. . 'i

0B/20/2003 10:41 B1B3273411 NEW AGE LANDMARK PAGE 30

IgftA/N AL Project Nnniber:

^5QTB

Fn|eet N*iiui/LM«tion: HyhiB|. Iwfc atte/Deniot. Midrigm

Contaliur Inventory Number

Additional Infonmtion

PlD(ppm) Radiebon

Hi-V -MtL

Biologicala

•—:—;;r— "fAnalyaa Date:

Reactivity (Yes.orNo)

Air: A/ ... Reactivity (Yes.orNo) Water hi ^lubility<S/PS/D )

r

Water ^lubility<S/PS/D ) r Solvent: <

Denaity L or H

pH: 1

Peroxide Test posorneg A/fCr OxidizcrTcst posorneg /l/frcSr Hdktgena posorneg Rlsnw Color

; '

Sulfide posorneg Contumation VaaAb pb% Pyanide poa or neg Cmlinnaticn Yaaffia tJSir Flubpoint pos or neg {aMO*? A/fO

RGB'S >10ar<10ppipn . Date Time

ms Name and Afliliatlon


fONTATNER INSPECTIOK RECORD yNombflr

Pr^JiectNanban

^ iiorHAZ ilCn?iNMiia

UM/NACodc CiMitalaiir IVne

Awv

EiniJaccNum/LiMBllaii: Svbm. hiB. SHnPeirirt. Mjdrigm

ContalBBrSliM SS-iaJL

GhandcRlNune

Caatabicr Cbntanf

t: YS' ThM

VHOO SamplariK

AddMonil bifivmation j yoAAiL'^ >j>A - njo i)A<!'i\iU _

-tiadL 1-

No/ofConniiun \ CONTBPrrSDBSCiaPTlON. / TtolAl MkWtemi

\ / ^ /

PhyBttal State \ / y {Color A ' / Clarity / \ / Thkdoieaa . ' .

PlDCppm) 0.(b a«H8af8Mi

BMosicab *

.ÎPntfOfylD: 3^ ]A»a]yseaDne; ••

Raaotivily (Yea or No)

Air: yes 5TÔ/06r kc. (^<kojr Raaotivily (Yea or No) Water:

Solubility (S/PS/Q Water: Solubility (S/PS/Q

Deaaity LorH L »B: -?. o

PttoxidcTott ptUiornqi fj £* 4r

QiddiwTeat posornsg | vore^ Halogena poaorneg FlanwColor vev • Sulfide . poeorneg Canfinnadtti VuMb

—

Cyanide poeorneg Canftnwian YGIMO ue(5r Flaabptilitt poiornqg ai4(fP

PCB'a >10or<10!ppm ..

/Vffe-

htiMk y _ . ̂ sk

^tohcd rCA—

RocaivedBy: ^ g-13- 0^ noo iiM5 1*523

:atl/20/2003 10:41 •blbg273411 NEW AGE LANDMARK PAGE 27

•OEU/NAL Frojert Nunfa^ Projeet Nnn«/Laoadon: SVfaill. Inc. Site/BiBaiot. Mfchigm MFGJtmu

CoBtalBBr Invaitory Number

CbcaiteslName l>nHI

CoataluM

Loggers •Gk fa ContaliMr COBI^ a 'W Sunplers

AdditaonHl Ihfbrmfttion I55<^

No. of Conlainers f

Layer Top (A)



Saiiq)lelD

PbysicaJ State

Color

Clarity

Tbiclqiesii

PID(ppm)

RadifltioD

Riologicals

j^PotatoiylD; miss-itzi' (Analyses Date:

Readiviiy (Yes or No)

Air N Readiviiy (Yes or No) Water u Solubility (S/PS/O Water Solubility (S/PS/O

Density LorH

pH: i

Peroxide Test posorneg tiJ£5-Oxidizer Test poaorneg A>ir6-Halogens posorneg Flame Coloi; •

Sulfide posorneg

ConfiniiBtian Yoa/Na

Cyanide posorneg

Gonfinnaiian YM/NO î^Qr

Flsahponit posorneg

&. 14tfT -• . pep's >10ar<10ppn>o

Time

n>HS NmandAlBlMon

fefidr r.(?A-—

08/20/2003 10:41 6169273411 NEW AGE LANDMARK PAGE. 28.

Pri4«et Number:

HAZ tIN/NACode

Krajcit N«w/Loe«Npn: Svbill; Inc. Site/Doriot. Michiwn

luvcutory

MFGNana

jCoutalaer Cpatnlner

Huv Loggers Nune

Container Coutent piHi

Si

Additional Tnfonnation

No. of Contmieya |

hss-CONTCNTS DESCRIFnON

MhldlafP) Bottom fCl Sample ID

Pbyrica] State Color

Clarity Thickneas

Prb iiuM. K Nt>»t

b RfX) Ml p^'^diLl. PIDfppm) Radiation

Sk.

m)S3-oz:?-lAiulyaes Date; Reacdviiy (Yea or No)

Air N Reacdviiy (Yea or No) Water: 7/ Solubility (S/PS/1) Water; Solubility (S/PS/1)

Solvent: Donai'ly. LorH

pH:

PnoKide Test pos or nog iUe-dr •

OxidtaerTeat posorneg Pos Halogens pos orneg Flame Color. Sulfide posorneg ConfiRnadon YMAVO

1

Cyanide posorneg Cpntiimaiian Yea/Ne Flaahpoint pos or neg & i40"P ^

RGB's >10ar<10ppin z/

Received By:

•. i^rnnGma/Mjanmon-

CfeA

;AL Project Number: Project Name/Locution: Sybill, Inc. Site/Detriot. Michigan

Container Inventory Number. - rsn-j.

D0THAZ MFGNiame Ctaemical Niune

tlN/N A Code Container Tjiic Container Sl» - Container Content

Date Time -mg)

Loggers Name Sailers Name WI4JH

Additional Information 'Tt/.rs rs c\ar:j^

No. of Containers

Layer Top (A)


Middle (B) BottomJC)

Sample ID

Physical State u Color

Clarity

Thickness

PIDO>pni) o.o Radiation

Biologicals

Laboratory ID:

Analyses Date:



Solubility (S/PS/I) Water Solubility (S/PS/I) Solvent: 1

Density . LorH

pH:



Halogens pos or neg Flame Color:

Sulfide pos or neg

Confirtnation Va/Na

Cyanide posorneg

ConfiTmation'y«s/No

Plashpoint posorneg

@ I40*F

^£2*3 >10or<10ppm

Relinquished By:

Received By:

^BUCSAL ^K64y

Project Number: Project Name/Location: Sybill, Inc. Site/Detriot. Midjiigan


TK POTHAZ MFGName Chemical Name

UN/NACode Com Container Size Container Content (1/4,l/2rl/4,liiii)

Lo^mName Name

Additional Information ^ . f i*vU?uv^

O.I crr£ No. of Containers ^

Layer Top (A)



Sample ID TK - OHM." 6

Physical State V"=so-cil. Color

I • f ui.'d

Cle^cuy

Oarity

Thickness

PID(ppm) Q>0 o-.o Radiation

\KQP-''JIU er^JL Biologicals

iRATORY TESTS Top (A? Middle (B) Bottom (C) Laboratory ID:

Analyses Date:

Reactivity (VcsorNo)

Air: Water:

^lability (S/PS/I) Water Solvent:

Density LorH

PH:


Oxidizer Test posorneg'

Halogens poa or neg

Flame Color:

Sulfide pos or neg

Confirmation Ves/No .

Cyanide poa or neg

Confinnation Yoa/No

Flashpoint poa or neg

@I40"F

jp > 10or<I0ppm

Relinquished By: j. 1-Date Time Name and Affiliation

Received By:

CA/N, 6^

lAL Project Nnmber; ProJ^ Neme/LfOcatlbii: Svbiil. liic. Site/Detriot. Michigan

Container I: Number

DOTHAZ MFC Name Chemical Name

mm A Code Container Container Sin ConUiner Content

TimeM*y3 Loe^^ lame V<AarW

Samplers Name

Additional' InformatiDn

Crt. No. of Containers |

Layer


TOD YA) Middle IB) Bottom fC)

Sample ID rX-m^-A Tic- 045T> Physical State Vs.L>"ci Color

\ Clfciiixn.

aarity r\.ecLsx Thickness

FID (ppm) oo o .0 Radiation IA ."k-i/i f\ 1A /Kp.A n Biologicals

\)u3>^<iL •RATORY TESTS Top (A) Middle (B) Bottom (C>

Laboratoi7 ID:

Analyses Date:


Air: Water:

Solubility (S/PSA) Water Solvent:

density LorH

PH:



Halogens pos or neg

Flame Color:

Sulfide posorneg

Confirmation Ysa/No

Cyanide pos or neg

Confinnation Yci/No

'lashpoint pos or neg

@ 140"?

> IOor< lOppm

Signature >

Relinquished By: Date Time Name and Affiliation

CR,A Received By:

H^NAL Project Nqmber: Project Name/Location: Svbill. InCi Site/Detriot. Michigan

bOTHAZ MFGName Chemical Name

Container Type ^ Container Size ^ '• Container Content (i/4,i/l^/4,niii)

bate Time •LoggenName L, • • Samplers Name

Additional Information . i Additional Information .

ci<>ji.,LUAA

- C0. u £a.o.i ClrfC/ No. of Containers ^ CONTENTS DESCRIPTION

ToD fAl Middle (B) Bottom (C) Laver


ToD fAl Middle (B) Bottom (C)

Sample ID '

Physical State ItoW Color C\LOU^

Clarity a><êK^\tL

Thickness \

PID(ppm) 0.0 Radiation X Biologicals X m •RATORY TESTS Top (A) Middle (B) Bottom(C)

Laboratory ID;

Analyses Date:


Air: Water:

Solubility (S/PS/t) Water: Solvent:

Density, LorH

pH:



Halogens pos or neg Flame Color

Sulfide pos or neg

Confirmation Vas/No

Cyanide posorneg

Confirmation Yoa/No

Flashpoint

(a I40'F

poa or neg

PCT's > 10 or < 10 ppm w Relmqi

Sl8„«ur. ̂

quished By:

Received By;


08/20/2003 10:41 61E9273411 NEW AGE LANDMARK PAGE 31

lidkA/MAL ̂ pjaet Niuabcr; iPrqJaet Nanc/Loeatf on: Svbill. Inc. Site/Detriotk MichiRan

CPntattcr Iipvcii«piy Nmnber TT-nHl

KTHAZ (JN/NACode

MFGName GbiBodcal Nune

CmttaliurTê r'jiMtiilwaii glM co«aiiuarDi»^^ Cantalner Contaatoi/Al'a3/4.ftia)

Date Ttne \5>' O"^

LoggenName Saniplen Name -SViAuiK CRA - W

Additloiu] Infonnatlon Jlj SnJ oavr ** V atetijA VlAjp. Additloiu] Infonnatlon Jlj

No. of Containen S

Layer

CONTENTS DESCRiPTIOM

TOD fAi IMDddh (Bl Bottom (€) SampleJP Tr-of^ niysicB] State \"'su.tA, • Color

•arity

thickness

FID(ppfD} 3>^0 -

Raiiiation.

Biologicala iA.<rw(, 1

UPoraianylD:

'lAnalyses Paie:

Reactivity OfaorNo)

Air \s^ Reactivity OfaorNo) Water kiesr

Solubility (S/PS/I) Water; •ps Solubility (S/PS/I)

Solveqt: s Density LorH N pH; -


Halogens poaorneg Flame Color Nee. SullUe poaorneg

Confiiimatibn YoiWa Wk Cyanide poa or neg

Confirmatian YMMD uek ^ • Flaahpqint poaorneg

@ 140't' PCBa > 10(}r< lO ppi^/,

8-13-01 • j^«ui6:anu fyjkUkiwtaun-

IML mL 4ML

08/20/2003 10:41 6169273411-. NEW AGE LANDMARK PAGE 32

idLt/MAL Prpjwt Nnmbtf:

•BAZ UN/NAGodc CogntaiiwrType

\>03

Twgy'.LtA, Time

FniJect Nwiiw/LaeatloE: SiifciB. fac. SitePetriat. McWiian MPGNnme

Container Siae uwtc

JW««

Container in FT- o

Cbcmleal Name

Container Content (l/tiUU/Vall)

Seimilen Name ku. Additional bifarmation ariAA'«jL Jl'.W. •+• UiJ tiu^s-s

ffeofCtottnian_j_ Layq Top(A)

CONTENTS DESCROmON MWdietBl Bottom fC)

Sample ID TT-gna A TT -OH'fV^ Phyrictd State

& Color

Garity cl-eao^

ciea/\ Thicknc gID(ppm) •g-Q 0.6 Radiation BiologicalB

VVuÔ

LABORATORY TESTS

Îjkmacny ID: —— SUSU

IV'-B Anaiyaes Date: I3-P3» Reactivity Air: lOofe (Yes or No) Water: t^^6- Mc'Cs

Solubility (S/PS/I) Water X. S Solubility (S/PS/I) 2 1.

Density LorH Z_ ItSPi.

pH: n.uo C.\ PteoxideTest pos orneg »/?&• Alffdr CMdizerTeat pos orneg

Halogens poa orneg Flame Colon A'Cti-

Sulfide pos or neg Conflnnadon YCVNO hl^

Cyanide pos orneg

Confiiznatian Y^/No

Flashpoint posornpg

® Mtl'F lu^Cr PCB's . ^lOor-ÎOppm

^jjjûisti^ By: Received By. g. lid

3±±x IdM.3

Time lico

JM

Name and A£51ifltion

hhetiy^

llf664/ [AL Project Number: Project Nanic/Locatton:

Sybill, Inc. Site/Detriot, Michigan Container Inventory Number

TT -POTHAZ IVfFG Name Chemical Name

UN/WACode Conbdner Type Container Size Container Content (l/4,l/2^/4,ftiii)

Date Time Loggers Name Samplers Name

Additional liifonnation rinA7(ix. lv^^'lrLy^

ViMS'Vv U-OVAIVK V<g ^ ^Ken'^rJ^.o

No. of Containcra {~^ CONTENTS DESCRIPTION

TopIA) Middle IB) Bottom fC) Layer


TopIA) Middle IB) Bottom fC)

Sample ID -

Physical State

Color

•arity

Thickness

PID(ppm)

Radiation

Siplogicals

•jpuOKA-rUKV TES'I S Top (A) Middle (B) Bottom (C) Laboratory ID:

Analyses Date:

Reactivity Air: (Yes or No) Water:


Density L or H

PH:




Sulfide pos or neg

Confirmation YOMO

Cyanide pos or neg

Confirmation Yai/No. .

Flashpoint posorneg

& I40*F |1S£B;S >10or<10ppm

Relinquished By;

Signature Date Time Narr le and Affiliation

Received By;


iCftAmAL Project Nnmber: PrtJoctNuit/LpBidUaii: Sybfll, hie. SHe/DetriM, Midiagwi

HAZ MlPGNuiii: PN/NACode

iGonfalner Inventory Nnmber TT- O'SO

ChoiilcalNi

Dxte r\'^01

ConfnlnerSiu Gontnlner Content {iM,i/2,3/'t.<wi)

Time i6ce>

Additional liifbrniatiaD ûl rhh. kul

r<

No. of Contaiiien \ Ltyer Top (A)

CONTENTS PESCBIPnON Mlddlem S£L

SamplciP Tt- gSoA Phyriod State Color

ITlaiity cl-tojs

CltAA Tbidoiesa

PlD^ppm) o.e> Kadifltion Biologicala

W>0U -Ve6FW

J^BOBATORY TESTS TonfAl MiddlctE) Bottom (O ^ôratoiylD: <&3a A I 03X f\ lâlyacs Date: 1 ;?

3

Reactivi^ Air: (Yes or No) Water: W£Gr

Solubility (S/PSA) Water S Solubility (S/PSA) <S T

penalty LorH i- • A/A-PH: . L,'\ <i.? 1

Peroxide Test posorneg fieGr jLiesr-Oxidizer Teat poaorneg l«6r Haldgena poaorneg Flame Color; (yr(r Sulfide poaorneg Confimiation Vaa^ Cyanide poaornq CcnrfiRnoiion Yei/ND \i^

Plaahpoint poaorneg

SNtrt' KigSr |pCT'a >10ar<10ppin *

Signature j

^lûuhedBy; ^ Date

Received By:

Time

n DD

Name and AlSliation

ihHea^

%jk cÂ

%0Lu >0î-


QI/NALi

- BT HAZ

iALProJtet NnmbcP!

UN/MA Code

Fni|ectNuiu/Ldeatlbn' Svtnil. inc. Slte/Detriiil. MicMiiBa MFGNone

ContsliBV Inventory timmba

CbemlealMHrie

Container Sbe Container Content (lM,X/U/4,iuli)

Date pê I 16

Loggers Name Samplers Ns— ^

AdditionBl Information "S43Q3O

No. of Containen Layer TOPW

CONTENTS DESCBIPTION Middle IB) Bottom fCl

Sample ]i> TT-niyrica] State Color

Clarity Thidneu

PlD(ppm) (5.0 Radiation -Vx^pM> Rioloeicais

ÎPnratoiylD; 033 Aiialyaea Dace: 8-- 13- 03 Raactiviiy (Yea or No)

Air: Raactiviiy (Yea or No) Water: WF&-

Solubility (S/PS/D Water X Solubility (S/PS/D Solvent: s . -

Dencity LorH H pH; 5.9 Peroxide Test poaorneg AiaSr Oxidizer Test posorneg

Halogens pos or neg Flame Color: UiSfe- •• Sulfide posorneg

. . tU(£&

Cyanide pos or neg ConfinnBtion YagAio

MS6f

'inshpomt posorneg

@140-F PCB"! >10ar<10ppm

^djjîrished By; ^ Hi ReeeivedBy:

Date

8-003 Tfoic

tide Name and AfRliaxion

CÂ-

jdMl.


ImU/NAL ftojciet Nqnbar:

WPl'HAZ

Frâet NuiuêiMlon: Svfaill. Inc. Site/Detriot. MjdMgBw

CoBtalBH- InviîT Nsodber

MFCNiunc ChmlaalNauna

•JW/WA Code îCdnt Goiitaiaer Ste Connlacf Con^t

Time 16-30

UggersName Siunfileri Name

Additional InfoimstioD

No, of Cantaiiiera

jyer Top (A)

CONTENTS DE8CBIPTION

MIddteifBl Bottom (Q

SmnplelD

Pfaytical State

Color

Garity _d££^

dc Hiietoima

^(ppm) RadiBtioD

0:(b

VUP-«1L Biologicala

lABORATORY TESTS Top (A) Middle on BOtQ>lB(C)

^VratorylD; 03H nalyaea Date: 03

iReactivity Air; lO^ (Yes or No) Water

SohibilityCS/PSA) Water S SohibilityCS/PSA) Solvent: i

Dwaity LorH • L pH: 7. 1 PenncideTest poaorneg

Oxidizer Test poaorneg K06&-

Halogena poaoriwe PtemeColoi-:

Sulfide pos or nog

Confimmiian VaMo -

Cyanide pos or neg Confirniaiian Yts/Ns

• Flaabpoint . pos or nq[

@I40*F PCB's > 10 or < 10 ppm

J

^lûiahedBy;

,^_jcdved By: t F OatB Time

SriS-o:^ i-lcn "S-lamp's lipo

lAL Project Number: :664/

Project Nune/Locatloii: Sybilli bic; Site/Detriot, Michigan

Contiilner Inventory Number -TTrJo^

DOT HAZ iK^GNnme Cbcmical Name

UN/NA Code Container Type Container Size Container Content (i/4,i/2^4.faii)

Date Time Loggers Name


Samplers Name

No, of Containers CONTENTS DESCRIPTION

TODIA^ Middle (B) Bottom (Q Laver


TODIA^ Middle (B) Bottom (Q

Sample ID

Physical State

Color

Garity

Thickness

PID(rt>m) Radiation

Biologicals

Laboratory ID:

Analyses Date:


Air: Reactivity (Yes or No) Water;

Solubility (S/PS/I) Water Solubility (S/PS/I) Solvent; '

Density L or H

pH:



Halogens pos or neg

Flame Color;

Sulfide pos or neg

Confirmation Yo/No

Cyanide pos or neg

Confiimation Yos/No


m HOT Sli^s >10or<10ppm

Relinquished By:

Received By;

^•664/ [AL Project Number: Project Ngme/Locatlon:

Syfaill, Inc. Site/Detriot. Michigan Container Inveni TT- <3

Number

bOTHAZ MFGName Cbcmicai Name

UN/NA Code Container Ty; Container Size Container Content

Date Time ILoggen Name Samplers Name


No. of Containera i CONTENTS DESCRIPTION




Sample ID

Physical State

Color • -Garity

Thicknew

iPID(ppni)

Radiation

Biologicals

Laboratory ID:

Analyses Dote: '

Reactivity CYesorNo)

Air: Reactivity CYesorNo) Water:


Density L or H

pH:

Peroxide Test pos or lieg



Rulfide pos or neg

Confirmation Ves/No

Cyanide pos or neg

Confirmation Yoa/No


?£S!9 >10or<10ppm • Relinquished By;

Received By:

miA/NAL Project Number: Project Name/Location: Sybilli Inc; Site/Detriot, Michigan

Container Inventory Number T-T' a?^

pOTHAZ MFC Name Cbemlcal Name

UN/NA Code

MFC Name Cbemlcal Name

IContainer type •

Container Size Container Content a/Al/ZJ/AAiil)

Date Time LoggcnName Samplers Name


No. of Containera - Q> CONTENTS DESCRIPTION

Top (A) Middle (B) Bottom (Q Layer


Top (A) Middle (B) Bottom (Q

Sample ID

Physical State

Color

Garity

Thickness

PID (ppm)

Radiation

Kologicals

JRATORY TESTS Top (A) Middle (B) Bottom (C) Laboratory ID:

Analyses Date:

Reactivity KYesorNo)

Air: Water:


Density LorH

PH:



Halogens pos or neg Fiame Color:

Sulfide posorneg.

Confirmation Yea/No

Cyanide pos or neg

Confirmation Yai/No

lashpoint pios or neg

(8 14Q*F

> liO or < lOppm

Signature Date Time Nome and Affiliation Relinquished By;

Received By:

08/20/2003 10:41 El 69273411 NEW AGE LANDMARK PAGE 36

Jl^/NALl

-•SBTHAZ

fAL Project Nnmbar: Project Nabu/Laeatioii: sîl. fee. SitoPeiriot. MichigM MFCNainc

CN/NACoiic

CoBtclneir liiveiitoi7 Niuiiba--TT'O^

Cbeiniieia NMHO

CoatBlaer Sl» Container

Date fe'0.-33

TIMC Loggen Name Samplers Ni

Additiona] Infoimation (vicut. | /l)£ conM^y

No. of Contautos \

Ujw_ Top (A)


Middle on BottoaifC)

Sample ID

Phyncel State

Color

aority ThicfawNi

Pn)(ppm} c5.0 Radiation trv.(yv-viL. BiologicBlB

^RjiPbeatory ID: 1 • r • . ,

(Anatyaes Dace: S-13-0-5. Reacdviiy (Yea 07 No)

Air: Mee-Reacdviiy (Yea 07 No) Water:

Solubility (S/PSrt) Water PS Solubility (S/PSrt) PS

benrity LorH tf -

pH:

PcraxideTest poaorneg i»/E=^

Oxidizer Test poaorneg Wegr Halogens pas or neg Plame Color:

1 ' • Sulfide poE or neg

Conlinnatioo VoaOio

Cyanide poa or neg Confinflation YuyNo R>^

Flashpoint posorn^

a 140^ IdSGr^

PCBfa >10ar<10ppm

oigiJiuinD

^^shedBy: '

RecoiyedBy:

Date

3-19-0-^ Time

neC)

I' Jê3_Das jdM.


rpNTAPCER lNa*lgCT10N BECORP ,ProJaetNniiib«r:

Additiona] Ihfantiation ASI

No. of Coniainen CONTENTS DB8GRIPTION

Siunpla JP u

Color v-fcUou Clarity rl-eoa\ Thictaiew P!0(ppm) o.o BaduliaD Biologieala

ORATORY TSSTS JAORATOR

..^BotttotyroT J5Ej5L Middle fB) Bottom fO

3? Analyaes DBCB:

Reactiviqr OTeaorMa)

Air: lor-fr WaCer: Ajir(&

Solubility (SI/PS/Q Water: rwiBWi

Deaaity LorH

PH:

*enxide.Test poBoroeg 1^KG^ OnidizCTTcit poaoriieg

Halogens poaornog lame Color. /vjrG

Sulfide poBorneg Coafinmliqn VnAio Ufdr

Cyaiilda poaoroeg ConfiriOBIWPVaaOfe

KjeCr

Flaishpaint poaorneg ai4Q*P

>10or<l0ppin

By:

Received By:

Dam Time Sh<Pi \no6 S. 13.(73 llDO

NamBÂflSiiation

08/20/2003 10:41 61B9273411 NEW AGE LANDMARK PAGE 41

r OTVT ATTVER INSPECTION RECOUP

m lAt Project Nnndiar:

MbOT'HAZ

Fn4cilNiuiM(L0Biilipn: Lfflttifl3BtriDLMBcluian OP - OSft

iwrCNiaie GbmtnlNune

CbirtciMrType CoHtalaarSliH ContaliMr Content

HMIM ^ TIBM " rs -o^ IH'AS

LogBDiiNl SnteptarcNMB^^

Additional tetemution

No. of CoiDteineiB

Layer tSon^klD

Too tip

coKnacro PKSCBlPTiON MMdhfin BottOMfCl

PfiyaiealSiote TT Color Co'lprljûs

Clarity dlgory HHokneaa

PlD(lHiina) OiP Hodiation

-WQT^Wjt) Piolopcale

.|||6RA^

îRoaory]^ .TORYTVSTS TopfA) Middle OB) BotteafO

AnalysaDatt; - ^0.

Raactiviqr (YaorNo)

AE. Water;

Solubility (S/fPS/D iSiSSl nsicss Daaaity LorH

PH:

PtewideTcst poaornqt

pKjdiaer Teat poaornog

Halogena poaorneg Flame Colon

^ fos y-szo Pos

f «p^»otT»«=ne»J =*? p/roKiaf

Sulfide poaorneg Cmiilnnaiicn Ywffie ioe6f

i^wido poaorneg Gw&myon YeiyMo KJ^6-naahpoint a»4<fF

poaornqg Mg-G-

l^'a >10ar<l0 PP" SignaiuK Date

&• 13-t)^ Tlnie

l"lC3<3 Name BBui Ajffib'ation

. lJVS> JODCL t^L


r oNTATNER INSPECTION RECORD Omlalmw Imreelery Nropiiier

Af:9 PnlwtrAinilMrli

DOTHAZ

GojBtalner

2B-: DiMe

UWNACodA

Tin fjLTtn*V>

Proût Nuni/LMidliint ayMD. Inc. :attfl3aaiot. MjcMgai M^Navfl

OBtatanrSlw

CtMinliBilNluM

Copodno- Content (|M,UZ,3AI,NIO

Suipleri Name

Addition^ In jbnxutian «>V aiAdlh. 1 »^4<A

NQ. of Cmitainan TnpW

co^m^TO»•scIlIFÔN MMdlatm BoCmmfQ

SuiQilelD

Iffaysical Suae u Color coWi L Cloity CVg-Coy Thkfaien

Pffi tppiii) 0.0 lUdiBtun

TORYTEaTS TopfAl Middle <B1 .^KnWorylD: lAnalysei Dale;

iRucdvity Air; io£î ICYeaorNo) Waien *jfa

|iSohibility(»PSA) Waten s |iSohibility(»PSA) X

Douity Lor»

PH:

PeiwcideTeat poa ar neg Pos lO mg/L QKidiaerTeat poBoriiog -wefe- Pos Kakêna poaorneg nanwCoIar Sulfide poaqrnag Cottfinnaiion YeWNo Cyanide poe or aeg Qimfinnatlan YdiMo nasfapoint poaorneg @1401P

PCB'a >10ar<]Qppin

(Ipuiahcd

Received By;

By; ®yt

j/X Name aid AfBIiation

Received By:


4AtProJtet1

rriiOT ATNffR INSPECTION BECOM)

w MWDarioL &Bcliiwn - Q 61

bOTlBAZ MFGNitDifl

Canttinnrfifae

ChsiiMcil NHM

Cantdnn- Content

LosaooNime

Ad4itionBi inJbnnatiaq

feiOfContanaiv CONTEPWS DSSCRIPTION Middi.nn tmttaalCi

EnpielD -MIL Wwil 1 1 i-

Colo^ UJU^

Clnity

liiiekitcw

PlDCnmi) 0-6 RBdiBtkm -

BMogicsli

^SoratoiylD: • ' Analyacfl Dtte: . IM-03 •

Raaedvity (Yea or No)

Air »UF6-Raaedvity (Yea or No) Wacen /W^Gr-

Solubility (S/PSO) Water: :rr • Solubility (S/PSO) Solvent s

Pmafty LorH H •7.2>

PtaroxideTest poaorneg neG OiudizerTsat paaor nog Ks€G Halogens poaorneg Flams Golor: Sulfide posornng. OwftitHtion VoiMo Cyanide poaorneg Confliiiiniian yeONo

h^(s

tPhuhpoint posornqc 1^40* iPCB-a >10oc<;i0ppm .

KeodvedBy!

U2:(2, hce>

133 m. Ml um-

rnNT AINER INSPECTION RECORD

i«iv«dBy;

08/20/2003 10:41 B1S9273411 NEW AGE LANDMARK PAGE 44

COIN ta|MULrn|>'Nin«»n

rr AMER msPECtic Ppâat Nama/Uicatlon; RuMH. loiL aHefliem'dt. Mielnf|Bn

)N RECORD GontnlBer iBVOBdoryNauiiber

— : mOTHAZ MfGNamo ChamiealNune

iCpBtiinrType CoataljaerSlae Coiifalner Conteiit (tAi.l/S,3MiMl)

Date iTlPm UVBBisNHma SuiplanNanne

, t. .

AddiSonBl Tnformation sitt— Li^r •-(•âdor , t. .

AddiSonBl Tnformation sitt—

-No. of CoUBiiun CONTENTS DBSCEOPTTON

Ton/A't MM-nefflf) Bottom (C) tas —.— Sample ID V3 A C<Â-c.\ck\

Fliyaical State • L u Color Hcxok Clarity WLo^k f^CGL0|il-2-

ThidcnoH

PID Oipiq) o.o 0./3 0-6 \ /w

Biologioah

JBPORATORYTBSTS T«rA» MuidlerBi itottomfa 1 .^KratorylD: A ^3 A lAnalyaeaDate: M OZ S'-19^03 • (Yea or No)

Air: <Meer /uro f (Yea or No) water: UJey k Solubility (S/PSA9 Water: iz: S Solubility (S/PSA9

PS. jg- ts ^

Danity LorH L PH: "7.© 7,0 PenncideTest poaorneg A/^ 6- . QxidaerTesi poaoriieg JURi- ta' •" ' - •

. . Halogena poaorneg PhnieCotof. iMg-6- Si

1, Sulfide poeortteg Coufiruiaiion Yaatb fS^y-

Qnnldo poaorneg Coulbiuaiian Yoi/Na

/ues-...

Plaalqxkiiit poaarii^ la 140*P j^B"! >10oc<10ppin 1

JO€<Ss- AJg-6r

Signature,

liiisHed By; Time

n->-5 NimaadAfflHatii

Q3£L. O 9.^ ̂ Mfv,


<Fnl«etNmnlien

rnTOTAtlSnRiR INSPECTION BECOBP r:= ICaygggtonrUBbher

DOTHAZ ClWHAOria

Fn|KtNMDnn^»<h» aYtim.lnc.aitafl3dTiot.Mi«3lii MFGNav«

Type

Tine

CoaliiliierBln ^flJl

Ni

ChttDlCBlNl

Caaulncr CoBteM

Semplera NeniB

AdcUtiaiial biformatiOD \iiiF 1 Ti"*-'' "•*" i

No. of CooieiiMn Layer Sample ID

Top (A)

COMTKNTS DBSCBIFTION

MMdlafB) BectemfQ

niyBkal State

Color CQ\6<1 uA.4ii., Ûoi<,

Clarity JLXecu Dikknen

PIP (ppm) Q Q, Radiatkm

Biolagicda Wj0rvvti

^Kntmy ID: M'i IS

jAnalyaea Date; Sr- m '03 *fH a- s;-i^-03

Raaciiviv (Yea or No)

Air -S—'V - OS^ ilJB^ Raaciiviv (Yea or No) Water Af£Cg- KJr(Sr-

Solubilily (S/F»Q WetaR S Solubilily (S/F»Q ' V * •l"*

DanaAy LorH >H: /H

PerandeTcai poaornqt Aje-^

OxidizerTen poaornag Aieo MaloBoia poaorneg Plama Colon Sulfide poa or nag Confimadon VoMe Ki^ /S-6r

1

cyanide poaorneg ConfiiiriBtian Yai/No

/y^6 A/r6-PlaahpcHiit poaorneg ^»tfF AJE4r ; hJ^Cs-FGBra ^]Dac<10ppm

:

5 • ?•. -. '!•

hedBy;

Beeoived By;

Date

.Q-/3-Q3 Thne

ll-gQ. Name and Aijiiiation


CONTAINER INSPECTION RECORD CoBtalntr Invcatoiy Nvnii v

rr 'dL'-CtaaMNw

VAL PirojBiit NinnbcR

-iDOTHAZ

rnjflct Name/Loenlloii: Tne. Siie/Detriot. Michigan Svbill.

MFGNanie

tlNyWACodB CovtalaBrl^c

.\|Q^

CantaiBcrStas Container Content (l/4iU2.3At(^

Date Thoe Loggen J^clegW

Sanfilenlê

Additiinial Thformation ^ri v/v£>AgStQiL

\pu>^ VAiSk ^

No. of Cootainers

Layer Top (A)


Middle tBl Bottom fO

Sample ID K niysical Stale 11 u Color

Parity

LJxr-U,

Thickness

PlD(ppm) 0.0 g.6 Radiatiop

Biologicols >i/Lerv^ ^4,en«g..

JârstoiylD;

lAnalyaesDole: e-(7-C>3 gi 17-03 Reactivity (Yea or No)

Air: we-4 Reactivity (Yea or No) Water;

Spliibilhy (S/PSA) Water: X s Spliibilhy (S/PSA) mm s . Density LorH

pH; M.-O -^.,0 PeraxidBXesi pasorneg roe<j? 10 £&

Oxidizer Teat poa or neg lOgfe-

Kalogena poa or neg Flame Color

W^tTd*" UC-^r-

Sulfide poaorneg

Gonfiimation Vei/Ne lO^fe.

Cyanide posorneg Conlinntion Ygi/No

Wf.Cr M£n&-

FbiaJipotiit pas orneg

miACP? t06Gr

PCB's >10or<10ppm

ajjj^ Signature ^jj^Riquiahed By; quiahed By;

Received By:

Date Time

B-H-03 iLic> Name snd AfBUation

-^h/Ua^ ceA •?(-W-6l liKl

08/20/2003 10:41 61:69273411 NEW' AGE LANDMARK PAGE 47

r OKTAINER INSPECTION RECORD MkÂL Projeat Nnmbdr: Projaet Ntene/LaieatloR;

Ryhiit, fne. Site/Detrioe^ Michil^

DDTHAZ MFGName CheniealNamc

UNmA COM Coatalncr Cotttept

Date Thne LoggBryyame ^ >27.b

Samplen Nanm . -$t~> y/lc-LeDti^

^.tdirintitd Tnfbnndinn lA. ^ lOftA r-^.|,tv>s^fyi of 9>^Ce,^ JQ^,

No. of Conunncrs \ CONTENTS DESCRIPTION .r--/A-, Middle ran Bottom fO

iPhyeicai State U-Color "7

-

Clarity Oprôf.

Thieknen p

PID(ppm)

Radiation

!|l!waratotylD: •

lAiuIysea Date: gr - no3 •


Air Reactivity (Yes or No) Water

Solubility (S/PS/I) Water 5 Solubility (S/PS/I) :2r Denaity LorH u pH:

1

Peroxide Test poaorncg


Halojeqia pos orneg Flame Color:

•

Suliide posorneg

Confintialion Vea/Ko JUff-e

Cyaiiide poaorneg

Continnanon y«*/ND

Fladipoint posorneg

M 140*F

1

PCB"! > 10 or< lOppm

quiih^ By;

Received By:

Date Time Name andAfRIiation

-Ms IA30 -gW fid-yf^ ^p.

- CJi^

ff-

COPfTAINER INSPECTION RECORD [AJLPrêctNnmlMr:

HAZ C«d«

Contatmr Type

i)#t« Time

Project Naim/tocalloD: SvMH. fac. «la/Detriot. Michigan MFGNano

Coffitnlner Sim

toggercNainc^

iContelner Inventory lumber

OtendeclNMitt

Container Content

Snmplen Name

Additionel Information VjiVyt.. tpi^^ g^- /Jcick./W\p

No. of Containera

'«XS. JSSLiM.

CONTENTS ©KSCRIPTION MMdUlefB) BottowfC)

Sample H)

Phyeioal State ^ X3 T

Color Clarity Thieknoaa

O \ pn)(ppm) Kadiation

Bôgtcalr

•RATORY TESTS Top (A) Middle fBl Bettem fC^ Laboratory ID; Analysea Date:

Raactlvtty (Yoa orNo)

Solubility (S/PS/I)

Air: Water Water

[)enaity LorH pH:

Peroxide Teat poeorneg

Oxidizer Teat poa or nog

falogena poaorneg âme Color

Sulfide poaorneg Confirmatian Vaa/No Cyanide poa or nag Confinmition YM/ND

@ 1401? posorneg

'CB'a >10or<iOoB»,

Signature By:

Date Tiino Name and Affiliation

eaaived!fiy;

LoflgenNtoi* Samptari Naiiio

Addkional InfonnatkMi O^'C AcrM^Von ..ibi'

Mo. of ContRinen

.aycr Sample IP

Phyaical ftate

.T»PCA}

CONTENTS DBSCHIPTION

Middle (g) Bottom (C)

Color COUC UNA

qarity ClecjA ThkikneM

PIP (ppm) 0.0 ae> Radiation

TORY TESTS Top(Al Middle flB) Beitem (C) Labontory ID;

Analyses Date:

Reactivity (VmorNo)

Air: Water

Solubility (3/PS/I) Water Solvent'

Density LorH pH:

Peroxide Test poa or nog

Oxidizer Teat poaorneg

Halogens poaorneg Flame Color:

SuMde poaorneg Conflrmation Vaamo

Cyanide poa or neg GonSiiimtton YM/NO

'iBshpoint poa or neg IdO'P

>10or<10ppm

Signature Relinqulahed By:


Received By:

C03N (TAMER TMSPy-rnON RECORD

Rfiiinqulahed By; Tinw Nameand Affiliation

ReooivedBy;

AT1WT?1J TOfiPFr'TTniM RECOIRD

>10or<10ppm

SigDVture ReHnquished By;

Date Time Name and AjfHliatipn

Reoeived By:

wivBd By:

Received By:

CONTAINER TNSPRCTION RECORD

•"••point po0orn^ H40^ 3'g >10 or <16 nam"

'^1^ Signatura

wived By:

Date Time Name and AflJHatton

CONTAINIR INSPECTION RECORD

^ Bis64/ lAL Project Ndmbcr: Prajict Nome/Locatloii;

SvMlL Inc. Slte/Detriot. Micfaigao

iContiiinar Inveatoiy Numbi Q-il

DOTHAZ MFC Name Cboiolcal Name

/#f ContabiorType n«r lypis /^<

I

ContaliierSlae Container Content (i/4,l/z^

Rate fl-m- Q"^

TUM

iosa. ILonwflNam Samplari Name.^;^^

Additipnal Information

gftrtririiii*'Ale

No. of Containera Top


Middle IBI Bottom (Q

Sample IP

Physical State

Color

aarlty

Thkkneu HQ,

Ettd' i>*>l

?IP(ppm)

Radiation

•RATORY TESTS T'y(A? Middle (B) Bottom (C)

jLaboratory ID:

Analyses, pate:


Air: Water:

Solubility (S/PS/t) Water: Solvent:

Density LorH

PH:


Oxidizer Teat posorneg

Halogens poa or neg Plame Color:

Sulfide pos or neg

Confimiatimi VaVNo

Cyanide posorneg

Confimrntion YaiMa

Plasiipoiint pos or neg

@140^

^ IO<g< IQppm

Signature Date Hme Relinquished By:.

Name and Affiliaition

Received By:

Received By:

Addkigml Information

No. of Containers O TOR (A)


MlddiafW BottnualO

Sample ID

Physical State

Color

Clarity

Thidmess

PIP (ppm) Radiation

Biologicali

linorM^

TORY TESTS Top (A) MiddteflBl Bottom iO ID:

Analysm Date:


Solubility (Sd>Sd)

Air: Water Water

Density LOTH

pH:

Peroxide Teat pes or neg

Oxidizer Teat ppaor neg

Halogens pas or neg Ptame Color:

SiiHide poaorneg Conflrmation YOIMQ

Cyanide . poa or neg Conflrmation vaiAin

> 10or< lOppin

^1^ Signature i^lKiiahed By:

Date Time Name and AflHiatlon

Reoeiyed By:

Top(Al Middle fBl BottemC) iAboratoiy ID; Anftlysoi Date: Koaetivity CYcaorNo)

Air: Water

Solubility Water

Deoaity LorH

PH:

Peroxide Teat poawnes

QxidiiterTeat poaorneg

Hatogena poaorneg name Color:

Sulfide poaorneg Confirmation YMTNO Cyanide poa or neg Coitfnwition YwWo

laahpomt poaorneg QldO'V

>10or<10ppin

Relinqufahed By; Signature Date Time Name and Affiliatkm

ReoeivedBy;

Relinquished By; Time None and AfflliBtion

Received By;

CONTAINER INSPECTION RECORD PiraJaetNiMDibaR

OMfflACodt POtHAZ

Pni«B(tN«m/Lacatlont Svbfll. iBfc ate/Detriot. Michigan MFGNftin*

CaadbOiiM' Imnmtory Numliw Tit > It

RlNa

ConlataerSIm CoatiOner Contaiit

5$5S jyHiL IijoagBn Nwnt Naina

AadiUaiwl Inibmtttkm

No. of ContEêra 1 CONTENTS 0KK3RIPTION TOBYAI Mlddlaffin Bottom (O Laveir /

CONTENTS 0KK3RIPTION TOBYAI Mlddlaffin Bottom (O

SaoiplelD . - 03.B - -* QlMi. 'DjfiiOM snno

Color Clarity niieknoM

PlDOipin) ENdUman Blologioali 1

&10or<10ppin

Sigpoturo

"IPlrtBy; ___ wivodfly;

Tinw Name and Affiliation

tonenNi

Additional Infonnatkm Tr '/gj ^ • g-z jT? <rv jr.r

Fatfii i TUfcMi, 4P'2^-, :;>7.ZV.

No. of ContBinen 3 4.».. t Sample ID

Phyaicd Stale L>(^| ̂

Color Garity

JseM CONTENTS DESCRIPTION

MlddtoiOB

jbSAJL

BottOWtC)

Thicknem pro Oppm) Radiation

: ôgi^

TORY TESTS Top (A) Middle ffl) Bottew (Ci Laboratory ID: Analyses Date: Reactivity (Yea or No)

Air: Water:

Solubility (S/PM) Water:

Density Lorli pH:

Peroxide Teat poa or nog

Oxidizer Teat poa or neg

Halogens poa or neg Plame Color: StiMdc poa or neg Conflnhation Vamt Cyanide poa or neg jCwflrmrtlpn YeeZNe Flashpoint posorneg

> 10 or< lOppm

Sigmture Relinquished By:

Reoeived By;

Date Tjino Name and AfRUation

ConttttanrSta* . -7 i.,CX!& :Kf4-

Container Contant

LoggenNune •^K Samvlen Name


Solubility CM>a^

3«bdfty LorH >H;

•taonMoTcit poeor neg

biidizerTott poeof nag

laiaam poaornog lemeColof:

>10or<10tipm

SIgDBttm

wived By; '

Data Time Name end AfliMatkm

rnNTATNmR INSPECTION RECORD

waived By;

RflUnquiahed By:

Reoaivod By;

Time Name and AfflliotJon


/QQ.

lAL Project Number:

POTHAZ m/NACode

Project Name/Loeatlon: SvMll. litc. Slte/Detriot. Midiigm MFC Name

ContalBer Inventory Number -rpc.-ofl.i

Ctaendcal Name

Container Type . "V puvJk

Contabier Sine \.0C=5

Container Content (i/-i,i«i3/eiiWD

Date Time Logger* Name, 'M.

Samplers Name


jNo. of Containers 4 CONTENTS DESCRIPTION TOD (A\ Middle fB) Bottom (Q Layer

CONTENTS DESCRIPTION TOD (A\ Middle fB) Bottom (Q

Sample ID / — V: Physical State i—

Color bicMi. L ,

Clarity Thickness

FID (ppm) G.6 Radiation Biologicols m iRATORY TESTS Top (A) Middled Bottom (C> Laboratory ID:

Analyses Date:


Solubility (S/PS/I)

Air: Water Water: Solvent:

Density LorH

PH:



Halogens posorneg 'âme Color

Sulfide pos'or neg Gonfirmation VosMb

Cyanide pos or neg Cmtfinnation YBBOSO

iBshpoint posorneg @ 1401?

PpB's >10 or <10 pom

Signature RellSqIiished ]

Date Time I By:


Received By:

At frajuct NnniiMir:

HAZ UW/NA Code

jprojoet Nanutfliocation: SÂil!, fee, S^taâtnat, Michigan MFGNams

£oiit«intir Ittvuuiofy Nuiiib«i €%' Chsinlcal Name

CwSiSiSi? Typs I CQBtamcr Ssss

Date iTImc Lowers Name n

Saaêrs Name

Autiitiooai in loanaiion oSee^. u>/i,Ln. W?;W 'Wata oA^h /gf 1P

No. of Container

L?yer Ssa^ptelD

Top (A)

CONTENTS ORSCSIiPTIf^N

lyilddiefm

A-im-c&nm-'in-K' Physicoi State

SI Bottom (O

Color

•niitdtncss

PID fppm)

Radiation

Biologicals

LABORATORY TESTS LABO

i* Itory ID;

{Analyses Dstc;

jRcacdvity KYeaorNo)

ISclubility (S/I»ai)

V/ater: Wacer Solvent:

Density L or H pK:

Perojcj'fe Test -pee or neg

DxidizerTest posorrieg

iakêng pgj, 3- -^g •lame Color:

iullide pos or neg ioiuiniwiioii ves/Wo ' 'yiaUc poi er 3=g oafitrwwtton Vtf/Ho

ia^point poa or neg S IdO'P -S's

Mlddifl (B) Soitajji {€)

> iuoi < iOppm j

Signaiufc fj-

Date is!d Bv;

Time Name and AfSlietiors

L-eivcd By;


gPtHAZ

AL Project NHmlMF: Projeet Nomc/Loeatlon; SvMll. he. ShdDctrlot. Michigan

Cowi««'"er Inventory Nnmber

'P-MPGNune ChcmicaiNmae

UN/NACode GnBtRincrTypc . • Container Size

-7 Container Content (1/4^1/2.3/44^11)

Time c R'lD

Loggers Naine

:111 Santptora Nante

Additional Information \IV:OAVCPA iS rv V ^ irvC.^^^r

No. of Containera

SISL Top (A)


Middle on Bottom (C)

Sample ID L-'âV05S2c^v -SIM' Physical State

Color

Clairity

Thickneaa

PIDIppm) O.D Radiation A-Biologicals

TORY TESTS Top(A) Middle IB) Bottom (C) ID:

Analyses Date:

Reactivity [Yes or No)

Air: Water

Solubility (S/PS/t) Water Solvent:

Density. LorH

pH:


DxidizerTest posor.neg

lalogena poa or nejj âme Color:

iuifide posorneg 'onfjnnation Vaa/No lyaoide posorneg 'onRnnation YsBO-to

lashpoint pos or neg

a 1401?

IJS'S - > 10 or < 10 ppm

Signature

I'ljjjjjjlêd By: ceived By;


Addiciomd Inlbrmation (SXJ^rStP^ i/ ^Ji CarAtky^-î^ \<VHV

^7\

No. of ContRineni Layer Sample JD

TOR (A)


MHHiiaffl Bottom fO

Phyaioal Stats Color

Clarity ThicimaM

PID(ppiii) 0.0 Radiation

Warvo^..,

îK ^cali

Laboratoty ID: Analyses Date: •

Reactivity (Yea or No)

Air-Reactivity (Yea or No) Water

Solubility (S/PS/I) Water Solubility (S/PS/I)

Denaity LorH >H; . Peroxide Teat poaorneg , DxidwerTaat poaorneg

Halpgena poaorneg FlameColor: SiiMMe poaorneg jConfirmation yod«>

Cyanide poaorneg CoiiflniHiUon YM/NO Plashpoint poaorneg

HOT PCBja >10or<10nmM

Eollnquished By;

Reoeivied By;

Signature Date Time Name and Ajmiiatloh

CONTAINER INSPECTION RECORD IgkÂL Project NHiBbcr: Project NainanLoeatton:

Sybill. Inc.,Site/Dotriot. MieMnan

Contalnw Inventory Number

MTHAZ MFC Name ChcmlealName

ContatmrType Container Content

Loggers Name SamideraNamc

_

Additional Informatioii

iv f-Al.

\\j, ^ — Additional Informatioii

iv f-Al. imV irvvi-d-/-VLAJP, c XDf. 1

No. of Containera ^ JR

Layer

^ CONTENTS DESCRIPTION

ToorAt MIddlefln Bottom (C)__

Sain(delt>

Phyaicai State

Color

Clarity

Thiekneaa

PID(ppin)

RadiatitA

Biologicals

iLABpRATORY TESTS Top (At MUdieflB) Bottom IQ I

^^^BitorylD; Ajhalyaes Date: - _y.

Reactivity (Yea or No) .

Air: Reactivity (Yea or No) . Water

SotiibiIity(S/PS^ Water I-SotiibiIity(S/PS^

Denaity LorH

PH; • ' Peroxide Teat poaorneg

DxidixerTeat poaorneg

-laiogena poaorneg fame Color

lulfide poaorneg .'onfimution Yoa/No

iyaoide poaorneg onllnnntion Y«i/Nii

laahpoint poo or n^

i 140'F

>10oT<10ppm

ceiy^By;

CONTAINER INSPECTION RECORD J^VNAL Project Nnmbers Projoct NanM/toeatlon:

Svbili. Inc. Sib^triot. Michinn

Container Inventoiy Nnmber •b-c3^n

IRTHAZ MFC Name GhenJcalName

UN/NACode ______ Container Type ContalimrSiae . Container Content aA4.l/2;}i>Mg!p

Date Time iooo

Loggers Nasne Samplers Name .

Additional Inibmiaticn

No. of Containers

Layer

SaniplelD Top (A)


Middle (ID

eil Bottom (C)

Physical State

Color.

Parity Thiclqieu

PIDCppm)

Radiation

RiologicalB

iRATORV TESTS Top (A) MiddleIB) Bottom IP ID;

Anatyses Date:

Reastivity CyeaorNo)

Air Water

Solubility (S/PSO) Water Solvent:

Denaity LorH

pH:


JxidizerTeat posorneg

-lalogena posorneg laneColor

iuHSde- posorneg ^nflimation Vasoto

lyanide posorneg Ortfinoation YHOXO

lasiipoint poe or neg aiAOT

Jffa >10or<lOppm^

Signature

Pj^phedBy;

eoived%:

Time Name and ARiIiation

r<rk!Krnr AWli*!} ira<SPMriTTON RECORD

-Vwo WVss

MJKmATORV TESTS

RoMtfvity !(Y«»grNo)

Solubility camM)

Air

MKhUeim

PH: LoirH

PWoxHaTat pwofnag

iGiilw:

NiffldB pMoriiK

•yinUo pMoraog

poaorn^

Opto Tbn» MamBNidAfllliitfon

No. of Goohdnen ^ cxwnmDEscaiim | TOD/AI MUUtoin BottomlQ 1 Lpyor

cxwnmDEscaiim | TOD/AI MUUtoin BottomlQ 1

SnqiblD U' ' <y^ I.- 35

PliyriealSUD L- U color ^ V,\AfK Clnity fi9<^WL lUalnMM

PlDOvnO 0.0 Eodiolhin iA 4 1 Molbgkidi

e 1 1

CONT^ iNSTO/mON BECORP

io.afCaaiKtam T ooffraNiBDEscaamoN ST" , ,

L- -V^ .WPlflJ , •• ,wwww J

l^riniaMB L iokir ColrtrbsS Sadly WiL ag>ou3(ut IMmm IDCppnO O.Q 0-0

Meaioab .ABORATCNRYTESTS jeatiAL JSBSysSL JSSSSJSL

MttUvhy f(U or No)

Ufr;

3iubiifty(avnM)

LorH

^ pooorwig maaOOar ' 1^-

aflnwitan^ fMaamag

PMoroqi

atfiUMBty: Tiim NmondAOlktlm)

Rug SB- G'R ORsia'a Russ~ RiJ 1 suiiortl^ 313 551 deal p. 2

Hue 26 03 01:26P Russ flalsmorth

313 aai UDSJ

Rug 2G 03 ai:27p Russ Rylsuiopth 313 551 0891 P-3

Amma mspECTTON RECORP 'IlMiiMALocatlaoi CMttalBMr y Nuinbcr

G iNlBtawrSfaie gS<y/2, CbOlB|ii«r CdntBDt (U«iy>,3ASMi)

hi [genNi

AddMhMMlJnlbiTnatkni

u>/ vA. ^

KAtajN baituv )Ai

Na of CdBtBinon

fcasL Top (A) COimNTSPiBCIRIPTION

Mlddtofln BottowtQ SHiqdelD -zn^ - c>3^ PlâlGrf Slate r Color

Clarity CtCftA

d.-C) PlDCppiw) SUiHalian

Blologteala LABORATORY TKST9

ug 26 03 ai:27p Russ nalsuiorth 313 551 0891 p. 4

mT>in 'ATNER INSPECTION BECOM)

Hiug EG 03 Qi:27p R:uss flalsuiorth 313 551 0031 p.5

ATNir.ll INSPECTION RECORD

Rug EG 03 QlrEflp Russ Ralsuiorth 313 551 0891 p.G

CON1' AINER INSPlCnON RECORP

Sep 09 03 02:OOp

CONTi

Russell RiilsUiorth 313-5.51-0891

UNIR INSPlCTIC»r RECORD UbUNAJL r]r«!H«t NanilM" m MtnMnfLoartlaiit

L faa SfNDoirfot. luflehJBaa -D -

iifjM'A jr*juiA • Ate U OMsrinlNicnM S3L ' •»• * •oBuupvinnp^

• (ijruAv

dantaiiier GontoBt

^s-csi n™ J

p.3

Jdkiaod InibmutioB /lû^ o-VN rtW

UAJj \o .>g:>A^>A^v^CtC -pUtftUA

ro-ofCmttdnfln

aiSL Jstm. cornvMiv PKfKauFnoN

Bciwwiiwa nnpialD u-QHH

Mhic vb/j\

Svlty •tsAe^

p.o Q.O

toloafa»ri« ^1.' f>LOrV>JL

AWnUTORYTBSTS

•bjllplD;

aadtlvlty faaar'So)

3iuba\tf&ma) Wi

W«tBtT

Top (A).

"0^ LorH f: ~~

•wddaTm pwar nag

(idiMrTw pMflrnpB

>>oam poa wMg MMCate: -'

Mimuum

Mde poBarnm nflmuuinn Yaifffc on'^'o pgaorn^g jjftawkm YtoOh

Sep 09 03 •e:QOp Russell Ralsuiorth 313-551-0891 P- 4

*AmMLPn4wtNmi«wni

iSWCCoite

1. W ataffioirliit. Mlriritm >N«nui

i r

coiner C»ataatOMii«»«^

•"""•rSEA . M-nMatm

Sep OS 03 0:2:00p Russell Ralsiiiarth 313-551-Q8S1 p.

*A/riAL Npmfcm klMk

tr^muafAMOitam SMLIM. SMDciriat MldiintB

WVUGMte MDPGffnil* Clianriaijillnw

riwytiNwIlliw CSootalOT GeaiMt OMiiOMtm

fl'0-63 TUD*

U0t5 tostanNan* irnin^-naMaiM

AllliwHiInfiiniutfion Uyer^ UaAcU. ACCuVilcw.4

Sep G9 03 OaiOlp Russell flalsuiorth 313-5:51-08? 1 p.e

TORPiefiTfON BECQRO

Sep 09 03 Q2:01p Russell Ralsiiiorth 313 551 0891

rnfrri^R INSPECTION RECORD RAMAL PniM NamlMn

w. mtimaiUit. ifl^na VB. - i c>n MDraNanw OMrtoSnmB

iwaMiHrTnM * vcJt- \?er<

c4^«" Oinbdaar CoaitMtaM,iAaMMO

T.iig^nIfnnM

P-7

* -luWiwI Bjfr

Sep 09 03 G2:a2p Russell flalsuiGrth 313-^551-0891 p. 8

CONTJONER TOSPECnON BÔim yU/Nitf^rnjiieeraanibM

iiN= wBlCdtte

i^^togrogyoîfljtigsL ttama

-HO.

'Tlf GanMlMT Goataiit OMUKMUiio

Tina

ydUbionil i UKinsiBtvoa V49vC U>nd - v|jTa^ 'Wvk. M

fo.<orCDBteiaen SBS. JtoElSL

<x)wr»gnrBiP«waMnrKMv jsajfeffl JmsJEL

•aptelD feyaMSMe

L- onOB03 - Ab4q

Uk« aariiy Weknfwi

IDCppm)

Unloalaala

•MBORATCmY TK9T9

Russell Ha 1smarth 313-55.1 - OGSl Sep 09 03 a2;02p I t

COtrojuNER INSPECTION RECOBB

p. 9

lUfffAL Pn»J«t Nmnhvi tlinm/Loautlan: . iBfl. SUHPtXtidL luBeMwn

Cortiiiwr iMMBtoiy Nnnbte ->• Vi-' I^.9-

" <3>-^

MUmAJaBannatioa Aolt \M>qL;c.4, ^.topjX

'> NVJ'SLIJ'

to. of GteMbian COimOfrS MSCRIPTIQN

•mpton) '&SO e _€ e.^. -nywwBm 1 ^ toior >0Vft^T5idM»»N Itority cx«:^de ainoA hktlrnniji . — IDOvnO 0-0 MiiMion

totagliMls

aaeifvity rcBorNo)

iiUiwrTaat Pwarnqg poioriMg

awCotac; ' "<to paflorneg 'jtaMSqa v-(Hi iricto pwornaB iwwton YM^NB

posprni^

g- > Id Or^gJlQmBmt

f. Sifpman VtOMJiy. Timo NândAflifltton

•ed'

Sep OS .03 oa.eap 313-551-0831 pk' • X W

iGllUfiS AL Projeet Nambar: jkoAca/

Pcojaet Name/Loeallbn: SvWlI. Inc. Slto/Dotriot. Michiaan

Container,Inventory Number | TEi.- 'Id3

PKTHAZ MFGNama ChemtealName 1

ilN/NAGbda MFGNama ChemtealName 1

Container Type Container ContBBt(l/i.»«i3«.««tl) ^ j

Date Time Loggers Name . Samplers Name 1 1 Additional Information VewJC. ^ 1

• . . ^ 1

No. of Containers CONTIWtTS DESCRIPTION | TopfA) MUdlalBl Bottom (O 1 Layer

CONTIWtTS DESCRIPTION | TopfA) MUdlalBl Bottom (O 1

Sample ID fPtcRG-^ ' < 9yn- 051 Physical State Color tolbrU>*». Clarity G\ear\ Ihiclaieas -Pn>(ppm) OÔ Radlatidn titArVin

Biologitâ

LABORATORY TESTS Top (A) Middle m Bottom IC) 1

rDate:

Rsictivity (Yes or No)

Air: Water:

Solubility (Sfl>S/D Water: mm Dannty LorH

Halogens poaorneg FlaineColon

Sulfide pos or nag eOmSmMtioii Vn/Na jyanidia poa or neg

'oniinaatfam YiirfNo

lasfapoint poaorneg 8 i-aCF :B'S


08/20/2003 10:41 6169273411

•V Li

NtW Abt UftNUPWKK rnui^ OJ.

667V^MmStceet SeooK Hauteb MidiigiB 49022

TidlBae(i^ 685-162* Ptt (269) 927-3411

FAX TRANSMISSION

TO:Lm 1J Jill ffc j'.. j'jiji J COMPANY; PAGES: FAX#; FAXf: SUBJECT;

COMMENTS:

CONTABNER INSPECTION RECORD CRA/NAL Project Nnniber: 32664/ DQTHAZ

Project Name^catioii: Sybill, Inc. Site/Detriot, Michigan

tskacsfi. Chemical Name

Mmoe.


iu'?.

Container Content (i/4,iy2^4ifiiii)

Samplers Name Gfeîurv [ f ft!

^0. of Containers Q CONTENTS DESCRIPTION

TopIA) Middle (B) Bottom (C) Layer


TopIA) Middle (B) Bottom (C)

^ysical State

Color

Clarity

Thickness

PID(ppm)

Radiation

Biologicals

Laboratory ID:

Analyses Date:



Solubility (S/PSA) Water: Solubility (S/PSA) Solvent:

Density L or H

pH:


Oxidi^Test posorneg

Halogens pos or neg

Flame Color:

Sulfide pos or neg

CotifitTnation Yes/No

Cyanide pos or neg

Confirmation Yei/No


(S 140'F PCB's > 10 or < 10 ppm

Signature

Relinquished By:

. Date Time

a-1)1 -03 13 Name and Amliation

ReceivedBy; • - •

OtA 32fiS4tlmliHniw Ii«~rt5o-

CONTAINER INSPECTION RECORD CRA/NAL Project Nnmber: 32664/ DOTHAZ UN/NACode Dsr

Prdject'Nunc/LocatioD: Sybill, Inc. Sitc/Detriot, Michigan MFG Name

" OYU kJ Chemical Name M SM. Container Type

note If I mm*

intalner Size Container Content (l

Loggen Name Samplers Ni

Additional Mormation

itent(i/4.i/y/4>nii0

EnipTH CX^

I'inci] No. of Containers H Layer Top (A)


Middle (B) Bottom (C) Sample ID

niysical State

Color

Clarity

Thickness

PID;(ppm)

Radiation

Biologicals

Laboratoiy ID:

Analyses Date:




Density LorH

pH:



Halogens pos or neg

Flame Color.

Sulfide pos or neg

Confinnation Vea/No

Cyanide pos or neg

Confiimation VeiMo Flashpoint pos or neg

©UO'T PCB's > 10 Or < 10 ppm

Signature

Relinquished By: jezKo


Received'By:

CRASaCMrrail

08/20/2003 10:41 Blb32r3411 NE.W HOC. UHllUlwruN

CRA/NAL ProJ^ Numb v; 32664/ POT UN®

HAZ [® A Cade 4hr3tr

Project Nunt/LacatiDD: Sybill, biR Site/Detriot. MtchiMUii iMFGNi

Npy^g-

Contaiaer Inventory Ni

(TiftintMl

OdntolnerXype CaBtaiacrSbe gD'u*»»-Samplen Ni

6(gdLn ft: Additional Infenoation

No. of ConteiBera IPESCRIPTION

Sample ID tMMmBoap 3 PbyncalStau

Color Clarity nuokmn PlD(ppoO kUdiadon Biologicals

LABORATORy TESTS TOD(A1 MUdleffl) Bottpm fQ LaboraioylD: <93 \ Analyeea Data: Reactivity Yea or No)

Air: S>tJ X Reactivity Yea or No) Water; \y

Solubility (S/PS/I> Water S X ' Solubility (S/PS/I>

Solvent: X X Density LorH \ pH: c>.ni \ Q

jPoioxideTest poaorn% > jSSddizeT Test posorneg / Halogens poa or neg Plamc Color AJdb

Sulfide posorneg Confinoatioa Ym/No

ue^ \

Cyanide posorneg Ccmfinnaiion YmMo \ Plasbpoint poa orneg O l4tfT ^ PCBb >10or<10pp/ /I hi

rsA

RelinquiebedBy;

ReceJvedBy;

Namemd cm-

I3H0 K*VL

08/20/2003 10:41 6169273411 NhW «at I WO

CONTAINER INSPECTION RECORD ORAmAL Project NHinber; 32664/ POtHAZ

Frojoct Name/Looitioo: SvMB. Inc. Ste/Petript Mictripm

BN/WACodo MPGNi CboniealNnie

Container She QO

SamplenN;

CoBtODt

Addttioml Infimnation fc

LabonidiylD: SSo^^co7 Analyses Date:


Air: lOO Reactivity (Yes or No) Waier: Ato

SoluWI(iy(S/PS/I) Water: JZ SoluWI(iy(S/PS/I) s iDcnsity L or H I. U 7.^ PdcnddcTest poc orncg UStsf


Halogens posorneg

Flame Cotor;

Sidltde posorneg

Cosdhnntion YH/NO Kic<5r

Cyanide posorneg

CanOmaiion YoMo N&t-

Flashpoint posorneg

aidtf* PCB'a > 10 or < 10 ppm

% I ^

'fi' -a ^

Rrifnqulshed By:

ReodvedBy: tiiM-

Name and AffiUat Uation GgA

i»fe ClU»<«CojilafciM aipfHim HniiidLifc

CRA/NAL Project Nnmber: 32664/ DOTHAZ UN/NACode

Project Name/Locatloii: Sybiil, Inc. Site/Detriot, Michigan MFG Niune Chemical Name

Container Ste /

LoKen Name ,

Container Content (y4,i/2^4,riiii)

Samplers Nanie\

LilFaM Additional Information

No. of Containers

Layer

V

TopfA)

mt/f/d rhi CONTENTS DESCRIPTION^ ^

Middle (B) Sample ID

Physical State

Color

Clarity

Thickness

FIDCppm)

Radiation

Biplogicals

Laboratory ID:

Analyses Date:

Reactivity (Yes or NO)

Air: Reactivity (Yes or NO) Water:

Solubility (S/PS/I) Water Solubility (S/PS/I) Solvent:

Density L or H

pH:



Halogens posorneg

Flame Color:

Sulfide posorneg

Confirmation Yes/No

Cyanide posorneg

Confirmation Yeô

Flashpoint pos or neg @140°F

PCB's >10or<10ppm

Signature

Relinquished By:

Received By:

C3tA3366<Cim

. -?iZZ- tH Date Time Name and Affiliation

dkS> \tloLc£y^

CONTAINER INSPECTION RECORD CRA/NAL Project Nomber: 32664/ DOTHAZ tiN/NACode

ProJect'Name/Locatlon: Sybill, Inc. Site/Detriot, Michiitan MFC Name

Container In

Chemieal Name.


--iiarTCr i /• No. of Containers Layer Top (A)

CONTENTS DESCRIPTION Middle (B) Bottom (C)

Sample ID

Physical State

Color

Clarity

Thickness

Pit) (ppm)

Radiation

Biologicals

Laboratory ID:

Analyses Date:


Air; Reactivity (Yes or No) Water:


Density LorH

pH:

Peroxide Test posoTneg


Halogens pos or neg

Flame Color:

Sulfide posorneg

Confirmation Yca/No

Cyanide pos or neg

Confirmation Yo/No

Flashpoint posorneg

@140T PCB's >10 or <10 ppm

Relinquished By:

Received By:

Signature I Date Time

;


GBASMIMrni

0B/20/2003 10:41 B1692r4411 NtW HIaC. I t*M-

AnalyecsDete: Reactivity Yes or No)

Air M fj Reactivity Yes or No) Water /J fj

Solubaity(S/PS/l) Water .^4^ MO Yts Solubaity(S/PS/l) Solvent: • IMO

Density LorH 44 »^Pi ' '

pH: ^9/ PeroxideTtet posorni^ fOeCr Oxidisa'Test pos orncg

Elalogeng posorneg Flame Color: uc VL/i^

Sulfide . pos ornpg CanlQnnation yomb (Cyanide pocorneg Gaofirnudon Yo/No iPlaahpoint pos or nog (Si 140»F tufa. Pea's >1DOF<10|(^

KcUaquiihedBy:

Received By:

CRAsaMCnwihNr

Time

'•5 NuM'and A fiction

08/20/2003 10:41 BlB32/34il INt-W HOC. t-HIIUPIHTOS nvH- uo


Received By: li S i?5s&

Name and Afiiliatian

00/20/2003 10:41 biib32/340.1 l>ICW HOC. L-HIIUPIHIS^

CONTAINER INSPECTION RECORD . CRA/NAL ProjectNnmbBn 32664/

^ject Naniôcation: Syfaill, IBO. Site/Detrioi. MlehiBMi

Chenlci) Nane

CoBtaiaar

Sanplen Sli

AddMood Infomnation

fa.ofContaing» | CONTENTS DESCRIPTION

SaiopleJD

Aysical State CjOUA.p^ Coin life-I ' Garity thickness • FID^qnn) o.O REclifltioii Nfc^ Biologicals "/r

UbontoiylD:

AnalyscB Data:


Air Reactivity (Yes or No) Waier q SoIabaity(S/PS/0 Water: rzr SoIabaity(S/PS/0

'IT Densi^ LorH

pH; 'i- .

PaoxideTeat pes or n^ hiSee OxidiaerTcsc poaornctg

Halogens poa or nag

Flame Color

Sulfide posornv

Confitmation Ycs/tto

Cyanide poa or nag

Confirmiitian YMMO Ne(r

Flashpoint posorneg

&\Axre Uf^ PCffa >10 or<10pi»/ >1

•>

' RdiiiquishcdBy: Date Tiim Name and A£B and ACBliation

CftA

DO/ ZD/ ZDDO XD; HX DJ.D3Z</0HXX I'tW 'HOC

CRA/NAL Project Nonibn-: 326frt/ DOTHAZ

PreJect Nunc/Location: Syfaill. he. Site/DBtriot MIehigm MFGName

'iunber

lIN/NACodc ChoiiiteBtNomB

Uz Addjtkmal bifbmunian

OW ft?

iLabonootylD:

lAnalyBcsDate; RoBctivity (YciorNo)

Air A/ JU RoBctivity (YciorNo) Weten A/ u Solubaity(S/PS/0 Water m Solubaity(S/PS/0

5 % Density LorH UA L. pH:

Peroxide Test poscrrneg Nek. ^<L Oxidizer Test poaorneg;

Halogens potorneg Flame Color t^&L Sulfide posoFneg Confiimation Vf^ Cyanide posormg ConGnvMdm yaeMo

fiJ&Gp'

Flashpolot posornog ai40Tf PCB'a > 10or< lOppi^; 1

.1

.•

Rielthquishad By:

RocdVodBy:

Date

S-M-cn Ttme

n"5d Now and.AGBliatlan

• CM-

MU: OU UHMCMOiatf hupoedan Xlicanbdi

CRA/NALnrajMtNniDber: 92664/ pofiaAZ UNWAOide

Fhôet NamMLocatloii; 3yfaiin.bio. SiH/PeliMft. Mfclagm MFGNavc

CbBtainarJb

ClmnlealNaBe Sit:

CoBtatBor

AddMoiul bftamation

No. of Contaaun

iaa. I

Top MA y M

w/vi^rf?f5V\

CONTENTS DBSCEIPTION Middlaff) Bottom fQ

$aa|ilen>

Pbyncd State Color

Cbiity êntOdYK

HadoMsa

IDfippm)

Biologlcalt

jLaboiataiylD:

Ana^nea Ebto:

RBacdvhy, .. (YacirNo)

Air ^ U RBacdvhy, .. (YacirNo) Water u SoliiUHty(S/PSA) Water: 1 x SoliiUHty(S/PSA) n:-Dcosby LQTH hi pH: ,

PorandeXtec posorncg d-feOr OxidiaEerTtet pOBorneg mat -v.'

... --..a-#... C*.. • . -v..

jlfalagens pot or

Fbono Colon Nsx Sulfide poa or

ConfinnatiOD yoima

A/r<fe-

Cyanide poaorneg

Gonfinnation YM/NO \

!

Pladvomt poaorneg

B1140* tJf4. PCBt >10ar<10ppi^

{tsHnqulahedBy:

RsoovadBy:

. CBAaOKtQ

MM Dole Tinie

S-U-CTB NOnte ai^ Affiliation

J^S—

CRA/NAL Project Nnnbcr: 32«M/ POTHAZ UWNACode

ProJect'Noaii^Locaifoii:

MFGNoBw GhoQladNoiiM

CoahrfnrTypc CmrtabMrSlR

LoncnNi 56^ CoBtoinr

SamplanNoiiie Glem^ (iuRl ̂ Addiiiaiul

No.orCiin(aiiw(s CONTENTS DESCRIPTION MMdteCm Bottom fO

Sample ID %yiicd Stale Color

Clariy TbidaiaB "TOQiipni) tadiation

BiologlcaU

lAboiatmy'ID:

AnalyaesDate: Reacdviqr nreeorNo)

Ain hi Reacdviqr nreeorNo) Water hi Solid>flity(S/PSA) Water Solid>flity(S/PSA)

Denaiqr LorH AM-pH:

Peroxide Teat poaorneg Me-Cs-QndizcrTeat poeorneg

Halqgena posoriug Piann Colon

•

Sulfide pes or nee Oonfirmation Yamfo

hosts'

iPyanide poaorneg buifirmttlanyecMo Plasiipoint poa orneg ai4(n

i

PCB% >ldoi-<10pp90

RdioquiabedBy: Time Name and AffiliatioD

£jh


CONTAINER INSPECTION RECORD CRA/NAL Project Nnmber: 32664/

ProjMt Name/Location: iSybill. InCi Site/Detriot, Michigan

Container

DOTHAZ MFGName Chemkal Name ON/NACode Container l^pe

TlAe

Container Size Container Content

m. Samplera Name 23 Additional Information

No^ of Containers

Top (A) CONTENHTS DESCRIPTION

Middled) Bottom (C) Sample ID

E%ysical State

Color |sJo Clarity Thickness

PIDO'pm)

Radiation

Biologicals

Laboratory ID:

Analyses Date:



Solubility (S/PSA) Water: Solubility (S/PSA) Solvent:

Density L or H

pH:


Oxidizer Test praorneg

Halogens pos or neg

Flame Color:

Sulfide pos or neg

Confinnation Yes/No

Cyanide pos or neg

Confinnation Yes/No


@ MOT PCB's >10or<10ppm

Signature Pate Time Name and Afliliation

Relinquished By: vjl CjV'-

Received By:

iMbamaiyJD'.

AiMdyKaDatB.' miUk IT

Besctivi^ CVesorHo) Wi

SaluinKfy(S/ra/l) Wfltar.-mm s "ar Jensfty LorH

B: ut

tcaxJdeVtet poaorn^

txtdsnTbat posariMS

alogans poaornas '•nie Color A/i^

ilfide pocornflg mflnnatioa YoAfo <aiiift poaoriMs nfinnadon YmJ^

Name nd AQIIlrtion

th fS at*} -laawAft-o JUWL

CONTAIPnER INSPECTION RECORD CRA/NAL Pnjwt Nuninr: 32654/ DOTHAZ HWWAOode

^jact Manu/Localioa: SyWUlnc. SlM/Detriol: MBdiiem

CovMBar

MPONane CtattdadNuM

'î/03 1/0^ AdditiaiuJ bfiinxiBtion

CoBteiiurCoiitMit

dti wi

LABORATORyTBSTS sssstm. »Cd<lte(B) BoHmnfQ jaboratofylD: Vaalysn Dale:

Uadiviiy Pea or No)

Ain Ws S

olubflfty(9/PSA) Warn:

easily LorH -K.

L ^'(rl rmddeTest poscr ius

-idimTest pesorneg

logms poaoraeg meCdloc: fide posorncg iflrtnatioiiYetmo aide posorneg ifirmaiioa YaMp hpoiut oiy*

poaorneg

•e > 10or<10ppm

Dste Time Name and Affiliatfon

isturffkc-

CONTAINER INSPECTION RECORD CRA/NAL Project Number: 32664/

Project Name/Location: Sybill.,Inc. Site/Detriot, Michigan


DOtHAZ MFC Name Chemical N UN/NACode

Container Content (i/4.i/23/4,iliio Container Siz^ ^

"C Samplers Name

Additionallnformation

No. of Containers

Layer •rop(A) CONTENTS DESCRIPTION


SampIelD

Physical State

Color

Clarity

Thickness

PID.(ppm)

Radiation

Biologicals

Laboratory ID:

Analyses Date:



Solubility (S/PS/I) Water: Solubility (S/PS/I) Solvent;

Density L or H

pH:



Halogens pos or neg

Fllune Color:

Sulfide pos or neg

Cpnfirrriation Yo/No

Cyanide pos or neg

Confirmation Yo/No


<ai40T PCB's > 10 or < 10 ppm

: — ' L y Relinquished By:


g-Ll-O

Received By:

I *-W MWt. *


odvedBy:

otAaoMp

Date Tiim NAW and AflBUition

Writes rg<s CHA. I'hK' iieesrîMA^

woe L>«Ni;flnHros

AddMonal liifennatioa

VAL ProjteC NuBtbcr: |Prg||eet NuM^LocMimi: SirMTl.lM. SWDrtrioi. MiiAiggi

Coatainer

Chamle«lNwne

J-isLBUBU*, QwPC

No. of Comalneirt j CONTENTS DBSCRimON TonfAl Middle fB) BtrttomfO Layer

CONTENTS DBSCRimON TonfAl Middle fB) BtrttomfO

jSampIelD wi. e #•»__« Fliysicu Stale

Colin Ouity Ihiekxuss

MDCppni} n.o-Radiadon Biological*

LABORATORY TRSTS Too fA1 Mlddla an Bottom (O 1

LabontotylD:

AnalyseeData: Reactivity CVesorNo)

Air. M Reactivity CVesorNo) Water 'M Solu)>iIiiy<S/PS/I) Water: Solu)>iIiiy<S/PS/I)

Deonty LorR M pH;

PeixnddeTcst posorneg

Oxidizer Tost posom^

Htlogems poBornag PlaniB Color: m •

SoUitfe posorn^ 3aofinnatlanYM/Na Cyanide posorneg nifinosdaa YeaMo tashipoint posorneg aioo^F 3*8 > io or < 16 ppm/*

CaiAaUMCIaiEMNr

Name snd Affiliitiatt

SM.

i-«_w HOt LSNunHros

AddhJiniBl bilbmntiaD

No. of Contamaa Uyer

CONTENTS DESCRIPTION MMdtodl) Bpttom (O

Sample ID

Phyaical State

Color

Claris Thidmeai FID(ppin) EUdiatlon

Biologlcals

liLaboiatnylD:

lAaalysBBDaito; lEtcactivlty inftawNo)

Air: A/, lEtcactivlty inftawNo) Waien Jj So)ubilhy(S/PSA} Water: So)ubilhy(S/PSA}

ESHS X Denaify LorH Ai» pH: {,.0 (9^ Peroxide Teat poaornes

OxidizerTeat pos arneg /Defer Halogens pos or neg

jpiatDO Color: ! • Isulfide pos or neg Confitnutian Y«t/Na

AftXer

Cyaiiide poaom^ Confirmalion y«i^

tJ&r-1

TlaApoint potorneg

•CB'a > 10 or < 10 pprj^ /

elhiqaiidicd

Daia Time Name and Affiliatioa

CONTAINER INSPECTION RECORD CRA/NAL Project Niiiiber: 132^64/ DOTHAZ UN/NACode

Project Name/Locatlbn: Syfaill, fac. Site/Detriot, Michigan MFC Name Chemical Name

Container Type Container Size Container Content a/4,1/2.3/4^

LoggenName


Uz. Samplera Name

No. of Ccnitaihers JD. Layer. Top (A)



San^lelD

Physical State

Color

Clarity

Thickness

iTDCppm)

Eladiaticm

Biologicals

Laboratoiy ID:

Analyises Date:



$blubfility(S/PS/I) Water: $blubfility(S/PS/I) Solvent:

Doisity LOTH

pH:



Halogens ^ or neg

Flame Color

S-

Siilfi^ pos or neg

Cbhtitni^tm

Cyainde posorneg

Confirmation Yea/No


®140PF PCB's > 10 or < 10 ppm


Relmquished By..

Received By:

CRA32tf4rm

, «.rT MUC. |_MI

CONTAHSIR mSFECnON RECORD ICRA/NAL ProilactNaiabar: jProdM^'Nanic/LocBfioii:

SybiU> Inc. Sita/Dctnot. MicidBBD CoBtaiacrlBviatfDryPhaBbaa^

DOTHAZ ' MFC Noma ChcmkalNsiiw inWNACode

MFC Noma ChcmkalNsiiw

Cantaiwiyiie » CoatainarSte /t A it CoBtalBcr Contaat (tAuoiiMMiin

Hi Nairn iNaawt \

AdditjoDal InjEbnintian

No.ofCoiinipen

kasL SanpkID

niyaoal State

Color

Chiity wimw.

CONTENTS DESCRIPTION MWiUeflD

-nriebien

nDOppoi) RadiaSon

Biologioab

EE

BnttowfO

XaboiaUiiylD: •' • : ..

fl-

lAaatyseaDate:

iRuelivity ICVeaorNo)

AIR u iRuelivity ICVeaorNo) WatBR %

Solubility CS/PS/I} Water . Solubility CS/PS/I} ± >ensiqr LorH

•B:

'boxide'rosc fotmmg

UidfagerTeat |H»ornc|g

alogena poaorneg 'ameCoior: hia dfido poBOrneg

nfinQatiaD YaaAto hJ€e

aalde. pos ornq BfirniatianyciOiib' ilpoM posornfs idOrp »-Va >l(iat<\Opf/^^ •

S

Hitw Name and AffiHodon a-ii-o-^ 'Sksnd.t^ oii^

•T.ag'V#^

nvA. l-Atlt 1/

OU/NAL Project Ntunben 32664/

Project Nimc/Locelioiu SyfaiU, iBfc Sftc/Dottlflit. Midueen

CSonteiMr Inveotnry Nnaiber

DOTHAZ MFGNanu VNMACoda

Ckemkal Name

AiUitional Mciination

WiS INBBW V

Cnfjfc)

fto. ofCaatmim Layer T0P(A?

21

CONTENTS OBSCBIPTZON Middle Bottom fQ

SanplelD

Phyncal State

Color

Clatlty

XMoknew

AJQ tadJatton

Bidloffloala

LabontoiylD:

AndysesDato:


Air: 1 Reactivity (Yes or No) Water i

Solubility (S/PS/I) Water: a: 1

Solubility (S/PS/I)

peiuiiy LorH L pH: '?i> peroxide Test posorneg


Halogens posorn^ plane Colon Mee Sulfide posorneg ôafinnatioD Yas/lto ryaidde pos or nag :teifinnationy«iAb lasiipoiiit posorneg ai4ll*P USrCr

1

1

CB's >]0or<I0ppiE^ \ \

Date Thne g-tt-03

Name and Afilliatian CM

fbs. ri»fe_ CKAaaMaCi

lJ«NlJriAKK rwit JLB

CHA/NAL lPn4iKt Nnmbcr: mi&a aMwaAz immACodt

PrajKt NuDe/Locatloii;

MPONi

Contaiaer lavemtwy Nanhar

ChenfadNuBB

CoBtrintrSw ContaiBM-CDBtaDt

LdgganNuoe SuqdmNi

AddMoiinl Infill inatioa gUaWktouajSMcJ

uboratotylD: ; :• • ' X

(AnatyaesDaN): kaastivity Air; yj [(YBaarNo) Water;

\ V '• |soluMlfty(S/P5/I) Water 2b V |soluMlfty(S/P5/I)

-5 ^ * Douiiy Lorji •L % A#i PK PeraodileTest poaornag

SucidizerTest posorneg iJ&Sr iakgcna ^poaorn^ lameiCblon kJf^ y4BA • :ulf{da posornag :oiifinnatianYei/Na

AiCigr iJmG-yanido poaornes enfiniiaiioDVMNa U0e-

* '

adipoiiu poaoriwg IMOT »B / >10or<l0p^

«

Date Time.

'j Srffi nts eeivadBy;

Name and AfiBUaiida

lA*r^l*AFr»e»/*

htSL

"^<-1. /IK*

CONTAINER INSPECTION RECORD CRA/NAL Project Nnmiwr: 32664/

Project Name/Location: Syfaili, Inc. Site/Detriot, Mjchigan

Contalaer Inventoiy Ni "tl-ns-T DOTHAZ MFC Name Chemical Name UN/NACede Container Type Container Sine Container Content o/4.i/2>3/44ni0

LoggenNi Samplen Name

Additional Infoimation

No-ofContainen n Layer Top (A)



Sample ID

Phyaica] State

Color

Oarity

Thickneaa

PID(ppm)

Radiation

Biologicala

LABORATORY TESTS Top (A) Middle (B) Bottom (CD Laboratory ID:

Analysea Date:

Reactivity CYaorNo)

Ain Water.

Solubility (S/PS/I) Waten Solvent:

Density LorH

PH:



Halogens pos or neg

name Colon

Sulfide posorneg

Confirmation Yei/i4o

C)ranide posorn^

Jonfinnation Y01MO

TIashpoint pos or neg

ai40'F *08*8 >10or<10ppm

Sigiiature Date Time Name and Affiliation

Ldinqiiished By:

eceiyedBy:

CRiWNAL Project Nnniim: 32664/ DOTHAZ

Project Nuae/Locotioii: Sybill. Ing SHe/Detriot, Michigm

Contaiiier Inventory Nnmbcr'

MFGName Cbemkal Name UN/NACodc

Container Sim Container Content

Layer Top (A) DESCIRIPTION

Middle fB) Bottom (Q Sample ID

Phyaical State

Color Clarity irtiiclaieis PIDO>|nn) Radiation Biologicals

LABORATORY TESTS TopfA) Middle (B) Bottom (C) LaboratoiylD:

Analyses Date:


Air Water:

Solubility (S/PSA) Water: Solvent:

Density LorH

PH: Peroxide Test posorneg


Halogens pos or neg Flame Color: Sulfide posorneg Confirmation Yo/No Cyanide posorneg Confinnatifm YM/NO 'lashpoint posorneg iai4tfT CD's > 10 or < 10 ppm


dinquished By:

BceivedBy.

CONTAINER INSPECTION RECORD CRA/NAL Project Nnmber: 32664/

Project Nome/Locatioii: SyWH, Inc. Site/Detriot, Michiigm

Coatainer Inventory Nnmber

ttOTHAZ MFGN Chemical Name UN/NACode Container Type Container Stan Container Content

Sampler! Ni CTCOPC ̂ Additirnial Infonnation

hi-TCtJ—KltCC

4o.ofContaber8 Layer TopfA)

CONTENTS DESCRIPTION Middle (B> Bottom (C)

Sample ID

Phyncal State

Color

Garity Thickneai PID(ppm) Radiation Biologicals

LABORATORY TESTS TopfA) Middle (B) Bottom (C)

Laboratoiy ID:

Analyaea Date:

Reactivity Air: (Yes or No) Water

Solubility (S/PS/I) Water: Solubility (S/PS/I) Solvoit

Dotaity LorH

PH:

Peroxide Teat poaorneg

Oxidizer Test poaorneg

Halogens poaorneg

Flame Colon

Sulfide posorn^

Confinnation YCSMO

Cyanide poa or neg

Coniinnaiion YMMO PlashpOint posorneg

®14(PP •CB^ >10or<10ppm

Signature Date Time Name and Affiliation 'nlinquiahed By:

eceivedBy:

CRA/NAL Project Nnmben 132664/

Project Neue/Locatioii: Syfaill, Inc. Site/Detriot, Michigan

Container Inventpiy Number

DOTHAZ MFC Name Chemical Name UN/NACode

Container Size Container Content (l/4,i/2^4iAill)

Loggers Maiê

Additional'

CK- Samplers Name

No. ofContainen

!dBSL Top(A)


Middle (TO Bottein(C)

Sample ID

Physical State

Color

Clarity

Thickness

PID(ppin)

Radiation

Biologicals

LABORATORY TESTS Top (A) Middle (B) Bottom (C) MboratoiylD:

Analyses Date:


Air Water:

Solubility (S/PS/i) Water Solvent:

Density LorH

pH:


OxidizerTest posorneg

Halogens posorneg

Flame Color:

Sulfide posorneg

iônfirnuition YOS/NO tyanide posorneg

Ikmfinnation YM/NO lashpoint pos or neg

8l4tfT CB's > 10or< lOppm


slinqiiished By:

iceivedBy:

Itw HUt LWNUMftKK PAGE 24

iGRA/NAt rnjnt Naniber: 08664/

^DOTHAZ

PnjMt NWBU/Lontton: S>Wlk fcic, gteflaetriot, lifidrigm MFGNuu

CantdUMT iBVcntDry Nwttbcr 1^03^ CbcmkalNaiu

CBBtahwrSiM

AdditianBl lhlbiinatiQa >5D'

ContalMF Cinteiit (IMJ/XSMJUI)

Ot^ "

MoôfContBtncas CONTENTS DBSCRirnON MddteHL

IDfann) RuliadDn

Bkdingiicili

Prp HO aariptî^ l

.|UbonitoiyJb:

lAnatysesDaie: Reactivity (VasqrNo)

Air: iCy Reactivity (VasqrNo) Waier

SohiblHiyCS'PS/O Waten s 1 SohiblHiyCS'PS/O

Demiqr LorH i

Pft 1

1

OxidiarTest poeoriieg

Hdogcne poaorneg Fkme Color:

'

Sulfide poeorneg (^wfinnBiion YH^Ô pyenide poeoFiMg awfinnefion YcriWq Ttaahpont posorneB laidtrp «CB% >I0w<10ppmy^

>S|^hatiiic 1 f Dale Tune ^ Name and AfflHtnkm leBiiqulAadBy: hAr--- 1^5

eceivedBy: il/ /VDT JiHl^ eceivedBy:

7 /

rc.W MA; LANUMARK PAGE 25

EEVSAL <32664/

FroJcetNuBlien

WTHAZ

Pmleetffune/towfloa: Sybffl.hc. Ki»fl3elriot. Iificlrigm

[TN/NACqde MFONa

CoataiiNr ibivantovy Nmnber

CboakalNi T>-03a

'TWK gtervtol "gK r^rf Inlbniiaticm

Contaliiar Costent

Saaqdeti]

LASORATORY TESTS MlddlafB) BottowfO ^ ̂ aboratoiylD:

Andyaa Dan:

teactivtty Cy«flrNo)

Air Water

SoInbifity(S/PSa) Water;

Denaily LorB A/>f pH: A2. jPjgmdjdaTeai poaorijiBg

d^dizerTcst pOBniiictg

Udo^. P£m Colon V -^

piK-QriiGig -i* VJ^t

ftiUlde. poaorneff baifhnntf on VM/iife Qipjide poooriNB

Name and AffiUaiton

5^ xzifr-

,itw HOC LrtSUWhK

AMdoaJ 6ilbnimlioB|i^J ̂ O

Na.afCi«titaMn

asL TPPIAI CONTBKIS DSBCRIPnOIf

MMhibfW BnMaia fO

SnqêlP

byaiBd State ClQldr

Chifty nddneaa

©(Ppm) RadMen

a_ .

1 5uiSZ5 i^ffnif*lf^ ""^TSe fie^.n»£bj^¥Uka. ̂

jMofym

{Aaalyaea Dale:

IMaKdvi^ (yaorNo)

Air V IMaKdvi^ (yaorNo) Wter.

3aiiiUily(»PS/D Wttar. 3aiiiUily(»PS/D

)anaily LorH HJ/h 1

5~^p > atexide Tcat pas or

gdfiierTeat pasorneg

dogeu poi orneg •neCotdir; •

dfUe posorneg aiSniiatiDDY«tMi Ue-& UMB poaornag idniaaiantfteMi P&G-

1

dipofac poaornqg idcrp hl&Qr .

*• >10ar<10]W' / .« ,

Oft 11»

S5 Name and AfBilatian .

mA~ pkl& l'^9^ 6£sr "

L.HINWWI<<K l-otlt. ^!

|GM/I«AL?roJwtflaiteR 2664/

-^rtPOTHAZ BiiMl. lac. aBBfl>Brtiil. Midrib

ChMilMirfi :x^

5B5>^!Bki'o-n dklfiC")

C^tadf CXmiEinS DESCRIPTION

ffiL

ydiaadoiylD: AnalyMsDtfe: •

Raatfvliy (y«arNo)

Air Raatfvliy (y«arNo) Wafer Z Sakibiniy($ffSflO Wafer Sakibiniy($ffSflO

Sblval: OBMiiy LorH iJr iH:

iv

'fenaddeTBst poaarisBs iOE& )fcidiiBBrT«ii p«arn«S înSr-UoigenB p(M«riM« hinBCobr.' •

•MMe posorneg eiiiiiuiBlkmYartte IMDldB pMoriwg nfinwaiaQimAfe pJ£23r Htpoait piM orneg ;l40rp K^Csr- . »$ >10ar<10nMQO

Tlinio BiodAISHaSon

Cf^4r

^TfTiilAU tf^

LW HOC. LMINtinW<K l-fltt JO

A3>/

Itw HUt PAGE 40

rONTAlNER 1WSPEC?T10N BECSOKP IdtAfftALFnOutNli

fBOTHAg

IWUiodlMz

UPlfllACifc Trp®

5&l62k ^•-5-g^rWa>

6?-

•ptanNi

* * ^ ^ - ^« - -AiHBQoiuu mimiuBioii -.H-itAL m>ovy>Ak

jMbkorCDOMbiaB

J^Mr

OCIWTBTOPMCiglPTIOfr 'r^rA\ ttUAtm HtnmtCi

8M#tJD —<«-• -niyHGBicrav U Cdor abMkh. v<XUu CMty d,4^ WctaM

IDOvoO O.O tedWofi MUoôA

AMmAmvTwrs I JbcHMOq^n*:

JM^ywiOne; /V ^3 • BHlfvi^ reacrKto)

Air lueTfc-BHlfvi^ reacrKto) Wei^. JMffe

iluUHlyCSffM) Witen s iluUHlyCSffM) s LorH

1: 'V.J? xgddBTtsi pwaraeg

idinrTeR pMiirjM« Mrfr A«*" poaoriuf wOolar! AJETS

•

Me poiarneB finuation VioMi vefr "M" pMorMg SniaaSoif VWte

W^6r

QxAit posoni^ MTP 1 21O0r<lOmi

Kj£r6

fiWwd]^

«49y:

A ai2:S mw

hpo

Aflffiatlon •eki^ CU

i_Mra;nAKK PAGE 41

f^niMTATNIgn iMSFECnON RECORD

aw4/ prnmut

09 - bsfl

jSStiyyuiJfc GBOMW GaatHK<piiM,WM«)

• • la.l- • r- ,••III•• MUniniH vuMiidnKau

'No.ofOpgMBqB coif iwis iMMtauyaow TîJA BOteteiff »«»««?> I-ayer

coif iwis iMMtauyaow TîJA BOteteiff »«»««?>

anvtolD .

Pbyriod State '•••"L caaite Color UAN

dCi»j\

>1D(M 0.0 tttlbtfpD

dnnteiyin -nttyasDtatt;

Miviqr 'sorlte)

fje^ Miviqr 'sorlte) Wi^> ¥Lf^

lidiiIftyCS«aS> WtfOR lidiiIftyCS«aS> X

nriHf LorR vlf\ • • . -N.O ^ 9 nddoTest pMornqi Pas t eM««ohwni>i>> roxAO'

SterTot ptecrn^ Pos ^ »B«i pteomoB aa Colon •

ite pararaog BntetonVteNo loear

1

iliJo pteqrmB InanianYfltAb 10^6-pate poaorneB ia»

^10qr<10nim fllMnoM

MrGr

liao

J3C1C_ HSftL

in_w HOC PAGE 42

rnNTAINER IWSPECnON HECX>BO 7S7/gfc. Al!9

m3& imss

- r AjdwoiMitauiuMkiu waL«» ~ V" •{ Ata^ V«J ttisjMfaniA

tr, M !fi».afOanliinan cxHfinmmnKaurnaN LBMT TrntCAl MUdtain

taqilelD

PbyriedflMe U rvj—. COWÛAA •

iCMiy C\AOLK llibtaieie

HP(P|M» 0.0 Rffttstfoii

1«

LMKmATORYTBSTS Tim(A1 MUdhm BrttomfO ^bomieqrlD:

\iH4yieiSme; '

\meAvtty Air STMcrNo) Wew. M6^

ohibflityOSMnMO WelBR ohibflityOSMnMO ooimn I

CMitr Lortt

!•

nxUbtmi paaarnv pos lO/nj/t ddiaerTem jmvntg -weft- Pes

pcMarnqg amColar. •

ado povdriMg itfanBBhw YtWWo niile poeflriwg OnalaiYMAb uiJier

fcpdiat poeerneB W

210ar<10ifipai

«Bd4r ^

DXB lime

noe>

^1&U3 XM.

I^tadAOIIiillai 'StfHcL^ rp/)-

I1C.W HOC. MV4JJMAKK PAGE 43

mm* AINER INSPECTION RECORD :^Q6i

fltoBpbXP -M'JL RgnMSMe L. CUlor •

CMly

lUckiMM

TOfairt O'd

Hbkiâdt

.AMkATOKyTun Mddtonn BoiiuBfCi 1 ^boratocylD: î2_ MtyaeaDMB: Sr- N'03 •

taorNo) CRI »UF6r

taorNo) CRI /UgCr-

iluUliQp(BffWQ WattR iluUliQp(BffWQ a

mMXg LorB y b •7 2> taOdaTem potorMft fi£&

tttwXBtt pteflrncg. ^/^6 tagBW pMorvcg rnOator. •

fi«fc pwornqg AndanvaMto X>6&-

nide pwqriMs •nptlonlhiMa îpent pMorncK 40*

» >lO«<iO]im

iss j30j_ Ml luni-

riWTAlNER INSPECTION RECORD OkArnLTnltetnmAm iie&y HJrrUAZ

B»MLlii0.atefl)fllriot.MicMwD

JWNACiie iMTOIiaim

ContRiNcr GontsM (UiiUMMiiD

AwullOIUU uilUflUAIUUI

No. of OoirtafiMn C) rm,tA\ MHMIafln BaltomCO Lover rm,tA\ MHMIafln BaltomCO

Suqileip

Pbyriod Slate

Cdkn* • C3arity HiidaHH

IDdpiai^ Radlalion

LAJMMRATORY TRSTS JSEtAL jsmssL BSSSBSEL UbonapiylD:

AnalyMi patK

Rontivity (YMCTNO)

Ain W«ten

Bolubitity(»I>8n) WatBR Solwnt:

DeHtty LorH iriH:

WJdeTert pMoriiet aridiawrTcit potorncg

Hbdogma pMorhql 1n» Colon

SuMWo pooiorncg CoaiitiiMiioii viiiffte Qywrfdo poooriug Onflra^mYMMi ?W«P««nt pMornqi

*CBff ^10or<10mmi

Slgnotuio WlnquliliodQy;

MohwdJ^.

Date Time None aid AflSUatfon

i_Hi?«bN«IHKK PAGE 44

KdUffiALrnlcieMBAWi asM

AddWoBdMbnuiiott \J L ^j/w>MUr «Môdh»r AddWoBdMbnuiiott

No. or

SnptelD Mikfi PIViisdSMr • L U <>

lUor Wowsik Vlotk feLxrk aarily CWdHMH

IDC^ o.o o-rt 0.(S> '•iWnrton «*«bib

ibaiMeiylD: *1.^ A H5 A luIyMoDMe: 8r- /v-fi3 sr-tt-os •oMqr UiR we^tsr ASC. (Morlto) *«iSr lMe&

UbOityOMFaa) S UbOityOMFaa) je-

Bitty LorH >C ——

• -7.e> 7.0 BoddoTert pooorw* Ate&> iliattTigit pot arms URr- *J

Vu poiariMf nOOnr. Ugtr-

t ifc poior,;^ SBMdanyMto fi^y-

h-

lido pooaroog nBMfcavoAfe hey Aiegr

pote pMoraeg afp

ÎOor<10p|Mn

lOreSr *J€-^

«==/ •dNiedNy:

HWB Nm n>5 . -^8^

•MAOIMlai^ ^ 'dvu^.CRA-

ad^y: J2SZ2.

iMtw «bt LANDMARK PAGE 19

CRA/NAL Prcitart Nqmlnn ilSM

pOfTBAZ ITONACode

•Tôfw rart

]pjrDjigct.Nuiu/LoedtidiB SyMl. he. SHB/Ddriol. MieWgan MFONuae

LogeanN

ICdnlBlBar Invoiilbiy Ni

Ni

GondOMrGoBtant'O/Ai ,

m^LX Addidand hRiiiiBdiQii

Mo. afConitiiiiGn

LSSL ToPt

GONTKNTS DESCRirnON MlddfafB) Bett—gn

SanptelD

Phystcal Stile

Ctolor Ctaifly TMdoieu PlDtppm) RidMon Mologicib

UboraioiylD:

lAulyieiDdc: Reactnrify jyesofNo)

Ain hj • Reactnrify jyesofNo) Water

5blQbi%(Sa^Sn) WetoT 5blQbi%(Sa^Sn) -5

Density LorH

pH: Z.i> PenoddeToR posorneg

Oxidizer Test poeerneg

Halogens posorneg ânio Color.

h^L •

jSiiUide posernag

Confinnntian YBÔ xTirfe

pynlde pasoriieg Oanfirmatioo Vaô Flaahpoinc posorneg ai4(rtP . (bS '

PCBI >10or<10pin/7 limo

jm /m-

JimemdAtBUatim

I^w Mat. LflNUMAkK PAGE 20

CBA/NAL rnijcct NbnlMr: 32664/

^ DOfTHAZ lACoih

)Plra|ect Natu/Lee«tiOB: SybflU haSiteiflPetriot. MMdiM

Contaiaer tBvmtary Nombcr POBO MFGNttu

aSDa '-^'

l-fUnn-w-yM I p

Npu of.Ooiitiinaa

[S£5L T^fAi

CONTE34TS DESCiaPTION MMdhifm Bottain(C)

SbnêlD 3a Piiysioai State Oolor

3ari|)r Thidmas PlDCppoO Radiatiop

0ioiq0oals

UbcnttiylD: "i-

lAnaHyaeaÔate; -

Reaoivfiy CVeaorNb)

Air. hJ 1 Reaoivfiy CVeaorNb) Watan td Sdlubflfty(8/PS/0 Watan £ 1

Sdlubflfty(8/PS/0

Densi^ LOTH H • pH; ^/>

Pundde Tcat potorneg fjecr OKidteerTeat pocorneg tJGC. tUogeiu posoriiag âmeColor .

•

lulflde poaornag 3anfinnaiionV«Wa TyanidB posgrneg SonSnivtiapYM/Ne ueCf

1

laafapoiiM poaoriiee 3140"?

1

G3b >10OT<10'pm^

)y IJ

EdLi 'r

•»Tfj

Date Time

9-ji-0^ ms Mif

Name and Afniiadcm

•^tiTAML.

Muw HOC. l-HNUnHKK PAGE 21

CRAWAL Prajwt Nnnlier: 32664/ „

VnJnrN^f/Locadon: SiWH, Inc. BitdDcdiiet. Midrium

Covt^BBTlnvafllnyNinnbtr ^

—5=034 JDOTHAZ 8 roWffIA Ciwto fJiJ

U7.ftto

4o. of CunlBiiiBni

dsis. SIttiiplelD

COinVNTS DBSCBIPTION Miildtem iSL

•hyiiial State

CUor •aiity

tMdCBCM BpftflpW

PIP (ppm) Radmticm Siidfigioab

Labonitoiy n>;

jAnalywsOater Rnwtiviiy (YoaorNp)

Air fJ Rnwtiviiy (YoaorNp) Water

B<MiiHly(SA>Sa} Water " B<MiiHly(SA>Sa}

• ^ Denai^ LorH

-T-A Peroxiidetest pos omeg liJ^ OaddiaarTeat Jioaorii^ iJ^Sr Halogeha pos orncg

DPIama Color.

• ySuNide pesoriwg ' C(mfirnatianYaM«

«

Gymidie pos or nog COnfinaadon YcPNo piadipDiiit posoriicsg ai40TP PCBls >10or<IOpB^ , 1 1

Date Time Name and Aflffiadon

thm nit fjjt.

I«_w Iiuc. i-HiwinHras. PAGE 22

PRA/NAL Pmlact NnmbaR 32664/

Fntlcct Nam/Loortlini: Svfaill. Ibc. Site/Deiript. MfeMwa

CnBtalim'

marwa. 'ar a iJt agp CoBtalMT Conteat^

Additiflnal Wimnatton

N«.ofConiabien

JSEL Jsem. 4

CONTEaSTS DB8CSIPTION MiMeOn Bottnn/C)

Sample ID

Pl^nealSMe

3blar

ClariQr ndcfawaa

TTTCr ET^

nD(ppm) lUHliMion Biologicals

laboraoiylD: iSffS-02.f lAnalysesDaie:

Reaetiviv (Yet or No)

Air kJP Reaetiviv (Yet or No) Wtfer. U

SaliibfliqrCS/PSA) Waken SaliibfliqrCS/PSA)

Dcnilqr LerH m-i^: 452? i

*/er&-OcidlBKrtest posorncg

Hbiogent posorneg namaCblca-:

'

Sulfide poeorncg ConSnnation Ya44o Cyanide posorneg 'Oonfimiation VeiMa

1

Flathpeint pocorneg ai46^ / 1

4

PCB't 2:iPior<lppptB^ i 1

SflHnqirishodDy;

iteeeivedDy:

Time Name and AfSHation

Cm-

'3

CRA/NAL Project Nninter: 32664/ DOTHAZ

Project Nauc/Locattain: Sybill.lnc. Site/Bctriot, Michigan MFGName

tlN/NACode

Container Inventory Nnigjinr

Ciienileal Name

Container Container Sine

Irfiggen Name

Container Content a/4.l/2^4,lW0

Sampler* Naine

*hysiinl State


Middle IB) Bottom (C)

Color

aarity

ilhidcness

*lD.(ppm)

Radiation

Biologicala

LABORATORV TESTS Top (A? Middle (B) Bottom (C) LaboratotylD:

Analyses Date:

leactiyity (Yes or No)

Air Water


Density LorH

pit


Test posorneg

pos orneg

Flame Color.

Sulfide posorneg

Confirmation Voi/Nb

Cyanide posorneg

^nftmation YoAXo lashpoint pos or n^

aidOT CD's > 10 or < 10 ppm

Signature Date Unie Name and Affiliation

dinquished By:

seeivedBy:

iW HUE. LHNUfWKK ZU

fCAiUNAL PnlwtntiBriMn 13664/

iilHyrniA3l

inilut NoaNflLMatkne fcc. ffllc©e»ii>L MieWttn

MfCftnw CtaJrHW— •Âl .A <3<? DNMAOods • 1 fi/ft/tR rTc/n •rs.T/aJ.. /-xêr^

"f •—hew AAdidouiMbnmtioii

"f •—hew AAdidouiMbnmtioii

, /J • 1 INo. oTCanlifaie^ | GOffrnnrsDBsciiPTioN

TOD/AI MHiUalin BottowlQ

ShovhlD •

PliyriealSMe Color

dait^

tWotalCH

iPlDCppnO Prb f t> /AAstMcy HSD talk peh^- JgLi. J hJhu^

1 1 Mftlnnfainh 1

iLAVOXATOSYTBSfS H»fAl MIAUelB) BottoaKQ | •jbonBoiylD:

ItedyoaDase:

tamtvily trcoorNo)

Aic V tamtvily trcoorNo) Winr: A> BolubllfirCSVPaVO Wottn BolubllfirCSVPaVO

PeeHy LorH Uk

r pnoddeTesI poflorneg iLir& ;

QxiiiterTeat poaorn^g fos Holngniw pmameg PbBBBGolor. • UMde pmoriMg awflllttMlUB YwWo

pooorn^ ônfiniwknYoiMi lariqwiot poo or aog 1140* £» 2;10iar<10p|ipfir

NnMndAffiltatioii QfeA 11^5

/iffiSa- ;^y/^Wrr

i-u-w HOC. FACS.

dfnqufdwd^

oivedBy:

Nma and AfiiKaban

|<)C.W HOC. I.MHUMARK PAGE 45

finwr ATNITB iWSPECnON RECOBP

PWHAOrta

IM.

AddttioBdAifttimtfiaii

ayMI,la«. «iB<D<ite.MhMwo

\Â.l kflAtt ^ ^ 9"^^cK. ^ .ûuJalj, Vo Wk.

(feofODittriiNni - ^-BsaBalS—— tjWBr TODCM MMutm - ^-BsaBalS——

bnidelD 1 fÂ'c-l«A • et.^)

•IViMAM L ôk* CaViÛtv iJct. . Ûc<<. Miy —

IDM 0.0 •

ABOaUTORVTtSTS TOP (A3 MMtein BottMiia i dmiBnylD: m IS 1 ^jnwIhaK »- in ^ 03 •rtvlQr Uk: SJti^ ^ r^.a05rr tJe^

paLMMcga A/SCf >0£iSr-lijipSBlnsai s '!

X or •• ^ LarfL 0 M

\ H 3tqde1Vsai poa criHs AJ e'iSr- • ^ teToR pMornct tJ&g- A/et^ igm; pnornv •CMOR 1

do pooorims inatthtnVaMe At(r Ut ptmatitg iDBHtoi«NMi ^€fs poiol pMorimB

^lDor<lOppai

kjE& ; hJ&Cs-

A

— ... 17-30.

CftAffMJL PiroJwtNnibaR ISUM

lOTHAZ hiLgHrtPelriotiilefcton

UNMAO^te

r T"- tni

qrHi

AddMonoi biffanm^ inKrI/LjL

¥ Mo. of CantaiMn

i9S.

CXnfRim DBSCUPTION T«>(Aa iwateflp

i»f<> O^jp SknnplelD SMB

Cdor MQT

WPft^proj) ^.5L i8>.orOf/agA>)

:d^

LABOKAIXmy TR8TS Jam. MMdteOn -BSSEBiEL LaboMtoiyiP:

,v«' AiulyMiDMe:

RnctiW^ I or No)

Air Wi

MuUKtyOWPSM) WaW: JOIVM g

LorH iH:

'MoyideTtit jKMoniv

OaidfawrTott pbi or img

PMoriteg WamoOoton ihdilde poaormB Ponfimiadon YaOHb pywrfdo poaoriMg OwUnaaliaBYwflto

ReoalvedBy:

dkAMALfii^srtNlnid^ m&v . BSMAL

{pniZNM musLS

MIGIIIMM JWflUCD^

n««titT iByiaibMty Pwiiiilwir S.'

ninH>iirC»Hrt(lHWI»<il^~

SJH Additloiud'InftiiiiBtioii

ftkofCoaiiriMm 3Zii?* ym :—I —i-SmplelD

Pbyatoal Stste

comvvnDi^^ mmiieia BtlwfQ

OAK

Odty

ThkfaieM

7.8 j/i.a 1DM

lioiogM>

LaboMQiyiP:

AnalyaaDwe: •

RaBctivity Air YetarNo) W«ttr.

S(riiibil<(y CWPS/I) Wato; S(riiibil<(y CWPS/I) SohoBt:

>0^ LorB pH;

PmxMBTeit pwoTMc

QuidfaBerTeat pwornce '

WofOM pHorneg PlmwGolon BuWde iMwornflg CSonfinnitfon y«Mi (Vanide PMOTIMB OoidlnMllaRYwMo

mi4tfF !CBii 2l»0i:<]0ppm

RflHnqulihedBy:

RaeeivsdBy:

DMe nme NamsndAfllilittkm

I1I.W i-iuL. ii-Hn rrHUC, ax

idbuNAL rniKt 02664/

Fni|HtNttu!/Loeirilip0s Cteidaar tevoilm NanAar -TT'-rtll*?

XTTHAZ DWNACBds

MPGNnM OnBieal'NBiaB

GM^Type CaaiaiBcraM Goattiiwa CoidHll ciAiVliW«.MQ

1MB TUM 0«(W>

LoocnNape '5IS;IK"&* - -a.w -Mic. AdJftfaml hfiHiuiUhiii

L-Â4K-om30T.-v»\. o6l Cj.g>l , CTP, m«;i.

Mo.afCaiilaiiiâ H corarsNis DUGRipnoN ItoCA) MMdtom BoaaailO Um

corarsNis DUGRipnoN ItoCA) MMdtom BoaaailO

loqpleJD TT- 0 <l^ •hyaicd State

Oolor

Claiity

nudoKH

®%e» Ksd&lioD

t/«.avhc

JOKVTKSn JSES^ mutton iSL ®emimylD:

|tea|yaeB0nB

pRaaaiyity AJR tVcaorNb) Water; Juesr ScAlUHty(S/P8A} Watar ys ScAlUHty(S/P8A} s Dwily LorH H iBi

^mddefni poaariMy

bddiMr TaR poacr ncs h/mtr Uogm poawiMB faeaa Color. •

ttMUe poawiiep NInnation VDi«to i raaldB pas or nag MifUusaluBTMWp Ayf6-

y

idvaol pos wn^ l.l4(fr Vt >10OT<10>PPI^

lUiiiuhedBy:

dved'^y:

NwndAl&liatidii

BusL. fflH

i«i.w fwc. LjvmnflKK

idMi/NAL rrojeet NWabar;' mm

--pOTHAZ lnc>gftBPalftot.McM»n

jWWACode

#V«HA«r»MM»a«niiy>lkMaiar

"TT- OH&^^ OwnlMllVi

uwlC

T-0-O3 nsc

Additifiwil Mmnatiai vA

iyuy^"J»\'A • en^

h%ei Va«i4fl<*v

Slo.otOoauiMn ( ccmtm&vmcxainnm Uutt ToofAJ MMdhOn MemtPl ampklD T-r-(jM0 A TT-f*l«^TS> Ptgnicdftato vfiluJkt CtOar bWlk cv-to^ amity cVeoA Wdsam

HD^PPiiO O.d lUdiadoa BinlWrofa

iLABORATOmr TESTS TnW iMbUkan BattmtCt ^jUmmotylDi "Su-B AndywsDue: 13-o-i RfMfvily Abr. Wcit yaorNo) Watan *i€6-

ScOubitivClSAPSAE) Water. s SolwBotrr S x.

Ooaiiy LorH u ?» nô ^HroKidBTen TMorma tWir timtr ^KidaaerTcat pwprii^ oteir Ui«atf pMoraqB IniBCQlotf i

idfide jioterneg eaSntuHonvtMo

hr&k mst^ ymtidt paaatnas aiAqnaion y«iM» •riqpont poaiornies 114019 kj^

NameaiidAffiln^ Hheck^

iL^

I«.w Hat LHNUMAKK PA6E 33

TiSSi/ SvbOl. lot SHBOMriat. Idhdiim

Gonialur laMirtviy NualMr

iDOTHAZ RilMAiSiiriB

MBGNme CfeHoritilNian

CiMtdinraiH CoiilateM'GimtiM(iHia,WMtaB>

rS-lSri)-^ 1600 UBBBnl'Bun '""''SSSL

UddMoiitfJiilb^^ rJbU kiA UddMoiitfJiilb^^

\flu«Lut r<. *

1 1

rantA\ MUdtem BotoawfO Livar rantA\ MUdtem BotoawfO iaoiiilelD' Tt - 0So A -Tl' 060 T2, IvriedSMe Teiot Aou,^. ! U&idl^ Ouby ClCAA WAatn

O.d &,e> Bmlnlioft

BfoloBteala

T«fA) MSmim BvtteflKC) 1 âhai^tvyJD: fi'33. A 030. ^

[AnallyicsDatB: w- a.cn, ^ -• •-Kaacavw Air lOBTV pesorNo) WttR MEt&r

lsQlvliUtiyOa/R8/)0 WaMi; 5 • lsQlvliUtiyOa/R8/)0 s :i:

DoMhy LdrR L. • A/A ?H: <i.S" ?kmKidBTeit posormg bie& aesr >KiifinrTeR pMarncg tUS&r

Uocaw panrnqs luMGaliir li;r(r •

Ufide potiariiBQ îiifiinMlKiu VMWB

• yinUe

aaflnaUMn YiMAfa yetf U0^

Mhpc^ PMornqg 1140^? W^Zr JB* 2l0ar<10nnn |'

cr_-j •

iBlwiedJ^

JTSS_ CkA

itcai bxba;<;/d4ii ISC.W Hbb i_HriupiHrQ^ rHbc. OH

OlU/NALVndcetNnBdMn 266</ tOTHAZ IWWAGwh

Pn4cat NMni/LMallDpi gvbni.liic.atefl>alrfiit.MkMpa MIGltaB*

3ZI Invwiofy NnAar

:3Si :

OMtte' GUMOtQIMiia^WtilO

tisu

1615 LogpR'Nane

MIonI'Manailw "Îtl -{nn^ i? 5' -ff l!l ^

^qvy r<. "543030 —

b. of Qntahieiii | COmBNTS DBSCatlFTiON •nmfju MUdla/m MnofQ Mm

COmBNTS DBSCatlFTiON •nmfju MUdla/m MnofQ

bqpkiK) TT- 0^\

liyBiedSMe

bloc tSj-Saiily M. b _•

niCBCBV •

IDCppm) O.O

Ibloetads

A80RAT0RYTBSTS •nwCAl ADddlean Bonamra 1 abanKxylD: 033 laalyaejiiDate:

onedviiy faorNo)

Ain onedviiy faorNo) Wittan

ohiWHly 0»PtM) Water x ohiWHly 0»PtM) s cmi^ LorB u Ht:

fue& iddteTeat poaornq usb-alqgan poaornag ame Colon ¥iesf

i'

dflde poadriMg Jdffanibiign VaoNb MtfCr

;i

1'

fluido poiidrneg »fimnlkmvqiWo

i

ndipoiiit poaornag I i4orp hl0f SBfi >.10iar< tOppin

MdifldBy;

BBlwdfiy: i: lUr P,,

Dm ^ 'RniB

8-t>07 .J2^

S-iyyi /7aa

None and AlRIkdan

yîat« Cfe(4-

—aMi-

UO/ X U . HX 0X03^7OHXX l-tw Mat UHI'tM»IHrO\ rMot d3

3ltA/NiUL.ffNA«t HmOtmrt 2564/ gvMU.iB6. SftePtfrfot. MAtoP »OTHAZ JTONACod

MTONMIB n

Ni

*^15-eg 16^0 ViddithHidlnftnmtioD

fetofOoDliiiia 1 CONIVNIS DBSORirnON

.•V0 Ttoi£A} Mume/m jpqpfeiP

IqnriGalSwe rUoT

3vity dcAy>.

iMhnaaa

IDQpiiiint) 0.<b .adhlidD

afaaiooiylD;

iHlyaaDdie: •

nclivHy faorNa)

Ah: JOI^ nclivHy faorNa) Water; tenser

oliMHfyCMPS/O Water s oliMHfyCMPS/O iBolveatf; 1

«iMly L«rH L 3: 7.< madde TbM poa oriMS Xtt-

ndfavToc poBcrius ,068-

aioaM poiorneg

BBsColor. ;

ilSd0 poBornqg

mBnniion VMto

ffDide pmori^g

infinmolHiYiMfa

peaornts

1146* JUfit-

>10ar<10ppin .

KnquUiedBy:

:8Hied:9y; p

DMr

S^/2^0-^ llDO

>

08/20/awkia ia:4i biba^/aqii INtW Htit LHIMWMfW. THiaC. oo

rhlCTAIWERIBtSPECTlok RECQBB (qlbUNAL PMicct mupiMn

pOTHAZ Owa<AiOiJe

SihaLhc.,Silafl>eBtoLMaiiiM

MSGKi

ilw'bmptoliir

r LaBBHsNMU Ni

AMdondMbnimlto iuct^ Wic ^

NtpuofOdDtaiMfi \

ShngkTO

PliyiiadStite

3EL

Cbhr JicMk.

ccKomsMcmTiaH vam^m

\^vgrvviL.

LABOKATQKVTBm MWdtefli) BattomfO ID:

Dnc

(Yes or No) Ain fJ&Sr

Ws

MiibfllqfOS/lRS/i) WsHn SLk LorH »f

KH:

Pewaddotteic posoring

^BdaBflbK pgs jnriwg

Hatagns

PlMMCb

poearnqg Color:

Suffide pes or ] ConfimMioa YoMo Qfndds paeorneg

CnofiBiiBlioB VaiWo

Ftadhpaiitf poiomeg ai40»

U&br-

PCB^ B:lDior<10pi>m

a|piohir0

_>qiiWi«IBy: Date

KeeahodBy:

Time

g-- i^^cQ tkst^

dLuNAL Projcet NamiMn 32664/

lPjt«|eet NaBMllMatlon: SvWn. Inc. Sile/Datriot. IdioUaaa

Contataer iBveartoiy NmdMr TT-O^

DOTHAZ UrVNAGode

MFGName

GiMitainer Tvne CoBtainerSIn ContalMT extent (l/4.ia4'4JM0

iw«« Xlme , n'bS

teggeraNaBM SBmplera Name

Additional finfinmation \aJ*^ V« V

Additional finfinmation \aJ*^ V« V

No. of Containem cotrmmmacBnriON TootA) MOddleiD) BottonrO Layer

cotrmmmacBnriON TootA) MOddleiD) BottonrO

SamplelD Pbyaical State color Ciaiity

Thidaieaa |ni>(^)

nKAlnftifials

LABORAtORV TESTS T«P(A) MWdteOn egssja. LabontoiylD: Mulyses Date:

teactiyity YoorNo)

Air Water:

ohiUlityC^PSA) Water

enaity LorH

I:

fondeTM poaoriiyg

MoerTcat poa er n^

poaorn^ ne Colon Me poaoriMg finnation YaiMa iMe poBorneg SmiBtianY««a •point poaornyg UfB i > 10 or< 10 ppm

SigiiBttire Date Thne Wiiaiwdfiy:

cdBy:

Name and Afflliation

dbuMAL Preject Nomben 32664/

rn|aet NaaiN/LoenllDB: SyUU. fate. fflte/DetrtotMidrigan ^

Contalaar Inventory Nambar

7 7 7?^3 DOTHAZ UN/NACode

MFC Name

CratalaBrlYpe CoatalaerStaa Contaliier Ceatant (iM.ia.vtteit>

Date ^ nnw ^ \^46

tpegenNaane SaamderiNanM —

Additional Infofmatkm MaT XCdola Additional Infofmatkm

NowofConteinen CONTENTS DESORlPnON TODCA) Middle (B) BetionrO

CONTENTS DESORlPnON TODCA) Middle (B) BetionrO

iSan^leiD

nqraical State

Color •

datfty

RiidaieBa (

npotpm) Radiation

Biolosieala

LABOkATORY TBSnrS Top (A) MUdiefln iSL LaboMotylD:

\iialy«eBXMe:

medvity ITaarNo)

Ain Water

3lulrili9(SA»S/l) Water Solvent*

»ei^ LorR

i:

xndde Teat pes or

idizerTeit poaorn^

poaoriM^ ae Color

We posorn^

finnation YaaMs

ride poB or

imiatioiiiViiWa

pmot posornes

>10or<10ppm

Signature Date ilme irikiedBy:

WBy:

Name and AfRIiadon

CiUmAL Pielaet NniabeF: 32664^

Pn|aet Naaae/Loeallon: SvbOI. Iiw. Site/Datriot. MidiiiBtn

DOTBAZ 1N/NA Cnihi

MPGNmne ChamkalNanm

CeetalwType . CoatalnarSiaa Container CotoBBt (1M,IA,3M»<UD

LoggeraNaaw SamplenName

Additioaal Infarmstion Additioaal Infarmstion

•

No. of Contatnen Cl5 Layer

CONTENTS DESCRiPTION TonrA^ MUdlafm Bottom (C)

Sample ID Phyaicat State Color Parity

TMdaieaa |F1D(iipm) Radiation BMogical*

jdmtatorylD;

uialyaeaDatm

eactivity fee or No)

Air eactivity fee or No) Water

ihiUlttyCS/PSA) Water ihiUlttyCS/PSA) ESS awity LorH ••

oxideTeat poaorneg

IdizerTeBt poaorneg

Ogena poaorm^ t» Color ide poaorneg 3iroalionYaaNe

1

iide poaorneg iiniation YMMI point poo or n^ OTP

>10or<10ppm !

Signature Date Hme Name and AfRlialion uiihedfiy:

Hi By.

dU/NAL Pnject NmalMn 32664/ iWdll. lac. ateiPetriot, MidiiBan

CoBtmner Ineantory Namber ^ -rr^ a9=r KiTBAZ inWiACode

MHSName CheaaicalNaaae

CiMitalaeriype *

CwrtaliMrSlM ContalMr Contona

Sate Thna v-sec?

LoggnsNaaaa SaaqdersNaaM^

Additional biionnation Additional biionnation ' '• "• • ••-•'J- / I

NO. of Contabien ^

Layer

CONTENTS DESCRIPTION TonfA) MMdlam Bottom (O

Sample ID

Physical State

color

Clarfty

HiidaieM

nponpm) 'Radiation

Biolocicals

LASORATORY TKSTS Top (A) Middle (B) llotteBi(C) otentoiylD;

Vnalyees Date:.

'Mcdvity /eaorNo)

Ain Water:

>liiMltty(SA^) Water

airi^ LorH

xwtkleTejrt poaoriieg

jdizerTeat poaornc^

iigeea poaormv

ae Color

ide poaortieg

Snnalloii v<aMo

luie poaorncit

imiBtionYHMo

poitit posorneg (TP

>10or<10}>pin

Sighatuie Date Time iiiaiiedBy:

TdBy:


ClUMAL ffk^ NmriiMn

DOTHAZ MFGNanw

-XM-ahi oeÎJ

inWIACddt CNMbMriyp* GanMovCMtfairtoAiiH^j^ |

IMi t5-^ Tta. •

fTjrp* » jbcwyw wo<>-

0^l£>

t.-ioLx /racW

Mah«d%:

VAHdMiillnlbniiiiiM

Ha-efCnUiMn oomiNnpiBaninioN IMMlfCI ysm

SMnpleK) / ^

MyrioiaMi / L Colar

Oarliy f CUejv ^ r / IbMllWM / /

HDOvm) O-d / /

1 ^ / V 1 / /

I.AmMRAT0RVn8TS

UbonaotylD; JEseiftL iSL

AMSymVmK ttMaUvity CYaorMi)

SoliiUlityCWra«0 ISISSLi

Uin CB3

rONTAPJER IN^FECHON RECQ]^ ^,hn.ffll«imanrfatMkid^ iWl

CkandMdNMW

CoBtidiNr OmtMrt

SunplMriNaiiM

AddMfmdlnftfniatidD

No-ofConiaiiMn OONTDm.lMSGRIPTION MhMhfln lEL

Stale

Color

GMty ThkkiMMe PlD{p|eB)

LABORATORY TB8TS MMdkim LabontoylD:

AnalyaeeDalB:

Reaciiivity CYaaorNo)

Afe Watan

SoluUHtyCRffSA) YH&. SoivcBt:

taahy LorH >H:

PeroKkteTeat poiorn^

OridtoTcit poaornag

Halogana poaoriMB Plama Color: SuMde poaornog GaedSraiation VaMto Pymida poaorneg ConfinBalianYaaNa. laafaiMiiit poioriiet

Li ^ 10or<10ppiH

Slaiwtim Data Reiinqulalied^

Tlim Name and AffiUatlon

ReoalvedBy:

IMM/ WTHAZ JW/WACoaa

SiftflLlDfl. ai^Datitot. MkMwo MIGNnM

iK'Olh trtMyltaail!

ChaoiieilNiuiii^

7 16^ 006 ?>4. jCoDddMr CoatMrt

A- V^ -.Pl £12QCL ^ddWiHul fafanHtfcn

Ne.ofCaiiliiMn

\SBL jEsttia. COMTBimBBaGRIPTION

MMdhfln ISL SnaplclD

PliyikMl State

Ctokir

3-ity

Signatuie RflUaquUiied^

Date Tbiio Name and Afiliiation

Received]^

mNTATNER INSWBCTION RECORD

mm-A1WER INSPECTION BECORP

loôfConiiiiiai H iE>

JtoaJtAL ooffnBNiB piscn^^

.B<wwBiq,

UAor

SSlSL

BtolqaMt LABORATORY TESTS JaeM. MMIsiSL 19. UbowtoiylD; AmtjiaeaDMB

EMOtfvily CY«orJto)

SohiUHtyCSm/O

lAin

JS^ LorR

FH:

laronMBTaat pw ociMg

)»faMwrT(BR pworn^

PMornqi

Mflde pMormg OoDftn^qn V<MM» CfmU» PMorsqe

rfiNT AIMER INSFECnON BECOBP

laflfOagnNnm O cmmmmacnnKm

W . •

tyrioinalD CMor • Clarity TbMnaw

iFlDCppin)

BiqiQlioalB

UUKWATORYTBm TMKAI JSmSSL JBSSBLfla. LriwmwylP; AmlyMiDaiK

RMWtfvHy EVaarNo)

SohibiliiyCMPgWl)

iAir

LorH riBb

'MwddBTBat pmornag aridtwrTnit paur ni^

pwornqg

MiMe pMcrms Ganflnnattoii viiMite

poforiMi VHM»

poaorimg

aiOcKlOypm

ltell»|iiUho«9y;

ReoahMdBy;

HIM ItamaadAfllUMton

nnMTAlMPg TOSwecTioyi RECORD

[ XH/A;C4. Uuk , uwl o^ wr4^

ItoCA)

J Uv. iniar

"fy K?HS

IPihpaO Q.Q

V\6fVVJb^

AWMUTOKYTEffTB

tfiMiBy:

Sigmdum RfiHnquUhodBy:

Reeatv^^.

DMe Tbm NnwMMlAflniitkN)

|<IC.W HOC. l-HINJJnWK t-Atjt i!3

ICKAyM 132664/

AyNALFroJwtNnndMr:

"porrtutz UKUNACodc

PnîBctNane/Ueiiilbiu SvfaiTl. Ina StoqSdriot MidugBi MFGffi

CaataiBtf

CanmkalNnne

CowMnw-Typ* CoBtalutrSin Omtaliiar Cratairt (i/4,iy23/4,AilO

TbM

Addidoml binmiBtion

Nim. HtC^

l4o. ̂ Otntaiiicni TapfA)

COimnSNTS OESCUPTtON jCL

Sanplelp >hîcaliState

Color

gaily

Ihlelenea

/AbaratoiylD: 03^5- 02.Z. A AnalysnDae:

Sescdvlv OTecorNo)

Air N M Sescdvlv OTecorNo) Water: N AJ Solubility @/PSA) Water rs Solubility @/PSA)

SblVaii; rL. rr DcMfiy LorH /if |dl;

PamddeTea poa orn^

OxidieerToa posarnag ue^ Haloeens pceorneg FlaneColor.

K/€Cr A/£r<t- •

Sulfide posorneg

Cmiihmaiiin YOMD

Cyanide posorn^ CoBfiftpeiiiDn VMMO UCS- >0gT6-

EBadmoiat poeornog a 1407 ?G»B > lO or < 10 ppm _

Dae Time Name aid AfiBHedon g->l-e3 CfeA

/VSL jwfi-

ClUmAL Pi^ Nanibart 32664/

Prelaat Naaaafl acatliMi; SvbiiL Ino..SitBri)atriot. Mtdrisaii

CoptalaeriiayaatoFy NaiBibar

DOTHAK UM/NACode

MPGNana ChenlealNaaia

CiwtBlaarSlaa ^ owk. <

Cootalacr CoBleat aMî/«3MifMt>

Data Tline Oî06 i Saaqdns Nama

1 Nr Ar«w«w^ 1 1

clayjiJlinK do^ 4(>JL 1

1 ^ ^.Q\ . CXtfL"' 1 NouofGontafaMn ̂

Layer

'CX3NTBNTS DESCRIPTION

TODM) MDddlatB) BotlomifO

SanqrialD

Pbyiical State IwoW; ' Cokr dtixA^ UseJlL Clarity

riikiaieH

nPQipni) o,o .

RiMliatioii

Biolpgleala %

LABORATORY TESTS Top,(A) Middle flit BettonfCI 1

LabontbiylD:

^nalyseaOote:

leaetivity Yea or No)

Air leaetivity Yea or No) Water

olubiKty^fl^) Water olubiKty^fl^)

anatfy LorH

1:

toiddeTest poaorn^

idiaarTeat pdaor iwg i •

iogena po>

me^CoioK

Me posortMR

tfirmation Y<HM6

iMe poBorn^

GtpMtianYMMi

ipohit poaorneg

tOTP • I >10or<10ppm .

Mr

•edBy:

Kftlat qb

labtffML mjed NunriieR VUttiAi

Kn4Mtl<MM/LoeailoR syun, imL SbeflDurioL tfiddum apy

jMirrilAZ MOraKkaw CiwndadNffne

OQ»bdMrTyP« .\ICXL 'ÔJOxxtfJL

'Sso iH-cycw.

No. of OaoHinen fXnnVNTSPBSCRlPIlON BOMKO tmumr TOBMI Mkuiian BOMKO

SmiilBlD

nvcferiSWe L. U Solar wJk. uJiU-U.

My ViWAfx ©feaiairf. • * • iipflniMi

IDCppna) 0.0 0.6 UidMioii iUli.|fr«li.

ABORATOHY TESTS TopfAl AOMIain B0ttami(O

dwnlaiylD'.

mlyaesDtfe! S- 81 17- o3 •BBQVI^ Air «^4 'MOTNO) Wua; «>6^

<liiliiKiy(S(PSS) WiUa: X s <liiliiKiy(S(PSS) S

luity LorH

M.xy ^.D onddeTBU poaor mg ' MCê

idizerTaat paiar n^ HJg*-agun pmoriios neColom

UtTi^ • ^

(Me pesariwK AnooailjhM "ii UlUMSMMl TCVNO

; loe^ci- i 1.

Bkb pocarnv SnautoiY«MB

WfCr

qwnit paaornet 4orp ^ >10iv<1Dp|iin

quUiedQy;

vedJ^

Due Time &'\H-'g3 IfcSQ

3L]±S

NonieaiidAiBIiUjoq e g A

HOC UMNIIMAKK PAGE 47

EE553K lam

rvffl^Naiiilwn ByMlL he, aae«>aitot.MicWgwi_

IDOTHAZ iMFCNnw DHWACa*

Sg,c«fle> mm 11^

pnNkBiv I.

yv<Aftctfei)> W % paeA, AddiiloQdlpfainatian

TfTrm pmlcdNi

OHijis^taa

Ûii. L>ftiJk UAAI^ y>t^

rkkdrcomriMn \ cowiiavTsiwsciarnoN Bo<tam(CI Lnw TenrAt BOddaCn Bo<tam(CI

tanplcID >liM!nl8tRtB u 3alw *7

3«iftr liiclnwn

% jyi

fDOnxB) 'f4ipT**" ioloBicda

ABdRATOHVtBm TopCAl MUduim JBonomlO itoitBiylD: MC. •

odyaaDm: Sr'1703 •

acdvily Air 1

'as or No) Wattn 1

mUKtyCS/PSD Waten s mUKtyCS/PSD fTira zzr ' aai^ LorB u • Sr,o oaddoToO poaorneg > idimTeat poaorov KfS'is'

OBana poaoriMB aaColor: li^ '

^ pos'oriwg finnatiaiiVMNo Atdrtfe

1

aide paeorneg SniiBilan VMAb

KJ^

qioait poBorniBS kietr

• 2;10or<10ppni

Dm ilme

SfLlS J£12. -!St NmnendAflRUstion

^.P,

iMfywIBy;

Kmoutfnfaimaikm Ftitfllt i ^ r TKteWi

CiBior

Chrty

[^y> BMogtoJt UakmATORYTICTS jsm. mmSSL msBUSL UbowtotylD; AlMtsmfDttK

RMwdvlty y«0rNe) Wi

mi laohwte

MiHy LorH H:

•wtMa Tat pw atBci »MlaaarT<t pMomeg

pworiMg Qfe '

itflde pMornqi wflnwrtiiB vwtte

potflrnqi

^Vont potOTiMc

livMlbr:

G^lMi/NAL Pnjeet Nnnaben 32664/

Pnjact NaHu/Locathn: SvbiO; Inaffite/Detriot. MkUxan T-y - •

DOtBAZ MFGNnme ChendealNnnM UM/NACode

MFGNnme ChendealNnnM

ContnlMirT^ Container ShN-^ *

Centdtamr Ckmtent aMkioMA*)

Djrta^ Tlnie ISiunilenNanie

Additional bfiimiatiQii TV . dlac.'^X^

u - "sn -oS Wo. of ContiiiiBra

!£QL Top (A) CONTENTB DBSCRIFTION

MiddkflP BoHomfQ Sample ID JCKi^ •hyaieal Slate t.

Cblor CieJxK Gbrity

thidmeaa

ID fawn) O.Q RwHatioa

VV-Cn^JU

UUBCMtATORY TESTS Top (A) MWdkim BottemfC) LdxwatorylD:

Date: Analyaeal

Wtivity (Yes or No)

Ain Water

Solubility (SA^ Water

>0181^ LorH •H: ennddeT^ poaorneg

widaerTeat poaorneg

alogau poaorncs aue Colon Ifide poeorneg nfiimation Y«Mi

poaornm idbmatian YapMa dipoint poa or l4<yT fa .>10of<l0 ppm

iquiahedBy; »

ivedBy.


PIUMAL nnplcet Noinban >2664/ DCTBAZ PNffllACodc

Pinijwt NaaN/LMatfM:

MFGffmw

CoBtalner Imwntory Nmib«r -nc - m ̂ — Cb«Bdcd;NMM

CMirtidiMrSbi^ Coablmr Coatant a/4,ia,3MiMB)

%M1 AddidonBl Iiiftiniation

TtaM^^'S6 VI in

NaiM Name

t-s rwlaaurtt'•^fcwl

u- - QPix^s^ --^M -aeoaH No.ofCaiitai]ien %. Layer

CONTENTS DRSCdRlPTION TOD/At Mtailla (BD Bottom fC)

SampIelD tk - OHH'5 Kyaical Slate Itpu.'d Oolor CleoA Clarity <yyôû*^

Hiidmew

nD.(ppni) O.C) 0.& Radialion

fwe«#aw|^wnav

IMBOKATORY TESTS Too/AV MUdlefm BattamfC) 1 iLabomlOiylD:

AnalyaaDate:

Reactivity Tea or No)

Air * Reactivity Tea or No) Watte: 1

lolulrility03/PS/I) Water: lolulrility03/PS/I)

lenaity LorH

H:

teoxideTeat poaorneg

udiarTeat poaorneig

liogena posoFneg mwCoion •

MMe pm or nag nffrmaiion YMIMO ttide poaorneg iftRMtonYwmo Apoiitt poa'.orn^ I40ty ^ 2:10or<10|ipin

'^''8>*a6<n ii

MNishedBy: V rl^—^ Date Thne Name and Affiliation m.

vedBy.

dU/NAL miad Nmaban 32664/

Fniaet NaaMAoaatioB; SyUll. Ino. StdDetiiot. Midiigan

DOTHAZ MFGNamo ChanlralNaiM UN/NACoda

MFGNamo ChanlralNaiM

OonMiMtTyiH; . iCoataiMrii^ *

Container Coadnrt

SaaqilenNanM

Additional fiiibiina6<» "iLtK JU^ -UOi •»'5 ( C/<VuZccA ^ Additional fiiibiina6<»

~-in- 0a^ ey.Oil , No.ofCoirtatiMn ( CQIinPBNTS DESCRIPTION

TOD/A^ MIddlenn BottomlO Layer CQIinPBNTS DESCRIPTION

TOD/A^ MIddlenn BottomlO Sample ID Tt-m5-A *Tlc- OH5T5> nqniadState Cotor Clarity rlôjv Thkbieaa nD(ppin) 0.0 o.o Radiation

ILTORY TESTS Top (A) MlddteOn !£L

Amlyiespte: Reaelivity :Y«sorNo)

Air: Wator

ioltibitity(S/PSa) Water:

Hamly LorH

H:

awddeTeat poaornies

wfaerTaat poaor iu^

dogaiM poaornqi nm Colon MWe posornag afirmatian Y<n^ uide poaoFiiig tfimnuion yMffiio

poaoriieg !4<PP f» >IOor<10ppin

Signature utirishedBy:

vedBy:

Date Tiitio NameandAfBiiation

Ul£W

Iic-w HCBL MWiUrWKK PAGE 37

rnwTATNBR INSaWKnÔN RECOIO) ,^^SSSL

mL issa^

MHlnrDv* lS6B3L$Sti6t

cumm CM/moMsnaim

o"^ \HPO ls•^tdÂ. A u. - <ue» At

N6. aroaeiiiiHn \ cowiJMiaipMgapwow 4W/A\ lllllddR<n

Single ID ac t3» IhyiMte L^yJtL L Cdflr Cl<6Ul

Cfarity TUetaKM

]nD(jvnO o.c>. <3.Q

MMMLTORVTBSTS Ta»(A) MMdkrm B0ttMnfO ..JlisnaeiiylD: 3G A •- 24^ AailymOns ^r-v» o3 itanth% ymarWi

AIn kllS-fe- luec. itanth% ymarWi Wite: fc/Ft- iUCT>

loiiUIi^CmaD —• m . . _ TrSm :E: PS loiiUIi^CmaD SM JT

iBMiQr LarB

H; t.s -7,0 •ni^lletf poiornqi Aie^ lAiteirTHt pMvnqi •togaoi pwnraeg nobCdfaR

Wg-^r MtS-fe

awe po»«Mg •dfaniifQnyaMo

•BUB pMornqg iAiBideny«Ab

ApBte PMcirnqg. Mfl* *» 210ar<lQnmi

j^6-

jquUiedBy;

«vedByi

Ibae

xm. .VrntrnrndAmmon

ILIIS) VI O O

LXNWMflKK PAGE 3B

rniWTATOltH INSPECTION IffiCCTTO

AddUaodtaftnDtfiOD

iCI Str BaafleiD)

•WW .-^-7

IViiQdflMta u. Coin VAixtk. -

Ictaiiy [iWckiiaw

iPIPtond oo

UBOKATORYnflTS TapiAl MUdiaan aottmlQ ydmnunylD: s*?. VadyanDMe •

AIn MTA-Yei«r1>(e) Waw: tv^Cr

^4iibDiiy(»Ma^ WMR PS ^4iibDiiy(»Ma^ Sohani: S

loMi^ L«B A/A 8; ^<0 mxideTeak fUorMg KiieTSr

•iitllmi TCK pdavntc l«^6r

8i«m pMorw* nvOBten lOg-ds •

UUci pnornBg ufitlBliua WHO lOE&

Hilda poaoriMB iteMlanYMiD

dvofat paaarties Mcrp n >10ar<iOnim \

atffubin ^diod^r

hn9d%:

NmnndAflOiaien

S£k. S=-!i£3J2eO_

I'K.vy HOC. LHNUMflKK PA6E 39

f^mwTATlCTrP 1WSWECT10N BECOBD

iSSSL-

C3ide

3yi,«lpPwto,lflcMe.

%

ioninliinnw

CMlMr GmrtMC

\HOO MAMMI

AddliinaaMbnnMkm a(^ îosAlc. A%u*^

^ »oAAft

^'of A

. VBW-> i'.

WL m

ALv. CflWUo Ai^ ^PUi

JtetiSL MMSISL \ /

giynyw w

Cokr

civiiy Z \

msL J2£L \sr»Aj

uMKMRATORyrsm jtwawylPi

JSEM. Jii.

MMI»W BoMWBfCa

MR rMo)

VSgs Wateft K>0

5rra.Qyo<& kc, C^'or

AMfly^WaVD

LorH

'F.O oKMeHBit pMarwug Me-6-MhoTm paanram iOe»

peaoriWK aaCrtoR MB pdaariws

lids pworiHS Y«Ma

jOe<5r

ipoiiit poa or nag

' &AO<ir<iOp^

/wf(6r

«dBy; £. P ^ Tbm

i-SS '->39 c^cyK S-'^03 /7Q0i

MAfBIiRtaan g£&

Documents

semspub.epa.gov · 2017. 1. 12. · CONESTOGA-ROVERS & ASSOCIATES 14496 Sheldon Road, Suite #200 Plymouth, Michigan 48170 Telephone: (734)453-5123 Fax: (734)453-5201 …