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FOR INTERNAL USE ONLY Summer Internship Project: Rockperm David Wagenmaker Note: Surfactant names have been edited out; proprietary information

2014 Internship Presentation

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FOR INTERNAL USE ONLY

Summer Internship Project: Rockperm

David Wagenmaker

Note: Surfactant names have been edited out; proprietary information

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Safety Moment

▌ The Importance of hearing protection

Damage is done without noticing

▌ Example from the lab

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About Me

▌ Missouri University of Science and Technology

▌ Petroleum Engineer

▌ Graduate this December

▌ Why I am here- the Shale Boom

“The biggest innovation in energy so far this century has been the development of shale gas and the associated resource known as ‘tight oil.’ Shale energy ranks at the top not only because of its abundance in the United States, but also because of its profound global impact – as events in 2014 will continue to demonstrate.” -Daniel Yergin

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Rockperm Service

▌ Column Flow Test (CFT)

Measures Surfactant effectiveness when exposed to the fracture environment

− Produced Water

− Produced Oil

− Formation Cuttings

− Fracturing Fluid

Process Description

Metrics

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Problems

▌ Test Inconsistency

▌ Orders have slowed down

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Problem Identification

▌ Voids

Large example at right

Could they form within the sediment column, out of view?

▌ Decided to test if modified use of the massager prevented formation

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Diagnosis

▌ Voids caused by massager

Clearly seen when used without sediment (see picture-->)

▌ Voids appear to form within sediment column

Example: column with calculated pore volume of 2.4 mL absorbed 6.5 mL of oil before breakthrough

▌ Solution: see if consistency improves without the massager

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Measuring Consistency

▌ Single Variable Analysis

Use same surfactant, cuttings, fluid, etc.

With massager and without

See if variability improves

▌ AAAAAAAAAA Surfactant used

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Single Variable Analysis Results

▌ With Cuttings

Massager dramatically affected Breakthrough Times

BTT is more consistent without the massager

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Single Variable Analysis Results: 100% Sand

▌ Massager made very little difference

Variation is much larger than the standard “victory” distance

▌ CFT is less reliable with 100% sand

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Single Variable Analysis Results

▌ Displaced Fluid unaffected by massager or sediment composition

▌ Massager affects time, not volume

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Measuring Consistency

▌ Primary analysis method: conduct CFT three times with massager and three times without

10 surfactants

See if ranking changes

▌ Different measurement metrics given, least important first

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First Metric: Breakthrough Time

Unmassaged

Massaged

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Second Metric: Displaced Fluid

Unmassaged

Massaged

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Displaced Fluid: The Numbers

▌ Massager makes little difference

▌ The most consistent Metric

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Third Metric: Displacement Rate

▌ The most important

▌ More consistent than Breakthrough Time, less than Displaced Fluid

▌ Again, better unmassaged

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Displacement Rate: the numbers

▌ No Massager gets the best results

LOSURF 300D won every time without the massager

The “winner” changed with the massager

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Conclusions

▌ Test Consistency, not Accuracy, improved

▌ Rival Surfactant Selection Method: Performance History

Presents long-term challenge to the CFT’s utility

▌ Future: Integration with the Laser-strat test

Take geologic composition, surfactant type (anionic, cationic, nonionic) into account

Travis Honeycutt’s breakout project may enhance the long-term usefulness of this service

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Number One reason to get rid of the massager-

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Questions?