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SEPARATION THEORYFrom basic separation to ALCAP system
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Separation efficiency is proportional
to settling area and inversely to Q
Inlet
Q
W
A
Separation effic iency
100
50
0A
Outlet
Basic separation
Separation effic iency100
50
0Q
4
Q = V Ag
Q = Throughput capacity, m3 /s
vg = Gravitational settling velocity, m/s
A = Settling area (l w), m2
Separation efficiency100
50
0Q
Throughput capacity directly proportional
to settling area and velocity
Inlet
Q
WA
Outlet
Continuous gravity separation
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Basics!
The efficiency of all separating equipmentis a function of:
Flow rate
Settling area
Settling velocity
6
Continuous gravity
separation vessel
Increased efficiency.
Enlarged settling area by
means of buffer plates
Improving the gravity separation vessel
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Separation by density difference
Density ~ 1000 kg/m3Continuous water phase
Oil droplet
Solid particle
Density < 1000 kg/m3
Density > 1000 kg/m3
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Conventional separator
= a TANK
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Conventional separator
With liquid
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With liquid &
solids
Conventional separator
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Separation of liquid & solids
only
What to do in order to getliquid / liquid / solid
separation ??
Conventional separator
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Install baffle
plates
Conventional separator
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Water seal
filled
Conventional separator
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Static separation of oil / water and
solids
Conventional separator
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Static separation with discs
Conventional separator
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Turning the
tank
Conventional separator
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Conventional separator
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Centrifugal Force
Centrifugal force; 1000s of G replacing the static 1 G
Conventional separator
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Feed to separator
Rotation of thetank
Light phase out
Heavy phase out
Gravity Disc
Level Ring
Solids out
Conventional separator= a rotating tank
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2 Basic Separation principles
# 1: SEPARATOR arranged for PURIFICATION
OIL / WATER / SOLIDS INLET
CLEANED OIL OUTLET
WATER OUTLET
SOLIDS /SLUDGE
OUTLET
OIL is cleaned from water and sol ids
Dewatering of oils
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# 2: SEPARATOR arranged for CLARIFICATION
2 Basic Separation principles
OIL / SOLIDS INLET CLEANED OIL OUTLET
SOLIDS / SLUDGE
OUTLET
NOTE !
No Water Outlet
Water Outlet i s Closed
Solids are removed from OIL
Polishing of oils
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2 Basic Separation principles
= Continuous cleaning of oils wi th max. density
991 Kg/m3 / 15oC
= Continuous removal of solids from oils.
Water removal is limited
Dewatering of oils
A Gravity Disc is used to match actual working condit ion,
but it s size is depending on the density of the oil, theseparation temperature and the required flow over the
separator
A Clar if ier Disc is used to seal of f water outlet
Polishing of oils
purifier
clarifier
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Conventional separator applications
Purifier Types for:
Clarifier Types for:
Fuel Oil Cleaning
- Lube Oil Cleaning
Hydraulic Oil Cleaning
Fuel Oil Polishing Hydraulic Oil Polishing
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Some basics!
The oil, water and particles must beimmiscible!
Do not form a stable chemical mixture , like
gin/tonic
There has to be a density differencebetween the oil, water and particles
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More basics!
The efficiency of all separating equipmentis a function of:
Flow rate
Settling area
Settling velocity
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The disc-stack
The disc-stack
Short settling paths, large settling area
Caulk(s) 0,5 - 0,8 mm
The disc stack is the most
important part of theseparator, here the
separation of the dirt
particals takes place.
Should the disc stack
get dirty, or blocked
in some way, the separation
efficiency will be drastically
reduced
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Flow between discs.
Caulk(s) 0,5 - 0,8 mm
The disc-stack
0,5 mm
FLOW
>5000 G
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Flow between discs
The river!n Parabolic velocity profile:
friction close to wall -> lower
velocity
centre of tube -> higher velocity
A pipe.
Between discs
0,5 - 0,8 mm
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1
2
1: G-Forces
2: Flow
Flow between discs
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Flow between discs
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Flow between discs
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Flow between discs
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Basic Separation principles
Purifier bowl
The disc-stack
Sludge
outlet
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Clarifier bowl
- Oil inlet- Clean Oil outlet
- Closed Water
outlet
- Sludge
outlet
Basic Separation principles
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Conventional separator
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Conventional separator:Conventional separator:
The purifierThe purifier
Factors affecting
interface position : 1
Density of oil decrease
Viscosity of oil decrease
Flow rate decrease
Temperature of oil
increase
- Water coming in
oil outlet
- Interface moving
towards centre:
- Water blocking
disc stack
- Risk for
Bad separationBad separation
Gravity disc too small
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Density of oil increase
Viscosity of oil increase
Flow rate increase
Temperature of oil
decrease
Disc stack dirty
- Oil in Water outlet
= broken Water seal
- Interface moving
towards periphery
Risk forBroken WaterBroken Water--sealseal
Conventional separator:Conventional separator:
The purifierThe purifier
Factors affecting
interface position : 2
Gravity disc too big
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How to find right GHow to find right G--disc:disc:
The purifierThe purifier
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Separation Efficiency
Factors effecting separation
Efficiency
40
Separator Filter
Particles < 4 m 65-85 5-10
Cat fines 60-90 ~ 5Iron 40-60 ~ 5
Sodium 40-50 < 5
Average samples from 44 ships during normal operation
source Alfa Laval SMT/F 9402
Separation Efficiency (%)
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Components in oils not effected by Separation
Density
Viscosity
CCAI
Flash point
Pour point
Micro Carbon Residue
Sulphur / Vanadium
Asphalthenes
Separation Efficiency (%)
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Water
Sodium
Aluminium Silicone
Iron
Magnesium
Ash
Calcium
Cat-fines
Components in oils strongly effected by Separation
Separation Efficiency (%)
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Water in separator bowl in general:
In order to get the best possible separation result
- Water must never enter the disc stack !!!
Separation Efficiency (%)
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Conventional separator: The purifier
Purifier optimum interface position: 1
Outside the outer edge of the disc-stack
Inside the outer edge of the top-disc
Separation Efficiency (%)
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Correct gravity disc size
Clean Disc-stack
Maintain following feed conditions:
Constant oil properties = viscosity & density Constant FLOW - rate
Constant TEMPERATURE
Conventional separator: The purifier
Purifier optimum interface position: 2
Separation Efficiency (%)
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Conventional separator: The purifier
Sensitivity of interface position
for Mineral oils in
Marine & Diesel
appl.
Separation Efficiency (%)
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Conventional separator system :
PURIFIER LIMITATIONS
The Gravity Disc
Maximum Density 991 kg/m3
Manual Adjustment
Optimum Separation hard to achieve
Need of qualified attention for optimum
result
Separation Efficiency (%)
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NOTE :
All MAPX type separators and All MOPX / WHPX typeseparators from before 1984/85 have a density limitaround 985 kg / m at 15 C
Water separation with oil densities above this densitylimit will cause problems with this separators whenoperated as purifiers
Separation Efficiency (%)
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Conventional separator system :
OPTIMUM SEPARATION RESULT on HFO
Maximum Density 991 kg/m3
PURIFIER followed by CLARIFIER
Operation in SERIES for optimum separation result
CLARIFIER act as SAFETY NET = POLISHER
CLARIFIER to be discharged at same interval as thepreceding purifier
Separation Efficiency (%)
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Conventional separators:
Density limit = 991 Kg /
m3 / 15 oC
Viscosity l imit = 600 cSt /
50 oC
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ALCAP THEORY
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When the oil crisis of early 70 s happened , refineries
were forced to remove more and more light fractions
from the crude oil.To achieve this , a number of different distillation
methods were developed resulting in a HFO quality that
was to bad for conventional purifiers to clean. The
density of the oil got too high as well as the viscosity and
we were forced to develop better separation techniques.
This resulted in the so called ALCAP system.
Need to develop new type separators:
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ALCAP type separators:
Working principle:
ALCAP means:
A = Alfa
L = laval
C = Clarifier
A = And
P = Purifier
It is a clarifier and a purifier
type separator in one
frame;
Giving the benefits (higher
separation efficiency) of the
clarifier and the water drain
capability of the purifier.
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Working principle benefit.
Before the ALCAP was on the market , the treatment of
HFO was mostly done by means of purifier / clarifier in
series operation.
Meaning:
a purifier to remove the water and the larger dirt particles
from the oil, then this pre-cleaned oil was led to the
clarifier were it was polished( removing the smaller dirt
particles).
With the ALCAP this task is done in just one separator.
ALCAP type separators:
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Working principle benefit
The ALCAP separator is actually a Clarifier , thus the
water removal capacity of the separator is very low as
the water outlet is closed.
In order to solve this we have installed a water drain
valve in the water outlet , thus giving the possibility to
drain out the water when required.
Therefore we could say that the ALCAP is basically aClarifier when in operation , but with the possibility to
remove the water during a temporary purifier function.
(opening the water outlet for a number of seconds)
ALCAP type separators:
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Density limit = 1010 Kg /
m3
/ 15o
CViscosity limit = 700 cSt /
50 oC
ALCAP type separators:
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- FOPX
- MFPX
- LOPX
Older types
- S type separators,
new type
ALCAP separators are:
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Are Always part of an ALCAP system
This System consists of;
- The separator- The control unit
- The transducer in the clean oil outlet
ALCAP type separators:
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SU configuration
ALCAP type separators:
MT : Transducer
PI : Pressure indicator
Pt 4 : Pressure transmitter
Back pressure regulation valve
RV4combined with shut-off
valve V4
Valve V5 in water outlet:
normally closed
Opens on signal from
control unit only
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HANDLING of FUELS
FOPX configuration
ALCAP type separators:
Mt4 : Transducer
PI : Pressure indicator
PS : Pressure sensor
FI : Flow indicator
Valve V5 in water outlet:
normally closed
Opens on signal from
control unit only
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Working principle
The basics of the ALCAP is the continuous supervision
of the cleaned oil quality.
The cleaned oil leaves the separator through the
transducer , this is a sensor that is continuously
measuring the percentage of water in the cleaned oil,
should this get too high , more then 0.2 % , the system
will take action to discharge the water.
This can be done via the drain valve V5 in the water
outlet , or by means of a sludge discharge cycle
ALCAP type separators:
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Working principle
The water content in the oil is measured by comparing
the di electric constant of oil and water.
Oil has a constant of approx. 4-6Water has a constant of approx 90-95
This means that only a little amount of water will
drastically increase the reading of the oil constant and
thus indicates water in the oil.
ALCAP type separators:
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Working principle
When a ALCAP system is started , as soon as oil is being fed into
the bowl , the system takes a reference value of the oil passing
through the transducer .This value is stored in the memory.
As we start with a clean bowl , we have the maximum efficiency
from the separation, so no water should be measured.
During separation , as sludge builds up in the bowl , some of the
water in the bowl will eventually be forced out with the clean oil.
This is measured with the transducer and signalled to the controller,the controller compares this value to the stored reference value and
if the deviation is to large the controller will take action to remove the
water from the bowl.
ALCAP type separators:
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Working principle
The reading of the water amount in the cleaned oil is displayed in
the control system display in the form of picofarad(pF),
The stored reference value is also in pF , the signal that indicates
the increase of water is called the trigger and 100% trigger equals
a water increase of 0,2 %.
As soon as the measured trigger reaches 100% the controller will
take action to remove the water from the bowl , either by draining
through valve V5 or by initiating a sludge discharge cycle.
Should the measured water amount not decrease a alarm is
triggered and the operators will be notified that something is wrong.
ALCAP type separators:
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Sludge
Water
Oil Interface
Bowl
ALCAP type separators:
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Oil inlet
Oil outlet (normally open)
Water outlet (normally closed)
Sludge / solids
outlet
Conditioning and displacement water inlet
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Transducer principle
FOPX / MFPX
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Transducer principle FOPX / MFPX
Stored reference value 0.2 %water in
cleaned oil
Time between discharges ( 30 min.) timer 60 =10
minutes + timer 61 = 20 minutes
Ref. time
Time
Transducer valueAt start up
trigger
range
0%
100 %
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Stored
reference
value
Time between discharges
Time
Transducer value
No 100% trigger
reached
Sludge discharge
sequence starts
No,or low water in the oil
Normal operation
trigger
range
0%
100 %
Timer 60, 10 minutes Timer 61, 20 minutes
Transducer principle FOPX / MFPX
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Stored
reference
value
trigger
range
0%
timer 60 , 10 minutes
Time
Transducer value
Low to normal water in the oil (1)
Normal operation
100 %
Trigger 100%,drain
valve V5 in water
outlet opens
Trigger 80%,drain
valve V5 in water
outlet closes againafter 20 seconds
( valve may stay openfor max. 2 minutes)
Timer 61, 20 minutes
Transducer principle FOPX / MFPX
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Stored
reference
value
trigger
range
0%
timer 60
Time
Transducer valueNormal operation
100 % Trigger 100%,
Sludge discharge
timer 61 , 20 minutes30 minutes
Low to normal water in the oil (2)
Transducer principle FOPX / MFPX
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Stored
reference
value
trigger
range
0%Time
Transducer value
High water in the oil
Normal operation
100 %
Trigger 100%,drain
valve V5 in water
outlet opens
Trigger 80%,drain
valve V5 in water
outlet closes again
after 20 seconds
timer 60 , 10 minutes Timer 61, 20 minutes
Trigger 100%,
Sludge discharge
Transducer principle FOPX / MFPX
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Stored
reference
value
trigger
range
0% Time
Transducer value
Very much water in the oil
Normal operation
100 %
Trigger 100%,drain valve V5 in water outlet opens and
stays open for two minutes, sludge discharge!
Again trigger 100%,drain valve V5 in water outlet opens
and again stays open for two minutes,Alarm A7-1 , feed-
valve in re-circulation
timer 60 , 10 minutes Timer 61, 20 minutes
Transducer principle FOPX / MFPX
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FOPX / MFPX separators
Sludge discharge is based on
TRIGGER
But time takes over
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Transducer principle
SU / SA
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Storedreference
value
trigger
range 0.2%
Time between dischargesRef. time
Time
Transducer value
At start up
Transducer principle SU / SA
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Stored
reference
value
Set time between discharges
Time
Transducer value
Sludge discharge
sequence starts
No,or low water content in the oil
Normal operation on Fuel oil
trigger
range
0%
100 %
Transducer principle SU / SA
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Stored
reference
value
trigger
range
0%
Set time between discharges
Time
Transducer value
Normal water in the oil
100 %
Trigger 100%,drain
valve V5 in water
outlet opens
Trigger 70%,drainvalve V5 in water
outlet closes again
Normal operation on Fuel oil
Transducer principle SU / SA
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Stored
reference
value
trigger
range
0%
Set time between discharges
Time
Transducer value
High water in the oil
100 %
Trigger 100%,drain
valve V5 in wateroutlet opens
Trigger 70%,drain
valve V5 in water
outlet closes again
Sludge discharge
Transducer principle SU / SA
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Stored
reference
value
trigger
range
0%
Set time between discharges
Time
Transducer value
100 %
Trigger 100%,drain
valve V5 in water
outlet opens,trigger
does not drop to 70%
so drain valve
remains open for thepreset time, then
closes for 5 seconds
and opens again forthe other preset
times
Sludge discharge
Much water in the oil
Transducer principle SU / SA
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Storedreference
value
trigger
range
0%
Set time between discharges
Time
Transducer value
100 %
Trigger 100%,drain
valve V5 in water outlet
opens, trigger stays
above 70% until time
for discharge or after
the preset number of
valve openings.
ALARM too high water
content in oil
Very much water in the oil
Transducer principle SU / SA
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SU / SA separators
Sludge discharge is based on
TIME
But trigger takes over
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Summary Continuous monitoring of the cleaned oil
Always optimum protection of the diesel engine
No gravity disc less operator dependent
Self adaptive
Single stage fuel oil treatment
Improved separation performance, ALCAP
always optimum cleaning result
very low oil losses at sludge discharge
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Continuous monitoring of the cleaned oil
Full flow measurement
Variations in dielectric constant are detected
dielectric constant for mineral oil: 2 6
dielectric constant for water : 90-95
Always optimum protection of the diesel engine
Interface control no water or sludge in the cleaning area continuous monitoring of water content
Summary