2 Analytical MP Chromatography

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www.mandel.ca For additional information please email [email protected] or call 1-888-883-3636

The Ultimate in Speed, Versatility, Ruggedness and Reproducibility

The Nexera is the next era in UHPLC. Shimadzu Nexera is a genuine all-around HPLC that enables various types of analysesincluding conventional LC, ultra fast LC and ultra high-pressure LC up to 19,000 psi (130 MPa) without compromising performance

and data quality. The maximized pressure, minimized delay volume and fast injection enable ultra-high speed cycle time along withmaximizing peak capacity. Nexera is the system of choice for a wide variety of applications :

High Speed

High-speed ow-through needle injection, extra-low gradient delay volume combined with the lowest carryover without rinsingenable ultra-high-speed cycle time

High Resolution

Widest pressure/ow range of19,000 psi up to 3mL/min allows for the use of long small-particle columns to maximizepeak capacity

Flexibility and Expandability

Modular design, pre-treatment autosampler, and valve options enable a wide variety of system congurations, including 2D,method development, and applicated systems

Flexible gradient capacity: Single pump, 4 solvent (quaternary) gradient capability

OR Multi-pump gradient capability

Reliability and Dependability

Engineered using the core competencies of Shimadzus experience, Nexera provides superior data quality, robustness, and long-term performance

Shimadzus Next Generation Nexera UHPLC

Nexera flls needs in all analysis felds:

Conventional High speed Ultra - high speed High resolution High temperature with no compromise in data integrity Green LC Multi-dimensional LC


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MANDELChromatography

Prices do not include applicable taxes and are subject to change without notice. Offers cannot be combined with any other promotions.

MANDEL SCIENTIFIC COMPANY INC.

The Shimadzu Prominence HPLC/UFLC achieves an exceptional level of performance in the elds of pharmaceuticals, biochemistry,chemistry, the environment, and food products.

Reliability

Prominence supports ultra-fast liquid chromatography, preparative LC, gel permeation chromatography (GPC), and LC/MS Modular components interact with the precision of an integrated system

Expandability

Prominence Systems can be eld-upgraded to ultrafast (UFLC) or high-pressure (UFLCXR) systems The modular nature of the Prominence Series means it can be congured for anything from a basic academic teaching lab to a

multi-stream high-throughput analysis lab The SIL-20 Rack Changer with Peltier temperature control (4 to 40C), stores and transports up to 12 standard or deep-well

microtiter plates and 1.5mL vials to the Prominence autosampler for a signicant advantage in sample capacity and throughput

System Adaptability:

Prominence Nano LC

Supports high-precision proteome analysis and automated method development systems

Accurate solvent delivery at nano ow rates (1nL/min to 5L/min) with newly-developed nano ow sensor Low solvent consumption with reux ow control system Data reliability through high retention time repeatability High degree of separation utilizing 2-dimensional LC

Prominence Prep LC

The NEW LC-20AP pumps allow you to run Analytical, Semi-prep and Prep scale without changing pump heads. Excellentreproducibility is achieved for all three levels.

Switch between Analytical, Semi Prep and Prep is easy or:

Manual or Automated injections Column switching Fraction collection All of Shimadzus detectors

LC-20AP Pump:

Flow RatePrecision

at 1.0 mL/min, 0.1% RSD or 0.02min SD

at 0.5 to 150 0.17% RSD or 0.02minSD

High-pressureSolvent Delivery

~42 MPa (0.01-100mL/min)

~30MPa (100.01-150mL/min)

RF-20A and RF-20Axs uorescence detectors

Newly designed optical system provides world-leading levels of sensitivity Water Raman S/N ratio > 2000 for RF-20Axs and >1200 for RF-20A Temperature-Controlled Cell results in increased sensitivity High-speed wavelength switching during a run Easy front access to ow cell and lamp to simplify maintenance Fully integrated into a Prominence UFLC or Nexera UHPLC systems Operates stand-alone on any other HPLC system

Prominence HPLC/UFLCHigh Performance Liquid Chromatograph

Genuine High Throughput

Extremely Low Sample Carryover

Hardware Expandability

Software Expandability


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LCMS-2020High speed. High sensitivity. High resolution. High performance.

The new Shimadzu LCMS-2020 is the worlds most sensitive, fastest scanning and fastest polarity-switching quadrupole massspectrometer available, allowing it to handle the fastest small-particle and high efciency columns. When combined with aProminence Ultra-Fast LC (UFLC/UFLCXR), you will achieve the ultimate in separation performance and productivity.

Innovative eatures include:

UFscanning technology (patent pending)

Achieves a mass spectrum measurement speed of 15,000 u/sec, without sacricing sensitivity or resolution

UFswitching technology (patent pending)

Allows switching between positive and negative ion modes in 15 milliseconds, for the most data without peak deterioration in asingle injection

UFsensitivity through Innovative Ion Optics

Newly developed Qarray ion optical system provides superior sensitivity, especially for ultra high-speed analysis Provides 50% to 300% greater sensitivity than any other single quadrupole analyzer Sensitivity increased by over 500% for masses above 1000Improved Flexibility

Easily handles ultra-fast analysis, conventional HPLC and semi-preparative analysis The ESI source can be exchanged with APCI source or with a dual ionization source (DUIS) for simultaneous operation of both ESI

and APCI ionization modes, quickly and without tools Create Fragment Ions using the In-source CID Desolvation line (DL) for sample introduction, can be uninstalled/installed for replacement or cleaning without breaking the vacuum

Sotware

LCMSsolution includes an improveddata browser function to help qualitativeprocessing of multiple data sets

Allows comparing multiple sets of data orconrming impurities by linking to LC orMS data

Manual peak integration canbe conducted on both LC & MSchromatograms simultaneously


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LCMS-IT-TOFIdentify with confidence

The Shimadzu LCMS-IT-TOF mass spectrometer is the most powerful MS available for component identication enabling LC/MSnhigh precision mass analysis. Coupling atmospheric pressure ionization with Ion-Trap (IT) and Time-of-Flight (TOF) technologies,the LCMS-IT-TOF delivers high mass accuracy and high mass resolution (10,000 at 1000 m/z) independent of MS mode.

Applications:

Accelerating Metabolite ID Structural Verication Natural Products/Nutraceuticals Impurities Identication Biomarker Discovery/Identication

A unique tool or component identifcation and characterization studies:

High mass accuracy MSn analysis with constant mass resolution High stability mass calibration Ultra-fast polarity switching

Software tools that take advantage of multiple levels of fragmentation, isotope pattern verication, and unique fragment-ion lteringtechniques to accurately determine the correct formula for unknown components Precise and reliable measurement of trace-level components Highly accurate identication of target analytes Faster analysis times and more efcient workow

Allows more qualitative inormation about a sample to be collected in a single run,

enabling researchers and scientists to:

Elucidate structures of new molecules Identify impurities and contaminants Analyze metabolites and biomarkers to evaluate biological pathways Predict accurate structural details

Obtain high-sensitivity detection of low concentration samples

New Technologies

Compressed Ion Injection (CII) (patented)

Controlled accumulation of ions before they are introduced into the ion trap

Ballistic Ion Extraction (BIE) (patented) combined with the Dual-Stage Reectron

(DSR) (patented)

Achieves faster, more stable, and higher resolution spectra

Temperature Control o the

Flight Tube

Enables extended stability in mass accuracyHigh-speed Ion Polarity

Switching

In only 0.1 sec or less


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Gilson GX-271 Semi-preparative to Preparative HPLCSize, performance, capacity

The GX-271 is the perfect blend of size, performance and capacity that takes up only 23 of linear bench space with a mediumbed capacity. All preparative injection modules feature a continuous ow path design for preparative system ow rates up to200 mL/min. The GX-271 can accommodate injection volumes up to 25 mL with minimal sample waste and carryover. The rinsestation system incorporates a owing jet wash and allows the use of two different rinse solvents for almost zero carryover.

Semi-preparative to preparative pumping solutions

171/172 DAD Detectors

Offer high spectral resolution and remote ow cell capabilities using ber optic technology

prepELS II Detector

Add a prepELS II Detector to any Gilson semi-preparative purication system for detecting impurities and compounds of interestnot found by UV detection alone

Precisely-controlled spray chamber and drift tube temperature with patented Thermo-Split Technology allows for optimization ofthe detector signal whether running gradient or isocratic conditions

Flow Rate Pressure

305/306 Pump 10 L/min - 200 mL/min 8,700 psi (600 bar)

321/322 (H1) Pumps 150 L/min - 15 mL/min 8,700 psi (600 bar)

321/ 322 (H2) Pumps 300 L/min - 30 mL/min 4,300 psi (300 bar)

331/332 Pumps 0.5 - 50 mL/min 8,700 psi (600 bar)

333/334 Pumps 1 - 200 mL/min 3,040 psi (210 bar)

TubeDiameter

GX-281SampleQuantity

GX-271SampleQuantity

10 mm 576 540

13 mm 576 300

15 mm 576 220

16 mm 450 220

17 mm 220

18 mm 420 220

25 mm 180 70

28 mm 162 70

Note: tubes up to 200 mm can be accommodated

GX-281(see p.24) & GX-271

Liquid Handler/ Injector

Bed Capacity


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Gilson GX-281 Preparative HPLC SystemLarge bed capacity

The GX-281 features a large bed capacity that uses only 35 of linear bench space. The revolutionary on-bed GX Prep SolventSystem accommodates sample aspiration and dispense ow rates up to 50 mL/min and volumes ranging from microliters to hundredsof milliliters. The GX-281 offers numerous injection options ranging from Gilsons innovative GX Z-Injection Module, which aspiratessample directly into the valve, to the GX Direct Injection Module that accommodates the largest range of injection volumes available

on the market.GX Z-Injection Module and GX Direct Injection Module

The GX Z-Injection Module allows fast injections with low carryover by aspirating the sample directly into the valve whichdecreases cycle times and reduces sample waste

The GX Direct Injection Module is compatible with both the GX-271 and GX-281 Liquid Handlers Features an innovative injection port design that attaches directly to the injection valve, reducing void volumes and minimizing

carryover associated with calibrated connection tubing

GX Prep Solvent System

The GX Prep Solvent System valve allows for immediate access to ve off -bed solvent reservoirs

Low Mount Fraction Collection

Separate injection and collection pathways eliminate contamination of fractions from the injection process

Automated Column Selection

Increase system exibility and throughput with automatic selection of up to ten different columns to purify a wide range of samplemasses without manual intervention

Gilsons industry-leading preparative HPLC systems are known for their performance, reliability and value.

Gilsons modular system design allows you to combine instruments to fit your specific needs and applications


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Gilson Prep LC/MS Purication SystemIts your chemistry... Make it easy!

Gilson has developed the rst easy-to-use and practical mass-based purication system in the market. The Gilson LC/MS PuricationSystem features complete control within TRILUTION LC utilizing the intuitive graphical user interface.

Mass-based purication has been a growing need in the purication market. While this type of purication can be an intimidatingtechnique for many chemists, Gilson has developed an LC/MS Purication System that is not only easy-to-use, but has one of the

largest mass ranges in the market today.

Features:

Complete integration into TRILUTION LC allows for MS control in software specically designed for purication Auto Tune and integrated calibration vials for positive and negative ion solutions allows the user to quickly optimize the MS High-range, electronically controlled splitter allows for a split ratio up to 1:100,000 for accommodating ow rates up to

200 mL/min Ability to collect based on Full Scan Extracted Mass signal, Full Scan Total Ion signal or SIM signal, with up to three adducts per

channel for the Extracted Mass and SIM signal The source features XYZ adjustments to optimize the spray in relation to the capillary entrance for higher ows and sample

concentrations

Rugged and simple-to-clean design allows cleaning and maintenance to be done without breaking vacuumlimiting down timefrom hours to a few minutes Quick-connect nozzle allows users to have their own probe, preventing any contamination between users Real-time spectrum display of each fraction collected Complete fraction collection control using conditional logic collection, based on up to seven MS channels using AND, OR,

AND/OR logic collection based on Slope or Level values Collect UV and MS signals based on Full Scan and up to seven different target masses


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Gilson PLC 2020 Purication SystemIts your chemistry ... Make it personal!

PLC 2020 Features:

Ability to hold up to four 1 litre solvent reservoirs Download/upload methods and results via USB drive, make sharing information

quick and easy

Run light indicators illuminate the bed during operation, turn off when a run iscomplete and ash if an error has occurred Dual, variable wavelength UV/VIS detection from 190700 nm with interchangeable

ow cell design to accommodate a wide variety of applications Manual injection of up to 5 mL per injection with software-based control of Load and

Inject positions Collect fractions at ow rates up to 100 mL/min Interchangeable pump heads let you decide the optimum ow range for your

application The PLC 2020 Purication Systems easy-to-use, integrated touchscreen controller

removes the need for a dedicated PC and saves space in your lab

Sotware Features:

Real time, graphical gradient modications and real-time sample tracking during run Manual fraction collection functions for Advance and Divert Conditional logic fraction collection based on up to two detector channels using any

combination of Slope and/or Level Auto-Print and Auto-Export of sample reports at the end of a run

The PLC 2020 Purification System is capable of performingmanual injection purification runs from 2100 mL/min with

pressures up to 4,060 psi.

Integrated variable, dual wavelength UV/VIS detection, fractioncollection and touchscreen controller allow the system to be

completely self-contained.

System Overview

Flow Rate 2100 mL/min

Pressure Up to 4060 psi (280 bar) depending on pump head

Detection Dual Variable Wavelength (UV/VIS 190700 nm)

Injection 100 L5 mL

Dimensions (w x d x h) 17 x 23 x 30 in. (42.5 x 57.5 x 75 cm)

Fraction Capacity

Tube Diameter Number ofFractions

13 mm 240

16 mm 132

18 mm 132

20 mLscintillation vials

42

40 mLscintillation vials

42

The instrument features a large capaci ty for fraction collection


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Gilson Fraction Collectors

FC 203B Fraction CollectorCompactThe FC 203B is the perfect compact fraction collector, capable of handling a wide variety ofcollection vessels, including microplates, vials and tubes. The built-in keypad makes setup andoperation simple and efcient. Collect fractions by time, drop or peak, to suit all your

LC applications.

In peak mode, collector monitors a detector signal and identies peaks using either anadaptive-slope algorithm or a specied millivolt threshold

Up to 10 programmable time windows can be added for collecting only what you want, whilediscarding the columns void volume, peaks of no interest and equilibration volumes

Stand-alone instrument with an easy-to-use keypad, or can be controlled through your PC viaTRILUTION Software

Optional 3-way diverter valve prevents contamination of collected fractions Multicolumn adapters for collecting up to 18 separate channels

FC 204 Fraction CollectorLarge bedThe FC 204 is the ideal large-bed fraction collector, capable of handling a wide variety ofcollection vessels, including microplates, vials and tubes. The built-in keypad makes set upand operation simple and efcient. Collect fractions by time, drop or peak, to suit all your LCapplications.

In peak mode, collector monitors a detector signal and identies peaks using either anadaptive-slope algorithm or a specied millivolt threshold

Up to 10 programmable time windows can be added for collecting only what you want, whilediscarding the columns void volume, peaks of no interest and equilibration volumes

Stand-alone instrument with an easy-to-use keypad, or can be controlled through your PC 3-way diverter valve prevents contamination of collected fractions Multicolumn adapters for collecting up to 18 separate channels

prepFC Fraction CollectorPreparativeThe prepFC Fraction Collector is a large capacity, compact footprint fraction collector, ideal for semi-preparative to preparative applications. The instrument features an adjustable tray to accommodatevarious test tubes heights as well as 500 mL and one litre bottles for large volume collection. The prepFC(Ethernet) Fraction Collector features stand-alone keypad control with a Pocket PC running prepFC ControlSoftware. The instrument can be added onto any HPLC system capable of accommodating contact

closures.

Can accommodate two Code 200, four Code 20 or one Code 90 Series Rack(s) Code 90 Series Racks allows for collection into vessels as large as one litre, a distinct advantage over funnels in that it does not

promote contamination issues that can come with collecting into the same funnels and funnel tubes Small footprint with large capacity (w) 19.8 x (d) 15.4 x (h) 13.7, and able to t into almost any size fume hood Allows for tube heights up to 200 mm, optimizing fraction collection Comes standard with a high-ow collection valve for accommodating ow rates up to 200 mL/min Increased X/Y speed decreases time spent moving from tube-to-tube which reduces sample loss Ability to connect up to four fraction collectors, expanding capacity to over 1280 samples prepFC Control Software provides control of all aspects of fraction collection including creating and adding custom racks, setting

parameters, modes and windows, selecting user-dened collection patterns and more


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See More - components and their relative proportions Recover More - fractions from multiple detector signals, reduced risk of

losing sample Complete More - easy to use, intuitive

Simple and Intuitive Interacing

Guides the user and gives status prompts and alerts together with online diagnosticsand network data retrieval

Adjustable single-panel touch screen is simple to navigate and control Fraction tracking is managed by a real-time colour display with peak-to-tube and tray

correlation making it easy to choose the right fractions for workup

Plug-n-Play Interaction

Incorporates automated solid or liquid sample loading, auto-air purge of spentcartridges, and a self-cleaning injection valve

Radio Frequency Identication (RFID) recognizes Reveleris cartridges and autopopulates cartridge, ow rate, and run-time parameters for ideal separations Fraction trays, also equipped with RFID tags and optical sensors, trigger run pausing

upon removal giving continuous access to fractions for post-run analysis

Compact Ergonomic Design

Features a small footprint that ts easily into a standard fume hood 12" tilt screen is fully adjustable to accommodate variable viewing heights and easy access to solvents Cartridges and service panels are conveniently located in the front of the system

Enhanced Solvent Flexibility

Delivers binary gradient functionality with four solvent selection, extended reservoir capacity, and chromophoric solvent capability Solvent management is simplied by automatic waste level and leak detection Simultaneously purge solvent lines for rapid solvent switching Solvent safety features include anti-static solvent lines, cartridge pressure sensing, and auto-ow stop if the collection tray is removed

Reveleris iES Flash System Improves Laboratory Productivity:

The RevealX detection technology independently triggers fraction collection from multiple detectors including UV and ELSD, bott lenecan be reduced or eliminated without reducing the recovery of compounds of interest

Offers improved detection capabilities with the exibility of ash chromatography Cartridge sizes range from 4g to 330g and samples from single milligram to multiple grams can be puried using a single system The Reveleris SRC ash cartridges use Radio Frequency ID (RFID) and higher pressures to improve purication by maximizing system

resolution, sample loading and recovery

Flash system capabilities are now further expanded with the new Reveleris C18 reversed-phase cartridges. The superior packed C18cartridges are inverted on the system to overcome the channelling and voiding that is often problematic in ash RP cartridges

Reveleris Flash Chromatography SystemsSaves time and eliminates guessworkin your purifications!

Included with the system:

- (2) 18 x 150mm Fraction Collection Trays- (1) 3g Adjustable Solid Loader Plunger- (1) 3g Filled Solid Loader- RevealX software control accessed via 12 touchscreen- RFID identication technology for cartridge/fraction tray- 4-Solvent gradient system (200mL/min max owrate and 200psi)- Necessary solvent tubing and lters


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Grace Davisil Chromatographic SilicaHigher performance The newly developed 35 Davisil silica shows improved surface area leading to up to 50% higher loading capacity combined

with 50% less solvent use for pharmaceutical small molecule (


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GC-8AReliable, Compact, Gas ChromatographThe reliable and compact GC-8A is Shimadzus basic gas chromatograph model fordedicated applications:

Economical and simple to use, the GC-8A supports a single detector, manual pressure orow control, on column injection port(s), and analogue output

Isothermal or single temperature ramp program models are available

GC 2010 PlusAchieves higher sensitivity and improves productivityThe GC-2010 Plus enables reliable, high-precision trace analysis with high repeatability, utilizing detectors such as FID and FPD thatfeature best-in-class sensitivity.

In addition, rapid oven cooling and backush technology shorten analysis time greatly for signicant improvements in productivity.

Shimadzus Gas ChromatographsFor over 50 years, Shimadzu has been delivering powerful,customer-focused GC solutionsSince introducing their rst Gas Chromatograph over 50 years ago, Shimadzu has set the standard for GC power, speed andprecision. Today, the GC-2010 Plus is the most powerful gas chromatography system available in the world, while the GC-2014,utilizing the high-end technology of the GC-2010, covers a wide range of applications from capillary to packed column analysis.

Using Shimadzu GC, you can count on faster analysis, reduced downtime, superior reproducibility, excellent stability, andapplication exibility. Most of all, you can be assured you will receive reliable, accurate results quickly.

The GC amily eatures:

Third-generation advanced ow control ideal for high-speed GC applications Digital control of detector gases Patented constant linear velocity

Fast-heating oven with 20 temperature ramps Wide range of detectors Compliant with all regulatory requirements Complete self-diagnostics capability Large LCD window shows the GCs operations graphically Comprehensive support provided by the Mandel QualityCare team

Trace Amount Analysis

A lineup of powerful detectors ensures the highest sensitivity - even for trace amount analysis.

Advanced Flow Technology

New ow-controlling technologies enable higher separation capability and faster anal

Functions to improve analytical efciency and productivity

Rapid oven cooling, backushing technology, gas saver function, etc.


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GC-2014High performance and reliability for capillary andpacked column applications

Shimadzus versatile GC-2014 gas chromatograph offers exceptional performance, value, and ease of use. Ideal for routine analysis,the GC-2014 utilizes the high-end technology of the GC-2010 to cover a wide range of applications from capillary to packed

column analysis.Advanced Flow Control

The GC-2014 has the same proven superior Automatic Flow Control as the GC-2010, resulting in unsurpassed retentiontime reproducibility

Digital control is standard for both capillary and packed columns Manual detector gas control is optional for most detectors on the GC-2014

Detectors

Completely redesigned, they incorporate the GC-2010 detector designs for capillary analyses and the GC-14 detector designs forpacked columns

The TCD unit is ideal for packed column measurements, employing the semi-diffusion cell design used in the TCD-14

The newly designed FPD-2014 takes advantage of the holophotal construction of the FPD-2010 Choose from a full line of detectors: FID, ECD, TCD, FTD (NPD), FPD, PID, PDID, ELCD, or SCD The system is equipped with a detector control system optimized for dual detectors (FID and TCD) and comes standard with auto-

ignition and relight features

Column Oven

By using the GC-2010 control electronics and cooling mechanisms, columnoven performance has been greatly improved

Oven capacity is increased while maintaining a small bench space, with enoughcapacity to accommodate both capillary and packed columns together

Injection Units

The optimum injection mode can be selected from four types ofinjection units

Users can choose from among a dual-packed, split/splitless, single packed,or direct injection unit

Easy Operation

Large LCD Window - shows all of the operation of the GC, including thedata results, temperature prole, and the chromatogram in progress

Intelligent Self-Diagnostics - provides complete self-diagnostics functionalityand complete logging functions, which are compliant with GLP/GMP

requirements Digital Control - Using the electronic ow controller, the column inletpressure, column ow rate, linear velocity and split ratio can be digitally set

Users can easily set carrier gas ow, and can choose between AdvancedPressure Control and low-cost manual ow controllers for the control ofdetector gas


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Congured and tested in Shimadzus System Integration Technology Lab, the system is shipped with proof of performance, QA/QCand a eld test standard.

Gas Chromatographs

The modular GC-2014 Series is the workhorse of the System GC program. Utilizing the high-end technology of the GC-2010 to cover

a wide range of applications from capillary to packed column analysis:

Systems:

Natural Gas and Liquid Natural Gas Analyzers - Systems for the analysis of Natural Gas, LP Gas and Renery Gas including gassamples from overhead and recycle streams:

System GCState-of-the-art performance and features

Natural Gas Analysis System by GPA Method 2261 Natural Gas and Permanent Gas Analysis Extended Natural Gas Analysis by GPA 2286 LP Gas Analysis by GPA 2177

Extended LP Gas Analysis by GPA 2186 Combined LP Gas and Natural Gas System

Fast Renery Gas Analysis Simulated Distillation by Gas Chromatography Detailed Hydrocarbon Analysis (PONA Analysis) Oxygenates in Gasoline

Benzene and Toluene in Gasoline

Ability to hold 4 detectors, 7 heated zones 12 channels of Advanced Pressure Control

16 time programmable relays available Large oven can accommodate many columns

Greenhouse Gas Analysis

Shimadzu has been building GC-based systems to analyzefor Greenhouse gases for 20+ years and have become themarket leader and the instrument of choice for universityand government researchers around the world. Theiranalyzers are ideally suited for addressing the new U.S.Environmental Protection Agency (EPA) Final MandatoryReporting of Greenhouse Gases Rule. In addition tomonitoring/quantifying CO2, Methane and Nitrous Oxide,the systems can be expanded to include the analysis of SF6,

perorochemicals and hydrouorocarbons. Greenhouse and Atmospheric Gas Analyzer Greenhouse Gas Analyzer

Biomass Feedstock Research

The emergence of the Biomass research eld has createda need for analytical tools to analyze reaction andfermentation products. Shimadzu has risen to the task byoffering a custom GC program to meet these needs.

Fuel Cell Gas Analyzer

Transormer Gas Analysis

Shimadzu has been building GC systems for ASTM-3612 for25+ years and pioneered the ASTM Method B Oil Strippersystem which eliminates the use of Mercury or vacuumextraction and have now expanded into building Method Csystems as well.

TOGAS by ASTM-D3612 Method A TOGAS by ASTM-D3612 Method B TOGAS by ASTM-D3612 Method C

Specialty Analyzers

Permanent Gas Analyzer Chlorine Gas Impurities Analyzer

Biouels

Shimadzu builds a variety of analyzers to meet the needs of Biofuel productionplants and research facilities and provide systems for QC analysis of Bioethanoland Biodiesel by ASTM standards.

BioEthanol System BioDiesel by ASTM-D6584


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GCMS-QP2010 UltraUltra fast data collection, ultra sensitive: the ultimate inGCMS performance

Shimadzus new GCMS delivers scan speeds thatno other GCMS can match. With a maximum

of 20,000 amu/s, the speed is double that ofprevious generation models. This extraordinaryperformance is achieved by the patentedAdvanced Scanning Speed Protocol (ASSP),designed by Shimadzu engineers in yoto, Japan.Using this unique technology, a breakthrough inscan speed has been achieved without sacricingsensitivity. Compared to data acquired withoutASSP, the sensitivity for compounds with highmolecular masses is increased by a factor of 5.

SIM/Scan in One Run with Unmatched Data Quality

Using its unique capability of high-speed data acquisition with ASSP (Advance Scanning Speed Protocol), SIM and Scan

measurements in one run in Comprehensive Mode lead to the highest quality results Example: the minimum dwell time for SIM can now be reduced to 1 ms. For the rst time, it is possible in Comprehensive GCto quantify a set of target compounds in SIM mode and at the same time identify other compounds present in the sample inscan mode

Functions to enhance productivity:

New Twin-Line MS system: by connecting two different columns to the MS system it is possible to smoothly acquire applicationdata on different columns without stopping the MS vacuum

The Shimadzu Quick changer system Easy Stop allows the septum and liner to be changed without breaking the vacuum,thereby saving valuable time

The AOC-20 autosampler enables programming of a two-step derivatization pretreatment method, eliminating the need fortedious derivatization prior to loading the autosampler

High-Speed Data Acquisition

Higher resolution of peaks and better identication power for Comprehensive GC (GC X GC) with Quadrapole MS detection

The First Environmentally Friendly GCMS

In compliance with the RoHS regulations of the European Union. In addition, an Ecology mode saves signicant energy, forexample:

In standby mode, energy is reduced by 37% compared with previous GCMS systems When ECO mode is entered, unnecessary power consumption by the GC, MS and PC is automatically eliminated Consumption of carrier gas is also reduced by 60% The Eco mode can be started automatically after analysis, e.g. after completion of nighttime analysis Can save up to 0.6 tons of CO2 per year

GCMSsolution Ver. 2.6 is Now Even Easier to Use

When analyzing ultra-trace component data, it is important to be aware of lower detection limits and to consider the inuenceof interfering components. Therefore, in order to provide more accurate data analysis, such data can now be processed whilecomparing the current analysis to reference data near the lower detection limit or from the analysis of samples with componentsadded. Data can also be compared with external signals, such as from an ECD, FPD, or other GC detector or sniffer, to allow abroader range of data processing applications.


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Utilizing many of the high-end features of theadvanced QP-2010 GCMS , the QP-2010S offershigh throughput and excellent productivity for routineanalysis applications, providing users with an excellentperformance-to-price ratio.

High Sensitivity

Features the same newly designed ion optics as ourbest selling QP-2010

For the highest sensitivity of target compounds andeasy identication of unknowns in the same run

Scan and SIM can be set in one method le

The Optimum or Fast GCMS

Features the fastest quadrupole on the market with its maximum data acquisition frequency of 50 Hz and maximum scan speed of10000 amu/sec

Designed for Fast GC with standard high pressure AFC (Advanced Flow Control) and unique Constant Linear Velocity for optimalchromatographic resolution, reducing retention times drastically

The SIM mode enables monitoring of up to 64 sets of ions with up to 64 ions per set - potentially determining hundreds ofcompounds simultaneously

Time-based Scan and SIM modes with 64 changes in each run maximize exibility and performance

Reliability

Injection systems of the GC-2010 and the mass stability of the QP2010S lead to the highest data reproducibility System check and QA/QC functions that make it easy to work in a GLP/GMP environment Audit trail functions and password-protected user-level assignments

Easy Maintenance

Filaments and lens system are easily accessible through the hinged door at the front of the instrument, making maintenanceprocedures like ion source cleaning an easy task

MSnavigator software shows troubleshooting and maintenance procedures step-by-step in pictures, and automatically givesremedies in case a QA/QC check fails

Flexibility

Direct Inlet - allows users to input samples directly into the ion source at temperatures up to 500C without disconnectingthe chromatograph

Additional Detectors - Ability to add up to three additional detectors (FID, TCD, ECD, FPD, FTD) Libraries - Classical spectrum permits rapid identication of unknowns using several commercial libraries (e.g., NIST, Wiley,

Pesticides, Polymer Additives, etc.), making the QP-2010s ideal for a variety of high-throughput applications Accessories - Choose from a number of accessories, including the AOC-20i/s, AOC-5000, and PY-2020 Pyrolyzer, for sampling

exibility or to create an application-specic system

Sotware:

GCMSsolution Software - Data Acquisition and control, which offers new and innovative solutions to the challenges of high-samplethroughput, instrument control, diverse data handling, and integration with regulatory compliance

GCMS QP-2010SHigh-quality results for routine analysis


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The SRI Family of Compact Gas ChromatographsStandard features of all SRI GC models: Built-in, single channel PeakSimple data system (except for the Model 110) Heavy duty, all-aluminum construction for lightweight durability Easy to read at-a-Glance panel display that reports the status of system heating, pressure, and voltage control zones Electronic Pressure Control (EPC) for all regulated gas pressures. EPC results in enhanced day-to-day reproducibility compared to

mechanical pressure regulators, and allows the carrier gas pressure to be ramped from the data system

Four, ve, or six simultaneous detector capabilitychoose from 16 detector types Two year warranty

Select the model which best fits your needs:

The ull-eatured 8610C & D

The most versatile and popular model. While it is very compact next to comparable laboratory GCs from other manufacturers, it islarge enough and exible enough to perform an amazing variety of applications.

Mounts up to Six Detectors and Five Injectors Ambient to 400 degrees Celsius Temperature Programmable Column Oven Implement virtually any EPA or ASTM method Controls up to 16 heated zones, three gas sampling valves, and seven EPC gas pressures.

Fits easily on a crowded laboratory bench The Model 8610D GC is identical to the 8610C, except that it has dual temperature programmable column ovens Dimensions: 19 wide x 13.5 high x 14.5 deep

Model 310

The smallest GC that still retains the performance of a full-sized laboratory instrument.

Column oven is temperature programmable from ambient to 400C, with unlimited ramps and holds, plus fast cool-down Accommodates capillary or packed 4-inch diameter columns Up to four detectors can be mounted simultaneously with a single On-column, Heated Flash Vapourization, Split/Splitless or

PTV injector All gases are controlled by electronic pressure controllers (EPC), and the carrier pressure is programmable Designed to satisfy the needs of chromatographers who demand the utmost in portability, small size, and high performance, but

whose application does not require gas sampling valves, purge & trap, or multiple injector types

Dimensions: 12.5 wide x 13.5 high x 14.5 deepModel 110

Ultra-compact Chassis can be congured as a stand-alone detector chassis, capable of mounting any combination of up to four detectors Connects to a host GC (SRI or another brand) via a heated transfer line Choose this chassis when you need to add detectors to an existing GC, or want GC detector performance without a

chromatographic separation (total hydrocarbon stream monitoring, etc.); Makes it easy to add detectors even to older units thatare out of production

Dimensions: 8.5 wide x 13.5 high by 14.5 deep Equipped with electronic pressure control (EPC) for each gas An optional, whisper quiet air compressor may be installed to provide air for FID, DELCD, and/or FPD detectors Equipped with analogue signal cable output (0-5V) for connection to your data system, integrator, or strip chart recorder

Model 8610C Chassis


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Chromatograph

PeakSimple SoftwareThe Ultimate in speed, versatility, ruggedness and reproducibility

PeakSimple software has been continuously developed, rened, and improved since 1988 by a dedicated team of workingchromatographers. These chromatographers use the software on a daily basis, and strive to simplify and enhance every aspect ofPeakSimple so our customers will benet. New features are added to PeakSimple several times per year, and the latest version isalways FREE to download online, along with helpful tutorials.

PeakSimple FEATURES:

Most PeakSimple functions are launched from the chromatogram window, and are so user friendly that most operators can produceresults almost immediately. ToolTips makes learning your way around PeakSimple even easierjust hold your mouse cursor over anyicon or checkbox to read the onscreen How-To instructions.

PeakSimple chromatography data systems consist of hardware and software. The hardware is available as a stand-alone data systemfor connection to almost any model GC, HPLC, or CE system. The same hardware is supplied as standard equipment with every SRI

8610C, 8610D, 410, and 310 GC. No hardware is installed in your computer, so a notebook or netbook PC may be used insteadof a full-sized desktop PC. PeakSimple chromatography acquisition and integration software for Windows is provided with each datasystem, and updates are FREE.

The data system hardware comes in two versions:

1) Single channel Model 333 for one detector (USB 2.0 compliant connection to PC)

2) Six channel Model 302 for up to six detectors on 1- 4 instruments (USB 2.0 compliant connection to PC)

3D chromatogram display Built-in FTP Capability Click & Drag Retention Windows Baseline Subtraction Chromatogram Overlay DDE Links Component Tables

Multi-level Calibrations Data Merge across channels Autosampler Queue Batch Reprocessing Built-in Data Validation ...and more!

Pre-congured SRI GCsOptimized for your application

SRI Instruments specializes in custom gas chromatographs, however, they have pre-congured a number of GCs for commonapplications. Pre-congured GCs are designed with inlet systems, detectors and accessories required for a specic application. Thepre-congured GCs are also supplied with an internal data acquisition system and PeakSimple software to control the GC andacquire and analyze the data.

Multiple gas analyzer Greenhouse Gas PCB BTEX

Easy-to-Learn, Easy-to-Use Packed with State-of-the-Art Features Updates are FREE to download Online Built into every SRI 8610, 410, and 310 GC

Available separately for use with most GCs and HPLCs Easy connection to your Windows computer 1 and 6 channel models available USB 2.0 compliant models

Documents

2 Analytical MP Chromatography