1a Testing for Contaminants Final Revised

5/22/2018 1a Testing for Contaminants Final Revised

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Table 1. Pesticides in the Medical Cannabis Industry in California: Initial Survey

Product NamePrimary Active

Ingredient

EPA

Pesticide

TypeManufacturer Product Type CAS# EPA PC

Code Insects Mites Fungi Bacteria OMRI EPA Status

Zero Tolerance

PesticideEssential Oils

(mixed)

Antimicrobial,biochemical,conventional

chemical

Quick TradingCompany

pesticide 57-06-7 004901 20047 Y N N YRegistration

review

Orthene acephate

Conventional

chemical

Whitmire

Microgen pesticide 30560-19-1103301

Y Y N N N

Registration

reviewShuttle O acequinocyl

Conventionalchemical

OHP pesticide 57960-19-7 006329 N Y N N N Registered

Avidavermectin

(B1?)

Antimicrobial,conventional

chemicalSyngenta pesticide 71751-41-2 122804 Y Y N N N Registration

review

Neem Oil azadirachtinBiochemical,conventional

chemicalDyna-Grow pesticide 108168-76-9 121701 Y Y N N N

Registrationreview

K Plus Neem azadirachtinBiochemical,conventional

chemicalOrganica pesticide 108168-76-10 121701 Y Y N N N

Registrationreview

Azamax azadiractinBiochemical,conventional

chemical

GeneralHydroponics

pesticide 108168-76-11 121701 Y Y N N YRegistration

review

Azatrol azadiractinBiochemical,conventional

chemicalGordons pesticide 108168-76-12 121701 Y Y N N Y

Registrationreview

Einstein Oil azadiractinBiochemical,conventional

chemicalpesticide 108168-76-13 121701 Y N N N N Registration

review

Azasol azadiractinBiochemical,conventional

chemicalArborjet pesticide 108168-76-14 121701 Y N N N N Registration

review

Serenade Bacillus subtilisBiochemical,conventional

chemicalAgraquest biofungicide - 006480 N N Y Y Y

Registrationreview

Serenade Max Bacillus subtilisBiochemical,conventional

chemicalAgraquest biofungicide - 006480 N N Y Y Y

Registrationreview

Silica Blast Bacillus subtilisBiochemical,conventional

chemicalBotanicare biofungicide - 006480 N N Y N N

Registrationreview

Safer Caterpillar

KillerBacillus

thuringiensis

Biochemical,conventional

chemicalWoodstream biopesticide 68038-71-1 006400 Y N N N N

Reregistration

Floramite bifenazateConventional

chemicalUniroyalChemical pesticide 149877-41-8 000586 N Y N N N

Registrationreview

Hot Pepper Wax capsaicinBiochemical,conventional

chemical

Hot PepperWax

repellent 404-86-4 070701 N N N N NRegistration

review

Zero Tolerance

Fungicidecinnamon oil Biochemical

Quick TradingCompany

fungicide - 129066 N N Y N N None

SNS 203 clove oil -Sierra Natural

Science pesticide- - Y N N N N None

Earth Tone

Garden Fungicidecopper

octanoateConventional

chemicalEspoma fungicide 20543-04-8 023306 N N Y N N Registered

Mildew Cure cottonseed oilConventional

chemicalSafergro fungicide 8001-29-4 031602 N N Y N Y None

Orange Guard d-limonene


chemical

repellent 138-86-3 079701 N N N N NRegistration

review

Phosphoload daminozideConventional

chemicalpgr 1596-84-5 035101

Registration

reviewTopload daminozide

Conventionalchemical

pgr 1596-84-6 35102 N N N N NRegistration

review

Flower Dragon daminozideConventional

chemicalpgr 1596-84-7 35103 N N N N N

Registrationreview

Insect Dustdiatomaceous

earthConventional

chemicalSt GabrielsOrganics

pesticide 7631-86-9 072605 Y N N N YRegistration

review

Spectracide

Immunoxdiazinon


chemical

SpectrumGroup

pesticide 333-41-5 057801 Y Y Y N NRegistration

review


9/67


Table 1. Pesticides in the Medical Cannabis Industry in California: Initial Survey contd


Ingredient

EPA

Pesticide

TypeManufacturer Product Type CAS#

EPA PC


Basudin diazinonBiochemical,conventional

chemicalCiba pesticide 333-41-6 57802 Y Y Y N N

Registrationreview

Physan 20dimethyl benzyl

ammoniumchloride


chemical

Maril ProductsInc. fungicide

53516-76-0 069104 N N Y Y N Reregistration

Etherel ethephonConventional

chemical Bayer pgr16672-87-0 099801 N N N N N

Registrationreview

Zeal etoxazoleConventional

chemicalValent pesticide 153233-91-1 107091 Y Y N N N Registered

Preclude TR fenoxycarb Biochemical,conventional

chemical

WhitmireMicrogen pesticide 72490-01-8 125301 Y Y N N N

Registrationreview

Garlic Barriergarlic extract

(Oil)


chemical

GarlicResearch Labs

repellent 8000-78-0 128827 N N N N Y Registrationreview

No Powdery

Mildewgeranium oil


chemical

GreenwayNutrients

fungicide 8000-46-2 597500 N N Y N N None

No Spider Mites geranium oilBiochemical,conventional

chemical

GreenwayNutrients

pesticide 8000-46-3 597500 N Y N N N None

Oxidatehydrogendioxide


chemical

BiosafeSystems LLC

fungicide 7722-84-1 000595 N N Y Y N Registrationreview

Hydroxhydrogenperoxide


chemical

Green Planet fungicide 7722-84-2 000595 N N Y Y N Registrationreview

Fungaflor TR imazalilConventional

chemicalWhitmireMicrogen

fungicide 35554-44-0 111901 N N Y N N Reregistration

Advantage imidaclopridAntimicrobial,conventional

chemicalBayer

neonicotinoidpesticide

138261-41-3 129099 Y Y N N NRegistration

review

Merit imidaclopridAntimicrobial,conventional

chemicalBayer

neonicotinoidpesticide


review

Liquid Ladybug lemon grass oil


chemical

ASAPProducts LLC pesticide

8007-02-1 040502 N Y N N NRegistration

review

Eagle 20 myclobutanil n/sDow

Agrosciencesfungicide 88671-89-0 128858 N N Y N N None

Gognats not specified ?HydrodyamicsInternational pesticide

- - Y Y N N N ?

Bushmaster paclobutrazol Conventional

chemicaltriazole pgr 76738-62-0 125601 N N N N N Registration

review

Gravity paclobutrazol Conventional

chemical pgr76738-62-1 125601 N N N N N

Registrationreview

Pure Spray Green petroleum oilAntimicrobial,conventional

chemicalPetro Canada pesticide 8008-20-6 063501 Y Y Y N Y None

OrganocideTM

Plant Doctorphosphoric acid


chemical

OrganicLaboratories

Inc.fungicide 7664-38-2 076001 N N Y N N Registration

review

Green Curepotassium

bicarbonate


chemical

H And IAgritech

fungicide 298-14-6 073508 N N Y N N None

Insect Killing Soappotassium salts

of fatty acids


chemical

Safer Brand pesticide 67701-09-1 079021 Y N N N Y Registrationreview

Total Release

Foggerpropoxurbutoxide


chemicalDoktor Doom pesticide 114-26-1 047802 Y N N N Registration

review

Xclude pyrethrin


chemical

BASF pesticide 8003-34-7 069001 Y Y N N N Registrationreview


10/67


Table 1. Pesticides in the Medical Cannabis Industry in California: Initial Survey contd


Ingredient

EPA

Pesticide

TypeManufacturer Product Type CAS# EPA PC


Spider Mite

Knockoutpyrethrin


chemical

Doktor Doom pesticide 8003-34-7 069001 Y Y N N NRegistration

review

Pro Control Plus pyrethrin

Antimicrobial,

biochemical,conventional

chemical

WhitmireMicrogen pesticide 8003-34-7

69001 Y Y N N N Registrationreview

Garden Insect

Spraypyrethrin


chemical

BonideProducts

pesticide 8003-34-7 69001 Y Y N N NRegistration

review

Earth Tone Insect

Controlpyrethrin


chemical

Espoma pesticide 8003-34-7 69001 Y Y N N NRegistration

review

Don't Bug Me pyrethrins


chemical

Foxfarm pesticide 8003-34-7 69001 Y Y N N NRegistration

review

Spider Mite

Controlrosemary oil


chemical

Sierra Natural

Sciencerepellent 8000-25-7 597700 N N N N N None

SNS 217

Organiciderosemary oil

sesame oil


chemicalConventional

chemical

SIerra NaturalScienceOrganic

LaboratoriesInc.

pesticide

pesticide8000-25-78008-74-0

597700072401

N

YY

YN

YN

NN

YNone

None

Oleotrol M soybean oilBiochemical,conventional

chemical

Natural Forces

LLCfungicide 8001-22-7 031605 N N Y N Y

Registration

review

Fungus Pharm soybean oilBiochemical,conventional

chemical

PharmSolutions

fungicide 8001-22-7 031605 N N Y N NRegistration

review

Monterey Garden

Insect Sprayspinosyn


chemical

Lawn andGarden

Products Incpesticide 131929-60-7 110003 Y N N N Y

Registrationreview

Captain Jacks

Dead Bug Brewspinosyn

Biochemical,

conventionalchemical

BonideProducts pesticide


review

Forbid 4F spiromesifen Conventional

chemical Bayer pesticide 283594-90-1 024875 Y Y N N N Pending

registration

Actinovatestreptomyces

lydicusBiochemical

Natural ForcesLLC

biofungicide - 006327 N N Y N N Registered

Sucrashieldsucrose

octonoateesters


chemical

Natural Forces

LLCpesticide 42922-74-7 035300 Y Y N N Y Registered

Garden Fungicide sulfurAntimicrobial,conventional

chemicalSafer Brand fungicide 7704-34-9 077501 N N Y N Y

Registrationreview

Bonide Sulfur sulfurAntimicrobial,conventional

chemical

BonideProducts fungicide 7704-34-9 077501 N N Y N N

Registrationreview

Earth Tone 3N1 sulfurAntimicrobial,

conventionalchemical

Espoma pesticide 7704-34-9 077501 Y Y Y N NRegistration

review

SNS 244thyme oil

(thymecamphor)

hort. oilsSierra Natural

Science fungicide89-83-8 080402 N N Y N N

Registrationreview

Earth Tone

Insecticidal Soapvegetable oil(sulfonated?)


chemicalEspoma pesticide 61790-19-0 079013 Y Y N N N None

Protek carbendazimAntimicrobial,

conventional

chemical

? cleaner 10605-21-7 128872 N N N N N None

Bang - ? ? pesticide - - Y Y N N N ?SM90 - ? Nutrilife ? - - ?

Nuke Em - ?FS PlantProducts pesticide -

- Y Y Y N N ?

Dr Nodes - ? ? pgr - - N N N N N ?Dr Do Right - ? ? pesticide - - Y N N N N ?

PM Wash - ?NPK

Industries fungicide - - N N Y N N ?

Mighty Wash - ?NPK

Industries cleaner - - N N N N N ?

Power Wash - ?NPK

Industries cleaner - - Y N N N N ?


11/67


Table 2. Pesticides in the Medical Cannabis Industry in California: MSDS and toxicology data.

Product NamePrimary

Active

IngredientForm MSDS pdf

LD50

Oral

mg/kg

LD50

Dermal

mg/kg

LD50

Inhalation

mg/lCarcinogen? Source

Zero Tolerance

Pesticide

EssentialOils

(Mixed)liquid

http://z-tolerance.com/uploads/msds/MSDS_ZT_PESTICI

DE_ReadyToUse_2011.pdf? ? ? n/a -

Orthene acephate liquidhttp://www.americanpest.net/docs/msds/orthene-

msds.pdf500-5000 2000 2-20 Possible npic.orst.edu

Shuttle O acequinocyl liquidhttp://greenhouse.ucdavis.edu/pest/pmsds/Shuttle

%20O.pdf >5000 >2000 >0.84 Not Likely cdpr.ca.gov

Avidavermectin

(B1?)liquid http://www.cdms.net/LDat/mp770018.pdf 10 330-

>2003.5 Weak pmep.cce.cornell.

edu

Neem Oil azadirachtin liquidhttp://www.dyna-

gro.com/Website%20pdf%20Files/MSDS%20Neem%20Oil.pdf

3540->5000 >2000

>2.4 n/a

K Plus Neem azadirachtin liquid

http://www.kellysolutions.com/erenewals/documentsubmit/KellyData%5CID%5Cpesticide%5CMSD

S%5C70191%5C70191-1%5C70191-1_ORGANICA_K+NEEM_INSECTICIDE_FUNGI

CIDE_12_30_2005_1_37_15_PM.pdf

3540->5000 >2000

>2.4 n/a

Azamax azadiractin liquidhttp://generalhydroponics.com/site/gh/docs/prod_

msds/azamax.pdf3540->5000

>2000 >2.4 n/a

Azatrol azadiractin liquid http://www.pbigordon.com/pdfs/Azatrol-MSDS.pdf3540->5000

>2000 >2.4 n/a

Einstein Oil azadiractin liquidhttp://www.hydrofarm.com/downloads/fc/msds%2

0001_32382.jpg3540->5000

>2000 >2.4 n/a

Azasol azadiractin http://www.arborjet.com/msds/AzaSolMSDS.pdf3540->5000

>2000 >2.4 n/a

SerenadeBacillussubtilis

http://www.agraquest.com/docs/labels-msds/SerSoil-MSDS-062110.pdf (Serenade Soil) >5000 >5000 >1.4 n/a agraquest.com

Serenade MaxBacillus

subtilis

liquid http://www.agraquest.com/docs/labels-

msds/SerMax-MSDS-051811.pdf

> 2,000 > 2,000 > 0.63 Not Likely agraquest.com

Silica BlastBacillus

subtilisliquid http://sunlightsupply.s3.amazonaws.com/docume

nts/product/732485_MSDS.pdf> 2,000 > 2,000 > 0.63 Not Likely agraquest.com

Safer

Caterpillar

Killer

Bacillusthuringiensis liquid

http://www.saferbrand.com/resource/MSDS/EN/5160.pdf >5000 >5000 >2.0 Not, per OSHA saferbrand.com

Floramite bifenazate liquidhttp://greenhouse.ucdavis.edu/pest/pmsds/Floram

ite.PDF>5000 >5000 >5.2 Not Likely greenhouse.ucda

vis.eduHot Pepper

Waxcapsaicin liquid http://www.gemplers.com/docs/msds/7253.pdf >2500 n/a n/a Mouse

Zero Tolerance

Fungicidecinnamon oil liquid

http://z-tolerance.com/uploads/msds/MSDS_ZT_FUNGIC

IDE_ReadyToUse_2011.pdf? ? ? n/a z-tolerance.com

SNS 203 clove oil liquidhttp://sierranaturalscience.com/wp-

content/uploads/2012/02/sns203-MSDS1.pdf5000 n/a n/a n/a sierranaturalscien

ce.comEarth Tone

Garden

Fungicide

copperoctanoate

liquid http://espoma.com/p_consumer/pdf/labels/GardenFungicide_MSDS.pdf

>2000 >2000 n/a Not, perOSHA,IARC

espoma.com

Mildew Curecottonseed

oil liquid http://1000bulbs.com/pdf/mildew-cure-msds.pdf>90

mL/kg n/a n/a Not Likelyfscimage.fishersci

. comOrange Guard d-limonene liquid http://1000bulbs.com/pdf/orange-guard-msds.pdf 4400 >5000 n/a Not Likely sciencelab.com

Phosphoload daminozidehttp://www.hydrofarm.com/downloads/fc/DM%20

Phosphoload%20MSDS_21227.pdf 8400 >1600 >147 Probable (EPA)pmep.cce.cornell.

edu

Topload daminozide x 8400 >1601 >148 Probable (EPA)pmep.cce.cornell.

edu

Flower Dragon daminozide x 8400 >1602 >149 Probable (EPA)pmep.cce.cornell.

edu

Insect Dustdiatomaceou

s earth solidhttp://www.domyownpestcontrol.com/msds/Insect

_Dust_msds.pdf n/a n/a n/aProven (human -

IARC) sciencelab.com

Spectracide

Immunoxdiazinon aerosol

http://www.homedepot.com/catalog/pdfImages/a3/a30ac883-2eaf-4486-af3c-9eb589b91e58.pdf 300-400 3600 3.5 Not Likely extoxnet.orst.edu

Basudin diazinon liquid

could only find this "Basudin"http://www.basudin.com/bindex.jsp, emailed

them, choice btwn Basudin 600 EW, 600 EC or10 GR

300 - 400 3600 3.5 Not Likely extoxnet.orst.edu

Physan 20

dimethylbenzyl

ammoniumchloride

liquidhttp://www.physan.com/Resources/MSDS-

Physan%2020.pdf 240 n/a n/a n/a sciencelab.com

Etherel ethephon liquidhttp://www.bayercropscience.com.au/resources/u

ploads/msds/file9067.pdf3400 -4229

139->5000 > 5 No

pmep.cce.cornell.edu

Zeal etoxazole liquid http://www.valent.com/Data/Labels/0268rev3.pdf > 5000 > 5000 > 2.28 Not Likelytoxnet.nlm.nih.go

v

Preclude TR fenoxycarbhttp://florawww.eeb.uconn.edu/msds/preclude_TR

_msds.pdf > 1600 > 5000 > 480 n/apmep.cce.cornell.

edu

Garlic Barrier garlic extract(Oil)liquid http://www.planetnatural.com/wp-content/uploads/garlic-barrier-msds.pdf

850(mouse)

n/a n/a n/a sciencelab.com

No Powdery

Mildewgeranium oil liquid http://sunlightsupply.s3.amazonaws.com/docume

nts/product/739155_MSDS.pdf5000 n/a n/a Not listed:

ACGIH,IARCsunlightsupply.s3.amazonaws.com

No Spider

Mitesgeranium oil liquid http://sunlightsupply.s3.amazonaws.com/docume

nts/product/704765_MSDS.pdf5000 n/a n/a Not listed:

ACGIH,IARCsunlightsupply.s3.amazonaws.com

Oxidatehydrogendioxide

liquid http://bwgs.blob.core.windows.net/docs/OxiDateRTUMSDS.pdf

5000 > 2000 n/a 7540 mg/kg/day(mouse)

toxnet.nlm.nih.gov

Hydroxhydrogenperoxide

liquid In folder 5000 > 2000 n/a 7540 mg/kg/day(mouse)

toxnet.nlm.nih.gov

Fungaflor TR imazalil solidhttp://betterplants.basf.us/products/msds-and-

labels/fungaflor_msds.pdf227 - 343 4200 -

4880n/a extoxnet.orst.edu

Advantage imidacloprid liquidhttp://www.westernu.edu/bin/safety/msds/VET-

MED-VACS/MSDS%20Advantage%20Bayer.pdf450 >5000

>69(aerosol),

>5323(dust)

Not extoxnet.orst.edu


12/67


Table 2. Pesticides in the Medical Cannabis Industry in California: MSDS and toxicology data, contd.

Product NamePrimary

Active

IngredientForm MSDS pdf

LD50

Oral

mg/kg

LD50

Dermal

mg/kg

LD50

Inhalation

mg/l

Carcinogen

?Source

Merit imidacloprid solid http://www.cdms.net/LDat/mp8H8001.pdf (0.3) 450 >5000

>69(aerosol),

>5323(dust)

Not Likely extoxnet.orst.edu

Liquid Ladybug lemon grassoilliquid http://www.arbico-organics.com/downloads/liquid-ladybug-msds.pdf

>5000 n/a n/a Not Likely 57aromas.com

Eagle 20 myclobutanilhttp://www.precisiondallas.com/Images/msds/Eagle%

2020EW.pdf1750 -1800 n/a n/a Not Likely

precisiondallas.com, toxipedia.com

Gognats not specified liquidhttp://sunlightsupply.s3.amazonaws.com/documents/p

roduct/720327_MSDS.pdf? ? ? ?

sunlightsupply.s3.amazonaws.com

Bushmaster paclobutrazol http://www.sunlightsupply.com/docs/Emerald%20Trian

gle/BushMaster%20MSDS.pdf 5346 > 1000 369 n/a cdms.net, epa.gov

Gravity paclobutrazol http://www.sunlightsupply.com/docs/Emerald%20Trian

gle/Gravity%20MSDS.pdf5346 > 1001 369 n/a cdms.net, epa.gov

Pure Spray

Greenpetroleum oil liquid

http://www.treecarescience.com/uploads/Labels/Insecticides/Pure%20Spray%20Green/Pure%20Spray%20G

reen%20MSDS.pdf>5000 >2000 >2500

Not listed:ACGIH,IAR

C

treecarescience.com

OrganocideTM

Plant Doctorphosphoric

acidliquid http://www.homedepot.com/catalog/pdfImages/0d/0d3

a51ec-0ac6-4fe7-b65b-e3516baaef0f.pdf1530 2740 n/a n/a sciencelab.com

Green Curepotassium

bicarbonatesolid

http://www.planetnatural.com/wp-content/uploads/green-cure-msds.pdf

2700 >5000 >2.3 n/a planetnatural.com

Insect Killing

Soap

potassiumsalts of fatty

acidsliquid

http://www.ces.ncsu.edu/fletcher/programs/xmas/pesticides/labels/Safer-insect-killing-soap-rtu-msds.pdf

74000 >5000 >2Not listed:

ACGIH,IARC

ces.ncsu.edu

Total Release

Foggerpropoxurbutoxide

aerosol http://sunlightsupply.s3.amazonaws.com/documents/product/704400_MSDS.pdf

83 - 150 500 n/a No pmep.cce.cornell.edu

Xclude pyrethrin liquid http://www.cdms.net/LDat/mp9II002.pdf200 -

>2600 >2000 > 6000 No

cdms.net,extoxnet.orst.edu,

pmep.cce.cornell.edu

Spider Mite

Knockoutpyrethrin aerosol

http://www.kellysolutions.com/erenewals/documentsubmit/KellyData%5COK%5Cpesticide%5CMSDS%5C7

2804%5C2724-568-72804%5C2724-568-72804_Doktor_Doom_Spider_Mite_Knock_Out_Insecticide_Plant_Spray_F_Tomatoes_and_Vegetables_1_

10_2011_3_38_16_PM.pdf

200 ->2600 >2000 > 6000 No

cdms.net,extoxnet.orst.edu,pmep.cce.cornell.

edu

Pro Control Plus pyrethrin aerosolhttp://www.batzner.com/docs/MSDS-Labels/Pro-

ControlPlusMSDS.pdf200 ->2600 >2000 > 6000 No


edu

Garden Insect

Spraypyrethrin liquid http://www.bonide.com/lbonide/msds/msds857.pdf

200 ->2600 >2000 > 6000 No


edu

Earth Tone

Insect Controlpyrethrin liquid

http://espoma.com/p_dealers/PDF/ETInsectRTU-MSDS.pdf

200 ->2600 >2000 > 6000 No


edu

Don't Bug Me pyrethrins liquidhttp://www.planetnatural.com/wp-

content/uploads/dont-bug-me-msds.pdf 200 ->2600 >2000 > 6000 No


eduSpider Mite

Controlrosemary oil liquid http://sierranaturalscience.com/wp-

content/uploads/2012/02/sns_217-mite-spray.pdf 5000 n/a n/a Not Likely sierranaturalscienc

e.com

SNS 217

Organiciderosemary oilsesame oil

liquidliquid

http://sierranaturalscience.com/wp-content/uploads/2012/02/sns_217-mite-spray.pdf

http://www.organiclabs.com/Images/MSDS/Plant%20Doctor%20MSDS.pdf

5000 n/a n/a Not Likely sierranaturalscience.com

Oleotrol M soybean oil liquidhttp://bwgs.blob.core.windows.net/docs/OleotrolMMS

DS.pdf5000 4000 n/a Not Likely

bwgs.blob.core.windows.net

Fungus Pharm soybean oil liquidhttp://www.justorganics.net.au/justorganics/Assets/FU

NGUS_PHARM_MSDS.pdf 5000 4000 n/a Not Likelybwgs.blob.core.

windows.net Monterey

Garden Insect

Sprayspinosyn liquid

http://www.biconet.com/botanicals/infosheets/MontereySprayMSDS.pdf > 2000 > 5000 > 5.18 No ec.europa.eu

Captain Jacks

Dead Bug Brewspinosyn liquid

http://www.bonide.com/lbonide/msds/msds250.pdf(RTU) > 2000 > 5000 > 5.18 No ec.europa.eu

Forbid 4F spiromesifen liquidhttp://pdf.tirmsdev.com/Web/692/15018/692_15018_M

SDS_English_.pdf?download=true > 2000 > 2000 1.8 No pdf.tirmsdev.com

Actinovatestreptomyces

lydicussolid

http://plantprodmany.compassites.com/?m=product_pdf&u=plantmany&p=products&id=6020001 (SP)

> 5050 > 5050 > 5050 Noplantprodmany.

compassites.com

Sucrashield

sucrose

octonoateesters liquid

http://www.naturalforcesllc.com/PDFs/20071129%20N

aturalForce%20SucraShield%20MSDS.pdf

10080 -

>20000 n/a n/a Not Likely gpo.gov

Garden

Fungicidesulfur liquid

http://www.saferbrand.com/resource/MSDS/EN/5456.pdf >5000 >5000 >5 Not Likely cospl.coalliance.org

Bonide Sulfur sulfur solid http://www.bonide.com/lbonide/msds/msds141.pdf Not Likely cospl.coalliance.org

Earth Tone 3N1 sulfur liquidhttp://espoma.com/p_dealers/PDF/ET3n1RTU_MSDS

.pdf >5000 >5000 n/a Not Likely cospl.coalliance.org

SNS 244thyme oil(thyme

camphor)liquid

http://sierranaturalscience.com/wp-content/uploads/2012/02/sns244-RTU-MSDS-

Final.pdf2840 > 5000 n/a n/a

spectrumchemical.com

Earth Tone

Insecticidal

Soap

vegetable oil(sulfonated?) liquid

http://espoma.com/p_dealers/PDF/ETSoapRTU-MSDS.pdf >5000 >5000 n/a n/a espoma.com

Protek carbendazim liquid http://www.protekchemical.com/sites/default/files/Pro > 15000 > 2000 n/a n/a superway.com


13/67


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#6#%(e'/ .6 4D,4 [email protected] 7$9 #/#2F'/ 89#/.68 @(@F'1) N79


18/67


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22/67


Figure 2. Sample extraction using Bond Elut Kit for QuEChERS

sample preparation. Adapted from Usher and Majors (2012).

Centrifuge 5 min at 5000 rpm

Add internal standard (Triphenyl phosphate)

Vortex 1 min

Add 4g MgSO4 and 1g NaCl

Shake vigourously 1 min

add 10 mL Acetonitrile

Vortex 1 min

Spike sample (as needed)

10 g homogenized sample in 50 mL disposable

centrifuge tube


23/67


Figure 3. Dispersive SPE cleanup for QuEChERS sample preparation.

Adapted from Usher and Majors (2012).

1 mL upper layer from last step in 2 mL centrifuge

tube withb 50 mg primary and secondary amine

sorbent (PSA) and 150 MgSO4

Inject 1.5 L into GC-MS or LC-MS/MS

0.5 ml into sample vial

Centrifuge 5 min

Vortex 30 sec


24/67


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CORESTA Guide No. 1, Jul 2013 (Nota recommended list of CPAs for tobacco, but representative

for analytical residue target as of the ublication date).

Primary Active GRL

2,4,5-T 0.05 2,4,5-T

2,4-D 0.20 2,4-D

Acephate 0.10 Acephate

Acetamiprid 2.50 Acetamiprid

Acibenzolar-S-methyl 5.00 Acibenzolar-S-methyl

Alachlor 0.10 Alachlor

Aldicarb (! ) 0.50sum of Aldicarb, Aldicarb sulfoxide and Aldicarb sulfone,

expressed as Aldicarb

Aldrin + Dieldrin 0.02 Aldrin + Dieldrin

Azinphos-ethyl 0.20 Azinphos-ethyl

Azinphos-methyl 0.30 Azinphos-methyl

Benalaxyl 2.00 Benalaxyl

0.06

Benomyl asum of Benomyl, Carbendazim, and Thiophanate-methyl

expressed as Carbendazim; see Carbendazim

Bifenthrin 2.50 Bifenthrin

Bromophos 0.04 Bromophos

Butralin 5.00 Butralin

Camphechlor (Toxaphene) 0.30 Camphechlor (mixture of chlorinated camphenes)

Captan 0.70 Captan

Carbaryl 0.50 Carbaryl

Carbendazim a 2.00 sum of Benomyl, Carbendazim, and Thiophanate-methyl

Carbofuran (! ) 0.50sum of Carbofuran and 3- Hydroxycarbofuran expressed as

Carbofuran

Chinomethionat 0.10 Chinomethionat

Chlorantraniliprole 10.00 Chlorantraniliprole

Chlordane (! ) 0.10 sum of cis-Chlordane and trans- Chlordane

Chlorfenvinphos (! ) 0.04 sum of (E)-Chlorfenvinphos and (Z)-Chlorfenvinphos

Chlorothalonil 2.00 Chlorothalonil

Chlorpyrifos 0.50 Chlorpyrifos

Chlorpyrifos-methyl 0.20 Chlorpyrifos-methyl

Chlorthal-dimethyl 0.50 Chlorthal-dimethyl

Clomazone 0.20 Clomazone

! ) 2.00

Cyhalothrin (! ) 0.50 Cyhalothrin (sum of all isomers)

Cymoxanil 0.10 Cymoxanil

Cypermethrin (! ) 1.00 Cypermethrin (sum of all isomers)

DBCP 0.05 DBCP (1,2-dibromo-3- chloropropane)

DDT (! ) 0.20sum of o,p'- and p,p'-DDT, o,p'- and p,p'-DDD (TDE), o,p'- and

p,p'-DDE expressed as DDT

Deltamethrin b 1.00 sum of Deltamethrin and Tralomethrin expressed as Deltamethrin

Appendix Table 1. Guidance residue levels (GRLs) for crop protection agents, reproduced from


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Primary Active

Ingredient

GRL

(ppm)Residue definition, Notes

Demeton-S-methyl (!) 0.10 sum of Demeton-S

-methyl, Oxydemeton-methyl (Demeton-S

-methyl sulfoxide) and Demeton-S-methyl sulfone expressed as

Demeton-S-methyl

Diazino 0.10 Diazinon

Dicamba 0.20 Dicamba

Dichlorvosc 0.10 sum of Dichlorvos, Naled and Trichlorfon expressed as Dichlorvos

Dicloran 1.00 Dicloran

Diflubenzuron 0.10 Diflubenzuron

Dimefox 0.01 Dimefox

Dimethoate d 0.05 sum of Dimethoate and Omethoate expressed as Dimethoate

Dimethomorph (!) 2.00 sum of (E)-Dimethomorph and (Z)-Dimethomorph

Dinocap (!) 0.60

sum of Dinocap isomers and 0.60 Dinocap phenols expressed as

Dinocap. Currently, Dinocap isomers expressed as Dinocap (!)

because Dinocap phenols standard is not available. Dinocapphenols should be also expressed as Dinocap (!) when standard

will be available.

Diphenamid 0.05 Diphenamid

Disulfoton (!) 0.10sum of Disulfoton, Disulfoton sulfoxide, and Disulfoton sulfone

expressed as Disulfoton

Dithiocarbamates e

(as CS2)5.00

Dithiocarbamates expressed as CS2. In countries where fungal

diseases such as blue mould are a persistent problem in the field

throughout the growing season, the use of dithiocarbamates (DTC)

fungicides may be an essential part of the season-long disease

management strategy and in keeping with GAP as a means of

ensuring crop quality and economic viability for the producer.

Under high disease pressure residues of dithiocarbamates (DTC)

fungicides slightly in excess of the specified GRL may be

observed. In countries where there is not a field fungal diseaseproblem the use of fungicides is not necessary, and there should

be no

Documents

1a Testing for Contaminants Final Revised