123

11 10 9 8 7 6 5 4 3 2 1 0 ppm0.0005

1.2454

1.9232

2.0563

2.1053

2.2903

2.3234

2.3466

2.3687

2.4170

2.5318

2.7111

2.7668

2.9045

3.2573

3.3097

3.6626

3.6991

3.9869

4.0015

4.8425

6.6517

6.7014

6.9459

6.9637

7.1059

7.1959

7.2158

7.2666

7.2871

7.3061

7.3496

7.3701

7.4011

7.5002

7.5380

7.5933

7.7564

7.7761

7.8521

8.1241

9.9294

-0.11

0.22

1.20

0.91

0.52

0.73

6.46

1.20

1.47

8.93

1.16

0.30

Current Data Parameters

NAME Feb25-2016

EXPNO 310

PROCNO 1

F2 - Acquisition Parameters

Date_ 20160225

Time 23.31

INSTRUM spect

PROBHD 5 mm PABBO BB-

PULPROG zg30

TD 65536

SOLVENT DMSO

NS 8

DS 2

SWH 12019.230 Hz

FIDRES 0.183399 Hz

AQ 2.7263477 sec

RG 128

DW 41.600 usec

DE 6.00 usec

TE 295.9 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

NUC1 1H

P1 10.90 usec

PL1 -3.00 dB

SFO1 400.1324710 MHz

F2 - Processing parameters

SI 32768

SF 400.1299916 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

SIgBRUKER

AVANCE II 400 NMR

Spectrometer

SAIFPanjab University

Chandigarh

[email protected]

5.65.86.06.26.46.66.87.07.27.47.67.88.08.28.4 ppm

6.6517

6.7014

6.9459

6.9637

7.1059

7.1959

7.2158

7.2666

7.2871

7.3061

7.3496

7.3701

7.4011

7.5002

7.5380

7.5933

7.7564

7.7761

7.8521

8.1241

8.93

1.16


NAME Feb25-2016

EXPNO 310

PROCNO 1


Date_ 20160225

Time 23.31

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT DMSO

NS 8

DS 2

SWH 12019.230 Hz

FIDRES 0.183399 Hz

AQ 2.7263477 sec

RG 128

DW 41.600 usec

DE 6.00 usec

TE 295.9 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

NUC1 1H

P1 10.90 usec

PL1 -3.00 dB

SFO1 400.1324710 MHz


SI 32768

SF 400.1299916 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

SIgBRUKER

AVANCE II 400 NMR

Spectrometer


Chandigarh

[email protected]

0.51.01.52.02.53.03.54.04.55.05.5 ppm

1.2454

1.9232

2.0563

2.1053

2.2903

2.3234

2.3466

2.3687

2.4170

2.5318

2.7111

2.7668

2.9045

3.2573

3.3097

3.6626

3.6991

3.9869

4.0015

4.8425

-0.11

0.22

1.20

0.91

0.52

0.73

6.46

1.20

1.47


NAME Feb25-2016

EXPNO 310

PROCNO 1


Date_ 20160225

Time 23.31

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT DMSO

NS 8

DS 2

SWH 12019.230 Hz

FIDRES 0.183399 Hz

AQ 2.7263477 sec

RG 128

DW 41.600 usec

DE 6.00 usec

TE 295.9 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

NUC1 1H

P1 10.90 usec

PL1 -3.00 dB

SFO1 400.1324710 MHz


SI 32768

SF 400.1299916 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

SIgBRUKER

AVANCE II 400 NMR

Spectrometer


Chandigarh

[email protected]

11 10 9 8 7 6 5 4 3 2 1 0 ppm0.7222

0.7783

0.8471

1.0953

1.2396

2.3902

2.5306

2.6790

3.1476

3.5956

3.6077

3.9778

6.6030

6.9140

7.2186

7.3654

7.3932

7.4282

7.4900

7.6504

7.6667

7.7060

8.0342

3.05

1.44

9.96

6.25

4.00


NAME Feb25-2016

EXPNO 320

PROCNO 1


Date_ 20160225

Time 23.36

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT DMSO

NS 8

DS 2

SWH 12019.230 Hz

FIDRES 0.183399 Hz

AQ 2.7263477 sec

RG 144

DW 41.600 usec

DE 6.00 usec

TE 295.9 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

NUC1 1H

P1 10.90 usec

PL1 -3.00 dB

SFO1 400.1324710 MHz


SI 32768

SF 400.1300488 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

S-2dBRUKER

AVANCE II 400 NMR

Spectrometer


Chandigarh

[email protected]

5.56.06.57.07.58.08.59.0 ppm

6.6030

6.9140

7.2186

7.3654

7.3932

7.4282

7.4900

7.6504

7.6667

7.7060

8.0342

6.25

4.00


NAME Feb25-2016

EXPNO 320

PROCNO 1


Date_ 20160225

Time 23.36

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT DMSO

NS 8

DS 2

SWH 12019.230 Hz

FIDRES 0.183399 Hz

AQ 2.7263477 sec

RG 144

DW 41.600 usec

DE 6.00 usec

TE 295.9 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

NUC1 1H

P1 10.90 usec

PL1 -3.00 dB

SFO1 400.1324710 MHz


SI 32768

SF 400.1300488 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

S-2dBRUKER

AVANCE II 400 NMR

Spectrometer


Chandigarh

[email protected]

5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 ppm

0.7222

0.7783

0.8471

1.0953

1.2396

2.3902

2.5306

2.6790

3.1476

3.5956

3.6077

3.9778

3.05

1.44

9.96


NAME Feb25-2016

EXPNO 320

PROCNO 1


Date_ 20160225

Time 23.36

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT DMSO

NS 8

DS 2

SWH 12019.230 Hz

FIDRES 0.183399 Hz

AQ 2.7263477 sec

RG 144

DW 41.600 usec

DE 6.00 usec

TE 295.9 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

NUC1 1H

P1 10.90 usec

PL1 -3.00 dB

SFO1 400.1324710 MHz


SI 32768

SF 400.1300488 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

S-2dBRUKER

AVANCE II 400 NMR

Spectrometer


Chandigarh

[email protected]

11 10 9 8 7 6 5 4 3 2 1 0 ppm

0.0003

1.2447

1.9326

2.0461

2.0944

2.1156

2.5397

2.5433

2.5474

3.8759

6.9488

6.9687

7.1056

7.1292

7.1370

7.1608

7.1674

7.1825

7.1886

7.2146

7.2250

7.2460

7.2595

7.2737

7.2797

7.2903

7.2976

7.3315

7.3536

7.3722

7.3765

7.4043

7.4144

7.4251

7.4368

7.4457

7.4502

7.4625

7.4704

7.4865

7.4955

7.5085

7.5309

7.5383

7.5537

7.5778

7.5879

7.5989

7.6101

7.6212

7.6345

7.6569

7.6638

7.6846

7.7021

7.7333

7.7611

0.20

1.61

2.04

4.26

6.99

2.32

4.48

3.50

8.16

3.67

5.43

2.96

1.20

1.00


NAME Feb25-2016

EXPNO 330

PROCNO 1


Date_ 20160225

Time 23.41

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT DMSO

NS 8

DS 2

SWH 12019.230 Hz

FIDRES 0.183399 Hz

AQ 2.7263477 sec

RG 144

DW 41.600 usec

DE 6.00 usec

TE 296.1 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

NUC1 1H

P1 10.90 usec

PL1 -3.00 dB

SFO1 400.1324710 MHz


SI 32768

SF 400.1299869 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

S3aBRUKER

AVANCE II 400 NMR

Spectrometer


Chandigarh

[email protected]

7.07.58.08.59.09.510.0 ppm

7.2250

7.2460

7.2595

7.2737

7.2797

7.2903

7.2976

7.3315

7.3536

7.3722

7.3765

7.4043

7.4144

7.4251

7.4368

7.4457

7.4502

7.4625

7.4704

7.4865

7.4955

7.5085

7.5309

7.5383

7.5537

7.5778

7.5879

7.5989

7.6101

7.6212

7.6345

7.6569

7.6638

7.6846

7.7021

7.7333

7.7611

7.7746

7.7944

8.0874

9.7512

3.50

8.16

3.67

5.43

2.96

1.20

1.00


NAME Feb25-2016

EXPNO 330

PROCNO 1


Date_ 20160225

Time 23.41

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT DMSO

NS 8

DS 2

SWH 12019.230 Hz

FIDRES 0.183399 Hz

AQ 2.7263477 sec

RG 144

DW 41.600 usec

DE 6.00 usec

TE 296.1 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

NUC1 1H

P1 10.90 usec

PL1 -3.00 dB

SFO1 400.1324710 MHz


SI 32768

SF 400.1299869 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

S3aBRUKER

AVANCE II 400 NMR

Spectrometer


Chandigarh

[email protected]

1.01.52.02.53.03.54.04.55.05.5 ppm

1.2447

1.9326

2.0461

2.0944

2.1156

2.5397

2.5433

2.5474

3.8759

0.20

1.61

2.04

4.26

6.99

2.32

4.48


NAME Feb25-2016

EXPNO 330

PROCNO 1


Date_ 20160225

Time 23.41

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT DMSO

NS 8

DS 2

SWH 12019.230 Hz

FIDRES 0.183399 Hz

AQ 2.7263477 sec

RG 144

DW 41.600 usec

DE 6.00 usec

TE 296.1 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

NUC1 1H

P1 10.90 usec

PL1 -3.00 dB

SFO1 400.1324710 MHz


SI 32768

SF 400.1299869 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

S3aBRUKER

AVANCE II 400 NMR

Spectrometer


Chandigarh

[email protected]

11 10 9 8 7 6 5 4 3 2 1 0 ppm

0.0076

0.8852

1.2558

2.0765

2.5513

3.6116

3.8741

5.0405

7.5022

8.0866

9.9490

10.1865

0.07

0.35

0.99

0.25

3.67

4.00

0.31


NAME Feb25-2016

EXPNO 340

PROCNO 1


Date_ 20160225

Time 23.46

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT DMSO

NS 8

DS 2

SWH 12019.230 Hz

FIDRES 0.183399 Hz

AQ 2.7263477 sec

RG 181

DW 41.600 usec

DE 6.00 usec

TE 296.1 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

NUC1 1H

P1 10.90 usec

PL1 -3.00 dB

SFO1 400.1324710 MHz


SI 32768

SF 400.1299851 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

S$bBRUKER

AVANCE II 400 NMR

Spectrometer


Chandigarh

[email protected]

6.06.57.07.58.08.59.09.510.0 ppm

7.5022

8.0866

9.9490

10.1865

4.00

0.31


NAME Feb25-2016

EXPNO 340

PROCNO 1


Date_ 20160225

Time 23.46

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT DMSO

NS 8

DS 2

SWH 12019.230 Hz

FIDRES 0.183399 Hz

AQ 2.7263477 sec

RG 181

DW 41.600 usec

DE 6.00 usec

TE 296.1 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

NUC1 1H

P1 10.90 usec

PL1 -3.00 dB

SFO1 400.1324710 MHz


SI 32768

SF 400.1299851 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

S$bBRUKER

AVANCE II 400 NMR

Spectrometer


Chandigarh

[email protected]

0.51.01.52.02.53.03.54.04.55.05.5 ppm

0.8852

1.2558

2.0765

2.5513

3.6116

3.8741

5.0405

0.07

0.35

0.99

0.25

3.67


NAME Feb25-2016

EXPNO 340

PROCNO 1


Date_ 20160225

Time 23.46

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT DMSO

NS 8

DS 2

SWH 12019.230 Hz

FIDRES 0.183399 Hz

AQ 2.7263477 sec

RG 181

DW 41.600 usec

DE 6.00 usec

TE 296.1 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

NUC1 1H

P1 10.90 usec

PL1 -3.00 dB

SFO1 400.1324710 MHz


SI 32768

SF 400.1299851 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

S$bBRUKER

AVANCE II 400 NMR

Spectrometer


Chandigarh

[email protected]

Documents

123