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7/24/2019 10. Alum(1)
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Experiment 10 Report Sheet
Synthesis of Alum
Name: Date:
1. Mass of Aluminum used (g)
. Mass of Alum S!nthesi"ed (g)
#. $heoreti%al !ield (g)
&. 'er%ent !ield ()
'ro%edural Notes
1) se a*out +0.,0grams of Aluminum foil not the -x- suare
) /n part / step &: nl! add a*out 101m2 of 34 solution and 5eep it under fume ho
#) After solution is %ooled pla%e mar5 on *ea5er 6ith mar5er or tape.
&) Slo6l! and 7arefull! add onl! 101 m2 of Sulfuri% a%id (4S&) to the 34 solution.
Rea%tion is 8ER9 exothermi% and a lot of heat 6ill *e released.
,) oil Solution gentl! until ;olume rea%hes the mar5 !ou pla%ed on the ilter using ;a%uum ?ltration. Remem*er to pre6eigh !ou ?lter paper. @ash 6ith et
) Dr! in o;en *elo6 B07.
Post Lab Questions
Instructions:'lease do NOTput units on !our ;alues as the units are alread! indi%atenum*er is displa!ed 6ith %orre%t signi?%ant ?gures i.e. 1.#&0 not 1.#&. 9ou ma! need tdigits displa!ed in the %ell using the in%rease or de%rease de%imal *uttons.
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1a. $he Aluminum foil did not %ompletel! rea%t.
1*. Alum sample 6as left in the *ea5er and not transferred to the ?lter paper.
1%. Alum Sample 6as not dried %ompletel! in the o;en.
1) Determine ho6 the follo6ing error 6ould ae%t %al%ulated the per%ent !ield of alum.ee%t). rie
) A pie%e of an aluminum %an 6as %ut into small pie%es. $hen 0.&g of the pie%es froprepare potassium alum a%%ording to the pro%edure used in la*. 4o6 man! grams shoa B#.B !ield (alum M@ F &&.&1gGmol)
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Se%tion:
d.
udents= *e %areful.
anol.
d. 'lease ma5e sure ea%ho adCust the num*er of
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(in%rease= de%rease= no
m the %an 6as used tould !ou expe%t if !ou had