1 Site Description and Background - FRTA – Public ...frta.org/wp-content/uploads/Sandy-Lane-Phase-II-Report.pdf · soil is warranted based on these data, the published the "natural"

F:\P2007\1650\A44\Deliverables\Envl Invest Report_Feb2017__00.docx

78 Interstate DriveWest Springfield, MA

01089t (413) 452-0445

(800) 286-2469f (413) 846-0497

www.FandO.com

Connecticut

Massachusetts

Rhode Island

South Carolina

Figure 1 – Subject SiteRear Turnpike Road

ID: 20-0-27 Book / Page: 1404 200

February 2, 2017Via email

[email protected]. Brett GroutFacilities ManagerFranklin Regional Transit Authority12 Olive StreetGreenfield, Massachusetts 01301

RE: Subsurface InvestigationSandy Lane (Rear Turnpike Road), Montague, MA

Dear Mr. Grout:

This letter outlines the results of the subsurface investigation performed by Fuss & O’Neill,Inc. (Fuss & O'Neill) at the above-referenced property in December 2016.

1 Site Description andBackground

Fuss & O’Neill performed a limitedsubsurface environmental investigation on aportion of the land identified as parcel 20-27within the Town of Montague (″subject site″).The investigation focused on the northernportion of the 24.25 acre parcel. The purposeof the assessment was to evaluate thepresence of oil and/or hazardous material(OHM) within environmental media anddetermine if a reporting condition exists tothe Massachusetts Department ofEnvironmental Protection (MassDEP).

In April 2015 Tighe & Bond completed aPhase I Environmental Site Assessment (Phase IESA) of four parcels including the subjectsite. The other parcels abut parcel 20-27 tothe south and east and are not part of Fuss &O’Neill’s investigation. The Phase I ESA wasprepared for the Franklin Regional Council ofGovernments.

mailto:[email protected]

Mr. Brett GroutFebruary 2, 2017Page 2


Figure 2 – Study Area(limits are approximate)

Overall, the subject parcel includes the Montague Recycling Center. The subsurfaceinvestigation was performed on the northern portion of the parcel and west of the Judd Wireparking lot (see Figure 2). The study area is largely an area of vacant, cleared land with uneventopography. The western perimeter is wooded.

1.1 PreviousEnvironmentalInvestigations

Fuss & O’Neill understand that there have been multiple environmental investigationshistorically performed for the overall area (that is, including the abutting properties).Historical assessment have focused on the Montague Sanitary Landfill (MSL), which is east ofthe subject site, and the "Old Burn Dump" that is located primarily on Parcel 21-0-006 (east-southeast of the study area). These historical assessments were largely performed in thecontext of 310 CMR 19.000, the Massachusetts Solid Waste Facility regulations.

As indicated, a Phase I ESA was prepared inApril 2015 by Tighe & Bond. Based on ourreview of the Phase I ESA, there were nospecific recognized environmental conditions1

associated with the northern portion of thesubject site. However, Tighe & Bond’s reportdid present the following recommendation withthe regard to the overall site:

Due to the ongoing use of the site for wastedisposal and fuel storage a Phase IISubsurface Investigation to determine if aportion of the site has been impacted from theUSTs removed from the Highway Departmentfueling area, the 55-gallon drums, otherstorage located throughout the site. Thesubsurface investigation should include theadvancement of soil borings and monitoringwells and the collection of soil and groundwatersamples for laboratory analysis.

1 recognized environmental condition means … the presence or likely presence of any hazardous substances orpetroleum products in, on, or at a property: (1) due to any release to the environment; (2) under conditionsindicative of a release to the environment; or (3) under conditions that pose a material threat of a future release tothe environment.



Based on this recommendation and the relatively close proximity of the study area to certainareas of concern raised by Tighe &Bond (e.g., 10,000 gallon aboveground fuel storage tanks),Fuss & O’Neill developed a sampling plan for the northern portion of parcel 20-27.

1.2 EnvironmentalReceptorsof StudyArea

Provided herein as Figure 3 is a MassDEP Priority Resource Map developed from MassGISdata layers. The map indicates that the study area is not within a Current Drinking WaterSource Area or a Potential Drinking Water Source Area.

There is an unnamed stream approximately 2,000 feet south of the study area and theConnecticut River is approximately 4,000 feet to the southwest. Based upon the Phase I ESA(and the location of the Connecticut River) groundwater flow at the site is expected to begenerally to the south. This is notable because the solid waste disposal areas as well as the oilstorage tanks and fueling systems are south (downgradient) of the study area.

There are residential properties along Turnpike Road north of the study area. These residentialproperties are within 500 feet.

2 Subsurface InvestigationThe environmental investigation included the following:

· Preliminary site review and mark-outs for utility clearance.

· Performance of shallow subsurface soil borings using Geoprobe™ drilling equipment.

· Installation of a single, temporary groundwater collection point.

· Laboratory analysis of soil samples consistent MassDEP methodologies.

On December 20, 2016, Fuss & O’Neill advanced eight soil borings (B-1 to B-8) at the siteusing a Geoprobe™ operated by our personnel. The approximate boring locations areindicated on Figure 4 that is included in Attachment A. The soil borings were slightly adjustedin the field based on topographic constraints and limitations of Geoprobe™ access.

Initially, each boring was advanced to 20 feet below grade (fbg). Borings B-5 through B-8 wereadvanced to 10 fbg. Refusal was not encountered at any of the borings. Underlying soils werelogged primarily as medium to fine sand.



With the exception of B-4 (located in the cleared area west of the Judd Wire parking lot),groundwater was not encountered in the borings. Groundwater was recorded at approximately17 fbg at B-4, and at this location a temporary groundwater collection point was installed.Copies of Fuss & O’Neill’s borings logs and field notes are included with Attachment A.

During the assessment, soil samples were screened in the field with a photoionization detector(PID) to measure the relative concentrations of total organic vapors (TOVs). In general, soilwas screened at each 5 foot interval along the full depth of the respective borings. PIDscreening is a qualitative means of measuring potential volatiles in the soil. No concentrationsof TOVs were detected in the soil samples collected from the eight borings.

Based on the non-detect of PID readings, a discrete soil sample was generally collected fromthe 2 to 4 fbg interval of the various borings. At boring B-4, the soil sample was collected at15-17 fbg, which is coincident with the depth of where groundwater was recorded.

The eight (8) soil samples and the one groundwater sample were submitted to Con-TestAnalytical Laboratory, Inc. (Con-Test) of East Longmeadow, Massachusetts under chain-of-custody protocol. Soil samples were tested for Volatile Petroleum Hydrocarbons (VPH),Extractable Petroleum Hydrocarbons (EPH), and total metals per method 6010. Thegroundwater sample was tested for EPH and VPH. Analytical testing was performedaccording to the MassDEP Methods, and "Presumptive Certainty" was achieved consistentwith 310 CMR 40. 1056(2)(k). The laboratory report from Con-Test is provided inAttachment B.

3 Evaluation of Analytical ResultsThe soil analytical results from the December 2016 investigation are summarized in Table 1.The results were compared to the Reportable Concentrations established by the MassachusettsContingency Plan (MCP, 310 CMR 40.0000). Based upon 310 CMR 40.0361(a)(1), theapplicable Reporting Category for the site is RCS-1 because the samples were collected within500 feet of residential dwelling.



Concentrations of EPH range hydrocarbons and/or target analytes were detected in soil fromborings B-1, B-2, B-3, B-4, B-7 and B-8, but at levels substantially lower than the applicableRCS-1 Reportable Concentrations. At borings B-5 and B-6, neither EPH range hydrocarbonsnor target compunds were detected in soil above method detection limits.

No concentrations of VPH range hydrocarbons or VPH target compounds were detected inthe eight soil samples.

Certain metals were reported in the various soil sampling results. Again, concentrations werelower than the applicable RCS-1 Reportable Concentrations, and generally consistent withbackground levels of metals – i.e., "natural" soil contaminant levels as established by theMassDEP.

As indicated a single groundwater sample was collected from temporary monitoring TP-04(same location as boring B-4). No detectable levels of EPH or VPH compounds werereported in the sample.

4 ConclusionsLaboratory analytical results of the soil samples collected from the northern portion of parcel20-0-27 showed no exceedances of the applicable RCS-1 Reportable Concentrations.Similarly, the single groundwater sampling point showed no exceedance of RCGW-1 orRCGW-2 reporting criteria. Therefore, no reporting to the MassDEP is required under theMCP (310 CMR 40.0315) based on these results.

If soil in this area is disturbed (excavated) during future site development, then it may be re-used on-site. If soil from the site needs to be moved off-site, then no special handling of thesoil is warranted based on these data, the published the "natural" soil background levels, andMassDEP’s Similar Soils performance standards.



If you have any questions regarding the information presented in this report, please contact meat 413-452-0445. Thank you for this opportunity to assist the Franklin Regional TransitAuthority

Sincerely,

Timothy F. Keane, P.E., LSPAssociate/Project Manager

Attachments: Table 1A – Site Sampling Plan, Boring Logs and Field NotesB – ConTest Analytical Laboratory Report


Table

Table 1SOIL ANALYTICAL DATA SUMMARY

Franklin Regional Transit AuthoritySandy Lane, Montague MA

Sampling LocationReportable Concentrations

(RCs)

Sample ID B-1 B-2 B-3 B-4 B-5 B-6 B-7 B-8F&O Sample # 867161220-01 867161220-02 867161220-03 867161220-04 867161220-05 867161220-06 867161220-07 867161220-08Sampling Date 20-Dec-16 20-Dec-16 20-Dec-16 20-Dec-16 20-Dec-16 20-Dec-16 20-Dec-16 20-Dec-16 RCS-1 RCS-2

Sample Depth (feet) 2-4 2-4 2-4 17 2-4 2-4 2-4 2-4Units

Extractable Petroleum Hydrocarbons (EPH)C9-C18 Aliphatics mg/Kg <10 <11 11 <11 <10 <11 23 <21 1000 3000C19-C36 Aliphatics mg/Kg 33 23 75 <11 <10 <11 100 61 3000 5000C11-C22 Aromatics mg/Kg 30 18 73 14 <10 <11 70 47 1000 3000

EPH Target AnalytesAcenaphthene mg/Kg <0.10 <0.11 0.25 <0.11 <0.10 <0.11 <0.11 <0.21 4 3000Acenaphthylene mg/Kg <0.10 <0.11 <0.11 <0.11 <0.10 <0.11 <0.11 <0.21 1 10Anthracene mg/Kg <0.10 <0.11 0.52 <0.11 <0.10 <0.11 <0.11 <0.21 1000 3000Benzo(a)anthracene mg/Kg 0.49 <0.11 1.1 <0.11 <0.10 <0.11 0.16 <0.21 7 40Benzo(a)pyrene mg/Kg 0.55 <0.11 1.2 <0.11 <0.10 <0.11 0.21 <0.21 2 7Benzo(b)fluoranthene mg/Kg 0.86 <0.11 1.4 <0.11 <0.10 <0.11 0.21 <0.21 7 40Benzo(g,h,i)perylene mg/Kg 0.38 <0.11 0.75 <0.11 <0.10 <0.11 0.14 <0.21 1000 3000Benzo(k)fluoranthene mg/Kg 0.31 <0.11 0.51 <0.11 <0.10 <0.11 <0.11 <0.21 70 400Chrysene mg/Kg 0.78 <0.11 1.3 <0.11 <0.10 <0.11 0.26 <0.21 70 400Dibenz(a,h)anthracene mg/Kg <0.10 <0.11 0.19 <0.11 <0.10 <0.11 <0.11 <0.21 0.7 4Fluoranthene mg/Kg 1.5 0.17 2.5 <0.11 <0.10 <0.11 0.25 <0.21 1000 3000Fluorene mg/Kg <0.10 <0.11 0.28 <0.11 <0.10 <0.11 <0.11 <0.21 1000 3000Indeno(1,2,3-cd)pyrene mg/Kg 0.41 <0.11 0.71 <0.11 <0.10 <0.11 <0.11 <0.21 7 402-Methylnaphthalene mg/Kg <0.10 <0.11 0.11 <0.11 <0.10 <0.11 <0.11 <0.21 0.7 80Naphthalene mg/Kg <0.10 <0.11 0.19 <0.11 <0.10 <0.11 <0.11 <0.21 4 20Phenanthrene mg/Kg 0.44 <0.11 2.3 <0.11 <0.10 <0.11 0.13 <0.21 10 1000Pyrene mg/Kg 1.4 0.18 2.6 <0.11 <0.10 <0.11 0.28 <0.21 1000 3000

Volatile Petroleum Hydrocarbons (VPH)C5-C8 Aliphatics mg/Kg <11 <12 <11 <9.9 <9.4 <12 <11 <9.7 100 500C9-C12 Aliphatics mg/Kg <11 <12 <11 <9.9 <9.4 <12 <11 <9.7 1000 3000C9-C10 Aromatics mg/Kg <11 <12 <11 <9.9 <9.4 <12 <11 <9.7 100 500

VPH Target AnalytesBenzene mg/Kg <0.054 <0.062 <0.054 <0.050 <0.047 <0.058 <0.054 <0.049 2 200Ethylbenzene mg/Kg <0.054 <0.062 <0.054 <0.050 <0.047 <0.058 <0.054 <0.049 40 1000Methyl tert-Butyl Ether (MTBE) mg/Kg <0.054 <0.062 <0.054 <0.050 <0.047 <0.058 <0.054 <0.049 0.1 100Naphthalene mg/Kg <0.27 <0.31 <0.27 <0.25 <0.23 <0.29 <0.27 <0.24 4 20Toluene mg/Kg <0.054 <0.062 <0.054 <0.050 <0.047 <0.058 <0.054 <0.049 30 1000m+p Xylene mg/Kg <0.11 <0.12 <0.11 <0.099 <0.094 <0.12 <0.11 <0.097 100 100o-Xylene mg/Kg <0.054 <0.062 <0.054 <0.050 <0.047 <0.058 <0.054 <0.049 100 100

F:\P2007\1650\A44\Soil Sampling Summary 12-20-2016.xls 1 of 2

Table 1SOIL ANALYTICAL DATA SUMMARY

Franklin Regional Transit AuthoritySandy Lane, Montague MA

Sampling LocationReportable Concentrations

(RCs)

Sample ID B-1 B-2 B-3 B-4 B-5 B-6 B-7 B-8F&O Sample # 867161220-01 867161220-02 867161220-03 867161220-04 867161220-05 867161220-06 867161220-07 867161220-08Sampling Date 20-Dec-16 20-Dec-16 20-Dec-16 20-Dec-16 20-Dec-16 20-Dec-16 20-Dec-16 20-Dec-16 RCS-1 RCS-2

Sample Depth (feet) 2-4 2-4 2-4 17 2-4 2-4 2-4 2-4

Metals Analyses (Total)Antimony mg/Kg <2.5 <2.8 <2.7 <2.7 <2.6 <2.7 <2.7 <2.5 1000 3000Arsenic mg/Kg <2.5 <2.8 <2.7 <2.7 <2.6 <2.7 3.2 2.7 20 20Barium mg/Kg 15 53 35 11 7.7 13 57 18 1000 3000Beryllium mg/Kg <0.25 <0.28 <0.27 <0.27 <0.26 <0.27 <0.27 <0.25 90 200Cadmium mg/Kg 0.34 0.47 0.55 <0.27 <0.26 <0.27 0.51 0.36 70 100Chromium mg/Kg 9.2 11 9.7 4.2 3.7 4.2 16 11 1000 3000Lead mg/Kg 14 39 87 2 1.6 4.2 44 5.5 200 600Nickel mg/Kg 7.5 8.4 14 3.4 3.2 3.4 14 10 600 1000Selenium mg/Kg <5.0 <5.5 <5.4 <5.4 <5.1 <5.4 <5.3 <5.0 400 700Silver mg/Kg 0.53 0.9 0.94 <0.54 <0.51 <0.54 1.3 1 100 200Thallium mg/Kg <2.5 <2.8 <2.7 <2.7 <2.6 <2.7 <2.7 <2.5 8 60Vanadium mg/Kg 14 17 15 6.8 6.4 8.8 25 21 400 700Zinc mg/Kg 25 54 71 9.1 8.5 9.9 65 30 1000 3000

NOTES:1. < symbol indicates not detected above the lab reporting limits.2. Reportable Concentration based upon 310 CMR 40.0360 through 40.0369 and as listed at 310 CMR 40.1600

F:\P2007\1650\A44\Soil Sampling Summary 12-20-2016.xls 2 of 2


Attachment A

Site Sampling Plan, Boring Logs and Field Notes

F:\P2007\1650\A44\Sampling Plan Figure 4.docx

LEGEND

B-#, Boring/ Soil Sampling LocationTP-#, Groundwater Sampling Location

Note: Sampling locations are approximate and basedon field measurements.

FIGURE 4

Franklin Regional Transit AuthoritySITE SAMPLING PLAN

Subsurface InvestigationSandy Ln (Rear Turnpike Rd) Montague, MA

Proj. No.: 20001650.A44 DATE: Feb. 2017 SCALE: NTS

B-1

B-2

B-3

B-4

B-5

B-6

B-7

B-8

TP-04


Attachment B

Con-Test Analytical Laboratory Report

39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332

January 3, 2017

Tim Keane

Fuss & O'Neill - West Springfield

78 Interstate Drive

West Springfield, MA 01089

Project Location: Montague, MA

Client Job Number:

Project Number: 20071650.A44

Laboratory Work Order Number: 16L1026

Enclosed are results of analyses for samples received by the laboratory on December 21, 2016. If you have any questions

concerning this report, please feel free to contact me.

Sincerely,

Lisa A. Worthington

Project Manager

Page 1 of 62

Table of Contents

Table of Contents

Sample Summary 4

Case Narrative 5

Sample Results 6

16L1026-01 6

16L1026-02 10

16L1026-03 14

16L1026-04 18

16L1026-05 22

16L1026-06 26

16L1026-07 30

16L1026-08 34

16L1026-09 38

16L1026-10 40

Sample Preparation Information 41

QC Data 43

Petroleum Hydrocarbons Analyses - EPH 43

B166718 43

B166933 46

Petroleum Hydrocarbons Analyses - VPH 49

B166442 49

B166444 50

Metals Analyses (Total) 52

B166431 52

Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) 54

B166688 54

Page 2 of 62

Table of Contents

Table of Contents (continued)

Flag/Qualifier Summary 55

Certifications 56

Chain of Custody/Sample Receipt 59

Page 3 of 62

Table of Contents


ANALYTICAL SUMMARY

1/3/2017

Fuss & O'Neill - West Springfield

78 Interstate Drive

West Springfield, MA 01089

ATTN: Tim Keane

20071650.A44

16L1026

The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.

PROJECT LOCATION:

PURCHASE ORDER NUMBER:

PROJECT NUMBER:

REPORT DATE:

WORK ORDER NUMBER:

FIELD SAMPLE # LAB ID: MATRIX TESTSAMPLE DESCRIPTION SUB LAB

Montague, MA

867161220-01 16L1026-01 Soil MADEP-EPH-04-1.1

MADEP-VPH-04-1.1

SM 2540G

SW-846 6010C-D

867161220-02 16L1026-02 Soil MADEP-EPH-04-1.1

MADEP-VPH-04-1.1

SM 2540G

SW-846 6010C-D

867161220-03 16L1026-03 Soil MADEP-EPH-04-1.1

MADEP-VPH-04-1.1

SM 2540G

SW-846 6010C-D

867161220-04 16L1026-04 Soil MADEP-EPH-04-1.1

MADEP-VPH-04-1.1

SM 2540G

SW-846 6010C-D

867161220-05 16L1026-05 Soil MADEP-EPH-04-1.1

MADEP-VPH-04-1.1

SM 2540G

SW-846 6010C-D

867161220-06 16L1026-06 Soil MADEP-EPH-04-1.1

MADEP-VPH-04-1.1

SM 2540G

SW-846 6010C-D

867161220-07 16L1026-07 Soil MADEP-EPH-04-1.1

MADEP-VPH-04-1.1

SM 2540G

SW-846 6010C-D

867161220-08 16L1026-08 Soil MADEP-EPH-04-1.1

MADEP-VPH-04-1.1

SM 2540G

SW-846 6010C-D

867161220-101 16L1026-09 Ground Water MADEP-EPH-04-1.1

MADEP-VPH-04-1.1

867161220-09 16L1026-10 Trip Blank Water MADEP-VPH-04-1.1

[TOC_1]Sample Summary[TOC]

Page 4 of 62

Table of Contents


CASE NARRATIVE SUMMARY

All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.

For method 6010, only a select list of metals was requested and reported.

[TOC_1]Case Narrative[TOC]

MADEP-EPH-04-1.1

Qualifications:

Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the two MS/MSD results is

within method specified criteria.Analyte & Samples(s) Qualified:

MS-22

C19-C36 Aliphatics

B166718-MS1

MADEP-EPH-04-1.1

SPE cartridge contamination with non-petroleum compounds, if present, is verified by GC/MS in each method blank per extraction batch and excluded from C11-C22 aromatic

range fraction in all samples in the batch. No significant modifications were made to the method.

MADEP-VPH-04-1.1

No significant modifications were made to the method. All VPH samples were received preserved properly at pH <2 in the proper containers as specified on the chain-of-custody

form unless specified in this narrative.

No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely

covered by methanol in the proper containers specified on the chain-of-custody form unless specified in this narrative.

SW-846 6010C/D SW-846 6020A/B

For NC, Metals methods SW-846 6010D and SW-846 6020B are followed, and for all other states methods SW-846 6010C and SW-846 6020A are followed.

The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.

I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed

in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the

best of my knowledge and belief, accurate and complete.

Lisa A. Worthington

Project Manager

Page 5 of 62

Table of Contents


Date Received: 12/21/2016

Work Order: 16L1026Sample Description:Project Location: Montague, MA

Sample ID: 16L1026-01

Field Sample #: 867161220-01

Sample Matrix: Soil

Sampled: 12/20/2016 10:50

[TOC_2]16L1026-01[TOC]

AnalystAnalyzedDilution Flag/QualRLResultsAnalyte

Date/Time

Units

Date

PreparedMethod

Petroleum Hydrocarbons Analyses - EPH

ND 10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11C9-C18 Aliphatics

33 10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11C19-C36 Aliphatics

37 10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics

30 10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11C11-C22 Aromatics

ND 0.10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Acenaphthene

ND 0.10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Acenaphthylene

ND 0.10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Anthracene

0.49 0.10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Benzo(a)anthracene

0.55 0.10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Benzo(a)pyrene

0.86 0.10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Benzo(b)fluoranthene

0.38 0.10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Benzo(g,h,i)perylene

0.31 0.10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Benzo(k)fluoranthene

0.78 0.10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Chrysene

ND 0.10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Dibenz(a,h)anthracene

1.5 0.10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Fluoranthene

ND 0.10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Fluorene

0.41 0.10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Indeno(1,2,3-cd)pyrene

ND 0.10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.112-Methylnaphthalene

ND 0.10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Naphthalene

0.44 0.10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Phenanthrene

1.4 0.10 12/28/16 17:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Pyrene

Surrogates % Recovery Recovery Limits Flag/Qual

Chlorooctadecane (COD) 48.4 12/28/16 17:4340-140

o-Terphenyl (OTP) 59.4 12/28/16 17:4340-140

2-Bromonaphthalene 75.1 12/28/16 17:4340-140

2-Fluorobiphenyl 85.8 12/28/16 17:4340-140

[TOC_1]Sample Results[TOC]

Page 6 of 62

Table of Contents

tkeane

Typewriter

B-1





Field Sample #: 867161220-01

Sample Matrix: Soil

Sampled: 12/20/2016 10:50


Date/Time

Units

Date

PreparedMethod

Soil/Methanol Preservation Ratio: 0.99

Petroleum Hydrocarbons Analyses - VPH

ND 11 12/22/16 23:24 EEHmg/Kg dry 12/22/16MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics

ND 11 12/22/16 23:24 EEHmg/Kg dry 12/22/16MADEP-VPH-04-1.11C5-C8 Aliphatics



ND 11 12/22/16 23:24 EEHmg/Kg dry 12/22/16MADEP-VPH-04-1.11C9-C10 Aromatics

ND 0.054 12/22/16 23:24 EEHmg/Kg dry 12/22/16MADEP-VPH-04-1.11Benzene

ND 0.054 12/22/16 23:24 EEHmg/Kg dry 12/22/16MADEP-VPH-04-1.11Ethylbenzene

ND 0.054 12/22/16 23:24 EEHmg/Kg dry 12/22/16MADEP-VPH-04-1.11Methyl tert-Butyl Ether (MTBE)

ND 0.27 12/22/16 23:24 EEHmg/Kg dry 12/22/16MADEP-VPH-04-1.11Naphthalene

ND 0.054 12/22/16 23:24 EEHmg/Kg dry 12/22/16MADEP-VPH-04-1.11Toluene

ND 0.11 12/22/16 23:24 EEHmg/Kg dry 12/22/16MADEP-VPH-04-1.11m+p Xylene

ND 0.054 12/22/16 23:24 EEHmg/Kg dry 12/22/16MADEP-VPH-04-1.11o-Xylene


2,5-Dibromotoluene (FID) 77.6 12/22/16 23:2470-130

2,5-Dibromotoluene (PID) 74.9 12/22/16 23:2470-130

Page 7 of 62

Table of Contents





Field Sample #: 867161220-01

Sample Matrix: Soil

Sampled: 12/20/2016 10:50


Date/Time

Units

Date

PreparedMethod

Metals Analyses (Total)

ND 2.5 12/23/16 22:01 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Antimony

ND 2.5 12/23/16 22:01 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Arsenic

15 2.5 12/23/16 22:01 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Barium

ND 0.25 12/23/16 22:01 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Beryllium

0.34 0.25 12/23/16 22:01 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Cadmium

9.2 0.50 12/23/16 22:01 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Chromium

14 0.76 12/23/16 22:01 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Lead

7.5 0.50 12/23/16 22:01 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Nickel

ND 5.0 12/23/16 22:01 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Selenium

0.53 0.50 12/23/16 22:01 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Silver

ND 2.5 12/23/16 22:01 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Thallium

14 1.0 12/23/16 22:01 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Vanadium

25 1.0 12/23/16 22:01 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Zinc

Page 8 of 62

Table of Contents





Field Sample #: 867161220-01

Sample Matrix: Soil

Sampled: 12/20/2016 10:50


Date/Time

Units

Date

PreparedMethod

Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)

96.7 12/28/16 8:45 MRL% Wt 12/27/16SM 2540G1% Solids

Page 9 of 62

Table of Contents





Field Sample #: 867161220-02

Sample Matrix: Soil

Sampled: 12/20/2016 11:25

[TOC_2]16L1026-02[TOC]


Date/Time

Units

Date

PreparedMethod









ND 0.11 12/28/16 18:03 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Benzo(a)anthracene

ND 0.11 12/28/16 18:03 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Benzo(a)pyrene

ND 0.11 12/28/16 18:03 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Benzo(b)fluoranthene

ND 0.11 12/28/16 18:03 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Benzo(g,h,i)perylene

ND 0.11 12/28/16 18:03 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Benzo(k)fluoranthene

ND 0.11 12/28/16 18:03 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Chrysene




ND 0.11 12/28/16 18:03 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Indeno(1,2,3-cd)pyrene



ND 0.11 12/28/16 18:03 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Phenanthrene




o-Terphenyl (OTP) 65.6 12/28/16 18:0340-140


2-Fluorobiphenyl 86.3 12/28/16 18:0340-140

Page 10 of 62

Table of Contents

tkeane

Typewriter

B-2





Field Sample #: 867161220-02

Sample Matrix: Soil

Sampled: 12/20/2016 11:25


Date/Time

Units

Date

PreparedMethod


















Page 11 of 62

Table of Contents





Field Sample #: 867161220-02

Sample Matrix: Soil

Sampled: 12/20/2016 11:25


Date/Time

Units

Date

PreparedMethod







11 0.55 12/23/16 22:06 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Chromium








Page 12 of 62

Table of Contents





Field Sample #: 867161220-02

Sample Matrix: Soil

Sampled: 12/20/2016 11:25


Date/Time

Units

Date

PreparedMethod


87.7 12/28/16 8:45 MRL% Wt 12/27/16SM 2540G1% Solids

Page 13 of 62

Table of Contents





Field Sample #: 867161220-03

Sample Matrix: Soil

Sampled: 12/20/2016 11:55

[TOC_2]16L1026-03[TOC]


Date/Time

Units

Date

PreparedMethod






0.25 0.11 12/28/16 18:23 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Acenaphthene


0.52 0.11 12/28/16 18:23 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Anthracene





0.51 0.11 12/28/16 18:23 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Benzo(k)fluoranthene


0.19 0.11 12/28/16 18:23 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Dibenz(a,h)anthracene


0.28 0.11 12/28/16 18:23 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Fluorene

0.71 0.11 12/28/16 18:23 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Indeno(1,2,3-cd)pyrene

0.11 0.11 12/28/16 18:23 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.112-Methylnaphthalene

0.19 0.11 12/28/16 18:23 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Naphthalene





o-Terphenyl (OTP) 53.1 12/28/16 18:2340-140


2-Fluorobiphenyl 86.8 12/28/16 18:2340-140

Page 14 of 62

Table of Contents

tkeane

Typewriter

B-3





Field Sample #: 867161220-03

Sample Matrix: Soil

Sampled: 12/20/2016 11:55


Date/Time

Units

Date

PreparedMethod


















Page 15 of 62

Table of Contents





Field Sample #: 867161220-03

Sample Matrix: Soil

Sampled: 12/20/2016 11:55


Date/Time

Units

Date

PreparedMethod









14 0.54 12/23/16 22:11 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Nickel






Page 16 of 62

Table of Contents





Field Sample #: 867161220-03

Sample Matrix: Soil

Sampled: 12/20/2016 11:55


Date/Time

Units

Date

PreparedMethod


91.3 12/28/16 8:45 MRL% Wt 12/27/16SM 2540G1% Solids

Page 17 of 62

Table of Contents





Field Sample #: 867161220-04

Sample Matrix: Soil

Sampled: 12/20/2016 12:30

[TOC_2]16L1026-04[TOC]


Date/Time

Units

Date

PreparedMethod
















ND 0.11 12/28/16 18:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Fluoranthene






ND 0.11 12/28/16 18:43 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Pyrene



o-Terphenyl (OTP) 56.8 12/28/16 18:4340-140


2-Fluorobiphenyl 78.3 12/28/16 18:4340-140

Page 18 of 62

Table of Contents

tkeane

Typewriter

B-4





Field Sample #: 867161220-04

Sample Matrix: Soil

Sampled: 12/20/2016 12:30


Date/Time

Units

Date

PreparedMethod



ND 9.9 12/23/16 0:52 EEHmg/Kg dry 12/22/16MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics

ND 9.9 12/23/16 0:52 EEHmg/Kg dry 12/22/16MADEP-VPH-04-1.11C5-C8 Aliphatics



ND 9.9 12/23/16 0:52 EEHmg/Kg dry 12/22/16MADEP-VPH-04-1.11C9-C10 Aromatics











Page 19 of 62

Table of Contents





Field Sample #: 867161220-04

Sample Matrix: Soil

Sampled: 12/20/2016 12:30


Date/Time

Units

Date

PreparedMethod






ND 0.27 12/23/16 22:16 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Cadmium


2.0 0.80 12/23/16 22:16 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Lead



ND 0.54 12/23/16 22:16 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Silver


6.8 1.1 12/23/16 22:16 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Vanadium

9.1 1.1 12/23/16 22:16 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Zinc

Page 20 of 62

Table of Contents





Field Sample #: 867161220-04

Sample Matrix: Soil

Sampled: 12/20/2016 12:30


Date/Time

Units

Date

PreparedMethod


91.0 12/28/16 8:45 MRL% Wt 12/27/16SM 2540G1% Solids

Page 21 of 62

Table of Contents





Field Sample #: 867161220-05

Sample Matrix: Soil

Sampled: 12/20/2016 13:50

[TOC_2]16L1026-05[TOC]


Date/Time

Units

Date

PreparedMethod




ND 10 12/28/16 19:03 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics

ND 10 12/28/16 19:03 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11C11-C22 Aromatics




















o-Terphenyl (OTP) 63.9 12/28/16 19:0340-140


2-Fluorobiphenyl 79.5 12/28/16 19:0340-140

Page 22 of 62

Table of Contents

tkeane

Typewriter

B-5





Field Sample #: 867161220-05

Sample Matrix: Soil

Sampled: 12/20/2016 13:50


Date/Time

Units

Date

PreparedMethod


















Page 23 of 62

Table of Contents





Field Sample #: 867161220-05

Sample Matrix: Soil

Sampled: 12/20/2016 13:50


Date/Time

Units

Date

PreparedMethod




7.7 2.6 12/23/16 22:21 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Barium











Page 24 of 62

Table of Contents





Field Sample #: 867161220-05

Sample Matrix: Soil

Sampled: 12/20/2016 13:50


Date/Time

Units

Date

PreparedMethod


96.0 12/28/16 8:45 MRL% Wt 12/27/16SM 2540G1% Solids

Page 25 of 62

Table of Contents





Field Sample #: 867161220-06

Sample Matrix: Soil

Sampled: 12/20/2016 14:05

[TOC_2]16L1026-06[TOC]


Date/Time

Units

Date

PreparedMethod




ND 11 12/28/16 19:24 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics

ND 11 12/28/16 19:24 SCSmg/Kg dry 12/28/16MADEP-EPH-04-1.11C11-C22 Aromatics




















o-Terphenyl (OTP) 45.3 12/28/16 19:2440-140


2-Fluorobiphenyl 79.6 12/28/16 19:2440-140

Page 26 of 62

Table of Contents

tkeane

Typewriter

B-6





Field Sample #: 867161220-06

Sample Matrix: Soil

Sampled: 12/20/2016 14:05


Date/Time

Units

Date

PreparedMethod


















Page 27 of 62

Table of Contents





Field Sample #: 867161220-06

Sample Matrix: Soil

Sampled: 12/20/2016 14:05


Date/Time

Units

Date

PreparedMethod















Page 28 of 62

Table of Contents





Field Sample #: 867161220-06

Sample Matrix: Soil

Sampled: 12/20/2016 14:05


Date/Time

Units

Date

PreparedMethod


90.8 12/28/16 8:45 MRL% Wt 12/27/16SM 2540G1% Solids

Page 29 of 62

Table of Contents





Field Sample #: 867161220-07

Sample Matrix: Soil

Sampled: 12/20/2016 14:25

[TOC_2]16L1026-07[TOC]


Date/Time

Units

Date

PreparedMethod

























o-Terphenyl (OTP) 47.1 12/28/16 19:4440-140


2-Fluorobiphenyl 77.5 12/28/16 19:4440-140

Page 30 of 62

Table of Contents

tkeane

Typewriter

B-7





Field Sample #: 867161220-07

Sample Matrix: Soil

Sampled: 12/20/2016 14:25


Date/Time

Units

Date

PreparedMethod


















Page 31 of 62

Table of Contents





Field Sample #: 867161220-07

Sample Matrix: Soil

Sampled: 12/20/2016 14:25


Date/Time

Units

Date

PreparedMethod



3.2 2.7 12/23/16 22:48 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Arsenic












Page 32 of 62

Table of Contents





Field Sample #: 867161220-07

Sample Matrix: Soil

Sampled: 12/20/2016 14:25


Date/Time

Units

Date

PreparedMethod


91.7 12/28/16 8:45 MRL% Wt 12/27/16SM 2540G1% Solids

Page 33 of 62

Table of Contents





Field Sample #: 867161220-08

Sample Matrix: Soil

Sampled: 12/20/2016 14:45

[TOC_2]16L1026-08[TOC]


Date/Time

Units

Date

PreparedMethod

























o-Terphenyl (OTP) 63.0 12/28/16 22:0640-140


2-Fluorobiphenyl 90.4 12/28/16 22:0640-140

Page 34 of 62

Table of Contents

tkeane

Typewriter

B-8





Field Sample #: 867161220-08

Sample Matrix: Soil

Sampled: 12/20/2016 14:45


Date/Time

Units

Date

PreparedMethod


















Page 35 of 62

Table of Contents





Field Sample #: 867161220-08

Sample Matrix: Soil

Sampled: 12/20/2016 14:45


Date/Time

Units

Date

PreparedMethod



2.7 2.5 12/23/16 22:53 QNWmg/Kg dry 12/22/16SW-846 6010C-D1Arsenic












Page 36 of 62

Table of Contents





Field Sample #: 867161220-08

Sample Matrix: Soil

Sampled: 12/20/2016 14:45


Date/Time

Units

Date

PreparedMethod


95.5 12/28/16 8:45 MRL% Wt 12/27/16SM 2540G1% Solids

Page 37 of 62

Table of Contents





Field Sample #: 867161220-101

Sample Matrix: Ground Water

Sampled: 12/20/2016 13:25

[TOC_2]16L1026-09[TOC]


Date/Time

Units

Date

PreparedMethod


ND 100 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11C9-C18 Aliphatics

ND 100 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11C19-C36 Aliphatics

ND 100 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics

ND 100 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11C11-C22 Aromatics

ND 2.0 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11Acenaphthene

ND 2.0 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11Acenaphthylene

ND 2.0 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11Anthracene

ND 2.0 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11Benzo(a)anthracene

ND 2.0 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11Benzo(a)pyrene

ND 2.0 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11Benzo(b)fluoranthene

ND 2.0 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11Benzo(g,h,i)perylene

ND 2.0 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11Benzo(k)fluoranthene

ND 2.0 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11Chrysene

ND 2.0 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11Dibenz(a,h)anthracene

ND 2.0 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11Fluoranthene

ND 2.0 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11Fluorene

ND 2.0 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11Indeno(1,2,3-cd)pyrene

ND 2.0 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.112-Methylnaphthalene

ND 2.0 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11Naphthalene

ND 2.0 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11Phenanthrene

ND 2.0 1/3/17 9:40 SCSµg/L 12/30/16MADEP-EPH-04-1.11Pyrene



o-Terphenyl (OTP) 55.6 1/3/17 9:4040-140


2-Fluorobiphenyl 75.0 1/3/17 9:4040-140

Page 38 of 62

Table of Contents

tkeane

Typewriter

tkeane

Typewriter

TP-04 grounwater





Field Sample #: 867161220-101

Sample Matrix: Ground Water

Sampled: 12/20/2016 13:25


Date/Time

Units

Date

PreparedMethod


ND 100 12/22/16 22:24 EEHµg/L 12/22/16MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics

ND 100 12/22/16 22:24 EEHµg/L 12/22/16MADEP-VPH-04-1.11C5-C8 Aliphatics



ND 100 12/22/16 22:24 EEHµg/L 12/22/16MADEP-VPH-04-1.11C9-C10 Aromatics

ND 1.0 12/22/16 22:24 EEHµg/L 12/22/16MADEP-VPH-04-1.11Benzene

ND 1.0 12/22/16 22:24 EEHµg/L 12/22/16MADEP-VPH-04-1.11Ethylbenzene

ND 1.0 12/22/16 22:24 EEHµg/L 12/22/16MADEP-VPH-04-1.11Methyl tert-Butyl Ether (MTBE)

ND 5.0 12/22/16 22:24 EEHµg/L 12/22/16MADEP-VPH-04-1.11Naphthalene

ND 1.0 12/22/16 22:24 EEHµg/L 12/22/16MADEP-VPH-04-1.11Toluene

ND 2.0 12/22/16 22:24 EEHµg/L 12/22/16MADEP-VPH-04-1.11m+p Xylene

ND 1.0 12/22/16 22:24 EEHµg/L 12/22/16MADEP-VPH-04-1.11o-Xylene



2,5-Dibromotoluene (PID) 105 12/22/16 22:2470-130

Page 39 of 62

Table of Contents





Field Sample #: 867161220-09

Sample Matrix: Trip Blank Water

Sampled: 12/20/2016 15:00

[TOC_2]16L1026-10[TOC]


Date/Time

Units

Date

PreparedMethod






ND 100 12/22/16 17:36 EEHµg/L 12/22/16MADEP-VPH-04-1.11C9-C10 Aromatics

ND 1.0 12/22/16 17:36 EEHµg/L 12/22/16MADEP-VPH-04-1.11Benzene

ND 1.0 12/22/16 17:36 EEHµg/L 12/22/16MADEP-VPH-04-1.11Ethylbenzene

ND 1.0 12/22/16 17:36 EEHµg/L 12/22/16MADEP-VPH-04-1.11Methyl tert-Butyl Ether (MTBE)

ND 5.0 12/22/16 17:36 EEHµg/L 12/22/16MADEP-VPH-04-1.11Naphthalene

ND 1.0 12/22/16 17:36 EEHµg/L 12/22/16MADEP-VPH-04-1.11Toluene

ND 2.0 12/22/16 17:36 EEHµg/L 12/22/16MADEP-VPH-04-1.11m+p Xylene

ND 1.0 12/22/16 17:36 EEHµg/L 12/22/16MADEP-VPH-04-1.11o-Xylene



2,5-Dibromotoluene (PID) 107 12/22/16 17:3670-130

Page 40 of 62

Table of Contents


Sample Extraction Data

Prep Method: SW-846 3546-MADEP-EPH-04-1.1

Lab Number [Field ID] Batch DateInitial [g] Final [mL]

B166718 12/28/1620.0 2.0016L1026-01 [867161220-01]

B166718 12/28/1620.0 2.0016L1026-02 [867161220-02]

B166718 12/28/1620.0 2.0016L1026-03 [867161220-03]

B166718 12/28/1620.0 2.0016L1026-04 [867161220-04]

B166718 12/28/1620.0 2.0016L1026-05 [867161220-05]

B166718 12/28/1620.0 2.0016L1026-06 [867161220-06]

B166718 12/28/1620.0 2.0016L1026-07 [867161220-07]

B166718 12/28/1620.0 2.0016L1026-08 [867161220-08]

Prep Method: SW-846 3510C-MADEP-EPH-04-1.1

Lab Number [Field ID] Batch DateInitial [mL] Final [mL]

B166933 12/30/161000 2.0016L1026-09 [867161220-101]

Prep Method: MA VPH-MADEP-VPH-04-1.1


B166442 12/22/1614.9 15.516L1026-01 [867161220-01]

B166442 12/22/1615.6 16.916L1026-02 [867161220-02]

B166442 12/22/1616.6 16.416L1026-03 [867161220-03]

B166442 12/22/1618.5 16.716L1026-04 [867161220-04]

B166442 12/22/1617.4 15.716L1026-05 [867161220-05]

B166442 12/22/1615.5 16.416L1026-06 [867161220-06]

B166442 12/22/1616.7 16.416L1026-07 [867161220-07]

B166442 12/22/1617.0 15.816L1026-08 [867161220-08]

Prep Method: MA VPH-MADEP-VPH-04-1.1

Lab Number [Field ID] Batch DateInitial [mL] Final [mL]

B166444 12/22/165 5.0016L1026-09 [867161220-101]

B166444 12/22/165 5.0016L1026-10 [867161220-09]

Prep Method: % Solids-SM 2540G

Lab Number [Field ID] Batch Date

B166688 12/27/1616L1026-01 [867161220-01]

B166688 12/27/1616L1026-02 [867161220-02]

B166688 12/27/1616L1026-03 [867161220-03]

B166688 12/27/1616L1026-04 [867161220-04]

B166688 12/27/1616L1026-05 [867161220-05]

B166688 12/27/1616L1026-06 [867161220-06]

B166688 12/27/1616L1026-07 [867161220-07]

B166688 12/27/1616L1026-08 [867161220-08]

Prep Method: SW-846 3051-SW-846 6010C-D


B166431 12/22/161.03 50.016L1026-01 [867161220-01]

B166431 12/22/161.03 50.016L1026-02 [867161220-02]

[TOC_1]Sample Preparation Information[TOC]

Page 41 of 62

Table of Contents


Sample Extraction Data

Prep Method: SW-846 3051-SW-846 6010C-D


B166431 12/22/161.01 50.016L1026-03 [867161220-03]

B166431 12/22/161.03 50.016L1026-04 [867161220-04]

B166431 12/22/161.02 50.016L1026-05 [867161220-05]

B166431 12/22/161.02 50.016L1026-06 [867161220-06]

B166431 12/22/161.02 50.016L1026-07 [867161220-07]

B166431 12/22/161.05 50.016L1026-08 [867161220-08]

Page 42 of 62

Table of Contents


Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte

Petroleum Hydrocarbons Analyses - EPH - Quality Control

QUALITY CONTROL

[TOC_2]Petroleum Hydrocarbons Analyses - EPH[TOC]

Batch B166718 - SW-846 3546[TOC_3]B166718[TOC]

Blank (B166718-BLK1) Prepared & Analyzed: 12/28/16

C9-C18 Aliphatics mg/Kg wet10ND


Unadjusted C11-C22 Aromatics mg/Kg wet10ND

C11-C22 Aromatics mg/Kg wet10ND

Acenaphthene mg/Kg wet0.10ND

Acenaphthylene mg/Kg wet0.10ND

Anthracene mg/Kg wet0.10ND

Benzo(a)anthracene mg/Kg wet0.10ND

Benzo(a)pyrene mg/Kg wet0.10ND

Benzo(b)fluoranthene mg/Kg wet0.10ND

Benzo(g,h,i)perylene mg/Kg wet0.10ND

Benzo(k)fluoranthene mg/Kg wet0.10ND

Chrysene mg/Kg wet0.10ND

Dibenz(a,h)anthracene mg/Kg wet0.10ND

Fluoranthene mg/Kg wet0.10ND

Fluorene mg/Kg wet0.10ND

Indeno(1,2,3-cd)pyrene mg/Kg wet0.10ND

2-Methylnaphthalene mg/Kg wet0.10ND

Naphthalene mg/Kg wet0.10ND

Phenanthrene mg/Kg wet0.10ND

Pyrene mg/Kg wet0.10ND

n-Decane mg/Kg wet0.10ND

n-Docosane mg/Kg wet0.10ND

n-Dodecane mg/Kg wet0.10ND

n-Eicosane mg/Kg wet0.10ND

n-Hexacosane mg/Kg wet0.10ND

n-Hexadecane mg/Kg wet0.10ND

n-Hexatriacontane mg/Kg wet0.10ND

n-Nonadecane mg/Kg wet0.10ND

n-Nonane mg/Kg wet0.10ND

n-Octacosane mg/Kg wet0.10ND

n-Octadecane mg/Kg wet0.10ND

n-Tetracosane mg/Kg wet0.10ND

n-Tetradecane mg/Kg wet0.10ND

n-Triacontane mg/Kg wet0.10ND

Naphthalene-aliphatic fraction mg/Kg wet0.10ND

2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10ND

mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD) 58.92.94

mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP) 68.23.41

mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 72.43.62

mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 87.64.38

LCS (B166718-BS1) Prepared & Analyzed: 12/28/16

Acenaphthene mg/Kg wet0.10 5.00 40-14064.53.23

Acenaphthylene mg/Kg wet0.10 5.00 40-14061.63.08

Anthracene mg/Kg wet0.10 5.00 40-14067.83.39

Benzo(a)anthracene mg/Kg wet0.10 5.00 40-14066.53.32

Benzo(a)pyrene mg/Kg wet0.10 5.00 40-14064.13.20

Benzo(b)fluoranthene mg/Kg wet0.10 5.00 40-14065.23.26

Benzo(g,h,i)perylene mg/Kg wet0.10 5.00 40-14062.93.14

Benzo(k)fluoranthene mg/Kg wet0.10 5.00 40-14064.13.21

Chrysene mg/Kg wet0.10 5.00 40-14066.73.33

[TOC_1]QC Data[TOC]

Page 43 of 62

Table of Contents


Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte


QUALITY CONTROL

Batch B166718 - SW-846 3546


Dibenz(a,h)anthracene mg/Kg wet0.10 5.00 40-14066.83.34

Fluoranthene mg/Kg wet0.10 5.00 40-14066.73.33

Fluorene mg/Kg wet0.10 5.00 40-14065.23.26

Indeno(1,2,3-cd)pyrene mg/Kg wet0.10 5.00 40-14063.63.18

2-Methylnaphthalene mg/Kg wet0.10 5.00 40-14059.02.95

Naphthalene mg/Kg wet0.10 5.00 40-14056.62.83

Phenanthrene mg/Kg wet0.10 5.00 40-14066.13.30

Pyrene mg/Kg wet0.10 5.00 40-14066.73.33

n-Decane mg/Kg wet0.10 5.00 40-14048.62.43

n-Docosane mg/Kg wet0.10 5.00 40-14067.43.37

n-Dodecane mg/Kg wet0.10 5.00 40-14056.62.83

n-Eicosane mg/Kg wet0.10 5.00 40-14068.43.42

n-Hexacosane mg/Kg wet0.10 5.00 40-14064.73.23

n-Hexadecane mg/Kg wet0.10 5.00 40-14070.93.54

n-Hexatriacontane mg/Kg wet0.10 5.00 40-14065.53.27

n-Nonadecane mg/Kg wet0.10 5.00 40-14067.53.37

n-Nonane mg/Kg wet0.10 5.00 30-14039.71.98

n-Octacosane mg/Kg wet0.10 5.00 40-14062.83.14

n-Octadecane mg/Kg wet0.10 5.00 40-14073.43.67

n-Tetracosane mg/Kg wet0.10 5.00 40-14067.13.35

n-Tetradecane mg/Kg wet0.10 5.00 40-14065.83.29

n-Triacontane mg/Kg wet0.10 5.00 40-14063.73.18

Naphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND

2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND





LCS Dup (B166718-BSD1) Prepared & Analyzed: 12/28/16

Acenaphthene mg/Kg wet0.10 5.00 2540-14061.1 5.523.05

Acenaphthylene mg/Kg wet0.10 5.00 2540-14058.1 5.692.91

Anthracene mg/Kg wet0.10 5.00 2540-14066.1 2.573.30

Benzo(a)anthracene mg/Kg wet0.10 5.00 2540-14065.1 2.103.25

Benzo(a)pyrene mg/Kg wet0.10 5.00 2540-14063.0 1.733.15

Benzo(b)fluoranthene mg/Kg wet0.10 5.00 2540-14064.2 1.523.21

Benzo(g,h,i)perylene mg/Kg wet0.10 5.00 2540-14061.1 2.983.05

Benzo(k)fluoranthene mg/Kg wet0.10 5.00 2540-14063.0 1.813.15

Chrysene mg/Kg wet0.10 5.00 2540-14065.0 2.523.25

Dibenz(a,h)anthracene mg/Kg wet0.10 5.00 2540-14064.9 2.813.25

Fluoranthene mg/Kg wet0.10 5.00 2540-14065.3 2.083.27

Fluorene mg/Kg wet0.10 5.00 2540-14062.4 4.323.12

Indeno(1,2,3-cd)pyrene mg/Kg wet0.10 5.00 2540-14062.5 1.693.13

2-Methylnaphthalene mg/Kg wet0.10 5.00 2540-14056.2 4.872.81

Naphthalene mg/Kg wet0.10 5.00 2540-14053.8 5.102.69

Phenanthrene mg/Kg wet0.10 5.00 2540-14064.2 2.973.21

Pyrene mg/Kg wet0.10 5.00 2540-14065.4 1.933.27

n-Decane mg/Kg wet0.10 5.00 2540-14046.6 4.282.33

n-Docosane mg/Kg wet0.10 5.00 2540-14066.6 1.193.33

n-Dodecane mg/Kg wet0.10 5.00 2540-14054.2 4.262.71

n-Eicosane mg/Kg wet0.10 5.00 2540-14067.1 1.933.35

n-Hexacosane mg/Kg wet0.10 5.00 2540-14064.2 0.7013.21

Page 44 of 62

Table of Contents


Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte


QUALITY CONTROL

Batch B166718 - SW-846 3546


n-Hexadecane mg/Kg wet0.10 5.00 2540-14069.0 2.653.45

n-Hexatriacontane mg/Kg wet0.10 5.00 2540-14065.3 0.3183.26

n-Nonadecane mg/Kg wet0.10 5.00 2540-14066.4 1.663.32

n-Nonane mg/Kg wet0.10 5.00 2530-14038.4 3.281.92

n-Octacosane mg/Kg wet0.10 5.00 2540-14062.6 0.4153.13

n-Octadecane mg/Kg wet0.10 5.00 2540-14072.4 1.343.62

n-Tetracosane mg/Kg wet0.10 5.00 2540-14066.3 1.133.31

n-Tetradecane mg/Kg wet0.10 5.00 2540-14061.9 6.013.10

n-Triacontane mg/Kg wet0.10 5.00 2540-14063.6 0.1193.18

Naphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND

2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND





Matrix Spike (B166718-MS1) Prepared: 12/28/16 Analyzed: 12/29/16 Source: 16L1026-01

C9-C18 Aliphatics mg/Kg dry10 31.0 40-14056.325.5 8.05

C19-C36 Aliphatics mg/Kg dry10 41.4 MS-2240-140142 *91.6 33.0

Unadjusted C11-C22 Aromatics mg/Kg dry10 87.9 40-14065.294.4 37.0

Acenaphthene mg/Kg dry0.10 5.17 40-14063.03.26 ND

Acenaphthylene mg/Kg dry0.10 5.17 40-14059.93.10 ND

Anthracene mg/Kg dry0.10 5.17 40-14059.93.16 0.0635

Benzo(a)anthracene mg/Kg dry0.10 5.17 40-14057.63.47 0.493

Benzo(a)pyrene mg/Kg dry0.10 5.17 40-14055.13.40 0.553

Benzo(b)fluoranthene mg/Kg dry0.10 5.17 40-14055.23.72 0.865

Benzo(g,h,i)perylene mg/Kg dry0.10 5.17 40-14054.43.20 0.383

Benzo(k)fluoranthene mg/Kg dry0.10 5.17 40-14056.93.25 0.311

Chrysene mg/Kg dry0.10 5.17 40-14056.73.71 0.780

Dibenz(a,h)anthracene mg/Kg dry0.10 5.17 40-14057.33.05 0.0871

Fluoranthene mg/Kg dry0.10 5.17 40-14053.34.22 1.46

Fluorene mg/Kg dry0.10 5.17 40-14062.43.23 ND

Indeno(1,2,3-cd)pyrene mg/Kg dry0.10 5.17 40-14053.03.14 0.406

2-Methylnaphthalene mg/Kg dry0.10 5.17 40-14059.63.08 ND

Naphthalene mg/Kg dry0.10 5.17 40-14057.42.97 ND

Phenanthrene mg/Kg dry0.10 5.17 40-14059.93.53 0.435

Pyrene mg/Kg dry0.10 5.17 40-14053.94.20 1.41

n-Nonane mg/Kg dry0.10 5.17 30-14039.12.02 ND

mg/Kg dry 5.17 40-140Surrogate: Chlorooctadecane (COD) 52.32.70

mg/Kg dry 5.17 40-140Surrogate: o-Terphenyl (OTP) 58.03.00

mg/Kg dry 5.17 40-140Surrogate: 2-Bromonaphthalene 67.63.50

mg/Kg dry 5.17 40-140Surrogate: 2-Fluorobiphenyl 84.74.38

Page 45 of 62

Table of Contents


Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte


QUALITY CONTROL

Batch B166718 - SW-846 3546

Matrix Spike Dup (B166718-MSD1) Prepared: 12/28/16 Analyzed: 12/29/16 Source: 16L1026-01

C9-C18 Aliphatics mg/Kg dry10 31.0 5040-14052.7 4.4324.4 8.05

C19-C36 Aliphatics mg/Kg dry10 41.4 5040-140112 14.579.2 33.0

Unadjusted C11-C22 Aromatics mg/Kg dry10 87.9 5040-14075.3 8.98103 37.0

Acenaphthene mg/Kg dry0.10 5.17 5040-14061.0 3.223.16 ND

Acenaphthylene mg/Kg dry0.10 5.17 5040-14057.5 3.962.98 ND

Anthracene mg/Kg dry0.10 5.17 5040-14059.3 1.023.13 0.0635

Benzo(a)anthracene mg/Kg dry0.10 5.17 5040-14061.2 5.323.66 0.493

Benzo(a)pyrene mg/Kg dry0.10 5.17 5040-14058.5 5.023.58 0.553

Benzo(b)fluoranthene mg/Kg dry0.10 5.17 5040-14061.1 7.934.02 0.865

Benzo(g,h,i)perylene mg/Kg dry0.10 5.17 5040-14055.0 0.9253.22 0.383

Benzo(k)fluoranthene mg/Kg dry0.10 5.17 5040-14058.9 3.193.36 0.311

Chrysene mg/Kg dry0.10 5.17 5040-14062.5 7.724.01 0.780

Dibenz(a,h)anthracene mg/Kg dry0.10 5.17 5040-14057.1 0.3503.04 0.0871

Fluoranthene mg/Kg dry0.10 5.17 5040-14071.3 19.95.15 1.46

Fluorene mg/Kg dry0.10 5.17 5040-14061.2 1.853.17 ND

Indeno(1,2,3-cd)pyrene mg/Kg dry0.10 5.17 5040-14055.6 4.183.28 0.406

2-Methylnaphthalene mg/Kg dry0.10 5.17 5040-14054.5 8.992.82 ND

Naphthalene mg/Kg dry0.10 5.17 5040-14049.3 15.22.55 ND

Phenanthrene mg/Kg dry0.10 5.17 5040-14071.5 15.64.13 0.435

Pyrene mg/Kg dry0.10 5.17 5040-14069.0 17.04.98 1.41

n-Nonane mg/Kg dry0.10 5.17 5030-14030.9 23.31.60 ND

mg/Kg dry 5.17 40-140Surrogate: Chlorooctadecane (COD) 52.32.71

mg/Kg dry 5.17 40-140Surrogate: o-Terphenyl (OTP) 57.02.94

mg/Kg dry 5.17 40-140Surrogate: 2-Bromonaphthalene 62.83.25

mg/Kg dry 5.17 40-140Surrogate: 2-Fluorobiphenyl 81.64.22

Batch B166933 - SW-846 3510C[TOC_3]B166933[TOC]

Blank (B166933-BLK1) Prepared: 12/30/16 Analyzed: 01/03/17

C9-C18 Aliphatics µg/L100ND


Unadjusted C11-C22 Aromatics µg/L100ND

C11-C22 Aromatics µg/L100ND

Acenaphthene µg/L2.0ND

Acenaphthylene µg/L2.0ND

Anthracene µg/L2.0ND

Benzo(a)anthracene µg/L2.0ND

Benzo(a)pyrene µg/L2.0ND

Benzo(b)fluoranthene µg/L2.0ND

Benzo(g,h,i)perylene µg/L2.0ND

Benzo(k)fluoranthene µg/L2.0ND

Chrysene µg/L2.0ND

Dibenz(a,h)anthracene µg/L2.0ND

Fluoranthene µg/L2.0ND

Fluorene µg/L2.0ND

Indeno(1,2,3-cd)pyrene µg/L2.0ND

2-Methylnaphthalene µg/L2.0ND

Naphthalene µg/L2.0ND

Phenanthrene µg/L2.0ND

Pyrene µg/L2.0ND

n-Decane µg/L2.0ND

n-Docosane µg/L2.0ND

n-Dodecane µg/L2.0ND

Page 46 of 62

Table of Contents


Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte


QUALITY CONTROL

Batch B166933 - SW-846 3510C


n-Eicosane µg/L2.0ND

n-Hexacosane µg/L2.0ND

n-Hexadecane µg/L2.0ND

n-Hexatriacontane µg/L2.0ND

n-Nonadecane µg/L2.0ND

n-Nonane µg/L2.0ND

n-Octacosane µg/L2.0ND

n-Octadecane µg/L2.0ND

n-Tetracosane µg/L2.0ND

n-Tetradecane µg/L2.0ND

n-Triacontane µg/L2.0ND

Naphthalene-aliphatic fraction µg/L2.0ND

2-Methylnaphthalene-aliphatic fraction µg/L2.0ND

µg/L 100 40-140Surrogate: Chlorooctadecane (COD) 61.061.0

µg/L 100 40-140Surrogate: o-Terphenyl (OTP) 68.468.4

µg/L 100 40-140Surrogate: 2-Bromonaphthalene 80.380.3

µg/L 100 40-140Surrogate: 2-Fluorobiphenyl 83.983.9

LCS (B166933-BS1) Prepared: 12/30/16 Analyzed: 01/03/17

Acenaphthene µg/L2.0 100 40-14064.464.4

Acenaphthylene µg/L2.0 100 40-14061.361.3

Anthracene µg/L2.0 100 40-14067.867.8

Benzo(a)anthracene µg/L2.0 100 40-14065.565.5

Benzo(a)pyrene µg/L2.0 100 40-14063.663.6

Benzo(b)fluoranthene µg/L2.0 100 40-14064.364.3

Benzo(g,h,i)perylene µg/L2.0 100 40-14061.761.7

Benzo(k)fluoranthene µg/L2.0 100 40-14064.464.4

Chrysene µg/L2.0 100 40-14066.466.4

Dibenz(a,h)anthracene µg/L2.0 100 40-14066.466.4

Fluoranthene µg/L2.0 100 40-14066.266.2

Fluorene µg/L2.0 100 40-14065.465.4

Indeno(1,2,3-cd)pyrene µg/L2.0 100 40-14063.463.4

2-Methylnaphthalene µg/L2.0 100 40-14058.358.3

Naphthalene µg/L2.0 100 40-14055.755.7

Phenanthrene µg/L2.0 100 40-14066.166.1

Pyrene µg/L2.0 100 40-14066.366.3

n-Decane µg/L2.0 100 40-14046.646.6

n-Docosane µg/L2.0 100 40-14067.267.2

n-Dodecane µg/L2.0 100 40-14056.456.4

n-Eicosane µg/L2.0 100 40-14067.667.6

n-Hexacosane µg/L2.0 100 40-14065.665.6

n-Hexadecane µg/L2.0 100 40-14069.869.8

n-Hexatriacontane µg/L2.0 100 40-14067.967.9

n-Nonadecane µg/L2.0 100 40-14067.267.2

n-Nonane µg/L2.0 100 30-14036.936.9

n-Octacosane µg/L2.0 100 40-14063.663.6

n-Octadecane µg/L2.0 100 40-14072.372.3

n-Tetracosane µg/L2.0 100 40-14067.367.3

n-Tetradecane µg/L2.0 100 40-14065.465.4

n-Triacontane µg/L2.0 100 40-14064.564.5

Naphthalene-aliphatic fraction µg/L2.0 100 0-5ND

2-Methylnaphthalene-aliphatic fraction µg/L2.0 100 0-5ND

Page 47 of 62

Table of Contents


Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte


QUALITY CONTROL

Batch B166933 - SW-846 3510C






LCS Dup (B166933-BSD1) Prepared: 12/30/16 Analyzed: 01/03/17

Acenaphthene µg/L2.0 100 2540-14071.2 9.9171.2

Acenaphthylene µg/L2.0 100 2540-14067.9 10.267.9

Anthracene µg/L2.0 100 2540-14071.7 5.6971.7

Benzo(a)anthracene µg/L2.0 100 2540-14069.1 5.4269.1

Benzo(a)pyrene µg/L2.0 100 2540-14066.8 4.8966.8

Benzo(b)fluoranthene µg/L2.0 100 2540-14068.7 6.6368.7

Benzo(g,h,i)perylene µg/L2.0 100 2540-14065.2 5.5665.2

Benzo(k)fluoranthene µg/L2.0 100 2540-14067.4 4.4367.4

Chrysene µg/L2.0 100 2540-14069.7 4.8369.7

Dibenz(a,h)anthracene µg/L2.0 100 2540-14069.8 5.0369.8

Fluoranthene µg/L2.0 100 2540-14070.5 6.2470.5

Fluorene µg/L2.0 100 2540-14070.1 6.8770.1

Indeno(1,2,3-cd)pyrene µg/L2.0 100 2540-14067.3 5.9967.3

2-Methylnaphthalene µg/L2.0 100 2540-14065.4 11.465.4

Naphthalene µg/L2.0 100 2540-14063.2 12.663.2

Phenanthrene µg/L2.0 100 2540-14070.7 6.6570.7

Pyrene µg/L2.0 100 2540-14070.6 6.3570.6

n-Decane µg/L2.0 100 2540-14049.7 6.4849.7

n-Docosane µg/L2.0 100 2540-14068.3 1.4968.3

n-Dodecane µg/L2.0 100 2540-14059.6 5.5759.6

n-Eicosane µg/L2.0 100 2540-14068.8 1.6668.8

n-Hexacosane µg/L2.0 100 2540-14066.7 1.6366.7

n-Hexadecane µg/L2.0 100 2540-14072.0 3.1472.0

n-Hexatriacontane µg/L2.0 100 2540-14069.4 2.1569.4

n-Nonadecane µg/L2.0 100 2540-14068.6 2.0668.6

n-Nonane µg/L2.0 100 2530-14038.8 5.1338.8

n-Octacosane µg/L2.0 100 2540-14065.0 2.1265.0

n-Octadecane µg/L2.0 100 2540-14073.7 1.9373.7

n-Tetracosane µg/L2.0 100 2540-14068.5 1.7268.5

n-Tetradecane µg/L2.0 100 2540-14069.1 5.3869.1

n-Triacontane µg/L2.0 100 2540-14066.0 2.2866.0

Naphthalene-aliphatic fraction µg/L2.0 100 0-5ND

2-Methylnaphthalene-aliphatic fraction µg/L2.0 100 0-5ND





Page 48 of 62

Table of Contents


Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte

Petroleum Hydrocarbons Analyses - VPH - Quality Control

QUALITY CONTROL

[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]

Batch B166442 - MA VPH[TOC_3]B166442[TOC]


Unadjusted C5-C8 Aliphatics mg/Kg wet10ND


Unadjusted C9-C12 Aliphatics mg/Kg wet10ND


C9-C10 Aromatics mg/Kg wet10ND

Benzene mg/Kg wet0.050ND

Butylcyclohexane mg/Kg wet0.050ND

Decane mg/Kg wet0.050ND

Ethylbenzene mg/Kg wet0.050ND

Methyl tert-Butyl Ether (MTBE) mg/Kg wet0.050ND

2-Methylpentane mg/Kg wet0.050ND

Naphthalene mg/Kg wet0.25ND

Nonane mg/Kg wet0.050ND

Pentane mg/Kg wet0.050ND

Toluene mg/Kg wet0.050ND

1,2,4-Trimethylbenzene mg/Kg wet0.050ND

2,2,4-Trimethylpentane mg/Kg wet0.050ND

m+p Xylene mg/Kg wet0.10ND

o-Xylene mg/Kg wet0.050ND

mg/Kg wet 3.33 70-130Surrogate: 2,5-Dibromotoluene (FID) 78.82.63

mg/Kg wet 3.33 70-130Surrogate: 2,5-Dibromotoluene (PID) 75.72.52


Benzene mg/Kg wet0.0010 0.100 70-13087.70.0877

Butylcyclohexane mg/Kg wet0.0010 0.100 70-13083.90.0839

Decane mg/Kg wet0.0010 0.100 70-13080.80.0808

Ethylbenzene mg/Kg wet0.0010 0.100 70-13087.40.0874

Methyl tert-Butyl Ether (MTBE) mg/Kg wet0.0010 0.100 70-13088.60.0886

2-Methylpentane mg/Kg wet0.0010 0.100 70-13099.80.0998

Naphthalene mg/Kg wet0.0050 0.100 70-13083.20.0832

Nonane mg/Kg wet0.0010 0.100 30-13072.10.0721

Pentane mg/Kg wet0.0010 0.100 70-13089.00.0890

Toluene mg/Kg wet0.0010 0.100 70-13087.20.0872

1,2,4-Trimethylbenzene mg/Kg wet0.0010 0.100 70-13089.80.0898

2,2,4-Trimethylpentane mg/Kg wet0.0010 0.100 70-13088.30.0883

m+p Xylene mg/Kg wet0.0020 0.200 70-13089.10.178

o-Xylene mg/Kg wet0.0010 0.100 70-13087.10.0871




Benzene mg/Kg wet0.0010 0.100 2570-13087.0 0.7530.0870

Butylcyclohexane mg/Kg wet0.0010 0.100 2570-13082.7 1.560.0827

Decane mg/Kg wet0.0010 0.100 2570-13079.6 1.550.0796

Ethylbenzene mg/Kg wet0.0010 0.100 2570-13086.5 0.9350.0865

Methyl tert-Butyl Ether (MTBE) mg/Kg wet0.0010 0.100 2570-13088.4 0.2210.0884

2-Methylpentane mg/Kg wet0.0010 0.100 2570-130100 0.4670.100

Naphthalene mg/Kg wet0.0050 0.100 2570-13081.6 1.910.0816

Nonane mg/Kg wet0.0010 0.100 2530-13071.4 0.9590.0714

Pentane mg/Kg wet0.0010 0.100 2570-13090.0 1.160.0900

Toluene mg/Kg wet0.0010 0.100 2570-13086.5 0.7250.0865

1,2,4-Trimethylbenzene mg/Kg wet0.0010 0.100 2570-13089.7 0.1310.0897

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Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte


QUALITY CONTROL

Batch B166442 - MA VPH


2,2,4-Trimethylpentane mg/Kg wet0.0010 0.100 2570-13088.2 0.05330.0882

m+p Xylene mg/Kg wet0.0020 0.200 2570-13088.6 0.5700.177

o-Xylene mg/Kg wet0.0010 0.100 2570-13086.7 0.4710.0867



Batch B166444 - MA VPH[TOC_3]B166444[TOC]


Unadjusted C5-C8 Aliphatics µg/L100ND


Unadjusted C9-C12 Aliphatics µg/L100ND


C9-C10 Aromatics µg/L100ND

Benzene µg/L1.0ND

Butylcyclohexane µg/L1.0ND

Decane µg/L1.0ND

Ethylbenzene µg/L1.0ND

Methyl tert-Butyl Ether (MTBE) µg/L1.0ND

2-Methylpentane µg/L1.0ND

Naphthalene µg/L5.0ND

Nonane µg/L1.0ND

Pentane µg/L1.0ND

Toluene µg/L1.0ND

1,2,4-Trimethylbenzene µg/L1.0ND

2,2,4-Trimethylpentane µg/L1.0ND

m+p Xylene µg/L2.0ND

o-Xylene µg/L1.0ND

µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID) 96.338.5

µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID) 10241.0


Benzene µg/L1.0 100 70-13094.694.6

Butylcyclohexane µg/L1.0 100 70-13095.695.6

Decane µg/L1.0 100 70-130106106

Ethylbenzene µg/L1.0 100 70-13097.497.4

Methyl tert-Butyl Ether (MTBE) µg/L1.0 100 70-13095.995.9

2-Methylpentane µg/L1.0 100 70-130102102

Naphthalene µg/L5.0 100 70-13076.076.0

Nonane µg/L1.0 100 30-130101101

Pentane µg/L1.0 100 70-13075.875.8

Toluene µg/L1.0 100 70-130100100

1,2,4-Trimethylbenzene µg/L1.0 100 70-13093.193.1

2,2,4-Trimethylpentane µg/L1.0 100 70-13099.599.5

m+p Xylene µg/L2.0 200 70-13094.3189

o-Xylene µg/L1.0 100 70-13092.992.9

µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID) 10541.9


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Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte


QUALITY CONTROL

Batch B166444 - MA VPH


Benzene µg/L1.0 100 2570-13094.5 0.082594.5

Butylcyclohexane µg/L1.0 100 2570-13095.3 0.29395.3

Decane µg/L1.0 100 2570-130107 1.02107

Ethylbenzene µg/L1.0 100 2570-13098.5 1.1198.5

Methyl tert-Butyl Ether (MTBE) µg/L1.0 100 2570-13099.1 3.3099.1

2-Methylpentane µg/L1.0 100 2570-13099.8 1.7999.8

Naphthalene µg/L5.0 100 2570-13081.2 6.5381.2

Nonane µg/L1.0 100 2530-130100 1.24100

Pentane µg/L1.0 100 2570-13073.4 3.2573.4

Toluene µg/L1.0 100 2570-130101 0.762101

1,2,4-Trimethylbenzene µg/L1.0 100 2570-13093.2 0.11593.2

2,2,4-Trimethylpentane µg/L1.0 100 2570-13098.5 0.96598.5

m+p Xylene µg/L2.0 200 2570-13095.0 0.782190

o-Xylene µg/L1.0 100 2570-13094.0 1.1194.0

µg/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID) 11646.3


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Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte

Metals Analyses (Total) - Quality Control

QUALITY CONTROL

[TOC_2]Metals Analyses (Total)[TOC]

Batch B166431 - SW-846 3051[TOC_3]B166431[TOC]


Antimony mg/Kg wet2.5ND

Arsenic mg/Kg wet2.5ND

Barium mg/Kg wet2.5ND

Beryllium mg/Kg wet0.25ND

Cadmium mg/Kg wet0.25ND

Chromium mg/Kg wet0.50ND

Lead mg/Kg wet0.75ND

Nickel mg/Kg wet0.50ND

Selenium mg/Kg wet5.0ND

Silver mg/Kg wet0.50ND

Thallium mg/Kg wet2.5ND

Vanadium mg/Kg wet1.0ND

Zinc mg/Kg wet1.0ND


Antimony mg/Kg wet4.7 88.2 0-210.3157139

Arsenic mg/Kg wet4.7 57.0 77.8-122.190.851.8

Barium mg/Kg wet4.7 110 82-117.486.795.4

Beryllium mg/Kg wet0.47 67.5 82.3-117.795.764.6

Cadmium mg/Kg wet0.47 77.8 81.9-118.291.771.4

Chromium mg/Kg wet0.94 65.0 78.7-120.694.361.3

Lead mg/Kg wet1.4 85.6 82.4-117.886.474.0

Nickel mg/Kg wet0.94 61.3 82.2-117.889.054.6

Selenium mg/Kg wet9.4 78.9 77.1-122.389.270.4

Silver mg/Kg wet0.94 54.2 74.3-125.491.449.6

Thallium mg/Kg wet4.7 178 78.2-121.692.5165

Vanadium mg/Kg wet1.9 56.3 64.8-135.293.252.5

Zinc mg/Kg wet1.9 198 79.7-120.889.8178

LCS Dup (B166431-BSD1) Prepared: 12/22/16 Analyzed: 12/23/16

Antimony mg/Kg wet4.8 88.2 300-210.3159 1.37140

Arsenic mg/Kg wet4.8 57.0 3077.8-122.192.4 1.6952.7

Barium mg/Kg wet4.8 110 3082-117.493.3 7.31103

Beryllium mg/Kg wet0.48 67.5 3082.3-117.797.4 1.8065.8

Cadmium mg/Kg wet0.48 77.8 3081.9-118.296.6 5.1375.1

Chromium mg/Kg wet0.97 65.0 3078.7-120.696.1 1.8762.5

Lead mg/Kg wet1.5 85.6 3082.4-117.887.9 1.6675.2

Nickel mg/Kg wet0.97 61.3 3082.2-117.892.3 3.6156.6

Selenium mg/Kg wet9.7 78.9 3077.1-122.391.1 2.0671.9

Silver mg/Kg wet0.97 54.2 3074.3-125.495.9 4.8052.0

Thallium mg/Kg wet4.8 178 3078.2-121.696.1 3.87171

Vanadium mg/Kg wet1.9 56.3 3064.8-135.292.4 0.81552.0

Zinc mg/Kg wet1.9 198 3079.7-120.892.5 2.95183

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Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte

Metals Analyses (Total) - Quality Control

QUALITY CONTROL

Batch B166431 - SW-846 3051

MRL Check (B166431-MRL1) Prepared: 12/22/16 Analyzed: 12/23/16

Lead mg/Kg wet0.74 0.742 80-12094.60.702

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Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes Analyte

Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control

QUALITY CONTROL

[TOC_2]Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)[TOC]

Batch B166688 - % Solids[TOC_3]B166688[TOC]

Duplicate (B166688-DUP4) Prepared: 12/27/16 Analyzed: 12/28/16 Source: 16L1026-01

% Solids % Wt 200.10396.6 96.7

Duplicate (B166688-DUP5) Prepared: 12/27/16 Analyzed: 12/28/16 Source: 16L1026-02

% Solids % Wt 202.4285.6 87.7

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FLAG/QUALIFIER SUMMARY

* QC result is outside of established limits.

� Wide recovery limits established for difficult compound.

� Wide RPD limits established for difficult compound.

# Data exceeded client recommended or regulatory level

Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the

calculation which have not been rounded.

No results have been blank subtracted unless specified in the case narrative section.

RL Reporting Limit

DL Method Detection Limit

MCL Maximum Contaminant Level

ND Not Detected

Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the

two MS/MSD results is within method specified criteria.

MS-22

[TOC_1]Flag/Qualifier Summary[TOC]

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CertificationsAnalyte

CERTIFICATIONS

Certified Analyses included in this Report

MADEP-EPH-04-1.1 in Soil

CT,NC,ME,NH-PC9-C18 Aliphatics


CT,NC,ME,NH-PUnadjusted C11-C22 Aromatics

CT,NC,ME,NH-PC11-C22 Aromatics

CT,NC,ME,NH-PAcenaphthene

CT,NC,ME,NH-PAcenaphthylene

CT,NC,ME,NH-PAnthracene

CT,NC,ME,NH-PBenzo(a)anthracene

CT,NC,ME,NH-PBenzo(a)pyrene

CT,NC,ME,NH-PBenzo(b)fluoranthene

CT,NC,ME,NH-PBenzo(g,h,i)perylene

CT,NC,ME,NH-PBenzo(k)fluoranthene

CT,NC,ME,NH-PChrysene

CT,NC,ME,NH-PDibenz(a,h)anthracene

CT,NC,ME,NH-PFluoranthene

CT,NC,MEFluorene

CT,NC,ME,NH-PIndeno(1,2,3-cd)pyrene

CT,NC,ME2-Methylnaphthalene

CT,NC,ME,NH-PNaphthalene

CT,NC,ME,NH-PPhenanthrene

CT,NC,ME,NH-PPyrene

MADEP-EPH-04-1.1 in Water



CT,NC,ME,NH-PUnadjusted C11-C22 Aromatics


CT,NC,ME,NH-PAcenaphthene

CT,NC,ME,NH-PAcenaphthylene

CT,NC,ME,NH-PAnthracene

CT,NC,ME,NH-PBenzo(a)anthracene

CT,NC,ME,NH-PBenzo(a)pyrene

CT,NC,ME,NH-PBenzo(b)fluoranthene

CT,NC,ME,NH-PBenzo(g,h,i)perylene

CT,NC,ME,NH-PBenzo(k)fluoranthene

CT,NC,ME,NH-PChrysene

CT,NC,ME,NH-PDibenz(a,h)anthracene

CT,NC,ME,NH-PFluoranthene

CT,NC,MEFluorene

CT,NC,ME,NH-PIndeno(1,2,3-cd)pyrene

CT,NC,ME2-Methylnaphthalene


CT,NC,ME,NH-PPhenanthrene

CT,NC,ME,NH-PPyrene

MADEP-VPH-04-1.1 in Soil

CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics


[TOC_1]Certifications[TOC]

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CertificationsAnalyte

CERTIFICATIONS

Certified Analyses included in this Report

MADEP-VPH-04-1.1 in Soil




CT,NC,ME,NH-PBenzene

CT,NC,ME,NH-PEthylbenzene

CT,NC,ME,NH-PMethyl tert-Butyl Ether (MTBE)


CT,NC,ME,NH-PToluene

CT,NC,ME,NH-Pm+p Xylene

CT,NC,ME,NH-Po-Xylene

MADEP-VPH-04-1.1 in Water






CT,NC,ME,NH-PBenzene

CT,NC,ME,NH-PEthylbenzene

CT,NC,ME,NH-PMethyl tert-Butyl Ether (MTBE)


CT,NC,ME,NH-PToluene

CT,NC,ME,NH-Pm+p Xylene

CT,NC,ME,NH-Po-Xylene

SW-846 6010C-D in Soil

CT,NH,NY,ME,VA,NCAntimony

CT,NH,NY,ME,VA,NCArsenic

CT,NH,NY,ME,VA,NCBarium

CT,NH,NY,ME,VA,NCBeryllium

CT,NH,NY,ME,VA,NCCadmium

CT,NH,NY,ME,VA,NCChromium

CT,NH,NY,AIHA,ME,VA,NCLead

CT,NH,NY,ME,VA,NCNickel

CT,NH,NY,ME,VA,NCSelenium

CT,NH,NY,ME,VA,NCSilver

CT,NH,NY,ME,VA,NCThallium

CT,NH,NY,ME,VA,NCVanadium

CT,NH,NY,ME,VA,NCZinc

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The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:

Code Description Number Expires

100033AIHA-LAP, LLC - ISO17025:2005AIHA 02/1/2018

M-MA100Massachusetts DEPMA 06/30/2017

PH-0567Connecticut Department of Publilc HealthCT 09/30/2017

10899 NELAPNew York State Department of HealthNY 04/1/2017

2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2017

LAO00112Rhode Island Department of HealthRI 12/30/2016

652North Carolina Div. of Water QualityNC 12/31/2017

MA007 NELAPNew Jersey DEPNJ 06/30/2017

E871027 NELAPFlorida Department of HealthFL 06/30/2017

LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2017

2011028State of MaineME 06/9/2017

460217Commonwealth of VirginiaVA 12/14/2017

2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2017

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MADEP MCP Analytical Method Report Certification Form

Laboratory Name: Con-Test Analytical Laboratory Project #:

Project Location:

This Form provides certifications for the following data set: [list Laboratory Sample ID Number(s)]

16L1026

16L1026-01 thru 16L1026-10

8260 VOC

CAM II A ( )

8151 Herbicides

CAM V C ( )

8330 Explosives

CAM VIII A ( )

6010 Metals

CAM III A (X)

7470/7471 Hg

CAM IIIB ( )

8270 SVOC

CAM II B ( )

8081 Pesticides

CAM V B ( )

MassDEP VPH

CAM IV A (X)

6020 Metals

CAM III D ( )

9014 Total

Cyanide/PAC

CAM VI A ( )

8082 PCB

CAM V A ( )

6860 Perchlorate

CAM VIII B ( )

MassDEP EPH

CAM IV A (X)

7010 Metals

CAM III C ( )

7196 Hex Cr

CAM VI B ( )

MassDEP APH

CAM IX A ( )

TO-15 VOC

CAM IX B ( )

Montague, MA

Matrices:

RTN:

Soil Water

CAM Protocol (check all that below)

Affirmative response to Questions A throughF is required for �Presumptive Certainty� status

ü

AYes No¹

Were all samples received in a condition consistent with those described on the Chain-of-Custody,

properly preserved (including temperature) in the field or laboratory, and prepared/analyzed within

method holding times?

ü

BYes No¹

Were the analytical method(s) and all associated QC requirements specificed in the selected CAM

protocol(s) followed?

ü

CYes No¹

Were all required corrective actions and analytical response actions specified in the selected CAM

protocol(s) implemented for all identified performance standard non-conformances?

ü

DYes No¹

Does the laboratory report comply with all the reporting requirements specified in CAM VII A,

Quality Assurance and Quality Control Guidlines for the Acquisition and Reporting of Analytical

Data?

ü

E aYes No¹

VPH, EPH, and APH Methods only: Was each method conducted without significant

modification(s)? (Refer to the individual method(s) for a list of significant modifications).

E bYes No¹

APH and TO-15 Methods only: Was the complete analyte list reported for each method?

ü

FYes No¹

Were all applicable CAM protocol QC and performance standard non-conformances identified and

evaluated in a laboratory narrative (including all No responses to Qestions A through E)?

G Were the reporting limits at or below all CAM reporting limits specified in the selected CAM

protocol(s)?ü Yes No¹

A response to questions G, H and I below is required for �Presumptive Certainty� status

Were all QC perfomance standards specified in the CAM protocol(s) achieved? Yes ü No¹H

Data User Note: Data that achieve "Presumptive Certainty" status may not necessarily meet the data usability

and representativeness requirements described in 310 CMR 40. 1056 (2)(k) and WSC-07-350.

ü

IYes No¹

Were results reported for the complete analyte list specified in the selected CAM protocol(s)?

I, the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of

those responsible for obtaining the information, the material contained in this analytical report is, to the best

of my knowledge and belief, accurate and complete.

¹All Negative responses must be addressed in an attached Environmental Laboratory case narrative.

Signature:

Printed Name:

Position:

Date:

Project Manager

Lisa A. Worthington 01/03/17

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Documents

1 Site Description and Background - FRTA – Public ...frta.org/wp-content/uploads/Sandy-Lane-Phase-II-Report.pdf · soil is warranted based on these data, the published the "natural"