Upload
whitney-cooper
View
215
Download
1
Tags:
Embed Size (px)
Citation preview
1
Heuristics19 Oct 12
2
Agitators and Mixing Equipment
• Suspend solids• Disperse gases and liquids• Emulsify one liquid in another• Promote heat transfer• Blending two or more materials together
Overmixing maybe undesirable• in biological application, high shear may damage
organisms• polymer molecules may be damaged by long mixing or
high shear
For design or consideration of mixing process should understand:• mechanism of mixing• scale-up criteria• power consumption• flow patterns• mixing time/rates• types of equipment available
Coulson and Richardson’s Chemical Engineering Volume 1, 6th ed.
3
Agitators and Mixing Equipment
Fluid mixing
Coulson and Richardson’s Chemical Engineering Volume 1, 6th ed.
4
Agitators and Mixing Equipment
Fluid mixing: Baffles
Coulson and Richardson’s Chemical Engineering Volume 1, 6th ed.
Unbaffled mixing tanks often used:• in transition region• for sticky materials• where perfect cleaning is required• in large tanks where baffle effects are
small• processes where it is not clear baffles
have an effect on mixing performance
G.B. Tatterson., Fluid Mixing and Gas Dispersion in Agitated Tanks, McGraw-Hill, 1991
5
Agitators and Mixing Equipment
Fluid mixing: off-center
Coulson and Richardson’s Chemical Engineering Volume 1, 6th ed.
Fluid mixing: Baffles
6
Agitators and Mixing Equipment
Side mounted mixers.
Paul, et.al., Handbook of Industrial Mixing, Wiley, 2004Coulson and Richardson’s Chemical Engineering Volume 1, 6th ed.
Flow patterns for side-entering propeller
7
Agitators and Mixing Equipment
Common Impellers
Coulson and Richardson’s Chemical Engineering Volume 1, 6th ed.
Figure 7.20 Commonly used impellers (a) Three-bladed propeller (b) Six-bladed disc turbine (Rushton turbine) (c) Simple paddle (d) Anchor impeller (e) Helical ribbon.
8
Agitators and Mixing Equipment
Various Turbine Impellers
Coulson and Richardson’s Chemical Engineering Volume 1, 6th ed.
9
Various Impeller Types
Paul, et.al., Handbook of Industrial Mixing, Wiley, 2004
Axial Flow Impellers
Radial Flow Impellers
Hydrofoil Impellers
High-Shear Impellers
10
Various Impeller Types
R. Hesketh, mixing notes
11
Various Impeller Types
12
Agitators and Mixing Equipment
Selecting Agitator Type
Coulson and Richardson’s Chemical Engineering Volume 1, 6th ed.
Used to make preliminary agitator selection based on tank volume and liquid viscosity.
• Turbines, Pitched Blade Turbines, and Propellers are typically used at high Re and low viscosity.
• Anchor, Helical Ribbon, and Paddle agitators are used for higher viscosity (more laminar-like Re) fluids.
13
Flow Patterns for Various Impellers
Flat Blade Turbine = FBTPitched Blade Turbine = PBT
Paul, et.al., Handbook of Industrial Mixing, Wiley, 2004
14
Typical Dimensions for Mixing Equipment
G.B. Tatterson., Fluid Mixing and Gas Dispersion in Agitated Tanks, McGraw-Hill, 1991
15
Typical Dimensions for Mixing Equipment
G.B. Tatterson., Fluid Mixing and Gas Dispersion in Agitated Tanks, McGraw-Hill, 1991
16
Power Consumption and Scale-up in Mixing
Consider geometry, fluid properties, flow patterns, power, and so on. Has been considered through dimensional analysis.
Tatterson & Colson and Richardson.
...22
53
dcba
P D
C
D
T
g
DNNDK
DN
PN
With:
numberFroudeNg
DN
orsPaityvisfluid
numberreynoldsNND
mimpellerofdiameterD
orHzimpellerofspeedN
densityfluid
WPowerP
numberPowerN
Fr
smkg
srotations
m
kg
P
2
Re
2
][cos
][
][
3
For geometrically similar vessels, ratios of all terms to right of the Froude number are negligible.
The Froude number is only important when significant vortex develops (in unbaffled tanks); for baffled tanks the NP does not depend on the Froude number.
17
Power Consumption and Scale-up in Mixing
Consider low viscosity, unbaffled systems.
Colson and Richardson.
ba
P g
DNNDKN
22
aP NKNNat ReRe :300
57.43.0
37.1
D
T57.4
3.0
37.1
D
H1
3.0
3.0
D
C
18
In-Class PS Exercise
Consider a solution of sodium hydroxide with the properties listed below. It is agitated by a propeller mixer that is 0.5m in diameter in a 2.28m diameter unbaffled tank. The liquid depth is 2.28m. The impeller is located 0.5m above the bottom of the tank. If the propeller is rotated at 2 Hz, what power is required?
cPityvis
densitym
kg
50cos
1650 3
19
Power Consumption and Scale-up in Mixing
Consider low viscosity, baffled systems.
Colson and Richardson.
a
P
NDKN
2
20
Power Consumption and Scale-up in Mixing
Consider low viscosity, baffled systems (wall baffles).
Colson and Richardson.Figure 10.59 Power correlations for turbine impellers in a tank with 4 baffles. [w, D, impeller width and diameter, respectively.]
21
In-Class PS Exercise
Assume you are mixing a small amount of material into water in a standard configuration baffled tank. The diameter of the pitched blade turbine is 1 m and it is desired to operate at 84 RPM. Estimate the power required.
22
Power Consumption and Scale-up in Mixing
Consider low viscosity, baffled systems (wall baffles).
N.P. Cheremisinoff, Handbook of Chemical Processing Equipment, B-H, 2000
23
Power Consumption and Scale-up in Mixing
Propeller pitch:
24
Other Terms in Mixing
Pumping Capacity: discharge flowrate from an impeller:
][arg
arg
:
][
3
3
sm
Q
Q
rateedischvolumetricQ
tcoefficienedischimpellerN
where
unitlessND
QN
Tip Speed of an impeller: ][ sm
t NDu
Torque: “twist” force acting on agitator shaft: ][22
52
sWDNN
N
PT P
q
Power per unit volume: 324
53
mWP
HT
DNN
V
P
Blend time (estimation to within 5% desired concentration):
sD
H
D
T
NNP
5.05.1
953
1
40.5
000,10
0.150.0
33.0
5.033.0
Re
NTH
TC
TD
25
Discharge Coefficient
N.P. Cheremisinoff, Handbook of Chemical Processing Equipment, B-H, 2000
26
Mixing Time
P.M. Doran, Bioprocess Engineering Principles, 2nd Ed., Academic Press 2012
NN
t
i
m
90
Blend time (estimation to within 10% desired concentration):
27
Mixing Time
P.M. Doran, Bioprocess Engineering Principles, 2nd Ed., Academic Press 2012
31
31
32
9.5
D
T
P
VTtm
Doran suggests that for turbulent mixing conditions, irrespective of the impeller type, that (baffled vessel, single impeller, H=T):
Verified under aerated conditions also (impeller not flooded) and for:
mDT
D
7.2
7.02.0
28
In-Class PS Exercise
A fermentation broth with properties as given below, is agitated in a 2.7 m3 baffled tank using a Rushton turbine with a diameter of 0.5 m and a stirred speed of 1 Hz. Estimate the mixing time.
sPaityvis
densitym
kg
210cos
1000 3
29
Additional Plots for Non-Standard Mixing
N.P. Cheremisinoff, Handbook of Chemical Processing Equipment, B-H, 2000
30
Additional Plots for Non-Standard Mixing
N.P. Cheremisinoff, Handbook of Chemical Processing Equipment, B-H, 2000
31
Additional Plots for Non-Standard Mixing
N.P. Cheremisinoff, Handbook of Chemical Processing Equipment, B-H, 2000
32
Additional Plots for Non-Standard Mixing
N.P. Cheremisinoff, Handbook of Chemical Processing Equipment, B-H, 2000
33
Heuristics
Questions?