1 2 3 4 5 ANALYTICAL REPORT 6 - US Department of Energy · application methods. TestAmerica s operations groups have reviewed the data for compliance with the laboratory QA/QC plan,

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica St. Louis13715 Rider Trail NorthEarth City, MO 63045Tel: (314)298-8566

TestAmerica Job ID: 160-18571-1Client Project/Site: ORNL Y-12 Outfall 200 Characterization

For:Alliant Corporation320 N Cedar Bluff RoadSuite 200Knoxville, Tennessee 37923

Attn: Doug Milloway

Authorized for release by:9/30/2016 5:48:18 PM

Erika Gish, Project Manager II(314)[email protected]

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents

Client: Alliant CorporationProject/Site: ORNL Y-12 Outfall 200 Characterization

TestAmerica Job ID: 160-18571-1

Page 2 of 59TestAmerica St. Louis

9/30/2016

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20

QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30

Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31

Subcontract Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32

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Case NarrativeClient: Alliant Corporation TestAmerica Job ID: 160-18571-1Project/Site: ORNL Y-12 Outfall 200 Characterization

Job ID: 160-18571-1

Laboratory: TestAmerica St. Louis

Narrative

CASE NARRATIVE

Client: Alliant Corporation

Project: ORNL Y-12 Outfall 200 Characterization

Report Number: 160-18571-1

With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control

limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses

performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmerica’s operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions

to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a % solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and

disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.”

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPTThe samples were received on 8/10/2016 9:20 AM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperature of the cooler at receipt was 20.0º C.

Receipt Exceptions

Samples are concrete cores and arrived with no thermal preservation: YMTFA81 9404 C1 (160-18571-1), YMTFA81 9404 C2 (160-18571-2), YMTFA81 9404 C3 (160-18571-3), YMTFA80 9418 C (160-18571-4) and YMTFA82 UNK1 C (160-18571-5). The client

instructed the lab to proceed.

Comments

Please see the attached subcontract report for analyses at TestAmerica Richland.

General Chemistry

These concrete core samples were disaggregated, dried then puck milled and split for a variety of analyses. The possible heat generation may have compromised the Tritium, Carbon-14 and Technetium-99 native to these samples. The data is provided with this narrative.

TestAmerica St. LouisPage 3 of 59 9/30/2016

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Job ID: 160-18571-1 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

YMTFA81 9404 C1 (160-18571-1), YMTFA81 9404 C2 (160-18571-2), YMTFA81 9404 C3 (160-18571-3), YMTFA80 9418 C (160-18571-4)

and YMTFA82 UNK1 C (160-18571-5)

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

POLYCHLORINATED BIPHENYLS (PCBS)

Samples YMTFA81 9404 C1 (160-18571-1), YMTFA81 9404 C2 (160-18571-2), YMTFA81 9404 C3 (160-18571-3), YMTFA80 9418 C (160-18571-4) and YMTFA82 UNK1 C (160-18571-5) were analyzed for Polychlorinated biphenyls (PCBs) with multi-incremental

preparation in accordance with 8082A. The samples were leached on 08/16/2016, prepared on 08/23/2016 and analyzed on 08/24/2016

and 08/26/2016.

Analytical Batch 160-266473 The following sample was diluted due to the abundance of PCB-1016: YMTFA81 9404 C2 (160-18571-2). As such, the elevated reporting

limits (RLs) are provided.

The internal standard eluted outside the retention time window for the following CCV: (CCVIS 160-266473/3). This retention time shift was taken into account when reviewing the sample(s) for target compounds.

The CCV recoveries for Aroclor 1260 and DCB are outside the lower QC limits on the secondary column, but within acceptable QC limits on the primary column. There were no hits above the RL for Aroclor 1260 and the surrogate recoveries in the samples were within acceptable QC limits on the primary column; therefore confirmation is not needed. (CCV 160-266473/39)

nalytical Batch 160-266183 The %RPD between the primary and confirmation column exceeded 40% for PCB-1016 for the following samples: YMTFA80 9418 C (160-18571-4). The lower values have been reported and qualified in accordance with the laboratory's SOP.

Surrogate recovery for the following sample was outside control limits: (160-18571-C-1-S MSD). Evidence of matrix interference is

present; therefore, re-extraction and/or re-analysis was not performed.

EPA Method 8082/8082A requires a minimum of 3 peaks to be used for PCB quantitation. Due to the presence of matrix interferences in the following sample, less than 5 peaks were used for quantitation.YMTFA81 9404 C1 (160-18571-1)

The matrix spike duplicate (MSD) recovery for PCB-1260 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS) and matrix spike (OMS) recoveries were within acceptance limits.

The matrix spike / matrix spike duplicate (MS/MSD) precision for PCB-1016 and PCB-1260 was outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample / laboratory control sample

duplicate (LCS/LCSD) precision was within acceptance limits.


TCLP METALS (ICP)

Samples YMTFA81 9404 C1 (160-18571-1), YMTFA81 9404 C2 (160-18571-2), YMTFA81 9404 C3 (160-18571-3), YMTFA80 9418 C

(160-18571-4) and YMTFA82 UNK1 C (160-18571-5) were analyzed for Metals (ICP) in accordance with SW-846 Method 1311/6010C. The samples were leached on 08/16/2016, prepared on 08/24/2016 and analyzed on 08/29/2016.

The following samples were diluted due to the nature of the sample matrix. Samples are high in salts: YMTFA81 9404 C1 (160-18571-1),

YMTFA81 9404 C2 (160-18571-2), YMTFA81 9404 C3 (160-18571-3), YMTFA80 9418 C (160-18571-4), YMTFA82 UNK1 C (160-18571-5),

(160-18613-A-1-Q MS ^), (160-18613-A-1-R MSD) and (160-18613-A-1-P SD ^). Elevated reporting limits (RLs) are provided.


TCLP MERCURY (CVAA)



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(160-18571-4) and YMTFA82 UNK1 C (160-18571-5) were analyzed for Mercury (CVAA) in accordance with SW-846 Method 1311/7470A.

The samples were leached on 08/16/2016, prepared on 08/24/2016 and analyzed on 08/25/2016.

The samples were re-digested/re-extracted due to a timer failure resulting in the samples digesting longer than permitted by the SOP.

Therefore the MS/MSD was spiked after preservation. YMTFA81 9404 C1 (160-18571-1), YMTFA81 9404 C2 (160-18571-2), YMTFA81 9404 C3 (160-18571-3), YMTFA80 9418 C (160-18571-4) and YMTFA82 UNK1 C (160-18571-5)


TRITIUMSamples YMTFA81 9404 C1 (160-18571-1), YMTFA81 9404 C2 (160-18571-2), YMTFA81 9404 C3 (160-18571-3), YMTFA80 9418 C

(160-18571-4) and YMTFA82 UNK1 C (160-18571-5) were analyzed for Tritium in accordance with DOE. The samples were prepared on 08/19/2016 and analyzed on 08/22/2016.

No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

RADIUM-226 BY ALPHA SPECTROMETRY

Samples YMTFA81 9404 C1 (160-18571-1), YMTFA81 9404 C2 (160-18571-2), YMTFA81 9404 C3 (160-18571-3), YMTFA80 9418 C (160-18571-4) and YMTFA82 UNK1 C (160-18571-5) were analyzed for Radium-226 by Alpha Spectrometry in accordance with ST-RC-0301. The samples were dried on 08/10/2016, prepared on 08/22/2016 and 08/30/2016 and analyzed on 09/15/2016 and 09/16/2016.

Sample YMTFA81 9404 C1 (160-18571-1) produced white crystals during the co-precipitation process. The filter was rinsed several times to help break up the crystals. A few larger crystal chunks remained on the filter.

The At-217 tracer recovery for the following samples was low outside the QC limits of 30%: LCS 160-266021/2-A: 28.2%. The DOE/DOD Quality Systems Manual for Environmental Laboratories (QSM Rev. 5.0) allows for reporting results as quantitative when tracer recoveries

are below 30% if a) the relative uncertainty associated with the tracer recovery is less than 10% (2 sigma), b) spectral resolution requirements are met and there are no indications of spectral interferences, and c) detection limit requirements are met. All three of these criteria are met for these samples: a) a minimum of 400 counts (which leads to 10% count uncertainty at 2 sigma) in the tracer peak, b) resolution of < 100 keV is met for all peaks, and c) the activity in the sample is well above the MDC. The data have been qualified and reported. YMTFA81 9404 C1 (160-18571-1), YMTFA81 9404 C2 (160-18571-2), YMTFA81 9404 C3 (160-18571-3), YMTFA80 9418 C

(160-18571-4), YMTFA82 UNK1 C (160-18571-5), (LCS 160-266021/2-A), (MB 160-266021/1-A), (160-18504-F-1-P) and (160-18504-F-1-Q DU)

The At-217 tracer recovery for the following sample was low outside the QC limits of 30%: (25.3) YMTFA81 9404 C1 (160-18571-1). The

DOE/DOD Quality Systems Manual for Environmental Laboratories (QSM Rev. 5.0) allows for reporting results as quantitative when tracer recoveries are below 30% if a) the relative uncertainty associated with the tracer recovery is less than 10% (2 sigma), b) spectral

resolution requirements are met and there are no indications of spectral interferences, and c) detection limit requirements are met. All

three of these criteria are met for these samples: a) a minimum of 400 counts (which leads to 10% count uncertainty at 2 sigma) in the tracer peak, b) resolution of < 100 keV is met for all peaks, and c) the activity in the sample is well above the MDC. The data have been

qualified and reported.


TOTAL BETA STRONTIUM (GFPC)

Samples YMTFA81 9404 C1 (160-18571-1), YMTFA81 9404 C2 (160-18571-2), YMTFA81 9404 C3 (160-18571-3), YMTFA80 9418 C (160-18571-4) and YMTFA82 UNK1 C (160-18571-5) were analyzed for Total Beta Strontium (GFPC) in accordance with SR-03-RC. The

samples were dried on 08/10/2016, prepared on 08/22/2016 and analyzed on 08/25/2016.

No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

TECHNETIUM-99 (LSC)


(160-18571-4) and YMTFA82 UNK1 C (160-18571-5) were analyzed for Technetium-99 (LSC) in accordance with TC_02_RC. The


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samples were prepared on 08/18/2016 and analyzed on 08/23/2016 and 08/24/2016.

The following samples have Tc-99 tracer recoveries below the 30% QC limit; (160-18571-C-1-C: 21.1% and 160-18571-C-1-D: 23.5%).

The LCS (laboratory control sample) has an acceptable spike recovery demonstrating acceptable sample preparation and instrument

performance. Matrix interference is suspected. The data have been qualified and reported. YMTFA81 9404 C1 (160-18571-1) and (160-18571-C-1-D DU).

The following samples counted off the upper end of the quench curve parameter (tSIE/AEC): YMTFA81 9404 C1 (160-18571-1), YMTFA81

9404 C2 (160-18571-2), YMTFA81 9404 C3 (160-18571-3), YMTFA80 9418 C (160-18571-4), YMTFA82 UNK1 C (160-18571-5), (LCS

160-265424/2-A), (MB 160-265424/1-A) and (160-18571-C-1-D DU). A small amount (10 uL) of quenching agent (nitromethane) was added to the affected vials and recounted. The recount results were within the quench curve parameter and are reported.

The following samples did not meet the detection goal of 1.00 pCi/g due to a high bias attributed to low tracer recoveries. The data have

been qualified and reported. YMTFA81 9404 C1 (160-18571-1) and (160-18571-C-1-D DU)



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Page 7 of 59 9/30/2016

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Login Sample Receipt Checklist

Client: Alliant Corporation Job Number: 160-18571-1

Login Number: 18571

Question Answer Comment

Creator: Clarke, Jill C

List Source: TestAmerica St. Louis

List Number: 1

TrueRadioactivity wasn't checked or is </= background as measured by a survey meter.

N/AThe cooler's custody seal, if present, is intact.

N/ASample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

FalseSamples were received on ice. Client instructed the lab to proceed.

FalseCooler Temperature is acceptable. Client instructed the lab to proceed.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time (excluding tests with immediate HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


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Definitions/GlossaryTestAmerica Job ID: 160-18571-1Client: Alliant Corporation

Project/Site: ORNL Y-12 Outfall 200 Characterization

Qualifiers

GC Semi VOA

Qualifier Description

U Undetected at the Limit of Detection.

Qualifier

S Surrogate is outside control limits

* MS/MSD RPD exceeded the control limit

N MS, MSD: Spike recovery is outside acceptance limits.

J Estimated: The analyte was positively identified; the quantitation is an estimation

J Estimated: The quantitation is an estimation due to discrepancies in meeting certain analyte-specific quality control criteria.

Metals


J Estimated: The analyte was positively identified; the quantitation is an estimation

Qualifier


Rad



Qualifier

S Tracer is outside acceptance limits.

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TestAmerica St. Louis

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Method SummaryTestAmerica Job ID: 160-18571-1Client: Alliant Corporation


Method Method Description LaboratoryProtocol

SW8468082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography TAL SL

SW8466010C TCLP Metals (ICP) TAL SL

SW8467470A Mercury (TCLP) TAL SL

DOEH3-04-RC Tritium (LSC) TAL SL

DOESR-03-RC Total Beta Strontium (GFPC) TAL SL

TAL-STLST-RC-0301 Radium-226 (Alpha Spectrometry) TAL SL

DOETC-02-RC Technetium-99 (LSC) TAL SL

NONEAm-241 General Sub Contract Method TAL RCH

NONEC-14 General Sub Contract Method TAL RCH

NONENp-237 General Sub Contract Method TAL RCH

NONEPu-238,

Pu-239/240

General Sub Contract Method TAL RCH

NONETh-228, Th-230,

Th-232


NONEU-233/234,

U-235/236, U-238


Protocol References:

DOE = U.S. Department of Energy

NONE = NONE

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TAL-STL = TestAmerica Laboratories, St. Louis, Facility Standard Operating Procedure.

Laboratory References:

TAL RCH = TestAmerica Richland, 2800 George Washington Way, Richland, WA 99352, TEL (509)375-3131

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566


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Sample SummaryTestAmerica Job ID: 160-18571-1Client: Alliant Corporation


Lab Sample ID Client Sample ID ReceivedCollectedMatrix

160-18571-1 YMTFA81 9404 C1 Solid 08/09/16 15:30 08/10/16 09:20

160-18571-2 YMTFA81 9404 C2 Solid 08/09/16 15:36 08/10/16 09:20

160-18571-3 YMTFA81 9404 C3 Solid 08/09/16 15:40 08/10/16 09:20

160-18571-4 YMTFA80 9418 C Solid 08/09/16 15:50 08/10/16 09:20

160-18571-5 YMTFA82 UNK1 C Solid 08/09/16 16:00 08/10/16 09:20


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Detection SummaryTestAmerica Job ID: 160-18571-1Client: Alliant Corporation


Client Sample ID: YMTFA81 9404 C1 Lab Sample ID: 160-18571-1

Sample Analysis Not Complete.





Client Sample ID: YMTFA80 9418 C Lab Sample ID: 160-18571-4


Client Sample ID: YMTFA82 UNK1 C Lab Sample ID: 160-18571-5



This Detection Summary does not include radiochemical test results.

Page 12 of 59 9/30/2016

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Client Sample ResultsTestAmerica Job ID: 160-18571-1Client: Alliant Corporation


Lab Sample ID: 160-18571-1Client Sample ID: YMTFA81 9404 C1Matrix: SolidDate Collected: 08/09/16 15:30

Date Received: 08/10/16 09:20

Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyRL MDL

PCB-1016 0.0096 U 0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 12:20 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 12:20 1PCB-1221 0.0096 U

0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 12:20 1PCB-1232 0.0096 U

0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 12:20 1PCB-1242 0.0096 U

0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 12:20 1PCB-1248 0.0096 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 12:20 1PCB-1254 0.0080 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 12:20 1PCB-1260 0.0080 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 12:20 1PCB-1262 0.0080 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 12:20 1PCB-1268 0.0080 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 12:20 1Polychlorinated biphenyls, Total 0.0080 U

DCB Decachlorobiphenyl (Surr) 81 23 - 146 08/23/16 10:23 08/24/16 12:20 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

Method: 6010C - TCLP Metals (ICP)RL MDL

Arsenic 0.050 U 0.13 0.050 mg/L 08/24/16 16:41 08/29/16 22:35 5


0.63 0.19 mg/L 08/24/16 16:41 08/29/16 22:35 5Barium 0.27 J

0.063 0.019 mg/L 08/24/16 16:41 08/29/16 22:35 5Cadmium 0.019 U

0.13 0.038 mg/L 08/24/16 16:41 08/29/16 22:35 5Chromium 0.038 U

0.13 0.038 mg/L 08/24/16 16:41 08/29/16 22:35 5Lead 0.038 U

0.19 0.063 mg/L 08/24/16 16:41 08/29/16 22:35 5Selenium 0.063 U

0.13 0.038 mg/L 08/24/16 16:41 08/29/16 22:35 5Silver 0.038 U

Method: 7470A - Mercury (TCLP)RL MDL

Mercury 0.00021 J 0.0010 0.000079 mg/L 08/24/16 12:29 08/25/16 09:25 1


Method: H3-04-RC - Tritium (LSC)

Analyte

Tritium 0.178 U

(2σ+/-)

0.184

(2σ+/-)

108/22/16 16:0708/19/16 13:28pCi/g0.2931.00

RL MDC

0.183

Dil FacAnalyzedPreparedUnitResult Qualifier

Count Total

Uncert. Uncert.

Method: SR-03-RC - Total Beta Strontium (GFPC)

Analyte

Strontium 89/90 -0.0149 U

(2σ+/-)

0.118

(2σ+/-)

108/25/16 13:5508/22/16 21:29pCi/g0.2153.00

RL MDC

0.118


Count Total

Uncert. Uncert.

Sr Carrier 40 - 110

Carrier

08/22/16 21:29 08/25/16 13:55 1

Dil FacAnalyzedPreparedQualifier Limits%Yield

84.1

Method: ST-RC-0301 - Radium-226 (Alpha Spectrometry)

Analyte

Radium-226 0.734

(2σ+/-)

0.218

(2σ+/-)

109/15/16 10:1908/22/16 18:53pCi/g0.1611.00

RL MDC

0.210


Count Total

Uncert. Uncert.

At-217 30 - 110

Tracer

S 08/22/16 18:53 09/15/16 10:19 1


25.3


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Method: TC-02-RC - Technetium-99 (LSC)

Analyte

Technetium-99 0.0971 U

(2σ+/-)

0.805

(2σ+/-)

108/24/16 10:5008/18/16 11:40pCi/g1.361.00

RL MDC

0.805


Count Total

Uncert. Uncert.

Tc-99m 30 - 110

Tracer

S 08/18/16 11:40 08/24/16 10:50 1


21.1




PCB-1221 0.0096 U 0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 13:27 1


0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 13:27 1PCB-1232 0.0096 U

0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 13:27 1PCB-1242 0.0096 U

0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 13:27 1PCB-1248 0.0096 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 13:27 1PCB-1254 0.0080 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 13:27 1PCB-1260 0.069

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 13:27 1PCB-1262 0.0080 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 13:27 1PCB-1268 0.0080 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 13:27 1Polychlorinated biphenyls, Total 1.6



Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography - DLRL MDL

PCB-1016 1.7 0.16 0.048 mg/Kg 08/23/16 10:23 08/26/16 08:35 5



Arsenic 0.050 U 0.13 0.050 mg/L 08/24/16 16:41 08/29/16 22:39 5


0.63 0.19 mg/L 08/24/16 16:41 08/29/16 22:39 5Barium 0.28 J

0.063 0.019 mg/L 08/24/16 16:41 08/29/16 22:39 5Cadmium 0.019 U

0.13 0.038 mg/L 08/24/16 16:41 08/29/16 22:39 5Chromium 0.038 U

0.13 0.038 mg/L 08/24/16 16:41 08/29/16 22:39 5Lead 0.038 U

0.19 0.063 mg/L 08/24/16 16:41 08/29/16 22:39 5Selenium 0.063 U

0.13 0.038 mg/L 08/24/16 16:41 08/29/16 22:39 5Silver 0.038 U


Mercury 0.00021 J 0.0010 0.000079 mg/L 08/24/16 12:29 08/25/16 09:27 1



Analyte

Tritium 0.184 U

(2σ+/-)

0.192

(2σ+/-)

108/22/16 16:3008/19/16 13:28pCi/g0.3111.00

RL MDC

0.192


Count Total

Uncert. Uncert.


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Analyte


(2σ+/-)

0.151

(2σ+/-)

108/25/16 13:5508/22/16 21:29pCi/g0.2933.00

RL MDC

0.151


Count Total

Uncert. Uncert.

Sr Carrier 40 - 110

Carrier

08/22/16 21:29 08/25/16 13:55 1


71.6


Analyte

Radium-226 0.566

(2σ+/-)

0.165

(2σ+/-)

109/15/16 10:1908/22/16 18:53pCi/g0.1101.00

RL MDC

0.158


Count Total

Uncert. Uncert.

At-217 30 - 110

Tracer

08/22/16 18:53 09/15/16 10:19 1


39.1


Analyte


(2σ+/-)

0.424

(2σ+/-)

108/23/16 17:4308/18/16 11:40pCi/g0.6901.00

RL MDC

0.422


Count Total

Uncert. Uncert.

Tc-99m 30 - 110

Tracer

08/18/16 11:40 08/23/16 17:43 1


65.3




PCB-1016 0.095 0.033 0.0095 mg/Kg 08/23/16 10:23 08/24/16 13:50 1


0.033 0.0095 mg/Kg 08/23/16 10:23 08/24/16 13:50 1PCB-1221 0.0095 U

0.033 0.0095 mg/Kg 08/23/16 10:23 08/24/16 13:50 1PCB-1232 0.0095 U

0.033 0.0095 mg/Kg 08/23/16 10:23 08/24/16 13:50 1PCB-1242 0.0095 U

0.033 0.0095 mg/Kg 08/23/16 10:23 08/24/16 13:50 1PCB-1248 0.0095 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 13:50 1PCB-1254 0.0080 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 13:50 1PCB-1260 0.0080 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 13:50 1PCB-1262 0.0080 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 13:50 1PCB-1268 0.0080 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 13:50 1Polychlorinated biphenyls, Total 0.095




Arsenic 0.050 U 0.13 0.050 mg/L 08/24/16 16:41 08/29/16 22:44 5


0.63 0.19 mg/L 08/24/16 16:41 08/29/16 22:44 5Barium 0.32 J

0.063 0.019 mg/L 08/24/16 16:41 08/29/16 22:44 5Cadmium 0.019 U

0.13 0.038 mg/L 08/24/16 16:41 08/29/16 22:44 5Chromium 0.038 U


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Method: 6010C - TCLP Metals (ICP) (Continued)RL MDL

Lead 0.038 U 0.13 0.038 mg/L 08/24/16 16:41 08/29/16 22:44 5


0.19 0.063 mg/L 08/24/16 16:41 08/29/16 22:44 5Selenium 0.063 U

0.13 0.038 mg/L 08/24/16 16:41 08/29/16 22:44 5Silver 0.038 U


Mercury 0.00020 J 0.0010 0.000079 mg/L 08/24/16 12:29 08/25/16 09:29 1



Analyte

Tritium 0.186 U

(2σ+/-)

0.188

(2σ+/-)

108/22/16 16:5308/19/16 13:28pCi/g0.2991.00

RL MDC

0.187


Count Total

Uncert. Uncert.


Analyte

Strontium 89/90 0.0598 U

(2σ+/-)

0.137

(2σ+/-)

108/25/16 13:5508/22/16 21:29pCi/g0.2343.00

RL MDC

0.137


Count Total

Uncert. Uncert.

Sr Carrier 40 - 110

Carrier

08/22/16 21:29 08/25/16 13:55 1


88.0


Analyte

Radium-226 0.736

(2σ+/-)

0.221

(2σ+/-)

109/16/16 10:1708/30/16 15:54pCi/g0.2271.00

RL MDC

0.212


Count Total

Uncert. Uncert.

At-217 30 - 110

Tracer

08/30/16 15:54 09/16/16 10:17 1


35.6


Analyte

Technetium-99 -0.0396 U

(2σ+/-)

0.441

(2σ+/-)

108/24/16 12:2308/18/16 11:40pCi/g0.7501.00

RL MDC

0.441


Count Total

Uncert. Uncert.

Tc-99m 30 - 110

Tracer

08/18/16 11:40 08/24/16 12:23 1


40.3

Lab Sample ID: 160-18571-4Client Sample ID: YMTFA80 9418 CMatrix: SolidDate Collected: 08/09/16 15:50



PCB-1016 0.013 J 0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 14:12 1


0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 14:12 1PCB-1221 0.0096 U

0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 14:12 1PCB-1232 0.0096 U

0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 14:12 1PCB-1242 0.0096 U

0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 14:12 1PCB-1248 0.0096 U


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Lab Sample ID: 160-18571-4Client Sample ID: YMTFA80 9418 CMatrix: SolidDate Collected: 08/09/16 15:50


Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)RL MDL

PCB-1254 0.0080 U 0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 14:12 1


0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 14:12 1PCB-1260 0.0080 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 14:12 1PCB-1262 0.0080 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 14:12 1PCB-1268 0.0080 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 14:12 1Polychlorinated biphenyls, Total 0.013 J




Arsenic 0.050 U 0.13 0.050 mg/L 08/24/16 16:41 08/29/16 22:48 5


0.63 0.19 mg/L 08/24/16 16:41 08/29/16 22:48 5Barium 0.38 J

0.063 0.019 mg/L 08/24/16 16:41 08/29/16 22:48 5Cadmium 0.019 U

0.13 0.038 mg/L 08/24/16 16:41 08/29/16 22:48 5Chromium 0.038 U

0.13 0.038 mg/L 08/24/16 16:41 08/29/16 22:48 5Lead 0.038 U

0.19 0.063 mg/L 08/24/16 16:41 08/29/16 22:48 5Selenium 0.063 U

0.13 0.038 mg/L 08/24/16 16:41 08/29/16 22:48 5Silver 0.038 U


Mercury 0.00023 J 0.0010 0.000079 mg/L 08/24/16 12:29 08/25/16 09:36 1



Analyte

Tritium 0.132 U

(2σ+/-)

0.177

(2σ+/-)

108/22/16 17:1508/19/16 13:28pCi/g0.2901.00

RL MDC

0.177


Count Total

Uncert. Uncert.


Analyte


(2σ+/-)

0.198

(2σ+/-)

108/25/16 13:5508/22/16 21:29pCi/g0.3623.00

RL MDC

0.198


Count Total

Uncert. Uncert.

Sr Carrier 40 - 110

Carrier

08/22/16 21:29 08/25/16 13:55 1


51.6


Analyte

Radium-226 0.354

(2σ+/-)

0.115

(2σ+/-)

109/15/16 10:1908/30/16 15:54pCi/g0.07711.00

RL MDC

0.111


Count Total

Uncert. Uncert.

At-217 30 - 110

Tracer

08/30/16 15:54 09/15/16 10:19 1


43.6


Analyte


(2σ+/-)

0.288

(2σ+/-)

108/23/16 18:2408/18/16 11:40pCi/g0.4951.00

RL MDC

0.288


Count Total

Uncert. Uncert.


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Tc-99m 30 - 110

Tracer

08/18/16 11:40 08/23/16 18:24 1


84.1

Lab Sample ID: 160-18571-5Client Sample ID: YMTFA82 UNK1 CMatrix: SolidDate Collected: 08/09/16 16:00



PCB-1016 0.0096 U 0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 14:35 1


0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 14:35 1PCB-1221 0.0096 U

0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 14:35 1PCB-1232 0.0096 U

0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 14:35 1PCB-1242 0.0096 U

0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 14:35 1PCB-1248 0.0096 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 14:35 1PCB-1254 0.0080 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 14:35 1PCB-1260 0.0080 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 14:35 1PCB-1262 0.0080 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 14:35 1PCB-1268 0.0080 U

0.033 0.0080 mg/Kg 08/23/16 10:23 08/24/16 14:35 1Polychlorinated biphenyls, Total 0.0080 U




Arsenic 0.050 U 0.13 0.050 mg/L 08/24/16 16:41 08/29/16 22:53 5


0.63 0.19 mg/L 08/24/16 16:41 08/29/16 22:53 5Barium 0.37 J

0.063 0.019 mg/L 08/24/16 16:41 08/29/16 22:53 5Cadmium 0.019 U

0.13 0.038 mg/L 08/24/16 16:41 08/29/16 22:53 5Chromium 0.038 U

0.13 0.038 mg/L 08/24/16 16:41 08/29/16 22:53 5Lead 0.038 U

0.19 0.063 mg/L 08/24/16 16:41 08/29/16 22:53 5Selenium 0.063 U

0.13 0.038 mg/L 08/24/16 16:41 08/29/16 22:53 5Silver 0.038 U


Mercury 0.00021 J 0.0010 0.000079 mg/L 08/24/16 12:29 08/25/16 09:38 1



Analyte

Tritium 0.213 U

(2σ+/-)

0.186

(2σ+/-)

108/22/16 17:3808/19/16 13:28pCi/g0.2881.00

RL MDC

0.185


Count Total

Uncert. Uncert.


Analyte


(2σ+/-)

0.121

(2σ+/-)

108/25/16 13:5508/22/16 21:29pCi/g0.2213.00

RL MDC

0.121


Count Total

Uncert. Uncert.

Sr Carrier 40 - 110

Carrier

08/22/16 21:29 08/25/16 13:55 1


85.4


Analyte

Radium-226 0.632

(2σ+/-)

0.171

(2σ+/-)

109/15/16 10:1908/30/16 15:54pCi/g0.1431.00

RL MDC

0.163


Count Total

Uncert. Uncert.


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Lab Sample ID: 160-18571-5Client Sample ID: YMTFA82 UNK1 CMatrix: SolidDate Collected: 08/09/16 16:00


At-217 30 - 110

Tracer

08/30/16 15:54 09/15/16 10:19 1


45.2


Analyte


(2σ+/-)

0.293

(2σ+/-)

108/23/16 18:4508/18/16 11:40pCi/g0.4931.00

RL MDC

0.292


Count Total

Uncert. Uncert.

Tc-99m 30 - 110

Tracer

08/18/16 11:40 08/23/16 18:45 1


87.9


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QC Sample ResultsTestAmerica Job ID: 160-18571-1Client: Alliant Corporation


Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography

Client Sample ID: Method BlankLab Sample ID: MB 160-266064/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 266183 Prep Batch: 266064

RL MDL

PCB-1016 0.0096 U 0.033 0.0096 mg/Kg 08/23/16 10:23 08/24/16 11:34 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

0.0096 U 0.00960.033 mg/Kg 08/23/16 10:23 08/24/16 11:34 1PCB-1221

0.0096 U 0.00960.033 mg/Kg 08/23/16 10:23 08/24/16 11:34 1PCB-1232

0.0096 U 0.00960.033 mg/Kg 08/23/16 10:23 08/24/16 11:34 1PCB-1242

0.0096 U 0.00960.033 mg/Kg 08/23/16 10:23 08/24/16 11:34 1PCB-1248

0.0080 U 0.00800.033 mg/Kg 08/23/16 10:23 08/24/16 11:34 1PCB-1254

0.0080 U 0.00800.033 mg/Kg 08/23/16 10:23 08/24/16 11:34 1PCB-1260

0.0080 U 0.00800.033 mg/Kg 08/23/16 10:23 08/24/16 11:34 1PCB-1262

0.0080 U 0.00800.033 mg/Kg 08/23/16 10:23 08/24/16 11:34 1PCB-1268

0.0080 U 0.00800.033 mg/Kg 08/23/16 10:23 08/24/16 11:34 1Polychlorinated biphenyls, Total

DCB Decachlorobiphenyl (Surr) 94 23 - 146 08/24/16 11:34 1

MB MB

Surrogate

08/23/16 10:23

Dil FacPrepared AnalyzedQualifier Limits%Recovery

Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-266064/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 266183 Prep Batch: 266064

PCB-1016 0.167 0.148 mg/Kg 89 52 - 134

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

PCB-1260 0.167 0.150 mg/Kg 90 50 - 132

DCB Decachlorobiphenyl (Surr) 23 - 146

Surrogate

100

LCS LCS

Qualifier Limits%Recovery

Client Sample ID: YMTFA81 9404 C1Lab Sample ID: 160-18571-1 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 266183 Prep Batch: 266064

PCB-1016 0.0096 U 0.166 0.0897 mg/Kg 54 23 - 140

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

PCB-1260 0.0080 U 0.166 0.0927 mg/Kg 56 20 - 131

DCB Decachlorobiphenyl (Surr) 23 - 146

Surrogate

68

MS MS


Client Sample ID: YMTFA81 9404 C1Lab Sample ID: 160-18571-1 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 266183 Prep Batch: 266064

PCB-1016 0.0096 U 0.165 0.218 * mg/Kg 132 23 - 140 83 30

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

PCB-1260 0.0080 U 0.165 0.232 N * mg/Kg 140 20 - 131 86 30

DCB Decachlorobiphenyl (Surr) S 23 - 146

Surrogate

154

MSD MSD



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Method: 6010C - TCLP Metals (ICP)

Client Sample ID: Method BlankLab Sample ID: LB 160-265574/1-CMatrix: Solid Prep Type: Total/NAAnalysis Batch: 267177 Prep Batch: 266424

RL MDL

Arsenic 0.010 U 0.025 0.010 mg/L 08/24/16 16:41 08/29/16 21:04 1

LB LB


0.038 U 0.0380.13 mg/L 08/24/16 16:41 08/29/16 21:04 1Barium

0.0038 U 0.00380.013 mg/L 08/24/16 16:41 08/29/16 21:04 1Cadmium

0.0075 U 0.00750.025 mg/L 08/24/16 16:41 08/29/16 21:04 1Chromium

0.0075 U 0.00750.025 mg/L 08/24/16 16:41 08/29/16 21:04 1Lead

0.013 U 0.0130.038 mg/L 08/24/16 16:41 08/29/16 21:04 1Selenium

0.0075 U 0.00750.025 mg/L 08/24/16 16:41 08/29/16 21:04 1Silver


Arsenic 2.50 2.35 mg/L 94 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Barium 2.50 2.33 mg/L 93 80 - 120

Cadmium 2.50 2.45 mg/L 98 80 - 120

Chromium 2.50 2.54 mg/L 102 80 - 120

Lead 2.50 2.60 mg/L 104 80 - 120

Selenium 1.25 1.31 mg/L 105 80 - 120

Silver 0.500 0.505 mg/L 101 80 - 120

Client Sample ID: Matrix SpikeLab Sample ID: 160-18613-A-1-Q MS ^5Matrix: Solid Prep Type: Total/NAAnalysis Batch: 267177 Prep Batch: 266424

Arsenic 0.050 U 2.50 2.41 mg/L 96 75 - 125

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Barium 0.20 J 2.50 2.54 mg/L 94 75 - 125

Cadmium 0.019 U 2.50 2.53 mg/L 101 75 - 125

Chromium 0.040 J 2.50 2.59 mg/L 102 75 - 125

Lead 0.038 U 2.50 2.62 mg/L 105 75 - 125

Selenium 0.063 U 1.25 1.28 mg/L 102 75 - 125

Silver 0.038 U 0.500 0.508 mg/L 102 75 - 125

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 160-18613-A-1-R MSD ^5Matrix: Solid Prep Type: Total/NAAnalysis Batch: 267177 Prep Batch: 266424

Arsenic 0.050 U 2.50 2.44 mg/L 97 75 - 125 1 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Barium 0.20 J 2.50 2.53 mg/L 93 75 - 125 0 20

Cadmium 0.019 U 2.50 2.53 mg/L 101 75 - 125 0 20

Chromium 0.040 J 2.50 2.59 mg/L 102 75 - 125 0 20

Lead 0.038 U 2.50 2.62 mg/L 105 75 - 125 0 20

Selenium 0.063 U 1.25 1.30 mg/L 104 75 - 125 2 20

Silver 0.038 U 0.500 0.501 mg/L 100 75 - 125 1 20


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Method: 7470A - Mercury (TCLP)

Client Sample ID: Method BlankLab Sample ID: LB 160-266377/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 266547 Prep Batch: 266377

RL MDL

Mercury 0.000079 U 0.0010 0.000079 mg/L 08/24/16 12:29 08/25/16 08:56 1

LB LB



Mercury 0.0250 0.0245 mg/L 98 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: Matrix SpikeLab Sample ID: 160-18613-A-1-N MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 266547 Prep Batch: 266377

Mercury 0.000079 U 0.0250 0.0255 mg/L 102 70 - 130

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 160-18613-A-1-O MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 266547 Prep Batch: 266377

Mercury 0.000079 U 0.0250 0.0248 mg/L 99 70 - 130 3 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD



Tritium

Analyte

U 108/22/16 10:2808/19/16 13:28pCi/g0.305

MDC

1.00

RL

0.1750.175

(2σ+/-) (2σ+/-)

MB

0.06905

MB

Dil FacPrepared AnalyzedUnitResult Qualifier

Uncert.

Count

Uncert.

Total


Tritium

Analyte

114-8010510.6610.1 1.17 1.00 0.303

RL MDC(2σ+/-)

LCS LCS

pCi/g

UnitResult Qual %RecAdded

Spike

Limits

%Rec.Uncert.

Total

Client Sample ID: Matrix SpikeLab Sample ID: 160-18570-C-2-D MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 266040 Prep Batch: 265690

Tritium

Analyte

122-7810610.7210.10.177 U 1.21 1.00 0.345

RL MDC(2σ+/-)

MS MS

pCi/g


Spike

Result

Sample Sample

Qual Limits

%Rec.Uncert.

Total


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Method: H3-04-RC - Tritium (LSC) (Continued)

Client Sample ID: DuplicateLab Sample ID: 160-18570-E-1-B DUMatrix: Solid Prep Type: Total/NAAnalysis Batch: 266040 Prep Batch: 265690

Tritium

Analyte

10.18U0.23350.154 U 0.224 1.00 0.357

RL MDC(2σ+/-)

DU DU

pCi/g

UnitResult Qual LimitResult

Sample Sample

Qual

Uncert.

Total

RER

RER



Strontium 89/90

Analyte

U 108/25/16 13:5108/22/16 21:29pCi/g0.201

MDC

3.00

RL

0.1170.117

(2σ+/-) (2σ+/-)

MB

0.05486

MB


Uncert.

Count

Uncert.

Total

Carrier

Sr Carrier 40 - 110 08/22/16 21:29 08/25/16 13:51 1

Dil FacPrepared AnalyzedQualifier Limits%Yield

91.6

MB MB


Strontium 89/90

Analyte

125-75796.7948.60 0.633 3.00 0.208

RL MDC(2σ+/-)

LCS LCS

pCi/g


Spike

Limits

%Rec.Uncert.

Total

Sr Carrier

Carrier

40 - 110

LCS

Qualifier Limits%Yield

88.9

LCS

Client Sample ID: DuplicateLab Sample ID: 160-18613-A-6-G DUMatrix: Solid Prep Type: Total/NAAnalysis Batch: 266490 Prep Batch: 266028

Strontium 89/90

Analyte

10.23U-0.00952

3

0.0402 U 0.104 3.00 0.190

RL MDC(2σ+/-)

DU DU

pCi/g


Sample Sample

Qual

Uncert.

Total

RER

RER

Sr Carrier

Carrier

40 - 110

DU


88.7

DU


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Radium-226

Analyte

109/15/16 10:2008/22/16 18:53pCi/g0.0787

MDC

1.00

RL

0.09560.0942

(2σ+/-) (2σ+/-)

MB

0.1953

MB


Uncert.

Count

Uncert.

Total

Tracer

At-217 30 - 110 08/22/16 18:53 09/15/16 10:20 1


36.5

MB MB


Radium-226

Analyte

130-7011714.0712.1 1.47 1.00 0.103

RL MDC(2σ+/-)

LCS LCS

pCi/g


Spike

Limits

%Rec.Uncert.

Total

At-217

Tracer

S 30 - 110

LCS


28.2

LCS

Client Sample ID: DuplicateLab Sample ID: 160-18504-F-1-Q DUMatrix: Solid Prep Type: Total/NAAnalysis Batch: 270180 Prep Batch: 266021

Radium-226

Analyte

10.310.65920.772 0.171 1.00 0.152

RL MDC(2σ+/-)

DU DU

pCi/g


Sample Sample

Qual

Uncert.

Total

RER

RER

At-217

Tracer

30 - 110

DU


50.0

DU



Technetium-99

Analyte

U 108/23/16 16:1908/18/16 11:40pCi/g0.436

MDC

1.00

RL

0.2620.261

(2σ+/-) (2σ+/-)

MB

0.1678

MB


Uncert.

Count

Uncert.

Total

Tracer

Tc-99m 30 - 110 08/18/16 11:40 08/23/16 16:19 1


107

MB MB


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Method: TC-02-RC - Technetium-99 (LSC) (Continued)


Technetium-99

Analyte

125-759332.2334.5 3.26 1.00 0.459

RL MDC(2σ+/-)

LCS LCS

pCi/g


Spike

Limits

%Rec.Uncert.

Total

Tc-99m

Tracer

30 - 110

LCS


102

LCS

Client Sample ID: YMTFA81 9404 C1Lab Sample ID: 160-18571-1 DUMatrix: Solid Prep Type: Total/NAAnalysis Batch: 266388 Prep Batch: 265424

Technetium-99

Analyte

10.25U-0.27930.0971 U 0.719 1.00 1.24

RL MDC(2σ+/-)

DU DU

pCi/g


Sample Sample

Qual

Uncert.

Total

RER

RER

Tc-99m

Tracer

S 30 - 110

DU


23.5

DU


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QC Association SummaryTestAmerica Job ID: 160-18571-1Client: Alliant Corporation


GC Semi VOA

ISM Prep Batch: 265251

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid Increment, Prep160-18571-1 YMTFA81 9404 C1 Total/NA

Solid Increment, Prep160-18571-2 - DL YMTFA81 9404 C2 Total/NA



Solid Increment, Prep160-18571-4 YMTFA80 9418 C Total/NA

Solid Increment, Prep160-18571-5 YMTFA82 UNK1 C Total/NA

Solid Increment, Prep160-18571-1 MS YMTFA81 9404 C1 Total/NA

Solid Increment, Prep160-18571-1 MSD YMTFA81 9404 C1 Total/NA

Prep Batch: 266064


Solid 3550C 265251160-18571-1 YMTFA81 9404 C1 Total/NA

Solid 3550C 265251160-18571-2 - DL YMTFA81 9404 C2 Total/NA



Solid 3550C 265251160-18571-4 YMTFA80 9418 C Total/NA

Solid 3550C 265251160-18571-5 YMTFA82 UNK1 C Total/NA

Solid 3550CMB 160-266064/1-A Method Blank Total/NA

Solid 3550CLCS 160-266064/2-A Lab Control Sample Total/NA

Solid 3550C 265251160-18571-1 MS YMTFA81 9404 C1 Total/NA

Solid 3550C 265251160-18571-1 MSD YMTFA81 9404 C1 Total/NA

Analysis Batch: 266183


Solid 8082A 266064160-18571-1 YMTFA81 9404 C1 Total/NA



Solid 8082A 266064160-18571-4 YMTFA80 9418 C Total/NA

Solid 8082A 266064160-18571-5 YMTFA82 UNK1 C Total/NA

Solid 8082A 266064MB 160-266064/1-A Method Blank Total/NA

Solid 8082A 266064LCS 160-266064/2-A Lab Control Sample Total/NA

Solid 8082A 266064160-18571-1 MS YMTFA81 9404 C1 Total/NA

Solid 8082A 266064160-18571-1 MSD YMTFA81 9404 C1 Total/NA



Solid 8082A 266064160-18571-2 - DL YMTFA81 9404 C2 Total/NA

Metals

ISM Prep Batch: 265251





Solid Increment, Prep160-18571-4 YMTFA80 9418 C Total/NA

Solid Increment, Prep160-18571-5 YMTFA82 UNK1 C Total/NA

Solid Increment, Prep160-18613-A-1-N MS Matrix Spike Total/NA

Solid Increment, Prep160-18613-A-1-O MSD Matrix Spike Duplicate Total/NA

Solid Increment, Prep160-18613-A-1-Q MS ^5 Matrix Spike Total/NA


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Metals (Continued)

ISM Prep Batch: 265251 (Continued)


Solid Increment, Prep160-18613-A-1-R MSD ^5 Matrix Spike Duplicate Total/NA

Leach Batch: 265574


Solid 1311 265251160-18571-1 YMTFA81 9404 C1 Total/NA



Solid 1311 265251160-18571-4 YMTFA80 9418 C Total/NA

Solid 1311 265251160-18571-5 YMTFA82 UNK1 C Total/NA

Solid 1311LB 160-265574/1-C Method Blank Total/NA

Solid 1311 265251160-18613-A-1-N MS Matrix Spike Total/NA

Solid 1311 265251160-18613-A-1-O MSD Matrix Spike Duplicate Total/NA

Solid 1311 265251160-18613-A-1-Q MS ^5 Matrix Spike Total/NA

Solid 1311 265251160-18613-A-1-R MSD ^5 Matrix Spike Duplicate Total/NA

Prep Batch: 266377







Solid 7470ALB 160-266377/1-A Method Blank Total/NA

Solid 7470ALCS 160-266377/2-A Lab Control Sample Total/NA

Solid 7470A 265574160-18613-A-1-N MS Matrix Spike Total/NA

Solid 7470A 265574160-18613-A-1-O MSD Matrix Spike Duplicate Total/NA

Prep Batch: 266424







Solid 3010A 265574LB 160-265574/1-C Method Blank Total/NA

Solid 3010ALCS 160-266424/2-A Lab Control Sample Total/NA

Solid 3010A 265574160-18613-A-1-Q MS ^5 Matrix Spike Total/NA

Solid 3010A 265574160-18613-A-1-R MSD ^5 Matrix Spike Duplicate Total/NA








Solid 7470A 266377LB 160-266377/1-A Method Blank Total/NA

Solid 7470A 266377LCS 160-266377/2-A Lab Control Sample Total/NA

Solid 7470A 266377160-18613-A-1-N MS Matrix Spike Total/NA

Solid 7470A 266377160-18613-A-1-O MSD Matrix Spike Duplicate Total/NA


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Metals (Continued)






Solid 6010C 266424160-18571-4 YMTFA80 9418 C Total/NA

Solid 6010C 266424160-18571-5 YMTFA82 UNK1 C Total/NA

Solid 6010C 266424LB 160-265574/1-C Method Blank Total/NA

Solid 6010C 266424LCS 160-266424/2-A Lab Control Sample Total/NA

Solid 6010C 266424160-18613-A-1-Q MS ^5 Matrix Spike Total/NA

Solid 6010C 266424160-18613-A-1-R MSD ^5 Matrix Spike Duplicate Total/NA

Rad

Leach Batch: 263919


Solid Dry and Grind160-18504-F-1-Q DU Duplicate Total/NA

Leach Batch: 264333


Solid Dry and Grind160-18571-1 YMTFA81 9404 C1 Total/NA



Solid Dry and Grind160-18571-4 YMTFA80 9418 C Total/NA

Solid Dry and Grind160-18571-5 YMTFA82 UNK1 C Total/NA

Leach Batch: 264650


Solid Dry and Grind160-18613-A-6-G DU Duplicate Total/NA

Prep Batch: 265424


Solid Ext_Chrom_LSC160-18571-1 YMTFA81 9404 C1 Total/NA



Solid Ext_Chrom_LSC160-18571-4 YMTFA80 9418 C Total/NA

Solid Ext_Chrom_LSC160-18571-5 YMTFA82 UNK1 C Total/NA

Solid Ext_Chrom_LSCMB 160-265424/1-A Method Blank Total/NA

Solid Ext_Chrom_LSCLCS 160-265424/2-A Lab Control Sample Total/NA

Solid Ext_Chrom_LSC160-18571-1 DU YMTFA81 9404 C1 Total/NA

Prep Batch: 265690


Solid LSC_Dist_Susp160-18571-1 YMTFA81 9404 C1 Total/NA



Solid LSC_Dist_Susp160-18571-4 YMTFA80 9418 C Total/NA

Solid LSC_Dist_Susp160-18571-5 YMTFA82 UNK1 C Total/NA

Solid LSC_Dist_SuspMB 160-265690/1-A Method Blank Total/NA

Solid LSC_Dist_SuspLCS 160-265690/2-A Lab Control Sample Total/NA

Solid LSC_Dist_Susp160-18570-C-2-D MS Matrix Spike Total/NA

Solid LSC_Dist_Susp160-18570-E-1-B DU Duplicate Total/NA


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Rad (Continued)

Prep Batch: 266021


Solid DPS-0 264333160-18571-1 YMTFA81 9404 C1 Total/NA



Solid DPS-0 264333160-18571-4 YMTFA80 9418 C Total/NA

Solid DPS-0 264333160-18571-5 YMTFA82 UNK1 C Total/NA

Solid DPS-0MB 160-266021/1-A Method Blank Total/NA

Solid DPS-0LCS 160-266021/2-A Lab Control Sample Total/NA

Solid DPS-0 263919160-18504-F-1-Q DU Duplicate Total/NA

Prep Batch: 266028





Solid DPS-0 264333160-18571-4 YMTFA80 9418 C Total/NA

Solid DPS-0 264333160-18571-5 YMTFA82 UNK1 C Total/NA

Solid DPS-0MB 160-266028/1-A Method Blank Total/NA

Solid DPS-0LCS 160-266028/2-A Lab Control Sample Total/NA

Solid DPS-0 264650160-18613-A-6-G DU Duplicate Total/NA


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Surrogate SummaryTestAmerica Job ID: 160-18571-1Client: Alliant Corporation


Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyPrep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (23-146)

DCB2

81160-18571-1

Percent Surrogate Recovery (Acceptance Limits)

YMTFA81 9404 C1

68160-18571-1 MS YMTFA81 9404 C1

85160-18571-3 YMTFA81 9404 C3

83160-18571-4 YMTFA80 9418 C

89160-18571-5 YMTFA82 UNK1 C

100LCS 160-266064/2-A Lab Control Sample

94MB 160-266064/1-A Method Blank

Surrogate Legend

DCB = DCB Decachlorobiphenyl (Surr)

Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyPrep Type: Total/NAMatrix: Solid


DCB1

154 S160-18571-1 MSD

Percent Surrogate Recovery (Acceptance Limits)

YMTFA81 9404 C1

101160-18571-2 YMTFA81 9404 C2

Surrogate Legend

DCB = DCB Decachlorobiphenyl (Surr)


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Tracer/Carrier SummaryTestAmerica Job ID: 160-18571-1Client: Alliant Corporation


Method: SR-03-RC - Total Beta Strontium (GFPC)Prep Type: Total/NAMatrix: Solid


Sr (C)

84.1160-18571-1

Percent Yield (Acceptance Limits)

YMTFA81 9404 C1

71.6160-18571-2 YMTFA81 9404 C2

88.0160-18571-3 YMTFA81 9404 C3

51.6160-18571-4 YMTFA80 9418 C

85.4160-18571-5 YMTFA82 UNK1 C

88.7160-18613-A-6-G DU Duplicate

88.9LCS 160-266028/2-A Lab Control Sample

91.6MB 160-266028/1-A Method Blank

Tracer/Carrier Legend

Sr (C) = Sr Carrier

Method: ST-RC-0301 - Radium-226 (Alpha Spectrometry)Prep Type: Total/NAMatrix: Solid


At-217

50.0160-18504-F-1-Q DU


Duplicate

25.3 S160-18571-1 YMTFA81 9404 C1

39.1160-18571-2 YMTFA81 9404 C2

35.6160-18571-3 YMTFA81 9404 C3

43.6160-18571-4 YMTFA80 9418 C

45.2160-18571-5 YMTFA82 UNK1 C

28.2 SLCS 160-266021/2-A Lab Control Sample

36.5MB 160-266021/1-A Method Blank


At-217 = At-217

Method: TC-02-RC - Technetium-99 (LSC)Prep Type: Total/NAMatrix: Solid


Tc-99m

21.1 S160-18571-1


YMTFA81 9404 C1

23.5 S160-18571-1 DU YMTFA81 9404 C1

65.3160-18571-2 YMTFA81 9404 C2

40.3160-18571-3 YMTFA81 9404 C3

84.1160-18571-4 YMTFA80 9418 C

87.9160-18571-5 YMTFA82 UNK1 C

102LCS 160-265424/2-A Lab Control Sample

107MB 160-265424/1-A Method Blank


Tc-99m = Tc-99m


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Analytical Data Package Prepared For

Radiochemical Analysis By

TESTAMERICA ST. LOUIS

TestAmerica Inc

2800 G.W. Way, Richland Wa, 99354, (509)-375-3131.

Data Package Contains ______ Pages

Assigned Laboratory Code: TA-RL

Client Sample ID (List Order) Lot-Sa No. Work OrderSDG No.

Report No.: 69430

Order No. Report DB ID Batch No.

Results in this report relate only to the sample(s) analyzed.

YMTFA80 9418 C(160-

18571-4)

9M84WD1051962 J6H180411-4 M84WD1AE 6231063

YMTFA80 9418 C(160-

18571-4)

9M84WD10J6H180411-4 M84WD1AG 6231064

YMTFA80 9418 C(160-

18571-4)

9M84WD10J6H180411-4 M84WD1AD 6231068

YMTFA80 9418 C(160-

18571-4)

9M84WD20J6H180411-4 M84WD2AF 6250022

YMTFA80 9418 C(160-

18571-4)

9M84WD20J6H180411-4 M84WD2AC 6252054

YMTFA80 9418 C(160-

18571-4)

9M84WD20J6H180411-4 M84WD2AA 6252059

YMTFA81 9404 C1(160-

18571-1)

9M84V710J6H180411-1 M84V71AA 6231040

YMTFA81 9404 C1(160-

18571-1)

9M84V710J6H180411-1 M84V71AE 6231063

YMTFA81 9404 C1(160-

18571-1)

9M84V710J6H180411-1 M84V71AG 6231064

YMTFA81 9404 C1(160-

18571-1)

9M84V710J6H180411-1 M84V71AD 6231068

YMTFA81 9404 C1(160-

18571-1)

9M84V720J6H180411-1 M84V72AF 6250022

YMTFA81 9404 C1(160-

18571-1)

9M84V720J6H180411-1 M84V72AC 6252054

YMTFA81 9404 C2(160-

18571-2)

9M84V910J6H180411-2 M84V91AA 6231040

YMTFA81 9404 C2(160-

18571-2)

9M84V910J6H180411-2 M84V91AE 6231063

YMTFA81 9404 C2(160-

18571-2)

9M84V910J6H180411-2 M84V91AG 6231064

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Client Sample ID (List Order) Lot-Sa No. Work OrderSDG No.

Report No.: 69430

Order No. Report DB ID Batch No.


YMTFA81 9404 C2(160-

18571-2)

9M84V91051962 J6H180411-2 M84V91AD 6231068

YMTFA81 9404 C2(160-

18571-2)

9M84V920J6H180411-2 M84V92AF 6250022

YMTFA81 9404 C2(160-

18571-2)

9M84V920J6H180411-2 M84V92AC 6252054

YMTFA81 9404 C3(160-

18571-3)

9M84WC10J6H180411-3 M84WC1AA 6231040

YMTFA81 9404 C3(160-

18571-3)

9M84WC10J6H180411-3 M84WC1AE 6231063

YMTFA81 9404 C3(160-

18571-3)

9M84WC10J6H180411-3 M84WC1AG 6231064

YMTFA81 9404 C3(160-

18571-3)

9M84WC10J6H180411-3 M84WC1AD 6231068

YMTFA81 9404 C3(160-

18571-3)

9M84WC20J6H180411-3 M84WC2AF 6250022

YMTFA81 9404 C3(160-

18571-3)

9M84WC20J6H180411-3 M84WC2AC 6252054

YMTFA82 UNK1 C(160-

18571-5)

9M84WE10J6H180411-5 M84WE1AA 6231040

YMTFA82 UNK1 C(160-

18571-5)

9M84WE10J6H180411-5 M84WE1AE 6231063

YMTFA82 UNK1 C(160-

18571-5)

9M84WE10J6H180411-5 M84WE1AG 6231064

YMTFA82 UNK1 C(160-

18571-5)

9M84WE10J6H180411-5 M84WE1AD 6231068

YMTFA82 UNK1 C(160-

18571-5)

9M84WE20J6H180411-5 M84WE2AF 6250022

YMTFA82 UNK1 C(160-

18571-5)

9M84WE20J6H180411-5 M84WE2AC 6252054

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Certificate of Analysis

September 30, 2016


13715 Rider Trail North

Earth City, MO 63045

Attention: Erika Gish

Date Received in Lab : August 18, 2016

Sample Type : Five (5) Solid

SDG Number : 51962

Job Number : 160-18571-1

Project Number/Name : 16005502/ORNL Y-12 Outfall 200 Characterization

CASE NARRATIVE

I. Introduction

On August 18, 2016, five solid samples were received at the TestAmerica Richland laboratory for

radiochemical analysis. Upon receipt the samples were assigned to Lot Number J6H180411 with the

laboratory ID number corresponding to the client ID as shown on the cover page.

II. Sample Receipt

The samples were received in good condition; no anomalies were noted upon check-in.

III. Analytical Results/Methodology

The analytical results for this report are presented by laboratory sample ID. Each set of data includes

sample identification information; analytical results and the appropriate associated statistical

uncertainties.

The analyses requested were:

Alpha Spectroscopy

Americium 241 by method RL-ALP-001

Neptunium-237 by method RL-ALP-013

Plutonium-238, -239/240 by method RL-ALP-002

Thorium-228,230,232 by method RL-ALP-001

Uranium 234, 235 and 238 by method RL-ALP-009

Liquid Scintillation Counting

Carbon-14 by method RL-LSC-008


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September 30, 2016

IV. Quality Control

The analytical result for each analysis performed includes a minimum of one laboratory control sample

(LCS), and one reagent blank sample analysis. Any exceptions have been noted in the “Comments”

section.

V. Comments

Alpha Spectroscopy

Americium 241 by method RL-ALP-003:

The LCS, batch blank, sample duplicate and sample results are within acceptance limits

Neptunium-237 by method RL-ALP-013:


Plutonium-238, -239/240 by method RL-ALP-002:

The Pu 239/240 activity for the blank is above the MDA and CRDL. The sample activity is below the

MDA and CRDL and acts as their own blank, data accepted. Except as noted, the LCS, batch blank,

sample duplicate and sample results are within acceptance limits.

Thorium-228,230,232 by method RL-ALP-001


Uranium 234, 235 and 238 by method RL-ALP-015:


Liquid Scintillation Counting

Carbon-14 by method RL-LSC-008:

The LCS, batch blank, sample duplicate and sample results are within acceptance limits.

I certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC, both technically

and for completeness, for other than the conditions detailed above. The Laboratory Manager or a

designee, as verified by the following signature has authorized release of the data contained in this hard

copy data package.

Reviewed and approved:

____________________________

Roger A. Stringer

Project Manager I

TestAmerica Inc. 4 of 28

Roger A. StringerDigitally signed by Roger A. Stringer

DN: cn=Roger A. Stringer, o, ou,

[email protected], c=US

Date: 2016.09.30 15:27:03 -07'00'

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DRINKING WATER ASTM METHOD CROSS REFERENCES

Referenced Method Isotope(s) TestAmerica Richland's SOP No.

EPA 901.1 Cs-134, I-131 RL-GAM-001

EPA 900.0 Alpha & Beta RL-GPC-001

EPA 00-02 Gross Alpha (Coprecipitation) RL-GPC-002

EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002

EPA 903.1 Ra-226 RL-RA-001

EPA 904.0 Ra-228 RL-RA-001

EPA 905.0 Sr-89/90 RL-GPC-003

ASTM D5174 Uranium RL-KPA-003

EPA 906.0 Tritium RL-LSC-005

TestAmerica Richland has adopted the internationally accepted approach to estimating

uncertainties described in “NIST Technical Note 1297, 1994 Edition”. The approach, "Law of Propagation

of Errors", involves the identification of all variables in an analytical method which are used to derive a

result. These variables are related to the analytical result (R) by some functional relationship, R = constants

* f(x,y,z,...). The components (x,y,z) are evaluated to determine their contribution to the overall method

uncertainty. The individual component uncertainties (ui) are then combined using a statistical model that

provides the most probable overall uncertainty value. All component uncertainties are categorized as type

A, evaluated by statistical methods, or type B, evaluated by other means. Uncertainties not included in the

components, such as sample homogeneity, are combined with the component uncertainty as the square root

of the sum-of-the-squares of the individual uncertainties. The uncertainty associated with the derived result

is the combined uncertainty (uc) multiplied by the coverage factor (1,2, or 3).

When three or more sample replicates are used to derive the analytical result, the type A

uncertainty is the standard deviation of the mean value (S/?n), where S is the standard deviation of the

derived results. The type B uncertainties are all other random or non-random components that are not

included in the standard deviation.

The derivation of the general "Law of Propagation of Errors" equations and specific example are

available on request.

Uncertainty Estimation

Drinking Water Method Cross References


rptGeneralInfo v3.72

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Action Lev An agreed upon activity level used to trigger some action when the final result is greater than or equal to the Action

Level. Often the Action Level is related to the Decision Limit.

Batch The QC preparation batch number that relates laboratory samples to QC samples that were prepared and analyzed

together.

Bias Defined by the equation (Result/Expected)-1 as defined by ANSI N13.30.

COC No Chain of Custody Number assigned by the Client or TestAmerica.

Count Error (#s) Poisson counting statistics of the gross sample count and background. The uncertainty is absolute and in the same

units as the result. For Liquid Scintillation Counting (LSC) the batch blank count is the background.

CSU (#s)

uc Combined

Standard Uncert.

All known uncertainties associated with the preparation and analysis of the sample are propagated to give a measure

of the uncertainty associated with the result, uc the combined standard uncertainty. The uncertainty is absolute and

in the same units as the result.

(#s), Coverage

Factor

The coverage factor defines the width of the confidence interval, 1, 2 or 3 standard deviations.

CRDL (RL) Contractual Required Detection Limit as defined in the Client’s Statement Of Work or TestAmerica “default”

nominal detection limit. Often referred to the reporting level (RL)

Lc Decision Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume

associated with the sample. The Type I error probability is approximately 5%. Lc=(1.645 *

Sqrt(2*(BkgrndCnt/BkgrndCntMin)/SCntMin)) * (ConvFct/(Eff*Yld*Abn*Vol) * IngrFct). For LSC methods the

batch blank is used as a measure of the background variability. Lc cannot be calculated when the background count

is zero.

Lot-Sample No The number assigned by the LIMS software to track samples received on the same day for a given client. The

sample number is a sequential number assigned to each sample in the Lot.

MDC|MDA|MDL Detection Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume

with a Type I and II error probability of approximately 5%. MDC = (4.65 *

Sqrt((BkgrndCnt/BkgrndCntMin)/SCntMin) + 2.71/SCntMin) * (ConvFct/(Eff * Yld * Abn * Vol) * IngrFct). For

LSC methods the batch blank is used as a measure of the background variability.

Primary Detector The instrument identifier associated with the analysis of the sample aliquot.

Ratio U-234/U-238 The U-234 result divided by the U-238 result. The U-234/U-238 ratio for natural uranium in NIST SRM 4321C is

1.038.

Rst/MDC Ratio of the Result to the MDC. A value greater than 1 may indicate activity above background at a high level of

confidence. Caution should be used when applying this factor and it should be used in concert with the qualifiers

associated with the result.

Rst/TotUcert Ratio of the Result to the Total Uncertainty. If the uncertainty has a coverage factor of 2 a value greater than 1 may

indicate activity above background at approximately the 95% level of confidence assuming a two-sided confidence

interval. Caution should be used when applying this factor and it should be used in concert with the qualifiers

associated with the result.

Report DB No Sample Identifier used by the report system. The number is based upon the first five digits of the Work Order

Number.

RER The equation Replicate Error Ratio = (S-D)/[sqrt(TPUs2 + TPUd2)] as defined by ICPT BOA where S is the original

sample result, D is the result of the duplicate, TPUs is the total uncertainty of the original sample and TPUd is the

total uncertainty of the duplicate sample.

SDG Sample Delivery Group Number assigned by the Client or assigned by TestAmerica upon sample receipt.

Sum Rpt Alpha

Spec Rst(s)

The sum of the reported alpha spec results for tests derived from the same sample excluding duplicate result where

the results are in the same units.

Work Order The LIMS software assign test specific identifier.

Yield The recovery of the tracer added to the sample such as Pu-242 used to trace a Pu-239/40 method.

Report Definitions

rptGeneralInfo v3.72

TestAmerica Inc


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30-Sep-16Date:

Parameter MDLUnits

Client Id

Work Order

Report No. : 69430

Result +- CSU ( s) Tracer

Yield

51962SDG No:

TestAmerica Inc TA-RL

Qual

Sample Results Summary

Ordered by Method, Batch No., Client Sample ID.

2 RER2CRDLBatch

6231063 L4SO

YMTFA80 9418 C(160-18571-4)

8.69E-02PLUTONIUM-238 PCI_GM84WD1AE -5.68E-03 67% +- 3.6E-02 1.00E+00U

6.51E-02PLUTONIUM-239/240 PCI_G1.70E-02 67% +- 3.6E-02 1.00E+00U

YMTFA81 9404 C1(160-18571-1)

8.96E-02PLUTONIUM-238 PCI_GM84V71AE 5.68E-03 81% +- 3.2E-02 1.00E+00U


YMTFA81 9404 C1(160-18571-1) D

7.66E-02PLUTONIUM-238 PCI_GM84V71AH -1.55E-03 68% 0.3 +- 3.9E-02 1.00E+00U

7.66E-02PLUTONIUM-239/240 PCI_G-1.55E-03 68% 0.6 +- 3.9E-02 1.00E+00U

YMTFA81 9404 C2(160-18571-2)

5.39E-02PLUTONIUM-238 PCI_GM84V91AE -4.54E-03 89% +- 2.1E-02 1.00E+00U


YMTFA81 9404 C3(160-18571-3)

1.03E-01PLUTONIUM-238 PCI_GM84WC1AE -9.24E-03 66% +- 3.9E-02 1.00E+00U

7.07E-02PLUTONIUM-239/240 PCI_G0.00E+00 66% +- 3.9E-02 1.00E+00U

YMTFA82 UNK1 C(160-18571-5)

6.86E-02PLUTONIUM-238 PCI_GM84WE1AE -5.78E-03 74% +- 2.7E-02 1.00E+00U

5.18E-02PLUTONIUM-239/240 PCI_G-1.05E-03 74% +- 2.6E-02 1.00E+00U

6231064 C0SR

YMTFA80 9418 C(160-18571-4)

7.06E-02URANIUM-233/234 PCI_GM84WD1AG 3.74E-01 75% +- 1.8E-01 1.00E+00

6.57E-02URANIUM-235/236 PCI_G3.58E-02 75% +- 5.1E-02 1.00E+00U

7.77E-02URANIUM-238 PCI_G3.19E-01 75% +- 1.6E-01 1.00E+00

YMTFA81 9404 C1(160-18571-1)

4.46E-02URANIUM-233/234 PCI_GM84V71AG 2.55E-01 87% +- 1.2E-01 1.00E+00



YMTFA81 9404 C1(160-18571-1) D

6.04E-02URANIUM-233/234 PCI_GM84V71AJ 1.97E-01 76% 0.7 +- 1.2E-01 1.00E+00

6.04E-02URANIUM-235/236 PCI_G0.00E+00 76% 0.6 +- 3.3E-02 1.00E+00U

6.04E-02URANIUM-238 PCI_G1.97E-01 76% 0.7 +- 1.2E-01 1.00E+00

YMTFA81 9404 C2(160-18571-2)

7.29E-02URANIUM-233/234 PCI_GM84V91AG 2.75E-01 73% +- 1.5E-01 1.00E+00



YMTFA81 9404 C3(160-18571-3)

9.42E-02URANIUM-233/234 PCI_GM84WC1AG 1.03E-01 54% +- 1.0E-01 1.00E+00

9.42E-02URANIUM-235/236 PCI_G0.00E+00 54% +- 5.1E-02 1.00E+00U

TestAmerica Inc

U Qual - Analyzed for but not detected above limiting criteria, Mdc/Mda/Mdl, Total Uncert, RDL or not identified by gamma scan

software.

RER2 - Replicate Error Ratio = (S-D)/[sqrt(sq(TPUs)+sq(TPUd))] as defined by ICPT BOA.

rptTALRchSaSum

mary2 V5.7 A2002


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30-Sep-16Date:

Parameter MDLUnits

Client Id

Work Order

Report No. : 69430


Yield

51962SDG No:


Qual



2 RER2CRDLBatch

6231064 C0SR

YMTFA81 9404 C3(160-18571-3)

9.42E-02URANIUM-238 PCI_GM84WC1AG 1.54E-01 54% +- 1.3E-01 1.00E+00

YMTFA82 UNK1 C(160-18571-5)

7.41E-02URANIUM-233/234 PCI_GM84WE1AG 1.22E-01 66% +- 9.7E-02 1.00E+00



6250022 L4S1

YMTFA80 9418 C(160-18571-4)

6.60E-02THORIUM-228 PCI_GM84WD2AF 2.10E-01 82% +- 1.2E-01 1.00E+00

5.30E-02THORIUM-230 PCI_G2.30E-01 82% +- 1.2E-01 1.00E+00


YMTFA81 9404 C1(160-18571-1)

8.52E-02THORIUM-228 PCI_GM84V72AF 6.02E-01 89% +- 2.3E-01 1.00E+00



YMTFA81 9404 C1(160-18571-1) D

6.80E-02THORIUM-228 PCI_GM84V72AL 4.88E-01 83% 0.8 +- 1.9E-01 1.00E+00

6.13E-02THORIUM-230 PCI_G2.47E-01 83% 0.0 +- 1.3E-01 1.00E+00

5.70E-02THORIUM-232 PCI_G4.49E-01 83% 0.1 +- 1.8E-01 1.00E+00

YMTFA81 9404 C2(160-18571-2)

6.47E-02THORIUM-228 PCI_GM84V92AF 1.46E-01 78% +- 1.0E-01 1.00E+00



YMTFA81 9404 C3(160-18571-3)

6.14E-02THORIUM-228 PCI_GM84WC2AF 3.67E-01 83% +- 1.7E-01 1.00E+00



YMTFA82 UNK1 C(160-18571-5)

6.59E-02THORIUM-228 PCI_GM84WE2AF 2.33E-01 82% +- 1.3E-01 1.00E+00



6252054 L4SX

YMTFA80 9418 C(160-18571-4)

9.22E-02AMERICIUM-241 PCI_GM84WD2AC 3.02E-02 76% +- 5.3E-02 1.00E+00U

YMTFA81 9404 C1(160-18571-1)

6.82E-02AMERICIUM-241 PCI_GM84V72AC -6.55E-03 72% +- 2.5E-02 1.00E+00U

YMTFA81 9404 C1(160-18571-1) D

8.99E-02AMERICIUM-241 PCI_GM84V72AK 3.62E-02 83% 1.4 +- 5.5E-02 1.00E+00U

TestAmerica Inc


software.


rptTALRchSaSum

mary2 V5.7 A2002


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30-Sep-16Date:

Parameter MDLUnits

Client Id

Work Order

Report No. : 69430


Yield

51962SDG No:


Qual



2 RER2CRDLBatch

6252054 L4SX

YMTFA81 9404 C2(160-18571-2)

6.44E-02AMERICIUM-241 PCI_GM84V92AC 2.32E-02 81% +- 3.8E-02 1.00E+00U

YMTFA81 9404 C3(160-18571-3)

9.34E-02AMERICIUM-241 PCI_GM84WC2AC 1.00E-02 76% +- 3.6E-02 1.00E+00U

YMTFA82 UNK1 C(160-18571-5)

9.72E-02AMERICIUM-241 PCI_GM84WE2AC 9.49E-03 77% +- 3.7E-02 1.00E+00U

6231068 E7XW

YMTFA80 9418 C(160-18571-4)

5.35E-02NEPTUNIUM-237 PCI_GM84WD1AD -1.08E-03 83% +- 2.7E-02 1.00E+00U

YMTFA81 9404 C1(160-18571-1)

5.67E-02NEPTUNIUM-237 PCI_GM84V71AD -1.64E-03 90% +- 2.7E-02 1.00E+00U

YMTFA81 9404 C1(160-18571-1) D

7.12E-02NEPTUNIUM-237 PCI_GM84V71AN 1.07E-02 90% 0.6 +- 3.0E-02 1.00E+00U

YMTFA81 9404 C2(160-18571-2)

6.22E-02NEPTUNIUM-237 PCI_GM84V91AD -3.65E-03 96% +- 2.6E-02 1.00E+00U

YMTFA81 9404 C3(160-18571-3)

5.84E-02NEPTUNIUM-237 PCI_GM84WC1AD 3.18E-02 87% +- 4.6E-02 1.00E+00U

YMTFA82 UNK1 C(160-18571-5)

3.91E-02NEPTUNIUM-237 PCI_GM84WE1AD 1.77E-02 95% +- 2.7E-02 1.00E+00U

6231040 RL-LSC-008

YMTFA68C(160-18632-2) DUP

1.88E-01CARBON-14 PCI_GM84081AJ -1.03E-01 100% 1.0 +- 9.2E-02 1.00E+01U

YMTFA81 9404 C1(160-18571-1)

1.90E-01CARBON-14 PCI_GM84V71AA 5.09E-03 100% +- 9.5E-02 1.00E+01U

YMTFA81 9404 C2(160-18571-2)

1.91E-01CARBON-14 PCI_GM84V91AA -9.56E-02 100% +- 9.3E-02 1.00E+01U

YMTFA81 9404 C3(160-18571-3)

1.88E-01CARBON-14 PCI_GM84WC1AA -1.09E-01 100% +- 9.1E-02 1.00E+01U

YMTFA82 UNK1 C(160-18571-5)

1.84E-01CARBON-14 PCI_GM84WE1AA -4.36E-02 100% +- 9.0E-02 1.00E+01U

6252059 RL-LSC-008

YMTFA80 9418 C(160-18571-4)

1.81E-01CARBON-14 PCI_GM84WD2AA 3.50E-02 100% +- 1.0E-01 1.00E+01U

66No. of Results:

TestAmerica Inc


software.


rptTALRchSaSum

mary2 V5.7 A2002


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11

12

13

14

15

30-Sep-16Date:

Parameter MDLUnits

Batch

Work Order

Report No. : 69430


Yield

51962SDG No.:


Qual

QC Results Summary

LCS

Recovery Bias

Ordered by Method, Batch No, QC Type,.

2

L4SO

6231063 BLANK QC,

7.12E-02PLUTONIUM-238 PCI_GM842H1AA 94% 9.09E-03 +- 2.9E-02 U

5.21E-02PLUTONIUM-239/240 PCI_G 94% 1.06E+00 +- 3.1E-01

6231063 LCS,

6.43E-02PLUTONIUM-239/240 PCI_GM842H2AC 86% 85% -0.23.58E+00 +- 8.1E-01

C0SR

6231064 BLANK QC,

9.12E-02URANIUM-233/234 PCI_GM842J1AA 58% -5.35E-03 +- 3.8E-02 U

7.01E-02URANIUM-235/236 PCI_G 58% -7.64E-04 +- 3.8E-02 U

7.54E-02URANIUM-238 PCI_G 58% -1.53E-03 +- 3.8E-02 U

6231064 LCS,

1.46E-01URANIUM-233/234 PCI_GM842J1AC 35% 86% -0.12.55E+00 +- 8.2E-01

1.24E-01URANIUM-238 PCI_G 35% 99% 0.03.06E+00 +- 9.4E-01

L4S1

6250022 BLANK QC,

3.62E-02THORIUM-228 PCI_GM869P1AA 87% 8.43E-03 +- 1.8E-02 U

3.78E-02THORIUM-230 PCI_G 87% 7.32E-03 +- 1.8E-02 U

3.20E-02THORIUM-232 PCI_G 87% -3.48E-04 +- 1.7E-02 U

6250022 LCS,

4.47E-02THORIUM-230 PCI_GM869P1AC 81% 97% 0.01.43E+00 +- 3.2E-01

L4SX

6252054 BLANK QC,

5.75E-02AMERICIUM-241 PCI_GM842K3AA 81% 3.42E-02 +- 4.3E-02 U

6252054 LCS,

4.77E-02AMERICIUM-241 PCI_GM842K3AC 85% 108% 0.12.69E+00 +- 5.9E-01

E7XW

6231068 BLANK QC,

8.16E-02NEPTUNIUM-237 PCI_GM842N1AA 75% -3.63E-03 +- 3.6E-02 U

6231068 LCS,

5.40E-02NEPTUNIUM-237 PCI_GM842N1AC 84% 115% 0.11.87E+00 +- 6.1E-01

RL-LSC-008

6231040 BLANK QC,

1.91E-01CARBON-14 PCI_GM841P1AA 100% -8.36E-02 +- 9.3E-02 U

6231040 LCS,

1.92E-01CARBON-14 PCI_GM841P1AC 100% 101% 0.07.47E+00 +- 5.3E-01

18No. of Results:

TestAmerica Inc

U Qual - Analyzed for but not detected above limiting criteria, Mdc/Mda/Mdl, Total Uncert, RDL or not identified by gamma scan software.

Bias - (Result/Expected)-1 as defined by ANSI N13.30.

rptSTLRchQcSum

mary V5.7 A2002


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No

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A80 9

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A2002

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A2002

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merica

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12

of

28

Page 43 of 59 9/30/2016

1

2

3

4

5

6

7

8

9

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11

12

13

14

15

Lo

t-S

am

ple

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.:

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YM

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404 C

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ix:

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8/2

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13

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28

Page 44 of 59 9/30/2016

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

Lo

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A2002

TestA

merica

Inc.

14

of

28

Page 45 of 59 9/30/2016

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

Lo

t-S

am

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A81 9

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2(1

60-1

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Matr

ix:

SO

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Receiv

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Date

:8/1

8/2

01

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merica

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15

of

28

Page 46 of 59 9/30/2016

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2

3

4

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6

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8

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15

Lo

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A2002

TestA

merica

Inc.

16

of

28

Page 47 of 59 9/30/2016

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

Lo

t-S

am

ple

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.:

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YM

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A2002

TestA

merica

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17

of

28

Page 48 of 59 9/30/2016

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

Lo

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am

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69430

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Sam

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V5.7

A2002

TestA

merica

Inc.

18

of

28

Page 49 of 59 9/30/2016

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

Lo

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merica

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19

of

28

Page 50 of 59 9/30/2016

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2

3

4

5

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7

8

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15

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merica

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20

of

28

Page 51 of 59 9/30/2016

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

DU

PL

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M

69430

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TL

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7 A

2002

TestA

merica

Inc.

21

of

28

Page 52 of 59 9/30/2016

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

DU

PL

ICA

TE

RE

SU

LT

S

30

-Sep-1

6D

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OR

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404 C

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ix:

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Date

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8/2

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M

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llecti

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/2016 3

:30:0

0 P

M

69430

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MD

L,

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me

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J6

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tal

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TestA

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22

of

28

Page 53 of 59 9/30/2016

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

DU

PL

ICA

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0 P

M

69430

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2002

TestA

merica

Inc.

23

of

28

Page 54 of 59 9/30/2016

1

2

3

4

5

6

7

8

9

10

11

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13

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15

BL

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Documents

1 2 3 4 5 ANALYTICAL REPORT 6 - US Department of Energy · application methods. TestAmerica s operations groups have reviewed the data for compliance with the laboratory QA/QC plan,