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ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Burlington30 Community DriveSuite 11South Burlington, VT 05403Tel: (802)660-1990
TestAmerica Job ID: 200-12779-1TestAmerica Sample Delivery Group: 200-12779Client Project/Site: RACER - Central Foundry Massena NY
For:ARCADIS U.S. IncMassena Facility, Route 37 East56 Chevrolet RoadMassena, New York 13662
Attn: Richard Boelter
Authorized for release by:9/24/2012 10:42:32 AM
Kathryn KellyProject Manager [email protected]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: ARCADIS U.S. IncProject/Site: RACER - Central Foundry Massena NY
TestAmerica Job ID: 200-12779-1SDG: 200-12779
Page 2 of 25TestAmerica Burlington
9/24/2012
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
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Definitions/GlossaryTestAmerica Job ID: 200-12779-1Client: ARCADIS U.S. Inc
SDG: 200-12779Project/Site: RACER - Central Foundry Massena NY
Qualifiers
Air - GC Semi VOA
Qualifier Description
U Indicates the analyte was analyzed for but not detected.
Qualifier
X Surrogate is outside control limits
Glossary
These commonly used abbreviations may or may not be present in this report.
☼ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CNF Contains no Free Liquid
DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample
EDL Estimated Detection Limit
EPA United States Environmental Protection Agency
MDL Method Detection Limit
ML Minimum Level (Dioxin)
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RL Reporting Limit
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica BurlingtonPage 3 of 25 9/24/2012
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Case NarrativeClient: ARCADIS U.S. Inc TestAmerica Job ID: 200-12567-1
Project/Site: RACER - Central Foundry Massena NY SDG: 200-12779
Job ID: 200-12567-1
Laboratory: TestAmerica Burlington
Narrative
CASE NARRATIVE
Client: ARCADIS U.S. Inc
Project: RACER - Central Foundry Massena NY
Report Number: 200-12567-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
This report has been revised to provide the prep information of 1 puf instead of 1 gram. Results provided in this submittal are from the
revised data set.
RECEIPT
The samples were received on 09/06/2012; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 2.0 C.
PCB IN AIR
Samples AIR1B-090512, AIR2A-090512 and AIR3-090512 were analyzed for PCB in Air in accordance with TO-4A. The samples were
prepared on 09/06/2012 and analyzed on 09/07/2012.
Due to glassware failure causing solvent evaporation Tetrachloro-m-xylene, Aroclor 1260 and Aroclor-1016 had low recoveries for LCS
200-44528/2-B, Aroclor 1260 and Aroclor-1016. Please refer to the QC report for details.
Samples AIR2A-090512[2X] and AIR3-090512[2X] required dilution prior to analysis. The reporting limits have been adjusted accordingly.
No other difficulties were encountered during the TO-4A analyses.
All other quality control parameters were within the acceptance limits.
Job ID: 200-12590-1
Laboratory: TestAmerica Burlington
Narrative
CASE NARRATIVE
TestAmerica BurlingtonPage 4 of 25 9/24/2012
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Case NarrativeClient: ARCADIS U.S. Inc TestAmerica Job ID: 200-12567-1
Project/Site: RACER - Central Foundry Massena NY SDG: 200-12779
Job ID: 200-12590-1 (Continued)
Laboratory: TestAmerica Burlington (Continued)
Client: ARCADIS U.S. Inc
Project: RACER - Central Foundry Massena NY
Report Number: 200-12590-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 09/07/2012; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 3.8 C.
PCB IN AIR
Samples AIR1B-090612, AIR2A-090612 and AIR3-090612 were analyzed for PCB in Air in accordance with TO-4A. The samples were
prepared on 09/07/2012 and analyzed on 09/10/2012.
Samples AIR1B-090612[2X], AIR2A-090612[10X] and AIR3-090612[10X] required dilution prior to analysis. The reporting limits have been
adjusted accordingly.
No difficulties were encountered during the TO-4A analyses.
All quality control parameters were within the acceptance limits.
Job ID: 200-12609-1
Laboratory: TestAmerica Burlington
Narrative
CASE NARRATIVE
Client: ARCADIS U.S. Inc
Project: RACER - Central Foundry Massena NY
Report Number: 200-12609-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
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Case NarrativeClient: ARCADIS U.S. Inc TestAmerica Job ID: 200-12567-1
Project/Site: RACER - Central Foundry Massena NY SDG: 200-12779
Job ID: 200-12609-1 (Continued)
Laboratory: TestAmerica Burlington (Continued)
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 09/08/2012; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 4.2 C.
PCB IN AIR
Samples AIR1B-090712, AIR2A-090712 and AIR3-090712 were analyzed for PCB in Air in accordance with TO-4A. The samples were
prepared on 09/10/2012 and analyzed on 09/11/2012.
Samples AIR1B-090712[10X], AIR2A-090712[30X] and AIR3-090712[50X] required dilution prior to analysis. The reporting limits have
been adjusted accordingly.
Tetrachloro-m-xylene recovery was outside control limits on the RTX-5 for the following sample: AIR3-090712. The recovery was within
control limits on the RTX-35.
No difficulties were encountered during the TO-4A analyses.
All quality control parameters were within the acceptance limits.
Job ID: 200-12622-1
Laboratory: TestAmerica Burlington
Narrative
CASE NARRATIVE
Client: ARCADIS U.S. Inc
Project: RACER - Central Foundry Massena NY
Report Number: 200-12622-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
TestAmerica BurlingtonPage 6 of 25 9/24/2012
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Case NarrativeClient: ARCADIS U.S. Inc TestAmerica Job ID: 200-12567-1
Project/Site: RACER - Central Foundry Massena NY SDG: 200-12779
Job ID: 200-12622-1 (Continued)
Laboratory: TestAmerica Burlington (Continued)
The samples were received on 09/11/2012; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 3.8 C.
PCB IN AIR
Samples AIR1B-090712(2), AIR2A-090712(2) and AIR3-090712(2) were analyzed for PCB in Air in accordance with TO-4A. The samples
were prepared on 09/11/2012 and analyzed on 09/12/2012.
Samples AIR1B-090712(2)[2X], AIR2A-090712(2)[5X] and AIR3-090712(2)[20X] required dilution prior to analysis. The reporting limits
have been adjusted accordingly.
No difficulties were encountered during the TO-4A analyses.
All quality control parameters were within the acceptance limits.
Job ID: 200-12635-1
Laboratory: TestAmerica Burlington
Narrative
CASE NARRATIVE
Client: ARCADIS U.S. Inc
Project: RACER - Central Foundry Massena NY
Report Number: 200-12635-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 09/12/2012; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 4.4 C.
PCB IN AIR
Samples AIR1B-091112 (200-12635-1), AIR2A-091112 (200-12635-2) and AIR3-091112 (200-12635-3) were analyzed for PCB in Air in
accordance with TO-4A. The samples were prepared on 09/12/2012 and analyzed on 09/13/2012.
Samples AIR2A-091112 (200-12635-2)[2X] and AIR3-091112 (200-12635-3)[10X] required dilution prior to analysis. The reporting limits
have been adjusted accordingly.
No difficulties were encountered during the TO-4A analyses.
TestAmerica BurlingtonPage 7 of 25 9/24/2012
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Case NarrativeClient: ARCADIS U.S. Inc TestAmerica Job ID: 200-12567-1
Project/Site: RACER - Central Foundry Massena NY SDG: 200-12779
Job ID: 200-12635-1 (Continued)
Laboratory: TestAmerica Burlington (Continued)
All quality control parameters were within the acceptance limits.
Job ID: 200-12656-1
Laboratory: TestAmerica Burlington
Narrative
CASE NARRATIVE
Client: ARCADIS U.S. Inc
Project: RACER - Central Foundry Massena NY
Report Number: 200-12656-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 09/13/2012; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 3.9 C.
PCB IN AIR
Samples AIR1B-091212, AIR2A-091212 and AIR3-091212 were analyzed for PCB in Air in accordance with TO-4A. The samples were
prepared on 09/13/2012 and analyzed on 09/14/2012.
DCB Decachlorobiphenyl and Tetrachloro-m-xylene failed the surrogate recovery criteria low for AIR3-091212. Refer to the QC report for
details.
Samples AIR1B-091212[10X], AIR2A-091212[20X] and AIR3-091212[30X] required dilution prior to analysis. The reporting limits have
been adjusted accordingly.
No other difficulties were encountered during the TO-4A analyses.
All other quality control parameters were within the acceptance limits.
Job ID: 200-12678-1
TestAmerica BurlingtonPage 8 of 25 9/24/2012
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Case NarrativeClient: ARCADIS U.S. Inc TestAmerica Job ID: 200-12567-1
Project/Site: RACER - Central Foundry Massena NY SDG: 200-12779
Job ID: 200-12678-1 (Continued)
Laboratory: TestAmerica Burlington
Narrative
CASE NARRATIVE
Client: ARCADIS U.S. Inc
Project: RACER - Central Foundry Massena NY
Report Number: 200-12678-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 09/14/2012; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 4.1 C.
PCB IN AIR
Samples AIR1B-091312, AIR2A-091312 and AIR-091312 were analyzed for PCB in Air in accordance with TO-4A. The samples were
prepared on 09/14/2012 and analyzed on 09/16/2012.
Samples AIR1B-091312[20X], AIR2A-091312[20X] and AIR-091312[40X] required dilution prior to analysis. The reporting limits have been
adjusted accordingly.
No difficulties were encountered during the TO-4A analyses.
All quality control parameters were within the acceptance limits.
Job ID: 200-12703-1
Laboratory: TestAmerica Burlington
Narrative
CASE NARRATIVE
Client: ARCADIS U.S. Inc
Project: RACER - Central Foundry Massena NY
Report Number: 200-12703-1
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Case NarrativeClient: ARCADIS U.S. Inc TestAmerica Job ID: 200-12567-1
Project/Site: RACER - Central Foundry Massena NY SDG: 200-12779
Job ID: 200-12703-1 (Continued)
Laboratory: TestAmerica Burlington (Continued)
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 09/15/2012; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 3.5 C.
PCB IN AIR
Samples AIR1B-091412, AIR2A-091412 and AIR3-091412 were analyzed for PCB in Air in accordance with TO-4A. The samples were
prepared on 09/17/2012 and analyzed on 09/18/2012.
Tetrachloro-m-xylene failed the surrogate recovery criteria high for AIR2A-091412. Refer to the QC report for details.
Samples AIR1B-091412[20X], AIR2A-091412[30X] and AIR3-091412[50X] required dilution prior to analysis. The reporting limits have
been adjusted accordingly.
No other difficulties were encountered during the TO-4A analyses.
All other quality control parameters were within the acceptance limits.
Job ID: 200-12741-1
Laboratory: TestAmerica Burlington
Narrative
CASE NARRATIVE
Client: ARCADIS U.S. Inc
Project: RACER - Central Foundry Massena NY
Report Number: 200-12741-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
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Case NarrativeClient: ARCADIS U.S. Inc TestAmerica Job ID: 200-12567-1
Project/Site: RACER - Central Foundry Massena NY SDG: 200-12779
Job ID: 200-12741-1 (Continued)
Laboratory: TestAmerica Burlington (Continued)
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 09/18/2012; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 4.7 C.
PCB IN AIR
Samples AIR1B-091412(2), AIR2A-091412(2) and AIR3-091412(2) were analyzed for PCB in Air in accordance with TO-4A. The samples
were prepared on 09/18/2012 and analyzed on 09/19/2012.
Samples AIR1B-091412(2)[2X], AIR2A-091412(2)[10X] and AIR3-091412(2)[20X] required dilution prior to analysis. The reporting limits
have been adjusted accordingly.
No difficulties were encountered during the TO-4A analyses.
All quality control parameters were within the acceptance limits.
Job ID: 200-12757-1
Laboratory: TestAmerica Burlington
Narrative
Job Narrative
200-12757-1
Comments
No additional comments.
Receipt
The samples were received on 9/19/2012 10:00 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 3.1º C.
Except:
The container label for the following sample(s) did not match the information listed on the Chain-of-Custody (COC): . The container labels
list the samples with a date suffix of 091312. The COC lists the suffix as the date of sampling, 091812, which was used for login.
GC Semi VOA
Method(s) TO-4A: Tetrachloro-m-xylene recovery was outside control limits on the RTX-5 for the following sample: AIR1B-091812.
No other analytical or quality issues were noted.
Organic Prep
No analytical or quality issues were noted.
Job ID: 200-12779-1
Laboratory: TestAmerica Burlington
Narrative
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Case NarrativeClient: ARCADIS U.S. Inc TestAmerica Job ID: 200-12567-1
Project/Site: RACER - Central Foundry Massena NY SDG: 200-12779
Job ID: 200-12779-1 (Continued)
Laboratory: TestAmerica Burlington (Continued)
CASE NARRATIVE
Client: ARCADIS U.S. Inc
Project: RACER - Central Foundry Massena NY
Report Number: 200-12779-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 09/20/2012; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 3.3 C.
PCB IN AIR
Samples AIR1B-091912, AIR2A-091912 and AIR3-091912 were analyzed for PCB in Air in accordance with TO-4A. The samples were
prepared on 09/20/2012 and analyzed on 09/21/2012.
Tetrachloro-m-xylene failed the surrogate recovery criteria high for AIR2A-091912. Refer to the QC report for details.
Samples AIR1B-091912[5X], AIR2A-091912[20X] and AIR3-091912[20X] required dilution prior to analysis. The reporting limits have been
adjusted accordingly.
No other difficulties were encountered during the TO-4A analyses.
All other quality control parameters were within the acceptance limits.
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Detection SummaryTestAmerica Job ID: 200-12779-1Client: ARCADIS U.S. Inc
SDG: 200-12779Project/Site: RACER - Central Foundry Massena NY
Client Sample ID: AIR1B-091912 Lab Sample ID: 200-12779-1
Aroclor 1242
RL
0.0018 ug/m3 PUF
MDL
0.00012
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
TO-4A Total/NA50.020
Client Sample ID: AIR2A-091912 Lab Sample ID: 200-12779-2
Aroclor 1242
RL
0.0062 ug/m3 PUF
MDL
0.00044
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
TO-4A Total/NA200.053
Client Sample ID: AIR3-091912 Lab Sample ID: 200-12779-3
Aroclor 1242
RL
0.0065 ug/m3 PUF
MDL
0.00045
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
TO-4A Total/NA200.064
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Client Sample ResultsTestAmerica Job ID: 200-12779-1Client: ARCADIS U.S. Inc
SDG: 200-12779Project/Site: RACER - Central Foundry Massena NY
Lab Sample ID: 200-12779-1Client Sample ID: AIR1B-091912Matrix: AirDate Collected: 09/19/12 07:53
Date Received: 09/20/12 11:30
Sample Container: PUF
Method: TO-4A - Pesticides and PCBs in Ambient AirRL MDL
Aroclor-1016 0.0018 U 0.0018 0.00011 ug/m3 PUF 09/20/12 13:41 09/21/12 11:18 5
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0018 0.00027 ug/m3 PUF 09/20/12 13:41 09/21/12 11:18 5Aroclor 1221 0.0018 U
0.0018 0.00031 ug/m3 PUF 09/20/12 13:41 09/21/12 11:18 5Aroclor 1232 0.0018 U
0.0018 0.00012 ug/m3 PUF 09/20/12 13:41 09/21/12 11:18 5Aroclor 1242 0.020
0.0018 0.00022 ug/m3 PUF 09/20/12 13:41 09/21/12 11:18 5Aroclor 1248 0.0018 U
0.0018 0.000096 ug/m3 PUF 09/20/12 13:41 09/21/12 11:18 5Aroclor 1254 0.0018 U
0.0018 0.000057 ug/m3 PUF 09/20/12 13:41 09/21/12 11:18 5Aroclor 1260 0.0018 U
0.0018 0.00010 ug/m3 PUF 09/20/12 13:41 09/21/12 11:18 5Aroclor 1262 0.0018 U
0.0018 0.000068 ug/m3 PUF 09/20/12 13:41 09/21/12 11:18 5Aroclor 1268 0.0018 U
DCB Decachlorobiphenyl 90 45 - 125 09/20/12 13:41 09/21/12 11:18 5
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Tetrachloro-m-xylene 106 09/20/12 13:41 09/21/12 11:18 530 - 130
Lab Sample ID: 200-12779-2Client Sample ID: AIR2A-091912Matrix: AirDate Collected: 09/19/12 07:04
Date Received: 09/20/12 11:30
Sample Container: PUF
Method: TO-4A - Pesticides and PCBs in Ambient AirRL MDL
Aroclor-1016 0.0062 U 0.0062 0.00037 ug/m3 PUF 09/20/12 13:41 09/21/12 11:42 20
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0062 0.00095 ug/m3 PUF 09/20/12 13:41 09/21/12 11:42 20Aroclor 1221 0.0062 U
0.0062 0.0011 ug/m3 PUF 09/20/12 13:41 09/21/12 11:42 20Aroclor 1232 0.0062 U
0.0062 0.00044 ug/m3 PUF 09/20/12 13:41 09/21/12 11:42 20Aroclor 1242 0.053
0.0062 0.00078 ug/m3 PUF 09/20/12 13:41 09/21/12 11:42 20Aroclor 1248 0.0062 U
0.0062 0.00034 ug/m3 PUF 09/20/12 13:41 09/21/12 11:42 20Aroclor 1254 0.0062 U
0.0062 0.00020 ug/m3 PUF 09/20/12 13:41 09/21/12 11:42 20Aroclor 1260 0.0062 U
0.0062 0.00036 ug/m3 PUF 09/20/12 13:41 09/21/12 11:42 20Aroclor 1262 0.0062 U
0.0062 0.00024 ug/m3 PUF 09/20/12 13:41 09/21/12 11:42 20Aroclor 1268 0.0062 U
DCB Decachlorobiphenyl 99 45 - 125 09/20/12 13:41 09/21/12 11:42 20
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Tetrachloro-m-xylene 137 X 09/20/12 13:41 09/21/12 11:42 2030 - 130
Lab Sample ID: 200-12779-3Client Sample ID: AIR3-091912Matrix: AirDate Collected: 09/19/12 07:38
Date Received: 09/20/12 11:30
Sample Container: PUF
Method: TO-4A - Pesticides and PCBs in Ambient AirRL MDL
Aroclor-1016 0.0065 U 0.0065 0.00039 ug/m3 PUF 09/20/12 13:41 09/21/12 12:07 20
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0065 0.00099 ug/m3 PUF 09/20/12 13:41 09/21/12 12:07 20Aroclor 1221 0.0065 U
0.0065 0.0011 ug/m3 PUF 09/20/12 13:41 09/21/12 12:07 20Aroclor 1232 0.0065 U
0.0065 0.00045 ug/m3 PUF 09/20/12 13:41 09/21/12 12:07 20Aroclor 1242 0.064
0.0065 0.00082 ug/m3 PUF 09/20/12 13:41 09/21/12 12:07 20Aroclor 1248 0.0065 U
0.0065 0.00035 ug/m3 PUF 09/20/12 13:41 09/21/12 12:07 20Aroclor 1254 0.0065 U
0.0065 0.00021 ug/m3 PUF 09/20/12 13:41 09/21/12 12:07 20Aroclor 1260 0.0065 U
0.0065 0.00038 ug/m3 PUF 09/20/12 13:41 09/21/12 12:07 20Aroclor 1262 0.0065 U
0.0065 0.00025 ug/m3 PUF 09/20/12 13:41 09/21/12 12:07 20Aroclor 1268 0.0065 U
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Client Sample ResultsTestAmerica Job ID: 200-12779-1Client: ARCADIS U.S. Inc
SDG: 200-12779Project/Site: RACER - Central Foundry Massena NY
Lab Sample ID: 200-12779-3Client Sample ID: AIR3-091912Matrix: AirDate Collected: 09/19/12 07:38
Date Received: 09/20/12 11:30
Sample Container: PUF
DCB Decachlorobiphenyl 94 45 - 125 09/20/12 13:41 09/21/12 12:07 20
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Tetrachloro-m-xylene 125 09/20/12 13:41 09/21/12 12:07 2030 - 130
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Surrogate SummaryTestAmerica Job ID: 200-12779-1Client: ARCADIS U.S. Inc
SDG: 200-12779Project/Site: RACER - Central Foundry Massena NY
Method: TO-4A - Pesticides and PCBs in Ambient AirPrep Type: Total/NAMatrix: Air
Lab Sample ID Client Sample ID (45-125) (45-125) (30-130) (30-130)
DCB1 DCB2 TCX1 TCX2
90 82 106 91200-12779-1
Percent Surrogate Recovery (Acceptance Limits)
AIR1B-091912
99 89 137 X 95200-12779-2 AIR2A-091912
94 88 125 90200-12779-3 AIR3-091912
84 87 91 94LCS 200-45190/2-B Lab Control Sample
81 82 99 99MB 200-45190/1-B Method Blank
Surrogate Legend
DCB = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
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QC Sample ResultsTestAmerica Job ID: 200-12779-1Client: ARCADIS U.S. Inc
SDG: 200-12779Project/Site: RACER - Central Foundry Massena NY
Method: TO-4A - Pesticides and PCBs in Ambient Air
Client Sample ID: Method BlankLab Sample ID: MB 200-45190/1-B
Matrix: Air Prep Type: Total/NA
Analysis Batch: 45248 Prep Batch: 45191
RL MDL
Aroclor-1016 0.10 U 0.10 0.0060 ug/m3 PUF 09/20/12 13:41 09/21/12 10:30 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
0.10 U 0.0150.10 ug/m3 PUF 09/20/12 13:41 09/21/12 10:30 1Aroclor 1221
0.10 U 0.0170.10 ug/m3 PUF 09/20/12 13:41 09/21/12 10:30 1Aroclor 1232
0.10 U 0.00700.10 ug/m3 PUF 09/20/12 13:41 09/21/12 10:30 1Aroclor 1242
0.10 U 0.0130.10 ug/m3 PUF 09/20/12 13:41 09/21/12 10:30 1Aroclor 1248
0.10 U 0.00540.10 ug/m3 PUF 09/20/12 13:41 09/21/12 10:30 1Aroclor 1254
0.10 U 0.00320.10 ug/m3 PUF 09/20/12 13:41 09/21/12 10:30 1Aroclor 1260
0.10 U 0.00580.10 ug/m3 PUF 09/20/12 13:41 09/21/12 10:30 1Aroclor 1262
0.10 U 0.00380.10 ug/m3 PUF 09/20/12 13:41 09/21/12 10:30 1Aroclor 1268
DCB Decachlorobiphenyl 82 45 - 125 09/21/12 10:30 1
MB MB
Surrogate
09/20/12 13:41
Dil FacPrepared AnalyzedQualifier Limits%Recovery
99 09/20/12 13:41 09/21/12 10:30 1Tetrachloro-m-xylene 30 - 130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 200-45190/2-B
Matrix: Air Prep Type: Total/NA
Analysis Batch: 45248 Prep Batch: 45191
Aroclor-1016 1.00 0.878 ug/m3 PUF 88 65 - 125
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Aroclor 1260 1.00 0.875 ug/m3 PUF 87 65 - 125
DCB Decachlorobiphenyl 45 - 125
Surrogate
87
LCS LCS
Qualifier Limits%Recovery
94Tetrachloro-m-xylene 30 - 130
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QC Association SummaryTestAmerica Job ID: 200-12779-1Client: ARCADIS U.S. Inc
SDG: 200-12779Project/Site: RACER - Central Foundry Massena NY
Air - GC Semi VOA
Prep Batch: 45191
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Air 3540C200-12779-1 AIR1B-091912 Total/NA
Air 3540C200-12779-2 AIR2A-091912 Total/NA
Air 3540C200-12779-3 AIR3-091912 Total/NA
Air 3540CLCS 200-45190/2-B Lab Control Sample Total/NA
Air 3540CMB 200-45190/1-B Method Blank Total/NA
Analysis Batch: 45248
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Air TO-4A 45191200-12779-1 AIR1B-091912 Total/NA
Air TO-4A 45191200-12779-2 AIR2A-091912 Total/NA
Air TO-4A 45191200-12779-3 AIR3-091912 Total/NA
Air TO-4A 45191LCS 200-45190/2-B Lab Control Sample Total/NA
Air TO-4A 45191MB 200-45190/1-B Method Blank Total/NA
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Lab ChronicleClient: ARCADIS U.S. Inc TestAmerica Job ID: 200-12779-1
Project/Site: RACER - Central Foundry Massena NY SDG: 200-12779
Client Sample ID: AIR1B-091912 Lab Sample ID: 200-12779-1Matrix: AirDate Collected: 09/19/12 07:53
Date Received: 09/20/12 11:30
Prep 3540C 09/20/12 13:41 MLT45191 TAL BUR
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis TO-4A 5 45248 09/21/12 11:18 SLD TAL BURTotal/NA
Client Sample ID: AIR2A-091912 Lab Sample ID: 200-12779-2Matrix: AirDate Collected: 09/19/12 07:04
Date Received: 09/20/12 11:30
Prep 3540C 09/20/12 13:41 MLT45191 TAL BUR
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis TO-4A 20 45248 09/21/12 11:42 SLD TAL BURTotal/NA
Client Sample ID: AIR3-091912 Lab Sample ID: 200-12779-3Matrix: AirDate Collected: 09/19/12 07:38
Date Received: 09/20/12 11:30
Prep 3540C 09/20/12 13:41 MLT45191 TAL BUR
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis TO-4A 20 45248 09/21/12 12:07 SLD TAL BURTotal/NA
Laboratory References:
TAL BUR = TestAmerica Burlington, 30 Community Drive, Suite 11, South Burlington, VT 05403, TEL (802)660-1990
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Certification SummaryClient: ARCADIS U.S. Inc TestAmerica Job ID: 200-12779-1
Project/Site: RACER - Central Foundry Massena NY SDG: 200-12779
Laboratory: TestAmerica BurlingtonAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
ACLASS 10-22-12ADE-1492DoD ELAP
Connecticut State Program 1 PH-0751 09-30-13
DE Haz. Subst. Cleanup Act (HSCA) State Program 3 NA 02-24-13
Florida NELAC 4 E87467 06-30-13
Louisiana NELAC 6 176292 06-30-13
Maine State Program 1 VT00008 04-17-13
Minnesota NELAC 5 050-999-436 12-31-12
New Hampshire NELAC 1 200610 12-18-12
New Jersey NELAC Primary AB 2 VT972 06-30-13
New York NELAC 2 10391 04-01-13
Pennsylvania NELAC 3 68-00489 04-30-13
Rhode Island State Program 1 LAO00298 12-30-12
USDA Federal P330-11-00093 02-17-14
Vermont State Program 1 VT-4000 12-31-12
Virginia NELAC 3 460209 12-14-12
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Method SummaryTestAmerica Job ID: 200-12779-1Client: ARCADIS U.S. Inc
SDG: 200-12779Project/Site: RACER - Central Foundry Massena NY
Method Method Description LaboratoryProtocol
EPATO-4A Pesticides and PCBs in Ambient Air TAL BUR
Protocol References:
EPA = US Environmental Protection Agency
Laboratory References:
TAL BUR = TestAmerica Burlington, 30 Community Drive, Suite 11, South Burlington, VT 05403, TEL (802)660-1990
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Sample SummaryTestAmerica Job ID: 200-12779-1Client: ARCADIS U.S. Inc
SDG: 200-12779Project/Site: RACER - Central Foundry Massena NY
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
200-12779-1 AIR1B-091912 Air 09/19/12 07:53 09/20/12 11:30
200-12779-2 AIR2A-091912 Air 09/19/12 07:04 09/20/12 11:30
200-12779-3 AIR3-091912 Air 09/19/12 07:38 09/20/12 11:30
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Login Sample Receipt Checklist
Client: ARCADIS U.S. Inc Job Number: 200-12779-1
SDG Number: 200-12779
Login Number: 12779
Question Answer Comment
Creator: Gagne, Eric
List Source: TestAmerica Burlington
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
Lab does not accept radioactive samples.
TrueThe cooler's custody seal, if present, is intact. 585488 & 585489
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded. 3.3ºC IR GUN ID 181. CF +0.3
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
FalseThere are no discrepancies between the containers received and the COC. IDs on containers do not match the COC.
Logged in per COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used. Refer to Job Narrative for details.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
N/AMultiphasic samples are not present.
N/ASamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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