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Methods in Enzymology
Volume 158
MetallobiochemistryPart A
James F. Riordan
Bert L . Vallee
CONTRIBUTORS TO VOLUME 158 vi i
PREFACE i X
VOLUMES IN SERIES X i
Section I . Sample Preparatio n
1. Preparation of Metal-Free Water
JAMES F . RIORDAN AN D
BERT L . VALLEE
3
2. Elimination of Adventitious Metals
BARTON HOLMQUIST
6
3. Metal-Free Dialysis Tubing
DAVID S . AULD
1 3
4. Metal-Free Chromatographic Media
MARK T . MARTIN
1 5
5. Preparation of Metal-Free Enzymes
FRED W . WAGNER
2 1
6. Metal-Buffered Systems
JOHN O . BAKER
3 3
7. Standards for Metal Analysis
CLAUDE VEILLON
5 6
8. Methods for Metal Substitution
DAVID S . AULD
7 1
9. Preparation of Metal-Hybrid Enzymes
WOLFGANG MARET AND
MICHAEL ZEPPEZAUER
79
10 . Introduction of Exchange-Inert Metal Ions into HAROLD E . VAN WART
95
Enzymes
11. Use of Chelating Agents to Inhibit Enzymes
DAVID S . AULD
11 0
Section II . Analytical Techniques
12. Atomic Absorption Spectrometry
WALTER SLAVIN
11 7
13 . Multielement Atomic Absorption Methods of JAMES M . HARNLEY AN D
Analysis
DONITA L . GARLAND
145
14. Ion Microscopy in Biology and Medicine
SUBHASH CHANDRA AN D
GEORGE H . MORRISON
157
15. Flame Atomic Emission Spectrometry
TERENCE H . RISBY
180
16 . Inductively Coupled Plasma-Emission Spectrome- KAREN A . WOLNIK
190
try
17 . Inductively Coupled Plasma-Mass Spectrometry Jost A . OLIVARES
20 5
18 . Atomic Fluorescence Spectrometry
ROBERT G . MICHEL
22 2
19 . Electrochemical Methods of Analysis
JANET OSTERYOUNG
24 3
20 . Neutron Activation Analysis
JACQUES VERSIECK
267
Section III . Analysis of Metals
21 . Aluminum
JOHN SAVORY, SUE BROWN ,
ROGER L . BERTHOLF ,
NANCY MENDOZA, AND
MICHAEL R . WILLS
28 9
22 . Measurement of Total Calcium in Biological Flu- GEORGE N . BOWERS, JR .ids : Flame Atomic Absorption Spectrometry
AND THEODORE C . RAINS
30 2
23 . Measurement of Ionized Calcium in Biological SALVADOR F . SENA AND
Fluids : Ion-Selective Electrode Method
GEORGE N. BOWERS, JR .
32 0
24 . Chromium
CLAUDE VEILLON
334
25 . Determination of Cobalt by Atomic Absorption ROBERT SHAPIRO AN D
Spectrometry
MARK T . MARTIN
344
26 . Measurement of Copper in Biological Samples by MERLE A . EVENSON
35 1Flame or Electrothermal Atomic AbsorptionSpectrometry
27 . Rapid Colorimetric Micromethod for the Quantita- WAYNE W. FISH
357tion of Complexed Iron in Biological Samples
28 . Atomic Absorption Spectrometry of Magnesium MARK T . MARTIN AN D
ROBERT SHAPIRO
365
29 . Molybdenum
JEAN L . JOHNSON
37 1
30 . Nickel Analysis by Electrothermal Atomic Ab- F . WILLIAM SUNDERMAN, JR . ,sorption Spectrometry
SIDNEY M . HOPFER, AND
M . CRISTINA CRISOSTOMO
38 2
31 . Determination of Selenium in Biological Matrices S . A . LEWIS
39 1
32 . Vanadium
DONNA M . MARTIN AN D
N . DENNIS CHASTEEN
40 2
33 . Determination of Zinc in Biological Samples by K. H . FALCHUK, K . L . HILT,Atomic Absorption Spectrometry
AND B . L . VALLEE
42 2
AUTHOR INDEX 43 5
SUBJECT INDEX 451
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