Air Sampling Techniques

s.no TYPES OF CHEMICAL123456789

1011121314151617181920212223242526272829303132333435363738394041424344454647

(Aqua Regia Ashing)1,1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE1-NITROPYRENE IN DIESEL PARTICULATES1-OCTANETHIOL2,4-D2-NITROPROPANEACETALDEHYDE by HPLCACETIC ACIDACETIC ANHYDRIDEACETONITRILEACIDS, INORGANICALCOHOLS COMBINEDALCOHOLS IIALCOHOLS IIIALCOHOLS IVALIPHATIC ALDEHYDESALKALINE DUSTSAMINES, ALIPHATICAMINES, AROMATICAMINOETHANOL COMPOUNDS IAMINOETHANOL COMPOUNDS IIAMMONIAANILINE, o-TOLUIDINE, AND NITROBENZENEantimony* chromium* lithium potassium tin zirconium*arsenic cobalt magnesium selenium titaniumARSENIC TRIOXIDEbarium copper manganese silver tungsten*beryllium iron* molybdenum strontium vanadiumBROMINEcadmium lanthanum nickel tellurium yttriumCHLORINATED AND ORGANONITROGEN HERBICIDESCHLOROACETIC ACID CHROMIUM, HEXAVALENTCRESOL (all isomers) and PHENOLDIAZOMETHANEDICHLOROFLUOROMETHANEDYES, BENZIDINE-, o-TOLIDINE-, o-DIANISIDINEELEMENTS by ICP 7301ESTERS 1ETHYL ACETATEETHYL BROMIDEETHYL CHLORIDEETHYL ETHERETHYLENE CHLOROHYDRINETHYLENIMINEFLUORIDES, aerosol and gasFORMALDEHYDE

484950515253545556575859606162636465666768697071727374757677787980818283848586878889909192939495

FORMALDEHYDE by GCFORMIC ACIDGLUTARALDEHYDEGLYCOL ETHERSGLYCOLSHEXACHLORO-1,3-CYCLOPENTADIENEHEXACHLOROBUTADIENEHYDRAZINEHYDROCARBON HALOGENATEDHYDROCARBONS, AROMATICHYDROGEN CYANIDEHYDROGEN SULFIDEHYDROQUINONEISOCYANATESISOCYANATES, MONOMERICISOPHORONEISOPROPYL ACETATEISOPROPYL ETHERKEPONEKETONES ILEAD by Flame AASLEAD in Air by Chemical Spot TestLEAD SULFIDEMERCAPTANS, METHYL-, ETHYL-, and n-BUTYLMETHANOLMETHYL AND ETHYL METHACRYLATEMETHYL BROMIDEMETHYL CELLOSOLVE ACETATEMETHYL CHLORIDEMETHYL ETHYL KETONMETHYL ETHYL KETONE PEROXIDEMETHYL IODIDEMETHYL tert-BUTYL ETHERMETHYLENE CHLORIDEMETHYLTIN CHLORIDESMONOMETHYLANILINEMONOMETHYLHYDRAZINENAPHTHASNAPHTHASNAPHTHYLAMINES, a and bNICKEL CARBONYLNICOTINENITRIC OXIDE and NITROGEN DIOXIDENITROAROMATIC COMPOUNDSNITROETHANENITROGLYCERINNITROMETHANENITROSAMINES

96979899

100101102103104105106107108109110111112113114115116117118119120121122123124125126

NITROUS OXIDEOIL MIST, MINERALORGANONITROGEN PESTICIDESORGANOPHOSPHORUS PESTICIDESPHENYL ETHERPHENYL GLYCIDYL ETHERPHOSPHINEp-NITROANILINEPOLYCYCLIC AROMATIC COMPOUNDS, TOTAL (PACsPOLYNUCLEAR AROMATIC HYDROCARBONSPOLYNUCLEAR AROMATIC HYDROCARBONSPROPYLENE DICHLORIDEPROPYLENE OXIDEQUARTZ in coal mine dust, by IR (redeposition)SILICA, CRYSTALLINE,SULFUR DIOXIDESULFURYL FLUORIDESUPER ABSORBENT POLYMERSTRIBUTYL PHOSPHATETRICHLOROETHYLENETRIFLUOROBROMOMETHANETUNGSTEN (soluble and insoluble)VANADIUM OXIDESVINYL ACETATEVINYL BROMIDEVINYL CHLORIDEVINYLIDENE CHLORIDEVOLATILE ORGANIC COMPOUNDSWARFARINZINC and compounds, as ZnZINC OXIDE

TYPES OF CHEMICAL1 HYDROCARBON HALOGENATED

2 ALCOHOLS III

3 ALCOHOLS COMBINED

5 ACETIC ACID

6 CHLOROACETIC ACID

7 VOLATILE ORGANIC COMPOUNDS

8 KETONES I

9 ACETIC ANHYDRIDE

10 ACETALDEHYDE by HPLC

11 POLYNUCLEAR AROMATIC HYDROCARBONS

12 GLYCOLS

13 ORGANOPHOSPHORUS PESTICIDES

14 BROMINE

15 AMMONIA

16 1,1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE

17 TRIFLUOROBROMOMETHANE

18 TUNGSTEN (soluble and insoluble)

19 TRICHLOROETHYLENE

20 TRIBUTYL PHOSPHATE

SILICA, CRYSTALLINE,21

22 SULFUR DIOXIDE

23 SULFURYL FLUORIDE

24 POLYCYCLIC AROMATIC COMPOUNDS, TOTAL (PACs

25 SUPER ABSORBENT POLYMERS

26 GLYCOL ETHERS

27 PROPYLENE DICHLORIDE

28 QUARTZ in coal mine dust, by IR (redeposition)

29 ALIPHATIC ALDEHYDES

30 PHENYL GLYCIDYL ETHER

31 PHENYLHYDRAZINE

32 CRESOL (all isomers) and PHENOL

33 PHENYL ETHER

34 PHOSPHINE

35 ORGANONITROGEN PESTICIDES

36 OIL MIST, MINERAL

37 1-OCTANETHIOL

38 VOLATILE ORGANIC COMPOUNDS

39 p-NITROANILINE

40 NITROUS OXIDE

41 NITROSAMINES

42 1-NITROPYRENE IN DIESEL PARTICULATES

43 2-NITROPROPANE

44 NITROMETHANE

45 NITROGLYCERIN

46 NITROETHANE

47 ANILINE, o-TOLUIDINE, AND NITROBENZENE

48 NITROAROMATIC COMPOUNDS

49 NITRIC OXIDE and NITROGEN DIOXIDE

50 NICOTINE

51 NICKEL CARBONYL

52 NAPHTHYLAMINES, a and b

53 NAPHTHAS

54 METHYL tert-BUTYL ETHER

55 METHYL ETHYL KETONE PEROXIDE

56 MONOMETHYLHYDRAZINE

57 MONOMETHYLANILINE

58 METHYLTIN CHLORIDES

59 METHYL IODIDE

60 METHYL ETHYL KETON

61 METHYL CHLORIDE

62 METHYL BROMIDE

63 METHYL AND ETHYL METHACRYLATE

64 METHYL CELLOSOLVE ACETATE

65 METHANOL

66 LEAD SULFIDE

67 ELEMENTS by ICP 7301(Aqua Regia Ashing)antimony* chromium* lithium potassium tin zirconium*arsenic cobalt magnesium selenium titaniumbarium copper manganese silver tungsten*

beryllium iron* molybdenum strontium vanadiumcadmium lanthanum nickel tellurium yttrium

68 ALKALINE DUSTS

69 LEAD in Air by Chemical Spot Test

70 LEAD by Flame AAS

71 KEPONE

72 NAPHTHAS

73 ISOPHORONE

74 ISOPROPYL ETHER

75 ISOPROPYL ACETATE

76 ISOCYANATES, MONOMERIC

77 ALCOHOLS II

78 HEXACHLOROBUTADIENE

79 HEXACHLORO-1,3-CYCLOPENTADIENE

80 HYDROQUINONE

81 HYDROGEN SULFIDE

82 HYDROGEN CYANIDE

83 HYDRAZINE

84 ISOCYANATES

85 ISOCYANATES

86 GLUTARALDEHYDE

87 FORMALDEHYDE by GC

88 POLYNUCLEAR AROMATIC HYDROCARBONS

89 FLUORIDES, aerosol and gas

90 FORMIC ACID

91 FORMALDEHYDE

92 PROPYLENE OXIDE

93 ETHYL BROMIDE

94 MERCAPTANS, METHYL-, ETHYL-, and n-BUTYL

95 ETHYL ETHER

96 ETHYLENIMINE

97 ESTERS 1

98 ETHYLENE CHLOROHYDRIN

99 HYDROCARBONS, AROMATIC

100 ETHYL CHLORIDE

ETHYL ACETATE101

102 ALCOHOLS IV

AMINOETHANOL COMPOUNDS I103

104 DYES, BENZIDINE-, o-TOLIDINE-, o-DIANISIDINE

105 DICHLOROFLUOROMETHANE

AMINES, ALIPHATIC106

107 AMINOETHANOL COMPOUNDS II

METHYLENE CHLORIDE108

109 DIAZOMETHANE

CHLORINATED AND ORGANONITROGEN HERBICIDES110

111 2,4-D

112 CHROMIUM, HEXAVALENT

113 ACIDS, INORGANIC

114 ACETONITRILE

115 ARSENIC TRIOXIDE

VINYL CHLORIDE

VINYL BROMIDE

VINYLIDENE CHLORIDE

VINYL ACETATE

AMINES, AROMATIC

WARFARIN

ZINC and compounds, as Zn

ZINC OXIDE

VANADIUM OXIDES

SOBRENT TYPES FLOW RATESOLID SORBENT TUBE 0.01 to 0.2 L/min(coconut shell charcoal, 100 mg/50 mg)SOLID SORBENT TUBE 0.01 to 0.2 L/min(coconut shell charcoal, 100 mg/50 mgSOLID SORBENT TUBE 0.01 to 0.2 L/min(Coconut shell charcoal, 100 mg/50 mg)SOLID SORBENT TUBE 0.01 to 1.0 L/min(coconut shell charcoal, 100 mg/50 mg)SOLID SORBENT TUBE 0.05 to 0.2 L/min(silica gel, 100 mg/50 mg)THERMAL DESORPTION TUBE (multi-bed sorbent tubes containing graphitized carbons and carbon molecular sieve sorbents [See Appendix])

SOLID SORBENT TUBE 0.01 to 0.2 L/min(Anasorb CMS, 150 mg/75 mg)

LIQUID IN BUBBLER 0.2 to 1.0 L/min(mixed bubbler with 10 mL alkalinehydroxylamine)

LIQUID IN BUBBLER(midget bubbler containing 15 mL 0.1 to 0.5 L/minGirard T solution @ pH 4.5)

FILTER + SORBENT TUBE(37-mm, 2-μm, PTFE + washed XAD-2, 100 2 L/minmg/50 mg)

XAD-7 OVS tube(glass fiber filter, 13-mm; XAD-7, 0.5 to 2 L/min200mg/100mg)

0.2 to 1 L/min13-mm quartz filter; XAD-2, 270 mg/140 mg

PREFILTER + FILTER 0.3 to 1 L/min(PTFE, 0.5-μm + silver membrane,25-mm, 0.45-μm)

SOLID SORBENT TUBE(sulfuric acid-treated silica gel) 0.1 to 0.2 L/min

FILTER/SOLID SORBENT TUBE (OVS-2 tube:

A 0.8-micron MCE prefilter may be used toremove particulate interferences.

SOLID SORBENT TUBE 0.01 to 0.05 L/min(coconut shell charcoal, 100 mg/50 mg

SOLID SORBENT TUBES 0.01 to 0.05 L/min(two coconut shell charcoal tubesin series, 400 mg/200 mg and100 mg/50 mg)

FILTER 1 to 4 L/min(0.8-μm cellulose ester membrane

SOLID SORBENT TUBE 0.01 to 0.2 L/min(coconut shell charcoal, 100 mg/50 mg)

1 to 3 L/min

cassettes in series

CYCLONE + FILTER HD cyclone: 2.2 L/min;(10-mm cyclone, nylon or Higgins- nylon cyclone: 1.7 L/minDewell (HD) + 0.8-:m MCE or 5-:mPVC)

FILTER + TREATED FILTER 0.5 to 1.5 L/min(cellulose + Na2CO3; preceded by0.8-μm cellulose ester membrane)

FILTER + SOLID SORBENT 1 to 2 L/min(2-μm, 37-mm, PTFE filter + washedXAD-2 resin, 100/50 mg )

MEMBRANE FILTER 1 to 3 L/min(PVC, 5-μm, 37-mm)

SOLID SORBENT TUBE 0.1 to 0.2 L/min(Anasorb® 747, 140 mg/70 mg)

SOLID SORBENT TUBE(petroleum charcoal, 100 mg/50 mg) 0.01 to 0.2 L/min

FILTER (0.8-μm mixed cellulose estermembrane); above 23 C, use two filter

CYCLONE + PREWEIGHED FILTER (10-mm HD cyclone: 2.2 L/mincyclone, nylon or Higgins-Dewell (HD), and nylon cyclone: 1.7 L/minPVC filter, 37-mm, 5-μm)

CARTRIDGE (containing silica gel 0.1 to 1.5 L/mincoated with acidified 2,4-dinitrophenylhydrazine)

SOLID SORBENT TUBE 0.01 to 1 L/min(coconut shell charcoal; 100 mg/50 mg)

GLASS MIDGET BUBBLER 0.2 to 1 L/min(containing 15 mL 0.1 M hydrochloricacid)

SOLID SORBENT TUBE(XAD-7, 100 mg/50 mg) 0.01 to 0.1 L/min

CHARCOAL TUBE 0.01 to 0.2 L/min(coconut shell charcoal, 100 mg/50 mg)

SORBENT TUBE 0.01 - 0.2 L/min(Hg(CN)2-coated silica gel, 300 mg/150 mg)

FILTER/SOLID SORBENT TUBE 0.1 to 1 L/min (OVS-2 Tube: 13-mm quartz fiber filter; XAD-2,270 mg/140 mg)

MEMBRANE FILTER 1 to 3 L/min(37-mm diameter, 0.8-:m MCE, 5-:mPVC, 2-:m PTFE, or glass fiber)

SOLID SORBENT TUBE 0.01 to 0.2 L/min(Tenax-GC, 100 mg/50 mg)

THERMAL DESORPTION TUBE TECHNIQUE 0.01 to 0.05 L/min(multi-bed sorbent tubes containing graphitized carbons and carbon molecularsieve sorbents

FILTER 1 to 3 L/min(0.8 μm mixed cellulose ester membrane

AMBIENT AIR OR BAG SAMPLE

SOLID SORBENT TUBE 0.2 to 2 L/min(Thermosorb/N™ air sampler

FILTER 1.0 to 2.0 L/min(Glass Fiber, 37-mm)

SOLID SORBENT TUBE 0.01 to 0.05 L/min(Chromosorb 106, 100 mg/50 mg)

SOLID SORBENT TUBE 0.01 to 0.05 L/min(Chromosorb 106, 600 mg/300 mg)

SOLID SAMPLER TUBE(Tenax-GC, 100 mg/50 mg) 0.2 to 1.0 L/min

SOLID SORBENT TUBES(XAD-2, 600 mg + 300 mg) 0.01 to 0.05 L/min

FILTER + SOLID SORBENT(Glass fiber filter, sulfuric acid treated + 0.2 L/minsilica gel sorbent tube, 520/260 mg)

SOLID SORBENT TUBE 0.01 to 0.02 L/min(Silica gel, 150 mg/75 mg)

SORBENT TUBES NO: 0.025 L/min(oxidizer + 2 triethanolamine-treated NO2: 0.025 - 0.2 L/minmolecular sieve)

SOLID SORBENT TUBE 1.0 L/minXAD-2 (100 mg/50 mg)

PREFILTER + SOLID SORBENT TUBE 0.05 to 0.2 L/min(low-Ni charcoal, 120 mg/60 mg;0.8-μm cellulose ester membrane

FILTER + SOLID SORBENT 0.2 to 0.8 L/min(glass fiber + silica gel, 100 mg/50 mg)

SOLID SORBENT TUBES 0.1 to 0.2 L/min(two charcoal tubes in series; front 400 mg;back 200 mg)

IMPINGER 0.5 to 2 L/min(15 mL dimethyl phthalate)

BUBBLER 0.5 to 1.5 L/min(0.1 M hydrochloric acid)

MIDGET BUBBLER 0.2 to 1.0 L/min(0.05 M sulfuric acid, 10 mL)

FILTER + SORBENT TUBE 0.25 to 1 L/min(OVS Tube: 13-mm glass fiber filter; XAD-2,270/140 mg)

SOLID SORBENT TUBE 0.01 to 1 L/min(coconut shell charcoal, 100 mg/50 mg)

SOLID SORBENT TUBE 0.01 to 0.2 L/min(beaded carbon, ~150 mg/~75 mg)

SOLID SORBENT TUBES 0.01 to 0.1 L/min(two coconut shell charcoal tubes in series, 400mg/200 mg and 100 mg/50 mg)

SOLID SORBENT TUBES 0.01 to 0.1 L/min(two petroleum charcoal tubes, 400 mg and200 mg; drying tube, 9-g Na2SO4,necessary at humidity >50%)

SOLID SORBENT TUBE 0.01 to 0.05 L/min(XAD-2, 400/200 mg)

SOLID SORBENT TUBE 0.02 to 0.2 L/min(silica gel, 100/50 mg)

CYCLONE + FILTER HD cyclone: 2.2 L/min(10-mm nylon or Higgins-Dewell (HD) cyclone nylon cyclone: 1.7 L/min

FILTER 1 to 4 L/min(0.8-μm, cellulose ester membrane, or5.0-μm, polyvinyl chloride membrane

FILTER 1 to 4 L/min(1-μm PTFE membrane)

FILTER 2 L/min(0.8-μm cellulose ester membrane)

FILTER + IMPINGER 0.5 to 1 L/min(0.8-μm cellulose ester membrane+ impinger with 0.1 M NaOH)

SOLID SORBENT TUBE 0.01 to 1 L/min(petroleum-based charcoal,100 mg/50 mg)

Solid Sorbent Tube 0.01 to 0.05 L/min(coconut shell charcoal; 100 mg/50 mg)

SOLID SORBENT TUBE 0.02 to 0.2 L/min(coconut shell charcoal, 100 mg/50 mg,

IMPINGER 1 L/min(solution of 1-(2-methoxyphenyl)-piperazine intoluene)

SOLID SORBENT TUBE 0.05 to 0.2 L/min(XAD-2; 100 mg/50 mg)

SOLID SORBENT TUBE(2 tubes, Porapak T, 75 mg and 25 mg) 0.01 to 0.2 L/min

FILTER + SOLID SORBENT TUBE 0.1 to 1.5 L/min

(Zefluor, 0.5 μm; coconut shell -RECOMMENDED: 0.2 L/mcharcoal, 400 mg/200 mg

SOLID SORBENT TUBE 0.05 to 0.2 L/min(soda lime, 600 mg/200 mg)

BUBBLER 0.2 to 1.0 L/min(15 mL 0.1 M HCl)

IMPINGER 1 to 2 L/min(tryptamine/DMSO; 20 mL)

SOLID SORBENT TUBE 0.05 to 0.5 L/min(silica gel coated with 2,4-dinitrophenylhydrazineHCl, 300 mg/150 mg

SOLID SORBENT TUBE 0.01 to 0.10 L/min(10% (2-hydroxymethyl)piperdine onXAD-2, 120 mg/60 mg

FILTER + SORBENT 2 L/min(2-μm, 37-mm PTFE + washed XAD-2,100 mg/50 mg)

FILTER + TREATED PAD(0.8-μm cellulose ester membrane + 1 to 2 L/minNa2CO3-treated cellulose pad)

FILTER + SOLID SORBENT TUBE 0.05 to 0.2 L/min(PTFE membrane, 5-μm + washed, silicagel, 400 mg/200 mg)

CARTRIDGE 0.03 to 1.5 L/min(Cartridge containing silica gel coated with2,4-dinitrophenylhydrazine)

FILTER 0.1 to 0.2 L/min

(glass fiber, 37-mm, impregnated withmercuric acetate)

Solid Sorbent Tube 0.01 to 0.2 L/min(coconut shell charcoal, 100 mg/50 mg)

BUBBLER 0.2 L/min(Folin's reagent

SOLID SORBENT TUBE 0.01 to 0.2 L/min(petroleum charcoal, 100 mg/50 mg)

SOLID SORBENT TUBE(coconut shell charcoal, 100 mg/50 mg)

SOLID SORBENT TUBES(2 coconut shell charcoal tubes, 0.02 to 0.05 L/min400 mg and 200 mg)

SOLID SORBENT TUBE 0.01 to 0.2 L/minute(coconut shell charcoal, 100 mg/50 mg)

SOLID SORBENT TUBE 0.01 to 0.05 L/min(Coconut shell charcoal, 100 mg/50 mg)

SOLID SORBENT TUBE 0.01 to 0.2 L/min(silica gel, 300 mg/150 mg)

FILTER 1 to 3 L/min(5-μm PTFE membrane

SOLID SORBENT TUBES 0.01 to 0.05 L/min(2 coconut shell charcoal tubes,400 mg and 200 mg)

SOLID SORBENT TUBE 0.01 to 1.0 L/min(silica gel, 150 mg / 75 mg)

IMPINGER 0.5 to 1 L/min(15 mL 2 mM hexanesulfonic acid)

SOLID SORBENT 0.01 to 0.2 L/min(2 coconut shell charcoal tubes, 100/50 mg

SOLID SORBENT TUBE 0.2 L/min(octanoic acid-coated XAD-2 resin,100 mg/50 mg)

FILTER/SOLID SORBENT TUBE 0.2 to 1 L/min(OVS tube: 11-mm quartz filter; XAD-2)

FILTER 1 to 3 L/min(glass fiber, binderless

FILTER 1 to 4 L/min(5.0-μm PVC membrane)

SOLID SORBENT TUBE 0.2 to 0.5 L/min(washed silica gel, 400 mg/200 mg withglass fiber filter plug)

SOLID SORBENT TUBE(coconut shell charcoal, 400/200 mg) 0.01 to 0.2 L/min

FILTER 1 to 3 L/mi(Na2CO3-impregnated, 0.8-μm celluloseester membrane + backup pad)

SOLID SORBENT TUBE 0.05 L/min(2 tandem tubes, each with 150 mg activatedcoconut charcoal)

SOLID SORBENT TUBE 0.1 to 0.2 L/min(carbon molecular sieve; 160 mg/80 mg;ORBO-92 or equivalent)

SOLID SORBENT TUBE(silica gel, 150 mg/75 mg)

FILTER 1 to 4 L/min(1-μm PTFE membrane)

FILTER 1 to 3 L/min(0.8-μm PVC membrane, 25-mm diameter, inopen-face cassette)

CYCLONE + FILTER HD cyclone: 2.2 L/min(10-mm cyclone or Higgins-Dewell (HD) + nylon cyclone: 1.7 L/min5-μm PVC membrane)

MEASUREMENT TECHNIQUEGAS CHROMATOGRAPHY, FID

GAS CHROMATOGRAPHY, FID

ION CHROMATOGRAPHY,CONDUCTIVITY DETECTION

VISIBLE ABSORPTIONSPECTROPHOTOMETRY

HPLC, UV

HPLC, FLUORESCENCE/UVDETECTION

GC, FLAME PHOTOMETRIC DETE

ION CHROMATOGRAPHY,CONDUCTIVITY

VISIBLE ABSORPTION

SPECTROPHOTOMETRY

GAS CHROMATOGRAPH, FID

ATOMIC ABSORPTION, FLAME

GC, FPD with a phosphorus filter

ION CHROMATOGRAPHY

ION CHROMATOGRAPHYCONDUCTIVITY DETECTION

FLOW INJECTION, FLUORESCENCEDETECTOR

ICP-AES OR AAS

GAS CHROMATOGRAPHY WITHELECTROLYTIC CONDUCTIVITYDETECTOR (HALL)

INFRARED ABSORPTIONSPECTROPHOTOMETRY (IR)

HPLC; UV DETECTION

UV-VIS SPECTROMETER

HPLC, UV detection

INFRARED SPECTROPHOTOMETRY

GAS CHROMATOGRAPHY, SULFURSPECIFICFPD

THERMAL DESORPTION, GAS CHROMATOGRAPHY, MASS SPECTROMETRY

HPLC, UV DETECTION

LONG-PATHLENGTH PORTABLEINFRARED SPECTROPHOTOMETER

(FIELD READOUT

GAS CHROMATOGRAPHY,

GAS CHROMATOGRAPHY, NITROGENCHEMILUMINESCENCE DETECTOR

GAS CHROMATOGRAPHY, FLAMEIONIZATION DETECTOR

GAS CHROMATOGRAPHY, NITROGENSPECIFICDETECTOR

GAS CHROMATOGRAPHY, ECD

GAS CHROMATOGRAPHY-NITROGENPHOSPHOROUS DETECTOR

ATOMIC ABSORPTION, GRAPHITEFURNACE

GAS CHROMATOGRAPHY, FIDANALYTE

VISIBLE SPECTROPHOTOMETRY

GAS CHROMATOGRAPHY, FPD

GAS CHROMATOGRAPHY, FI

GAS CHROMATOGRAPHY, ATOMICEMISSION DETECTION (GC-AED)monitoring Br, C and H channels

GAS CHROMATOGRAPHY, FI

X-RAY POWDER DIFFRACTION

INDUCTIVELY COUPLED ARGONPLASMA, ATOMIC EMISSIONSPECTROSCOPY (ICP-AES)

ACID-BASE TITRATION

CHEMICAL SPOT TEST KIT (Rhodizonate-based)

ATOMIC ABSORPTIONSPECTROPHOTOMETER, FLAME

HPLC, ELECTROCHEMICAL ANDUV DETECTION

GAS CHROMATOGRAPHY/ECD

GAS CHROMATOGRAPHY, 63Ni ECD

HPLC, UV DETECTION

ION CHROMATOGRAPHY,

CONDUCTIVITY

SPECTROPHOTOMETRY,VISIBLE ABSORPTION

SPECTROPHOTOMETRY, VISIBLEABSORPTION

HPLC, FLUORESCENCE DETECTOR/ELECTROCHEMICAL DETECTOR

HPLC, UV DETECTION

GAS CHROMATOGRAPHY, CAPILLARYCOLUMN, FID

ION-SPECIFIC ELECTRODE

ION CHROMATOGRAPHY,CONDUCTIVITY DETECTION

HPLC, UV DETECTION

GAS CHROMATOGRAPHY

GAS CHROMOTOGRAPHY, FID

HPLC, UV DETECTION

SOLID SORBENT TUBES(2 coconut shell charcoal tubes,400 mg and 200 mg)

HPLC, UV DETECTION

ION CHROMATOGRAPHY, ion pairing

GAS CHROMATOGRAPHY/ ELECTRONCAPTURE DETECTOR (GC/ECD)

HPLC, UV DETECTION

ION CHROMATOGRAPHY

HPLC, UV DETECTION

ATOMIC ABSORPTION, FLAME

X-RAY POWDER DIFFRACTION

TYPES OF CHEMICAL SOBRENT TYPES FLOW RATESOLID SORBENT TUBE 0.01 to 0.2 L/min(coconut shell charcoal, 100 mg/50 mg)

HYDROCARBON HALOGENATED

TYPES OF CHEMICALALCOHOLS III

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.01 to 0.2 L/min(coconut shell charcoal, 100 mg/50 mg

TYPES OF CHEMICALALCOHOLS COMBINED

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.01 to 0.2 L/min(Coconut shell charcoal, 100 mg/50 mg)

TYPES OF CHEMICALACETIC ACID

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.01 to 1.0 L/min(coconut shell charcoal, 100 mg/50 mg)

TYPES OF CHEMICALCHLOROACETIC ACID

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.05 to 0.2 L/min(silica gel, 100 mg/50 mg)

MEASUREMENT TECHNIQUEION CHROMATOGRAPHY,CONDUCTIVITY DETECTION

TYPES OF CHEMICALKETONES I

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.01 to 0.2 L/min(Anasorb CMS, 150 mg/75 mg)

TYPES OF CHEMICALACETIC ANHYDRIDE

SAMPLING MEDIA FLOW RATELIQUID IN BUBBLER 0.2 to 1.0 L/min(mixed bubbler with 10 mL alkalinehydroxylamine)

MEASUREMENT TECHNIQUEVISIBLE ABSORPTIONSPECTROPHOTOMETRY

TYPES OF CHEMICALACETALDEHYDE by HPLC

SAMPLING MEDIA FLOW RATELIQUID IN BUBBLER(midget bubbler containing 15 mL 0.1 to 0.5 L/minGirard T solution @ pH 4.5)

MEASUREMENT TECHNIQUE

HPLC, UV

TYPES OF CHEMICALPOLYNUCLEAR AROMATIC HYDROCARBONS

SAMPLING MEDIA FLOW RATEFILTER + SORBENT TUBE(37-mm, 2-μm, PTFE + washed XAD-2, 100 2 L/minmg/50 mg)

HPLC, FLUORESCENCE/UVDETECTION

TYPES OF CHEMICALGLYCOLS

SAMPLING MEDIA FLOW RATEXAD-7 OVS tube(glass fiber filter, 13-mm; XAD-7, 0.5 to 2 L/min200mg/100mg)

TYPES OF CHEMICALORGANOPHOSPHORUS PESTICIDES

SAMPLING MEDIA FLOW RATEFILTER/SOLID SORBENT TUBE (OVS-2 tube: 0.2 to 1 L/min13-mm quartz filter; XAD-2, 270 mg/140 mg

MEASUREMENT TECHNIQUEGC, FLAME PHOTOMETRIC DETE

TYPES OF CHEMICALBROMINE

SAMPLING MEDIA FLOW RATEPREFILTER + FILTER 0.3 to 1 L/min(PTFE, 0.5-μm + silver membrane,25-mm, 0.45-μm)

MEASUREMENT TECHNIQUEION CHROMATOGRAPHY,CONDUCTIVITY

TYPES OF CHEMICALAMMONIA

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE(sulfuric acid-treated silica gel) 0.1 to 0.2 L/minA 0.8-micron MCE prefilter may be used toremove particulate interferences.

TYPES OF CHEMICAL

1,1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE

SAMPLING MEDIA FLOW RATE

GAS CHROMATOGRAPH, FID

TYPES OF CHEMICALTRIFLUOROBROMOMETHANE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBES 0.01 to 0.05 L/min(two coconut shell charcoal tubesin series, 400 mg/200 mg and100 mg/50 mg)

TYPES OF CHEMICALTUNGSTEN (soluble and insoluble)

SAMPLING MEDIA FLOW RATEFILTER 1 to 4 L/min(0.8-μm cellulose ester membrane

MEASUREMENT TECHNIQUEATOMIC ABSORPTION, FLAME

TYPES OF CHEMICALTRICHLOROETHYLENE

TYPES OF CHEMICALTRIBUTYL PHOSPHATE

SAMPLING MEDIA FLOW RATEFILTER (0.8-μm mixed cellulose ester 1 to 3 L/minmembrane); above 23 C, use two filtercassettes in series

MEASUREMENT TECHNIQUEGC, FPD with a phosphorus filter

TYPES OF CHEMICAL

SILICA, CRYSTALLINE,

SAMPLING MEDIA FLOW RATECYCLONE + FILTER HD cyclone: 2.2 L/min;(10-mm cyclone, nylon or Higgins- nylon cyclone: 1.7 L/minDewell (HD) + 0.8-:m MCE or 5-:mPVC)

TYPES OF CHEMICALSULFUR DIOXIDE

SAMPLING MEDIA FLOW RATEFILTER + TREATED FILTER 0.5 to 1.5 L/min(cellulose + Na2CO3; preceded by0.8-μm cellulose ester membrane)

MEASUREMENT TECHNIQUEION CHROMATOGRAPHY

TYPES OF CHEMICALSULFURYL FLUORIDE

MEASUREMENT TECHNIQUEION CHROMATOGRAPHYCONDUCTIVITY DETECTION

TYPES OF CHEMICALPOLYCYCLIC AROMATIC COMPOUNDS, TOTAL (PACs

SAMPLING MEDIA FLOW RATEFILTER + SOLID SORBENT 1 to 2 L/min(2-μm, 37-mm, PTFE filter + washedXAD-2 resin, 100/50 mg )

MEASUREMENT TECHNIQUEFLOW INJECTION, FLUORESCENCEDETECTOR

TYPES OF CHEMICALSUPER ABSORBENT POLYMERS

SAMPLING MEDIA FLOW RATEMEMBRANE FILTER 1 to 3 L/min(PVC, 5-μm, 37-mm)

MEASUREMENT TECHNIQUEICP-AES OR AAS

TYPES OF CHEMICALGLYCOL ETHERS

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.1 to 0.2 L/min(Anasorb® 747, 140 mg/70 mg)

TYPES OF CHEMICALPROPYLENE DICHLORIDE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE(petroleum charcoal, 100 mg/50 mg) 0.01 to 0.2 L/min

MEASUREMENT TECHNIQUEGAS CHROMATOGRAPHY WITHELECTROLYTIC CONDUCTIVITYDETECTOR (HALL)

TYPES OF CHEMICALQUARTZ in coal mine dust, by IR (redeposition)

SAMPLING MEDIA FLOW RATECYCLONE + PREWEIGHED FILTER (10-mm HD cyclone: 2.2 L/mincyclone, nylon or Higgins-Dewell (HD), and nylon cyclone: 1.7 L/minPVC filter, 37-mm, 5-μm)

MEASUREMENT TECHNIQUEINFRARED ABSORPTIONSPECTROPHOTOMETRY (IR)

TYPES OF CHEMICALALIPHATIC ALDEHYDES

SAMPLING MEDIA FLOW RATECARTRIDGE (containing silica gel 0.1 to 1.5 L/mincoated with acidified 2,4-dinitrophenylhydrazine)

MEASUREMENT TECHNIQUEHPLC; UV DETECTION

TYPES OF CHEMICAL

PHENYL GLYCIDYL ETHER

SOLID SORBENT TUBE 0.01 to 1 L/min(coconut shell charcoal; 100 mg/50 mg)

TYPES OF CHEMICALPHENYLHYDRAZINE

SAMPLING MEDIA FLOW RATEGLASS MIDGET BUBBLER 0.2 to 1 L/min(containing 15 mL 0.1 M hydrochloricacid)

TYPES OF CHEMICAL

CRESOL (all isomers) and PHENOL

SOLID SORBENT TUBE(XAD-7, 100 mg/50 mg) 0.01 to 0.1 L/min

TYPES OF CHEMICALPHENYL ETHER

SAMPLING MEDIA FLOW RATECHARCOAL TUBE 0.01 to 0.2 L/min(coconut shell charcoal, 100 mg/50 mg)

TYPES OF CHEMICALPHOSPHINE

SAMPLING MEDIA FLOW RATESORBENT TUBE 0.01 - 0.2 L/min(Hg(CN)2-coated silica gel, 300 mg/150 mg)

MEASUREMENT TECHNIQUEUV-VIS SPECTROMETER

TYPES OF CHEMICALORGANONITROGEN PESTICIDES

SAMPLING MEDIA FLOW RATEFILTER/SOLID SORBENT TUBE 0.1 to 1 L/min (OVS-2 Tube: 13-mm quartz fiber filter; XAD-2,270 mg/140 mg)

MEASUREMENT TECHNIQUEHPLC, UV detection

TYPES OF CHEMICALOIL MIST, MINERAL

SAMPLING MEDIA FLOW RATEMEMBRANE FILTER 1 to 3 L/min(37-mm diameter, 0.8-:m MCE, 5-:mPVC, 2-:m PTFE, or glass fiber)

MEASUREMENT TECHNIQUEINFRARED SPECTROPHOTOMETRY

TYPES OF CHEMICAL1-OCTANETHIOL

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.01 to 0.2 L/min(Tenax-GC, 100 mg/50 mg)

MEASUREMENT TECHNIQUEGAS CHROMATOGRAPHY, SULFURSPECIFICFPD

TYPES OF CHEMICAL

VOLATILE ORGANIC COMPOUNDS

THERMAL DESORPTION TUBE TECHNIQUE 0.01 to 0.05 L/min(multi-bed sorbent tubes containing graphitized carbons and carbon molecularsieve sorbents

THERMAL DESORPTION, GAS CHROMATOGRAPHY, MASS SPECTROMETRY

TYPES OF CHEMICAL

p-NITROANILINE

FILTER 1 to 3 L/min(0.8 μm mixed cellulose ester membrane

HPLC, UV DETECTION

TYPES OF CHEMICALNITROUS OXIDE

SAMPLING MEDIA FLOW RATEAMBIENT AIR OR BAG SAMPLE

MEASUREMENT TECHNIQUELONG-PATHLENGTH PORTABLEINFRARED SPECTROPHOTOMETER(FIELD READOUT

TYPES OF CHEMICALNITROSAMINES

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.2 to 2 L/min(Thermosorb/N™ air sampler

MEASUREMENT TECHNIQUEGAS CHROMATOGRAPHY,

TYPES OF CHEMICAL1-NITROPYRENE IN DIESEL PARTICULATES

SAMPLING MEDIA FLOW RATEFILTER 1.0 to 2.0 L/min(Glass Fiber, 37-mm)

MEASUREMENT TECHNIQUEGAS CHROMATOGRAPHY, NITROGENCHEMILUMINESCENCE DETECTOR

TYPES OF CHEMICAL2-NITROPROPANE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.01 to 0.05 L/min(Chromosorb 106, 100 mg/50 mg)

MEASUREMENT TECHNIQUEGAS CHROMATOGRAPHY, FLAMEIONIZATION DETECTOR

TYPES OF CHEMICALNITROMETHANE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.01 to 0.05 L/min(Chromosorb 106, 600 mg/300 mg)

MEASUREMENT TECHNIQUEGAS CHROMATOGRAPHY, NITROGENSPECIFICDETECTOR

TYPES OF CHEMICALNITROGLYCERIN

SAMPLING MEDIA FLOW RATESOLID SAMPLER TUBE(Tenax-GC, 100 mg/50 mg) 0.2 to 1.0 L/min

TYPES OF CHEMICALNITROETHANE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBES(XAD-2, 600 mg + 300 mg) 0.01 to 0.05 L/min

TYPES OF CHEMICALANILINE, o-TOLUIDINE, AND NITROBENZENE

SAMPLING MEDIA FLOW RATEFILTER + SOLID SORBENT(Glass fiber filter, sulfuric acid treated + 0.2 L/minsilica gel sorbent tube, 520/260 mg)

TYPES OF CHEMICALNITROAROMATIC COMPOUNDS

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.01 to 0.02 L/min(Silica gel, 150 mg/75 mg)

TYPES OF CHEMICALNITRIC OXIDE and NITROGEN DIOXIDE

SAMPLING MEDIA FLOW RATESORBENT TUBES NO: 0.025 L/min(oxidizer + 2 triethanolamine-treated NO2: 0.025 - 0.2 L/minmolecular sieve)

TYPES OF CHEMICALNICOTINE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 1.0 L/minXAD-2 (100 mg/50 mg)

MEASUREMENT TECHNIQUEGAS CHROMATOGRAPHY-NITROGENPHOSPHOROUS DETECTOR

TYPES OF CHEMICALNICKEL CARBONYL

SAMPLING MEDIA FLOW RATEPREFILTER + SOLID SORBENT TUBE 0.05 to 0.2 L/min(low-Ni charcoal, 120 mg/60 mg;0.8-μm cellulose ester membrane

MEASUREMENT TECHNIQUEATOMIC ABSORPTION, GRAPHITEFURNACE

TYPES OF CHEMICALNAPHTHYLAMINES, a and b

SAMPLING MEDIA FLOW RATEFILTER + SOLID SORBENT 0.2 to 0.8 L/min(glass fiber + silica gel, 100 mg/50 mg)

MEASUREMENT TECHNIQUEGAS CHROMATOGRAPHY, FIDANALYTE

TYPES OF CHEMICALNAPHTHAS

TYPES OF CHEMICALMETHYL tert-BUTYL ETHER

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBES 0.1 to 0.2 L/min(two charcoal tubes in series; front 400 mg;back 200 mg)

TYPES OF CHEMICAL

METHYL ETHYL KETONE PEROXIDE

IMPINGER 0.5 to 2 L/min(15 mL dimethyl phthalate)

TYPES OF CHEMICAL

MONOMETHYLHYDRAZINE

BUBBLER 0.5 to 1.5 L/min(0.1 M hydrochloric acid)

VISIBLE SPECTROPHOTOMETRY

TYPES OF CHEMICAL

MONOMETHYLANILINE

MIDGET BUBBLER 0.2 to 1.0 L/min(0.05 M sulfuric acid, 10 mL)

TYPES OF CHEMICALMETHYLTIN CHLORIDES

SAMPLING MEDIA FLOW RATEFILTER + SORBENT TUBE 0.25 to 1 L/min(OVS Tube: 13-mm glass fiber filter; XAD-2,270/140 mg)

MEASUREMENT TECHNIQUEGAS CHROMATOGRAPHY, FPD

TYPES OF CHEMICALMETHYL IODIDE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.01 to 1 L/min(coconut shell charcoal, 100 mg/50 mg)

TYPES OF CHEMICALMETHYL ETHYL KETON

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.01 to 0.2 L/min(beaded carbon, ~150 mg/~75 mg)

MEASUREMENT TECHNIQUEGAS CHROMATOGRAPHY, FI

TYPES OF CHEMICALMETHYL CHLORIDE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBES 0.01 to 0.1 L/min(two coconut shell charcoal tubes in series, 400mg/200 mg and 100 mg/50 mg)

TYPES OF CHEMICALMETHYL BROMIDE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBES 0.01 to 0.1 L/min(two petroleum charcoal tubes, 400 mg and200 mg; drying tube, 9-g Na2SO4,necessary at humidity >50%)

MEASUREMENT TECHNIQUEGAS CHROMATOGRAPHY, ATOMICEMISSION DETECTION (GC-AED)monitoring Br, C and H channels

TYPES OF CHEMICAL

METHYL AND ETHYL METHACRYLATE

SOLID SORBENT TUBE 0.01 to 0.05 L/min(XAD-2, 400/200 mg)

TYPES OF CHEMICALMETHYL CELLOSOLVE ACETATE

MEASUREMENT TECHNIQUEGAS CHROMATOGRAPHY, FI

TYPES OF CHEMICALMETHANOL

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.02 to 0.2 L/min(silica gel, 100/50 mg)

TYPES OF CHEMICALLEAD SULFIDE

SAMPLING MEDIA FLOW RATECYCLONE + FILTER HD cyclone: 2.2 L/min(10-mm nylon or Higgins-Dewell (HD) cyclone nylon cyclone: 1.7 L/min

MEASUREMENT TECHNIQUEX-RAY POWDER DIFFRACTION

TYPES OF CHEMICAL

(Aqua Regia Ashing)antimony* chromium* lithium potassium tin zirconium*arsenic cobalt magnesium selenium titaniumbarium copper manganese silver tungsten*beryllium iron* molybdenum strontium vanadiumcadmium lanthanum nickel tellurium yttrium

ELEMENTS by ICP 7301

FILTER 1 to 4 L/min(0.8-μm, cellulose ester membrane, or5.0-μm, polyvinyl chloride membrane

INDUCTIVELY COUPLED ARGONPLASMA, ATOMIC EMISSIONSPECTROSCOPY (ICP-AES)

TYPES OF CHEMICALALKALINE DUSTS

SAMPLING MEDIA FLOW RATEFILTER 1 to 4 L/min(1-μm PTFE membrane)

MEASUREMENT TECHNIQUEACID-BASE TITRATION

TYPES OF CHEMICALLEAD in Air by Chemical Spot Test

SAMPLING MEDIA FLOW RATEFILTER 2 L/min(0.8-μm cellulose ester membrane)

MEASUREMENT TECHNIQUECHEMICAL SPOT TEST KIT (Rhodizonate-based)

TYPES OF CHEMICALLEAD by Flame AAS

MEASUREMENT TECHNIQUEATOMIC ABSORPTIONSPECTROPHOTOMETER, FLAME

TYPES OF CHEMICALKEPONE

SAMPLING MEDIA FLOW RATEFILTER + IMPINGER 0.5 to 1 L/min(0.8-μm cellulose ester membrane+ impinger with 0.1 M NaOH)

MEASUREMENT TECHNIQUEGAS CHROMATOGRAPHY, ECD

TYPES OF CHEMICALNAPHTHAS

TYPES OF CHEMICAL

ISOPHORONE

SOLID SORBENT TUBE 0.01 to 1 L/min(petroleum-based charcoal,

TYPES OF CHEMICAL

ISOPROPYL ETHER

Solid Sorbent Tube 0.01 to 0.05 L/min(coconut shell charcoal; 100 mg/50 mg)

TYPES OF CHEMICAL

ISOPROPYL ACETATE

SOLID SORBENT TUBE 0.02 to 0.2 L/min(coconut shell charcoal, 100 mg/50 mg,

TYPES OF CHEMICAL

ISOCYANATES, MONOMERIC

IMPINGER 1 L/min(solution of 1-(2-methoxyphenyl)-piperazine intoluene)

HPLC, ELECTROCHEMICAL ANDUV DETECTION

TYPES OF CHEMICAL

ALCOHOLS II

TYPES OF CHEMICALHEXACHLOROBUTADIENE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.05 to 0.2 L/min(XAD-2; 100 mg/50 mg)

MEASUREMENT TECHNIQUEGAS CHROMATOGRAPHY/ECD

TYPES OF CHEMICALHEXACHLORO-1,3-CYCLOPENTADIENE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE(2 tubes, Porapak T, 75 mg and 25 mg) 0.01 to 0.2 L/min

GAS CHROMATOGRAPHY, 63Ni ECD

TYPES OF CHEMICALHYDROQUINONE

MEASUREMENT TECHNIQUEHPLC, UV DETECTION

TYPES OF CHEMICALHYDROGEN SULFIDE

SAMPLING MEDIA FLOW RATEFILTER + SOLID SORBENT TUBE 0.1 to 1.5 L/min(Zefluor, 0.5 μm; coconut shell -RECOMMENDED: 0.2 L/mcharcoal, 400 mg/200 mg

MEASUREMENT TECHNIQUEION CHROMATOGRAPHY,CONDUCTIVITY

TYPES OF CHEMICALHYDROGEN CYANIDE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.05 to 0.2 L/min(soda lime, 600 mg/200 mg)

MEASUREMENT TECHNIQUESPECTROPHOTOMETRY,VISIBLE ABSORPTION

TYPES OF CHEMICALHYDRAZINE

SAMPLING MEDIA FLOW RATEBUBBLER 0.2 to 1.0 L/min(15 mL 0.1 M HCl)

MEASUREMENT TECHNIQUESPECTROPHOTOMETRY, VISIBLEABSORPTION

TYPES OF CHEMICALISOCYANATES

SAMPLING MEDIA FLOW RATEIMPINGER 1 to 2 L/min(tryptamine/DMSO; 20 mL)

MEASUREMENT TECHNIQUEHPLC, FLUORESCENCE DETECTOR/ELECTROCHEMICAL DETECTOR

TYPES OF CHEMICALGLUTARALDEHYDE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.05 to 0.5 L/min(silica gel coated with 2,4-dinitrophenylhydrazineHCl, 300 mg/150 mg

TYPES OF CHEMICALFORMALDEHYDE by GC

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.01 to 0.10 L/min(10% (2-hydroxymethyl)piperdine onXAD-2, 120 mg/60 mg

TYPES OF CHEMICALPOLYNUCLEAR AROMATIC HYDROCARBONS

SAMPLING MEDIA FLOW RATEFILTER + SORBENT 2 L/min(2-μm, 37-mm PTFE + washed XAD-2,100 mg/50 mg)

MEASUREMENT TECHNIQUEGAS CHROMATOGRAPHY, CAPILLARYCOLUMN, FID

TYPES OF CHEMICALFLUORIDES, aerosol and gas

SAMPLING MEDIA FLOW RATEFILTER + TREATED PAD(0.8-μm cellulose ester membrane + 1 to 2 L/minNa2CO3-treated cellulose pad)

ION-SPECIFIC ELECTRODE

TYPES OF CHEMICALFORMIC ACID

SAMPLING MEDIA FLOW RATEFILTER + SOLID SORBENT TUBE 0.05 to 0.2 L/min(PTFE membrane, 5-μm + washed, silicagel, 400 mg/200 mg)

MEASUREMENT TECHNIQUEION CHROMATOGRAPHY,CONDUCTIVITY DETECTION

TYPES OF CHEMICALFORMALDEHYDE

SAMPLING MEDIA FLOW RATECARTRIDGE 0.03 to 1.5 L/min(Cartridge containing silica gel coated with2,4-dinitrophenylhydrazine)

TYPES OF CHEMICALPROPYLENE OXIDE

TYPES OF CHEMICALETHYL BROMIDE

TYPES OF CHEMICALMERCAPTANS, METHYL-, ETHYL-, and n-BUTYL

SAMPLING MEDIA FLOW RATEFILTER 0.1 to 0.2 L/min(glass fiber, 37-mm, impregnated withmercuric acetate)

MEASUREMENT TECHNIQUEGAS CHROMATOGRAPHY

TYPES OF CHEMICALETHYL ETHER

SAMPLING MEDIA FLOW RATESolid Sorbent Tube 0.01 to 0.2 L/min(coconut shell charcoal, 100 mg/50 mg)

MEASUREMENT TECHNIQUEGAS CHROMOTOGRAPHY, FID

TYPES OF CHEMICALETHYLENIMINE

SAMPLING MEDIA FLOW RATEBUBBLER 0.2 L/min(Folin's reagent

TYPES OF CHEMICALESTERS 1

TYPES OF CHEMICALETHYLENE CHLOROHYDRIN

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.01 to 0.2 L/min(petroleum charcoal, 100 mg/50 mg)

TYPES OF CHEMICALHYDROCARBONS, AROMATIC

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE(coconut shell charcoal, 100 mg/50 mg)

TYPES OF CHEMICALETHYL CHLORIDE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBES(2 coconut shell charcoal tubes, 0.02 to 0.05 L/min400 mg and 200 mg)

SOLID SORBENT TUBES(2 coconut shell charcoal tubes,400 mg and 200 mg)

TYPES OF CHEMICALETHYL ACETATE

SOLID SORBENT TUBE 0.01 to 0.2 L/minute(coconut shell charcoal, 100 mg/50 mg)

TYPES OF CHEMICALALCOHOLS IV

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.01 to 0.05 L/min(Coconut shell charcoal, 100 mg/50 mg)

TYPES OF CHEMICALAMINOETHANOL COMPOUNDS I

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.01 to 0.2 L/min(silica gel, 300 mg/150 mg)

TYPES OF CHEMICALDYES, BENZIDINE-, o-TOLIDINE-, o-DIANISIDINE

SAMPLING MEDIA FLOW RATEFILTER 1 to 3 L/min(5-μm PTFE membrane

TYPES OF CHEMICALDICHLOROFLUOROMETHANE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBES 0.01 to 0.05 L/min(2 coconut shell charcoal tubes,400 mg and 200 mg)

TYPES OF CHEMICALAMINES, ALIPHATIC

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.01 to 1.0 L/min(silica gel, 150 mg / 75 mg)

TYPES OF CHEMICALAMINOETHANOL COMPOUNDS II

SAMPLING MEDIA FLOW RATEIMPINGER 0.5 to 1 L/min(15 mL 2 mM hexanesulfonic acid)

MEASUREMENT TECHNIQUEION CHROMATOGRAPHY, ion pairing

TYPES OF CHEMICALMETHYLENE CHLORIDE

SAMPLING MEDIA FLOW RATESOLID SORBENT 0.01 to 0.2 L/min(2 coconut shell charcoal tubes, 100/50 mg

TYPES OF CHEMICALDIAZOMETHANE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.2 L/min(octanoic acid-coated XAD-2 resin,100 mg/50 mg)

TYPES OF CHEMICALCHLORINATED AND ORGANONITROGEN HERBICIDES

SAMPLING MEDIA FLOW RATEFILTER/SOLID SORBENT TUBE 0.2 to 1 L/min(OVS tube: 11-mm quartz filter; XAD-2)

MEASUREMENT TECHNIQUEGAS CHROMATOGRAPHY/ ELECTRONCAPTURE DETECTOR (GC/ECD)

TYPES OF CHEMICAL2,4-D

SAMPLING MEDIA FLOW RATEFILTER 1 to 3 L/min(glass fiber, binderless

TYPES OF CHEMICALCHROMIUM, HEXAVALENT

SAMPLING MEDIA FLOW RATEFILTER 1 to 4 L/min(5.0-μm PVC membrane)

TYPES OF CHEMICALACIDS, INORGANIC

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.2 to 0.5 L/min(washed silica gel, 400 mg/200 mg withglass fiber filter plug)

MEASUREMENT TECHNIQUEION CHROMATOGRAPHY

TYPES OF CHEMICALACETONITRILE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE(coconut shell charcoal, 400/200 mg) 0.01 to 0.2 L/min

TYPES OF CHEMICAL

ARSENIC TRIOXIDE

FILTER 1 to 3 L/mi(Na2CO3-impregnated, 0.8-μm celluloseester membrane + backup pad)

TYPES OF CHEMICALVANADIUM OXIDES

SAMPLING MEDIA FLOW RATECYCLONE + FILTER HD cyclone: 2.2 L/min(10-mm cyclone or Higgins-Dewell (HD) + nylon cyclone: 1.7 L/min5-μm PVC membrane)

TYPES OF CHEMICALZINC OXIDE

SAMPLING MEDIA FLOW RATEFILTER 1 to 3 L/min(0.8-μm PVC membrane, 25-mm diameter, inopen-face cassette)

TYPES OF CHEMICALZINC and compounds, as Zn

MEASUREMENT TECHNIQUEATOMIC ABSORPTION, FLAME

TYPES OF CHEMICALWARFARIN

SAMPLING MEDIA FLOW RATEFILTER 1 to 4 L/min(1-μm PTFE membrane)

TYPES OF CHEMICALAMINES, AROMATIC

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE(silica gel, 150 mg/75 mg)

TYPES OF CHEMICALVINYL ACETATE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.1 to 0.2 L/min(carbon molecular sieve; 160 mg/80 mg;ORBO-92 or equivalent)

TYPES OF CHEMICALVINYLIDENE CHLORIDE

TYPES OF CHEMICALVINYL BROMIDE

TYPES OF CHEMICALVINYL CHLORIDE

SAMPLING MEDIA FLOW RATESOLID SORBENT TUBE 0.05 L/min(2 tandem tubes, each with 150 mg activatedcoconut charcoal)

Air Sampling Techniques

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